#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:11:09 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181909 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/09/2240936.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240936 _cell_angle_alpha 94.056 _cell_angle_beta 92.059 _cell_angle_gamma 97.882 _cell_length_a 11.7708 _cell_length_b 13.3657 _cell_length_c 16.1209 _exptl_crystal_F_000 1276.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file wm5185Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 384.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 133.14 148.02 60.75 o 3 0 0 30305.16 36704.66 983.59 o 4 0 0 693.69 667.13 49.95 o 5 0 0 21289.29 24360.72 1185.24 o 6 0 0 15414.63 20104.83 744.38 o 7 0 0 14.78 15.08 11.52 o 8 0 0 13031.50 17982.67 591.76 o 9 0 0 11056.77 14284.23 742.50 o 10 0 0 8.42 -25.09 199.69 o 11 0 0 315.66 340.11 101.35 o 12 0 0 3804.62 3928.06 409.75 o 13 0 0 1.29 28.20 91.60 o 14 0 0 7541.27 7509.49 521.89 o 15 0 0 831.51 1004.30 169.42 o -15 1 0 330.00 42.90 195.51 o -14 1 0 6945.86 6057.52 719.17 o -13 1 0 956.83 762.85 164.18 o -12 1 0 3945.92 4305.31 376.30 o -11 1 0 1108.11 1047.63 168.27 o -10 1 0 1378.18 1478.53 199.71 o -9 1 0 25881.11 30443.31 1153.63 o -8 1 0 8518.72 11437.28 447.55 o -7 1 0 358.26 682.64 132.59 o -6 1 0 24338.38 31017.78 988.88 o -5 1 0 29571.51 39581.02 2365.93 o -4 1 0 21544.42 25621.61 778.64 o -3 1 0 1159.35 1406.13 118.44 o -2 1 0 5672.24 7637.88 385.42 o 2 1 0 6337.15 8642.03 1709.95 o 3 1 0 22954.72 26485.21 822.51 o 4 1 0 8452.36 13545.02 677.28 o 5 1 0 14733.70 16191.90 531.06 o 6 1 0 4962.16 5643.04 287.43 o 7 1 0 7.08 22.99 32.87 o 8 1 0 9675.80 10563.64 517.18 o 9 1 0 23899.55 30250.97 957.82 o 10 1 0 236.54 148.43 81.68 o 11 1 0 178.51 208.11 70.55 o 12 1 0 6920.80 7144.83 781.25 o 13 1 0 1555.89 1528.83 205.66 o 14 1 0 11405.76 11443.59 876.93 o -15 2 0 2837.81 2806.05 285.32 o -14 2 0 1248.21 1356.10 220.89 o -13 2 0 3350.48 3246.22 346.01 o -12 2 0 3005.90 3257.00 317.37 o -11 2 0 5.88 -8.46 53.70 o -10 2 0 11809.90 12559.92 727.78 o -9 2 0 52010.52 57403.19 1831.17 o -8 2 0 10749.95 12523.66 549.65 o -7 2 0 1005.56 1419.92 183.01 o -6 2 0 19641.25 25248.42 2601.23 o -5 2 0 11395.36 11342.82 1381.44 o -4 2 0 40007.56 49956.30 4598.16 o -3 2 0 30607.60 42022.10 1073.05 o -2 2 0 8378.45 8891.79 269.26 o -1 2 0 47427.55 84255.42 2600.89 o 0 2 0 6384.76 9160.46 2390.37 o 1 2 0 3739.00 3842.84 152.25 o 2 2 0 9276.87 11353.41 1517.94 o 3 2 0 5660.47 6859.89 1210.72 o 4 2 0 2368.67 2749.28 157.66 o 5 2 0 20036.93 22609.74 948.72 o 6 2 0 67.70 107.40 32.72 o 7 2 0 48.11 68.61 29.80 o 8 2 0 21172.26 24947.47 960.58 o 9 2 0 11677.53 12530.19 403.51 o 10 2 0 3676.11 4172.44 231.86 o 11 2 0 758.96 678.96 89.05 o 12 2 0 1689.81 1740.46 332.17 o 13 2 0 5722.25 5694.83 516.67 o 14 2 0 10747.03 11043.21 1021.61 o -15 3 0 3018.26 3035.17 314.76 o -14 3 0 2219.92 2082.81 253.31 o -13 3 0 3765.61 3506.58 317.32 o -12 3 0 9578.98 9930.06 721.66 o -11 3 0 195.48 295.29 84.33 o -10 3 0 11293.40 13732.43 667.24 o -9 3 0 59640.92 61178.09 1526.13 o -8 3 0 1698.24 1990.28 161.89 o -7 3 0 2859.94 3109.96 199.06 o -6 3 0 20553.16 20835.12 570.60 o -5 3 0 177.20 296.41 93.06 o -4 3 0 75003.02 78120.49 2458.10 o -3 3 0 1570.46 1812.70 125.04 o -2 3 0 16730.56 18864.35 748.25 o -1 3 0 22471.16 23472.71 536.06 o 0 3 0 5979.89 5772.26 125.37 o 1 3 0 435.71 447.50 29.63 o 2 3 0 309.83 345.43 44.99 o 3 3 0 2528.34 2732.54 192.91 o 4 3 0 7181.44 7666.06 438.68 o 5 3 0 21307.44 22232.40 784.45 o 6 3 0 173.90 99.95 34.37 o 7 3 0 1445.26 1521.21 144.07 o 8 3 0 41094.81 44952.05 1714.97 o 9 3 0 5502.27 5430.48 400.40 o 10 3 0 6021.79 5963.65 558.59 o 11 3 0 1506.04 1576.65 262.91 o 12 3 0 2079.13 2197.01 269.69 o 13 3 0 9336.61 9373.28 598.81 o 14 3 0 7973.26 7933.84 639.55 o -15 4 0 5344.08 5807.20 439.27 o -14 4 0 741.24 597.49 135.54 o -13 4 0 10847.66 12175.61 590.41 o -12 4 0 8394.96 8477.32 456.92 o -11 4 0 308.50 309.43 82.76 o -10 4 0 19595.20 19506.59 761.60 o -9 4 0 27891.01 28475.79 785.18 o -8 4 0 9.61 33.41 24.35 o -7 4 0 60.94 157.48 49.97 o -6 4 0 1525.31 1432.81 150.31 o -5 4 0 6662.80 6814.37 321.87 o -4 4 0 36910.01 37666.40 1042.07 o -3 4 0 9127.79 10111.43 457.71 o -2 4 0 26.35 47.09 12.43 o -1 4 0 19549.94 18872.18 351.07 o 0 4 0 888.40 871.57 44.06 o 1 4 0 18766.86 19115.15 548.62 o 2 4 0 2051.35 2099.55 120.41 o 3 4 0 11271.39 11372.24 340.57 o 4 4 0 21000.12 21264.62 593.03 o 5 4 0 43657.54 45901.11 822.45 o 6 4 0 29.02 35.58 23.26 o 7 4 0 11277.67 12377.18 380.77 o 8 4 0 46953.99 49015.04 959.67 o 9 4 0 533.18 159.28 186.54 o 10 4 0 4225.00 4040.96 400.99 o 11 4 0 2692.27 2785.66 354.75 o 12 4 0 75.91 94.61 89.33 o 13 4 0 8844.79 7453.52 533.72 o 14 4 0 4985.80 3838.37 635.03 o -15 5 0 4546.62 4219.41 454.45 o -14 5 0 4.77 -33.89 62.08 o -13 5 0 16559.60 16129.45 800.70 o -12 5 0 8246.41 9104.59 517.18 o -11 5 0 13.67 41.70 47.82 o -10 5 0 23328.79 24248.98 748.39 o -9 5 0 11280.45 10659.66 513.42 o -8 5 0 3256.98 3274.59 214.53 o -7 5 0 34.05 91.11 37.78 o -6 5 0 478.16 391.12 71.16 o -5 5 0 7416.67 7650.51 346.28 o -4 5 0 16407.55 16300.52 369.03 o -3 5 0 21.42 38.39 16.04 o -2 5 0 4953.97 5244.68 126.52 o -1 5 0 113362.12 111488.05 1799.24 o 0 5 0 3929.60 4053.39 103.87 o 1 5 0 8692.23 8565.30 201.52 o 2 5 0 8871.96 9036.43 234.42 o 3 5 0 4860.74 5309.84 186.61 o 4 5 0 45983.79 47056.91 882.03 o 5 5 0 27654.64 27140.18 749.96 o 6 5 0 799.03 970.85 98.97 o 7 5 0 7600.04 7362.79 392.08 o 8 5 0 18394.32 17789.76 663.03 o 9 5 0 277.39 161.43 59.58 o 10 5 0 1376.81 1459.58 253.24 o 11 5 0 646.41 444.74 205.89 o 12 5 0 55.46 17.50 93.65 o 13 5 0 5256.83 4960.01 396.57 o -14 6 0 1206.82 1079.54 175.39 o -13 6 0 16956.85 17252.74 697.22 o -12 6 0 34.49 52.95 85.71 o -11 6 0 868.79 891.77 136.73 o -10 6 0 12598.67 12553.97 292.60 o -9 6 0 697.12 696.16 102.53 o -8 6 0 5487.87 5357.50 281.63 o -7 6 0 24.09 29.36 35.72 o -6 6 0 154.34 132.18 40.03 o -5 6 0 14933.46 14979.31 380.16 o -4 6 0 10160.62 9372.93 236.26 o -3 6 0 346.76 421.96 45.59 o -2 6 0 3160.90 3026.98 101.77 o -1 6 0 50659.77 48655.22 960.66 o 0 6 0 274.53 258.56 28.34 o 1 6 0 10332.82 9805.27 202.22 o 2 6 0 1702.48 1744.33 97.71 o 3 6 0 3245.75 3244.50 118.82 o 4 6 0 48030.70 47323.59 1048.73 o 5 6 0 24701.19 24328.35 647.01 o 6 6 0 408.54 344.96 57.35 o 7 6 0 6347.72 6159.84 425.60 o 8 6 0 13595.26 13734.63 624.28 o 9 6 0 172.90 111.61 41.54 o 10 6 0 1664.66 1681.15 186.88 o 11 6 0 500.36 184.63 99.18 o 12 6 0 294.39 116.90 89.03 o 13 6 0 11006.45 9675.54 839.63 o -14 7 0 4639.72 4603.68 460.34 o -13 7 0 6898.55 7167.70 429.64 o -12 7 0 170.36 227.71 84.83 o -11 7 0 1621.39 1428.37 172.65 o -10 7 0 4772.26 4751.22 236.14 o -9 7 0 394.83 341.11 60.44 o -8 7 0 7148.21 7375.75 356.57 o -7 7 0 54.24 -3.14 43.88 o -6 7 0 3138.21 3155.32 165.12 o -5 7 0 34067.14 33832.15 580.25 o -4 7 0 30705.47 29575.59 519.44 o -3 7 0 599.12 635.78 61.42 o -2 7 0 5896.89 5494.94 137.52 o -1 7 0 64183.04 60265.66 966.08 o 0 7 0 332.20 416.65 37.35 o 1 7 0 16528.22 16009.32 272.49 o 2 7 0 3254.73 2825.72 131.08 o 3 7 0 6793.18 6794.71 204.15 o 4 7 0 23656.17 22811.90 455.56 o 5 7 0 3439.78 3451.32 162.83 o 6 7 0 751.36 657.10 77.13 o 7 7 0 5821.01 5903.70 259.66 o 8 7 0 8201.99 8110.14 370.94 o 9 7 0 1778.26 1628.39 150.22 o 10 7 0 3751.99 3924.97 386.29 o 11 7 0 16.07 -52.64 80.37 o 12 7 0 3899.29 3975.28 439.90 o -14 8 0 7398.53 7291.83 584.41 o -13 8 0 7713.42 8306.06 595.51 o -12 8 0 8.10 -144.90 139.38 o -11 8 0 1352.69 1456.07 165.91 o -10 8 0 9609.81 9074.66 340.43 o -9 8 0 419.90 525.02 82.58 o -8 8 0 9576.57 9244.04 411.60 o -7 8 0 1291.78 1230.44 128.56 o -6 8 0 357.29 374.14 48.73 o -5 8 0 46259.86 43890.98 656.06 o -4 8 0 25616.56 25427.87 461.68 o -3 8 0 16.76 -3.79 15.28 o -2 8 0 17729.51 16503.81 312.89 o -1 8 0 27889.18 26841.02 419.07 o 0 8 0 479.93 629.49 48.95 o 1 8 0 3515.28 2987.17 135.16 o 2 8 0 26.93 -6.73 18.38 o 3 8 0 2029.18 2002.26 108.25 o 4 8 0 15183.63 15375.01 480.22 o 5 8 0 2020.00 2056.41 113.10 o 6 8 0 442.97 506.41 73.55 o 7 8 0 10607.60 10522.58 465.10 o 8 8 0 2493.89 2231.25 216.25 o 9 8 0 9493.89 7970.62 688.01 o 10 8 0 2424.51 2803.88 328.22 o 11 8 0 63.33 -215.52 143.68 o 12 8 0 12236.96 12378.88 1545.16 o -14 9 0 6737.60 7351.48 587.08 o -13 9 0 4493.14 4369.74 430.20 o -12 9 0 321.51 251.11 130.89 o -11 9 0 3068.33 2945.93 244.66 o -10 9 0 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45.15 28.81 o -3 10 0 628.11 312.48 114.41 o -2 10 0 11059.90 10805.38 263.71 o -1 10 0 264.51 234.60 32.36 o 0 10 0 7569.12 7578.49 204.70 o 1 10 0 2062.26 2079.10 111.91 o 2 10 0 98.05 83.24 35.99 o 3 10 0 8096.29 7810.81 333.51 o 4 10 0 28474.68 28615.76 651.17 o 5 10 0 452.82 554.04 71.77 o 6 10 0 605.78 526.45 71.30 o 7 10 0 7277.27 7132.72 411.15 o 8 10 0 622.46 495.38 212.38 o 9 10 0 14892.26 12447.64 1196.35 o 10 10 0 729.85 640.73 192.96 o 11 10 0 119.82 -210.63 140.42 o -13 11 0 1965.99 2656.60 345.04 o -12 11 0 31.35 21.15 81.00 o -11 11 0 6578.93 6796.08 505.77 o -10 11 0 3088.59 3282.71 325.24 o -9 11 0 5000.34 4981.49 390.34 o -8 11 0 1937.05 1987.21 234.92 o -7 11 0 26.24 -12.83 30.99 o -6 11 0 7507.18 7183.87 326.42 o -5 11 0 17850.36 18041.63 481.49 o -4 11 0 11.18 33.65 38.53 o -3 11 0 2.36 14.95 21.92 o -2 11 0 7831.34 7508.58 203.04 o -1 11 0 859.85 821.55 80.02 o 0 11 0 14603.91 14726.55 480.99 o 1 11 0 3086.79 2987.74 189.48 o 2 11 0 618.18 479.23 83.91 o 3 11 0 43020.52 41996.87 1543.42 o 4 11 0 18944.38 18716.46 1151.13 o 5 11 0 1186.92 1300.58 241.47 o 6 11 0 260.72 400.43 122.47 o 7 11 0 4335.63 4544.07 689.13 o 8 11 0 5642.63 5328.64 464.46 o 9 11 0 11986.19 12821.79 1552.92 o 10 11 0 94.20 122.09 110.93 o -12 12 0 376.48 230.89 180.26 o -11 12 0 3742.73 3871.71 379.14 o -10 12 0 228.86 202.02 176.70 o -9 12 0 9039.12 8821.29 641.69 o -8 12 0 299.69 303.35 119.57 o -7 12 0 237.33 211.39 69.07 o -6 12 0 11918.69 12473.74 424.56 o -5 12 0 12173.79 12069.00 380.28 o -4 12 0 109.41 95.55 35.67 o -3 12 0 6.91 3.54 30.21 o -2 12 0 11846.46 12299.41 380.70 o -1 12 0 3237.74 3515.49 168.14 o 0 12 0 26721.79 27425.20 741.09 o 1 12 0 963.76 662.54 116.68 o 2 12 0 1955.21 1580.69 204.46 o 3 12 0 36354.23 33719.29 2745.49 o 4 12 0 8383.65 7815.30 629.45 o 5 12 0 743.66 749.61 176.04 o 6 12 0 416.58 670.94 208.03 o 7 12 0 2343.55 2211.09 300.57 o 8 12 0 4512.47 5063.32 806.14 o 9 12 0 6285.76 6208.14 666.86 o -11 13 0 1787.76 1795.45 258.17 o -10 13 0 1259.22 1105.02 204.26 o -9 13 0 5716.18 5183.52 416.43 o -8 13 0 534.67 474.96 125.58 o -7 13 0 1707.90 1855.96 197.06 o -6 13 0 15116.96 15401.48 581.39 o -5 13 0 7035.89 7323.37 280.74 o -4 13 0 310.66 328.45 59.20 o -3 13 0 238.38 397.05 53.66 o -2 13 0 7086.31 7275.96 246.97 o -1 13 0 1964.81 2330.79 149.11 o 0 13 0 25261.21 24895.48 1024.37 o 1 13 0 233.11 246.60 91.81 o 2 13 0 2344.75 1939.85 243.05 o 3 13 0 16368.89 14365.05 1430.85 o 4 13 0 2497.28 2937.53 332.66 o 5 13 0 3335.03 2925.87 481.47 o 6 13 0 418.80 271.13 152.38 o 7 13 0 296.58 578.78 160.99 o 8 13 0 6778.85 7688.22 697.07 o -10 14 0 987.90 1280.96 229.79 o -9 14 0 9779.17 9559.48 515.35 o -8 14 0 773.69 595.50 118.18 o -7 14 0 680.65 684.48 116.90 o -6 14 0 20860.87 21366.74 840.53 o -5 14 0 7482.75 8470.35 569.80 o -4 14 0 2776.43 3081.39 254.73 o -3 14 0 1428.49 1252.74 133.38 o -2 14 0 2530.82 2939.14 199.21 o -1 14 0 13532.71 14762.99 773.59 o 0 14 0 10225.70 10168.10 566.59 o 1 14 0 1.14 -52.75 69.79 o 2 14 0 2605.67 2551.59 333.82 o 3 14 0 7148.44 7270.28 497.71 o 4 14 0 24.92 445.15 588.86 o 5 14 0 499.34 389.73 125.20 o 6 14 0 147.45 82.24 107.07 o 7 14 0 101.43 143.53 131.22 o -9 15 0 11296.49 11250.74 569.02 o -8 15 0 607.02 540.32 119.95 o -7 15 0 1460.32 1745.48 235.97 o -6 15 0 16790.83 18269.58 977.64 o -5 15 0 1090.29 1800.92 608.85 o -4 15 0 813.81 969.80 190.58 o -3 15 0 361.79 337.96 99.12 o -2 15 0 236.79 617.02 125.37 o -1 15 0 7541.40 7940.15 502.39 o 0 15 0 4155.82 4390.53 553.38 o 1 15 0 135.60 124.44 106.69 o 2 15 0 810.20 739.75 150.99 o 3 15 0 3403.32 3736.46 369.91 o 4 15 0 66.76 -13.40 107.64 o 5 15 0 1812.54 1641.08 280.14 o -7 16 0 1219.82 842.39 229.37 o -6 16 0 10036.33 10524.01 724.93 o -5 16 0 138.73 808.05 1560.18 o -4 16 0 3222.53 3673.12 353.52 o -3 16 0 157.95 4.70 131.37 o -2 16 0 923.98 878.65 379.60 o -1 16 0 8769.18 10042.05 769.51 o 0 16 0 713.47 807.35 192.82 o 1 16 0 443.80 484.15 117.76 o 2 16 0 3552.84 4198.75 462.24 o 3 16 0 2551.01 2962.60 422.55 o -5 17 0 658.95 1841.92 661.22 o -4 17 0 1011.27 1264.41 528.90 o -3 17 0 34.42 13.50 239.34 o -2 17 0 1731.66 2449.18 398.72 o -1 17 0 7798.06 9396.89 774.65 o 0 17 0 1224.66 1567.22 303.77 o -1 -17 1 36.48 -47.34 72.48 o 0 -17 1 248.35 382.58 142.91 o 1 -17 1 539.61 783.50 318.65 o 2 -17 1 5030.28 6790.76 636.24 o 3 -17 1 2748.62 3311.05 610.25 o 4 -17 1 33.42 301.97 186.43 o 5 -17 1 4170.52 4045.51 805.75 o -3 -16 1 5643.82 5472.65 626.01 o -2 -16 1 14.50 217.08 185.03 o -1 -16 1 388.20 223.37 104.61 o 0 -16 1 1962.80 2250.92 275.38 o 1 -16 1 471.01 576.92 268.39 o 2 -16 1 7082.70 7308.32 635.58 o 3 -16 1 229.85 -237.22 158.15 o 4 -16 1 59.65 886.59 317.49 o 5 -16 1 9648.38 10603.05 699.73 o 6 -16 1 2920.62 3780.43 1915.23 o 7 -16 1 1380.98 1876.70 716.38 o -5 -15 1 161.08 211.20 141.19 o -4 -15 1 3412.83 3191.94 334.05 o -3 -15 1 4770.73 5281.78 437.22 o -2 -15 1 289.07 492.47 150.78 o -1 -15 1 130.89 58.85 141.42 o 0 -15 1 1065.07 1447.80 230.20 o 1 -15 1 3407.30 3632.29 383.23 o 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