#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:11:09 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181909 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/09/2240918.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240918 _cell_angle_alpha 90.000 _cell_angle_beta 107.478 _cell_angle_gamma 90.000 _cell_length_a 10.9866 _cell_length_b 9.5679 _cell_length_c 17.2114 _exptl_crystal_F_000 748.00 _reflns_d_resolution_high 0.7600 _cod_data_source_file wm5179IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' C37 H543 Cl2 N2 P Pd in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 182.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -11 0 189.32 184.37 124.54 o 3 -11 0 474.64 707.70 158.53 o 4 -11 0 233.86 300.47 130.10 o 5 -11 0 362.32 312.29 129.26 o 6 -11 0 17.32 -82.67 97.42 o 0 -10 0 362.37 328.93 93.11 o 1 -10 0 14.72 77.75 83.62 o 2 -10 0 619.35 646.39 107.05 o 3 -10 0 105.35 121.32 104.04 o 4 -10 0 726.34 591.81 138.92 o 5 -10 0 98.13 -33.09 87.07 o 6 -10 0 188.34 126.69 101.10 o 7 -10 0 19.85 -97.97 97.97 o 8 -10 0 640.41 340.25 124.59 o 1 -9 0 346.78 298.13 53.76 o 2 -9 0 93.11 112.60 62.25 o 3 -9 0 2358.16 2406.95 137.74 o 4 -9 0 31.34 59.15 61.32 o 5 -9 0 627.03 458.48 117.79 o 6 -9 0 4.73 25.86 83.48 o 7 -9 0 320.88 268.61 110.39 o 8 -9 0 62.41 11.32 81.65 o 9 -9 0 720.25 614.29 149.57 o 0 -8 0 433.37 377.54 85.48 o 1 -8 0 245.15 205.34 66.86 o 2 -8 0 712.57 613.56 113.36 o 3 -8 0 25.72 8.59 56.48 o 4 -8 0 731.24 642.13 105.22 o 5 -8 0 263.12 262.72 74.98 o 6 -8 0 681.15 618.77 126.64 o 7 -8 0 27.24 11.68 74.82 o 8 -8 0 177.41 49.28 86.51 o 9 -8 0 194.34 212.00 104.10 o 10 -8 0 977.09 751.44 147.93 o 1 -7 0 1519.32 1263.96 98.47 o 2 -7 0 613.28 453.70 96.27 o 3 -7 0 366.77 421.16 70.90 o 4 -7 0 787.98 833.34 92.88 o 5 -7 0 2359.74 2554.40 136.89 o 6 -7 0 309.94 420.16 110.40 o 7 -7 0 1370.40 1467.31 162.51 o 8 -7 0 352.96 425.21 120.50 o 10 -7 0 151.67 73.31 96.75 o 11 -7 0 700.37 487.86 142.10 o 0 -6 0 6583.21 5936.02 808.47 o 1 -6 0 29.44 4.98 25.79 o 2 -6 0 1469.85 1232.20 104.87 o 3 -6 0 54.57 45.87 41.66 o 4 -6 0 863.40 1050.83 87.77 o 5 -6 0 461.95 463.63 78.00 o 6 -6 0 3446.00 3636.33 218.10 o 7 -6 0 356.96 438.63 113.70 o 8 -6 0 1040.13 985.57 144.09 o 9 -6 0 50.17 -7.60 76.08 o 10 -6 0 432.61 390.44 118.36 o 11 -6 0 88.77 128.30 96.93 o 12 -6 0 1162.23 958.51 174.50 o 1 -5 0 7767.45 6763.58 520.11 o 2 -5 0 1198.43 891.89 155.31 o 3 -5 0 1565.54 1657.60 200.95 o 4 -5 0 203.71 213.06 60.63 o 5 -5 0 1823.86 1904.96 155.49 o 6 -5 0 208.51 147.07 83.61 o 7 -5 0 4379.81 4798.42 244.44 o 8 -5 0 1327.72 1322.44 155.38 o 9 -5 0 902.23 878.53 146.49 o 10 -5 0 24.46 41.60 89.12 o 11 -5 0 891.62 846.45 160.68 o 12 -5 0 150.80 184.10 118.16 o 0 -4 0 7278.09 6562.54 570.56 o 1 -4 0 746.19 569.50 55.38 o 2 -4 0 7691.99 8235.96 713.14 o 3 -4 0 205.37 198.45 50.86 o 4 -4 0 3803.74 4183.15 266.25 o 5 -4 0 257.57 280.06 55.70 o 6 -4 0 2735.25 2993.90 178.27 o 7 -4 0 2763.92 2971.78 190.94 o 8 -4 0 4920.18 5360.59 260.13 o 9 -4 0 1235.69 1442.43 162.56 o 10 -4 0 1055.24 1107.33 168.04 o 11 -4 0 123.54 331.16 119.87 o 12 -4 0 746.88 667.99 167.25 o 13 -4 0 267.59 281.39 142.78 o 1 -3 0 1557.05 1194.91 106.18 o 2 -3 0 36.35 58.47 30.24 o 3 -3 0 17699.06 22068.71 2884.20 o 4 -3 0 196.31 227.66 52.90 o 5 -3 0 4171.89 4428.72 308.19 o 6 -3 0 439.87 553.82 93.83 o 7 -3 0 1562.84 1704.75 144.22 o 8 -3 0 45.85 125.81 85.00 o 9 -3 0 4905.81 5259.77 269.28 o 10 -3 0 531.51 460.99 130.59 o 11 -3 0 207.90 269.37 119.36 o 12 -3 0 150.48 165.98 100.79 o 13 -3 0 329.41 348.50 135.72 o 0 -2 0 15794.13 13916.82 881.52 o 1 -2 0 8241.40 9303.93 1297.90 o 2 -2 0 11076.25 13682.18 2017.41 o 3 -2 0 263.03 285.10 38.18 o 4 -2 0 10113.33 11181.64 536.32 o 5 -2 0 3592.47 4108.21 166.17 o 6 -2 0 4621.02 4731.17 189.14 o 7 -2 0 406.19 427.22 89.62 o 8 -2 0 4525.79 4617.14 226.15 o 9 -2 0 43.01 66.06 86.79 o 10 -2 0 2259.84 2706.81 214.34 o 11 -2 0 442.17 354.89 122.10 o 12 -2 0 306.11 337.29 122.94 o 13 -2 0 138.73 100.88 105.59 o 1 -1 0 28934.41 40352.44 6401.72 o 2 -1 0 76.44 117.61 26.34 o 3 -1 0 9959.08 11054.71 281.89 o 4 -1 0 3957.13 4025.59 226.41 o 5 -1 0 7277.32 7098.07 452.34 o 6 -1 0 221.04 255.40 33.50 o 7 -1 0 5212.18 4715.49 309.67 o 8 -1 0 1612.69 1518.00 89.69 o 9 -1 0 1754.07 1684.87 211.98 o 10 -1 0 55.59 -23.72 78.41 o 11 -1 0 1180.15 1149.86 168.55 o 12 -1 0 255.00 266.54 115.77 o 13 -1 0 1437.58 1375.62 208.78 o 1 0 0 1535.55 1371.68 35.02 o 2 0 0 3504.70 3665.59 319.38 o 3 0 0 1216.11 1200.45 46.09 o 4 0 0 599.57 538.51 41.32 o 5 0 0 3267.19 3353.48 92.61 o 6 0 0 16589.03 17865.81 310.81 o 7 0 0 362.15 366.70 45.86 o 8 0 0 2739.73 2500.23 99.83 o 9 0 0 7.28 5.48 33.95 o 10 0 0 933.20 1006.73 137.22 o 11 0 0 92.89 98.90 94.38 o 12 0 0 3240.32 3096.70 247.29 o 13 0 0 277.14 457.97 137.52 o 1 1 0 29030.28 27597.38 227.32 o 2 1 0 83.52 129.33 38.92 o 3 1 0 10105.55 10342.23 189.56 o 4 1 0 4012.37 3850.21 138.90 o 5 1 0 7235.33 7525.18 145.57 o 6 1 0 213.31 203.70 42.49 o 7 1 0 5271.53 5366.36 141.45 o 8 1 0 1610.29 1508.66 103.67 o 9 1 0 1812.85 1716.46 116.66 o 10 1 0 60.40 98.30 45.11 o 11 1 0 1203.85 1186.54 96.76 o 12 1 0 253.52 248.10 105.04 o 13 1 0 1402.03 1429.16 199.91 o 1 2 0 8308.16 8312.87 127.01 o 2 2 0 10909.03 9324.30 151.64 o 3 2 0 259.39 288.42 52.93 o 4 2 0 10198.64 9978.89 226.23 o 5 2 0 3647.27 3830.96 167.67 o 6 2 0 4564.90 4582.70 162.42 o 7 2 0 413.72 403.52 57.65 o 8 2 0 4478.57 4538.05 148.04 o 9 2 0 40.53 -13.46 42.73 o 10 2 0 2232.11 2222.46 217.83 o 11 2 0 454.19 429.57 74.15 o 12 2 0 309.60 314.63 66.97 o 13 2 0 136.07 146.57 111.22 o 1 3 0 1420.71 1320.83 68.84 o 2 3 0 37.24 67.19 31.64 o 3 3 0 17821.47 15979.07 247.79 o 4 3 0 195.44 146.05 66.20 o 5 3 0 4128.28 4111.35 138.07 o 6 3 0 448.06 514.54 86.61 o 7 3 0 1457.64 1351.76 118.64 o 8 3 0 46.51 79.66 42.75 o 9 3 0 4980.95 4660.94 545.97 o 10 3 0 521.79 494.08 76.85 o 11 3 0 191.04 243.02 66.88 o 12 3 0 157.10 112.58 56.77 o 13 3 0 309.35 190.31 98.79 o 1 4 0 742.34 725.73 73.77 o 2 4 0 7471.33 7052.74 165.06 o 3 4 0 200.95 149.30 56.39 o 4 4 0 3653.44 3518.38 150.25 o 5 4 0 255.72 290.05 60.88 o 6 4 0 2688.51 2526.43 242.84 o 7 4 0 2772.00 2634.70 210.26 o 8 4 0 4890.89 4596.31 161.37 o 9 4 0 1230.63 1123.74 118.44 o 10 4 0 979.55 983.41 99.02 o 11 4 0 118.33 69.47 56.23 o 12 4 0 753.97 709.84 95.40 o 13 4 0 274.76 170.42 73.38 o 1 5 0 7682.79 7652.85 189.25 o 2 5 0 1167.20 1065.36 88.41 o 3 5 0 1548.63 1342.05 96.65 o 4 5 0 217.58 231.82 66.52 o 5 5 0 1776.58 1419.64 119.57 o 6 5 0 215.40 196.74 70.70 o 7 5 0 4400.70 4114.42 243.87 o 8 5 0 1349.05 1237.62 114.61 o 9 5 0 879.46 928.66 107.07 o 10 5 0 22.43 7.00 46.80 o 11 5 0 882.20 775.82 99.75 o 12 5 0 155.25 120.30 61.83 o 1 6 0 27.79 17.43 46.75 o 2 6 0 1386.51 1462.87 104.03 o 3 6 0 55.95 64.15 54.80 o 4 6 0 821.74 809.31 97.14 o 5 6 0 463.14 387.68 79.94 o 6 6 0 3323.38 3219.26 144.13 o 7 6 0 365.48 303.67 60.25 o 8 6 0 1123.60 986.29 91.14 o 9 6 0 46.07 50.09 45.98 o 10 6 0 422.25 412.40 77.62 o 11 6 0 91.46 32.70 53.19 o 12 6 0 1153.02 1062.15 118.53 o 1 7 0 1537.01 1557.92 117.71 o 2 7 0 624.64 613.73 89.84 o 3 7 0 368.20 442.63 85.53 o 4 7 0 803.10 773.28 109.88 o 5 7 0 2362.79 2169.09 120.28 o 6 7 0 313.47 345.20 85.08 o 7 7 0 1358.04 1159.58 159.92 o 8 7 0 350.93 345.80 85.93 o 9 7 0 297.60 307.82 64.18 o 10 7 0 158.34 115.69 55.58 o 11 7 0 730.37 632.94 135.24 o 0 8 0 427.32 386.48 83.24 o 1 8 0 245.06 264.67 76.84 o 2 8 0 746.43 742.87 103.93 o 3 8 0 24.44 -19.88 60.49 o 4 8 0 754.82 741.14 114.04 o 5 8 0 258.85 229.08 75.62 o 6 8 0 615.49 685.99 97.75 o 7 8 0 26.09 48.02 50.27 o 8 8 0 168.19 207.02 60.03 o 9 8 0 194.90 223.27 82.90 o 10 8 0 994.76 750.15 140.56 o 1 9 0 372.40 408.92 84.33 o 2 9 0 91.69 87.32 69.66 o 3 9 0 2287.36 2166.77 149.39 o 4 9 0 32.30 14.64 60.73 o 5 9 0 697.96 819.21 98.11 o 6 9 0 3.83 21.36 60.61 o 7 9 0 301.13 383.39 183.08 o 8 9 0 62.54 44.49 73.37 o 9 9 0 731.64 642.87 184.28 o 0 10 0 422.10 450.67 87.21 o 1 10 0 17.18 24.73 60.69 o 2 10 0 623.28 720.92 150.84 o 3 10 0 102.99 310.42 124.22 o 4 10 0 743.70 683.28 164.78 o 5 10 0 104.16 88.91 71.97 o 6 10 0 199.22 263.18 81.44 o 7 10 0 22.00 73.78 97.67 o 8 10 0 659.70 743.26 165.71 o 1 11 0 811.09 1069.90 163.28 o 2 11 0 184.19 410.71 128.38 o 3 11 0 462.03 443.10 115.12 o 4 11 0 233.27 244.45 80.95 o 5 11 0 350.55 520.24 152.01 o 6 11 0 16.69 182.92 76.82 o 3 12 0 34.61 161.63 74.24 o 4 12 0 246.20 387.91 146.71 o -6 -11 1 768.64 436.31 145.91 o -5 -11 1 415.91 309.23 137.11 o -3 -11 1 282.25 147.64 115.11 o -2 -11 1 484.06 422.18 120.15 o -1 -11 1 474.38 263.90 120.46 o 2 -11 1 507.57 529.01 151.70 o 3 -11 1 84.91 184.44 122.23 o 4 -11 1 164.77 159.61 124.84 o 5 -11 1 140.61 176.84 113.33 o 6 -11 1 385.81 373.02 141.52 o -8 -10 1 273.77 142.47 109.73 o -7 -10 1 220.11 272.22 117.56 o -6 -10 1 161.83 224.60 109.21 o -5 -10 1 414.30 421.56 96.10 o -4 -10 1 433.17 526.91 99.56 o -3 -10 1 1227.15 1385.85 186.75 o -2 -10 1 186.17 225.76 73.88 o -1 -10 1 30.46 34.52 83.21 o 0 -10 1 103.29 87.24 81.21 o 2 -10 1 361.13 423.28 132.15 o 3 -10 1 1058.20 1246.48 185.73 o 4 -10 1 42.88 108.21 102.75 o 5 -10 1 117.75 224.94 109.96 o 6 -10 1 35.31 39.68 95.47 o 7 -10 1 399.35 333.29 118.14 o 8 -10 1 416.64 345.32 133.66 o -9 -9 1 345.09 314.36 116.53 o -8 -9 1 417.28 312.97 117.46 o -7 -9 1 480.52 423.48 124.86 o -6 -9 1 51.80 -28.17 62.33 o -5 -9 1 875.37 839.68 185.71 o -4 -9 1 1546.95 1565.89 120.93 o -3 -9 1 51.28 46.60 56.41 o -2 -9 1 1265.37 1324.03 117.17 o -1 -9 1 164.17 197.28 82.27 o 0 -9 1 21.98 52.84 71.82 o 1 -9 1 279.51 313.50 99.62 o 2 -9 1 704.57 862.96 144.67 o 3 -9 1 873.98 845.01 144.66 o 4 -9 1 1622.56 1795.03 180.92 o 5 -9 1 119.86 153.15 93.99 o 6 -9 1 227.78 206.88 103.63 o 7 -9 1 265.04 167.77 99.96 o 8 -9 1 148.20 99.93 101.63 o 9 -9 1 219.06 220.76 111.02 o -10 -8 1 630.46 531.09 136.64 o -9 -8 1 520.93 524.31 128.28 o -8 -8 1 984.11 1020.99 158.54 o -7 -8 1 143.74 152.99 93.50 o -6 -8 1 632.10 657.81 98.15 o -5 -8 1 1377.47 1349.14 116.07 o -4 -8 1 630.57 628.67 92.50 o -3 -8 1 306.66 348.98 72.28 o -2 -8 1 581.48 541.22 127.63 o -1 -8 1 804.30 783.51 117.02 o 0 -8 1 243.28 219.03 52.42 o 1 -8 1 666.41 608.09 75.94 o 2 -8 1 549.81 514.41 65.61 o 3 -8 1 728.18 708.56 128.42 o 4 -8 1 307.48 276.98 102.37 o 5 -8 1 430.57 332.25 105.97 o 6 -8 1 124.46 112.63 93.38 o 7 -8 1 234.64 147.16 93.51 o 8 -8 1 214.12 118.52 90.79 o 9 -8 1 375.59 301.61 124.05 o 10 -8 1 86.92 163.20 104.39 o -11 -7 1 553.52 471.34 140.37 o -10 -7 1 452.11 343.41 118.74 o -9 -7 1 341.73 396.34 116.06 o -8 -7 1 364.38 424.57 114.94 o -7 -7 1 517.62 596.16 91.51 o -6 -7 1 2131.69 2189.33 135.02 o -5 -7 1 2267.02 2413.67 133.03 o -4 -7 1 1057.80 1046.58 96.66 o -3 -7 1 533.87 492.78 72.07 o -2 -7 1 837.71 735.11 77.95 o -1 -7 1 1012.50 794.15 77.22 o 0 -7 1 1604.16 1397.59 119.08 o 1 -7 1 1355.85 1130.03 135.36 o 2 -7 1 473.40 403.25 64.38 o 3 -7 1 260.20 301.48 66.66 o 4 -7 1 438.78 525.85 113.65 o 5 -7 1 728.28 800.17 137.17 o 6 -7 1 1567.56 1454.25 161.24 o 7 -7 1 268.61 256.64 100.31 o 8 -7 1 73.94 40.17 82.49 o 9 -7 1 112.71 145.56 89.69 o 10 -7 1 425.54 307.00 120.64 o 11 -7 1 145.45 105.75 86.17 o -12 -6 1 506.04 590.73 150.11 o -11 -6 1 1072.56 1035.09 175.38 o -10 -6 1 526.15 436.36 128.00 o -9 -6 1 156.22 126.74 84.19 o -8 -6 1 548.72 703.89 132.02 o -7 -6 1 1707.40 1705.15 119.50 o -6 -6 1 1336.42 1448.90 111.16 o -5 -6 1 1833.51 1902.88 116.69 o -4 -6 1 260.31 261.56 84.64 o -3 -6 1 476.29 435.95 108.91 o -2 -6 1 1472.26 1214.81 73.28 o -1 -6 1 3286.60 2843.40 169.16 o 0 -6 1 2271.51 2075.90 112.87 o 1 -6 1 1972.12 1632.48 98.44 o 2 -6 1 890.49 769.75 88.24 o 3 -6 1 58.73 47.28 44.54 o 4 -6 1 566.72 655.10 113.83 o 5 -6 1 1495.02 1670.67 159.45 o 6 -6 1 804.94 800.12 139.02 o 7 -6 1 702.81 763.65 131.85 o 8 -6 1 117.26 115.84 87.98 o 9 -6 1 65.53 21.27 82.85 o 10 -6 1 31.44 114.39 99.00 o 11 -6 1 579.85 364.60 127.89 o -12 -5 1 338.46 391.98 136.30 o -11 -5 1 550.57 606.43 146.33 o -10 -5 1 1520.66 1565.84 183.38 o -9 -5 1 371.84 366.36 113.56 o -8 -5 1 1558.06 1683.44 165.71 o -7 -5 1 3231.69 3306.78 148.03 o -6 -5 1 1500.27 1589.60 105.17 o -5 -5 1 1061.15 1151.67 136.45 o -4 -5 1 2480.78 2870.37 239.55 o -3 -5 1 933.81 1094.93 106.70 o -2 -5 1 1010.87 841.43 66.19 o -1 -5 1 6044.77 5492.71 420.58 o 0 -5 1 2126.19 1820.24 131.39 o 1 -5 1 3420.82 3000.40 180.65 o 2 -5 1 2194.35 1947.06 197.75 o 3 -5 1 915.29 950.72 120.27 o 4 -5 1 2322.78 2687.12 168.57 o 5 -5 1 637.12 703.16 116.68 o 6 -5 1 53.00 51.31 80.48 o 7 -5 1 1363.03 1418.60 157.60 o 8 -5 1 908.39 862.03 140.60 o 9 -5 1 171.87 206.89 103.40 o 10 -5 1 570.20 496.90 128.40 o 11 -5 1 39.14 27.85 88.02 o 12 -5 1 400.52 245.27 123.15 o -13 -4 1 164.93 137.49 107.50 o -12 -4 1 213.05 158.48 107.71 o -11 -4 1 1264.65 1379.48 188.29 o -10 -4 1 159.61 137.52 99.36 o -9 -4 1 1718.32 1697.98 170.79 o -8 -4 1 1028.77 1148.47 147.34 o -7 -4 1 1826.85 1980.02 115.24 o -6 -4 1 2944.70 3280.49 128.91 o -5 -4 1 2751.80 3078.04 335.91 o -4 -4 1 1597.46 1901.27 190.79 o -3 -4 1 4527.94 4957.45 743.88 o -2 -4 1 396.50 439.29 89.92 o -1 -4 1 1508.39 1133.31 61.52 o 0 -4 1 1204.46 1177.18 41.99 o 1 -4 1 4034.65 3631.16 122.78 o 2 -4 1 3700.31 3593.12 155.75 o 3 -4 1 3748.91 4065.61 439.11 o 4 -4 1 2212.97 2821.33 162.82 o 5 -4 1 1156.93 1278.72 125.23 o 6 -4 1 304.63 405.58 99.48 o 7 -4 1 1390.19 1686.92 158.57 o 8 -4 1 477.88 429.16 114.92 o 9 -4 1 1586.03 1676.33 175.68 o 10 -4 1 306.26 292.41 109.91 o 11 -4 1 559.61 418.88 133.00 o 12 -4 1 200.66 175.01 116.53 o -13 -3 1 167.28 197.14 117.73 o -12 -3 1 214.53 220.08 117.21 o -11 -3 1 566.64 598.23 139.10 o -10 -3 1 1230.33 1505.70 170.36 o -9 -3 1 70.57 77.79 77.17 o -8 -3 1 1578.37 1748.44 158.40 o -7 -3 1 1150.45 1372.44 131.72 o -6 -3 1 685.44 724.03 69.62 o -5 -3 1 1296.32 1380.73 114.91 o -4 -3 1 10812.09 11887.90 1054.13 o -3 -3 1 1965.40 2315.11 356.91 o -2 -3 1 7202.87 8071.82 1360.73 o -1 -3 1 689.82 713.25 71.32 o 0 -3 1 2155.02 1975.63 41.37 o 1 -3 1 285.30 259.22 27.27 o 2 -3 1 12116.99 14536.18 1384.13 o 3 -3 1 3593.30 4243.15 398.33 o 4 -3 1 6786.96 8440.49 250.15 o 5 -3 1 545.72 693.08 100.58 o 6 -3 1 523.87 554.77 100.00 o 7 -3 1 1007.37 1114.59 131.07 o 8 -3 1 4416.56 4980.67 252.53 o 9 -3 1 694.23 825.47 139.96 o 10 -3 1 1395.78 1466.53 178.47 o 11 -3 1 292.59 310.41 121.72 o 12 -3 1 264.15 104.67 109.05 o 13 -3 1 112.64 207.76 134.61 o -13 -2 1 82.48 67.37 107.22 o -12 -2 1 159.12 87.72 99.39 o -11 -2 1 802.59 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