#------------------------------------------------------------------------------ #$Date: 2015-08-13 05:17:52 +0300 (Thu, 13 Aug 2015) $ #$Revision: 153380 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/09/2240993.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2240993 loop_ _publ_author_name 'Ameram, Nadiah' 'Adam, Farook' _publ_section_title ; Crystal structure of 2-methyl-N-{[2-(pyridin-2-yl)ethyl]carbamothioyl}benzamide ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o636 _journal_paper_doi 10.1107/S2056989015013559 _journal_volume 71 _journal_year 2015 _chemical_formula_iupac 'C16 H17 N3 O S' _chemical_formula_moiety 'C16 H17 N3 O S' _chemical_formula_sum 'C16 H17 N3 O S' _chemical_formula_weight 299.38 _chemical_name_systematic ; 2-Methyl-N-{[2-(pyridin-2-yl)ethyl]carbamothioyl}benzamide ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 86.1868(13) _cell_angle_beta 83.3739(13) _cell_angle_gamma 73.8746(13) _cell_formula_units_Z 2 _cell_length_a 8.5434(4) _cell_length_b 8.7477(4) _cell_length_c 11.0530(5) _cell_measurement_reflns_used 8347 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.33 _cell_measurement_theta_min 2.43 _cell_volume 787.73(6) _computing_cell_refinement ; SAINT (Bruker, 2009) ; _computing_data_collection ; APEX2 (Bruker, 2009) ; _computing_data_reduction ; SAINT (Bruker, 2009) ; _computing_molecular_graphics ; SHELXTL (Sheldrick, 2008) and Mercury (Macrae et al., 2008) ; _computing_publication_material ; SHELXL2014 (Sheldrick, 2015) and PLATON (Spek, 2009) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS2013 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker APEX DUO CCD area-detector' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0450 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 30520 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.292 _diffrn_reflns_theta_min 1.856 _exptl_absorpt_coefficient_mu 0.208 _exptl_absorpt_correction_T_max 0.8669 _exptl_absorpt_correction_T_min 0.6700 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2009) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.262 _exptl_crystal_description plate _exptl_crystal_F_000 316 _exptl_crystal_size_max 0.532 _exptl_crystal_size_mid 0.424 _exptl_crystal_size_min 0.224 _refine_diff_density_max 0.373 _refine_diff_density_min -0.216 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.029 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 199 _refine_ls_number_reflns 4698 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.029 _refine_ls_R_factor_all 0.0664 _refine_ls_R_factor_gt 0.0447 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0515P)^2^+0.2342P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1098 _refine_ls_wR_factor_ref 0.1287 _reflns_number_gt 3412 _reflns_number_total 4698 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file su5173sup1.cf _cod_data_source_block I _cod_database_code 2240993 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.898 _shelx_estimated_absorpt_t_max 0.955 _shelx_hkl_file ; -1 0 0 173.062 7.46524 3 -1 0 0 171.020 7.42661 8 -1 0 0 158.818 7.35347 7 -1 0 0 166.046 7.46352 4 -1 0 0 170.106 7.42476 2 1 0 0 164.814 7.44473 5 1 0 0 164.425 7.54085 9 1 0 0 162.133 7.35217 7 1 0 0 163.539 7.47099 1 1 0 0 185.122 7.51348 6 -2 0 0 443.442 19.2313 8 -2 0 0 458.558 19.4913 9 -2 0 0 454.406 19.3213 3 -2 0 0 444.325 19.3195 4 -2 0 0 444.749 19.2267 2 -2 0 0 412.682 19.0781 7 2 0 0 436.123 19.0848 7 2 0 0 434.683 19.3407 1 2 0 0 419.479 19.4585 9 2 0 0 440.128 19.3596 6 2 0 0 434.444 19.2839 5 2 0 0 424.345 19.2901 4 -3 0 0 491.642 21.0870 3 -3 0 0 467.641 20.9105 2 -3 0 0 455.409 20.7029 7 -3 0 0 456.987 21.0326 4 -3 0 0 471.731 20.9309 8 3 0 0 470.622 21.1234 6 3 0 0 477.455 21.0519 4 3 0 0 472.798 21.3293 9 3 0 0 471.497 21.0257 5 3 0 0 473.013 21.1145 1 3 0 0 484.193 20.7221 7 -4 0 0 -0.2607 0.23403 7 -4 0 0 -0.5237 0.31722 2 -4 0 0 -0.1665 0.36310 3 -4 0 0 -0.0599 0.41639 8 -4 0 0 -0.3358 0.36689 4 4 0 0 -0.0442 0.40624 9 4 0 0 -0.0434 0.35426 4 4 0 0 0.06062 0.46688 6 4 0 0 0.16139 0.38672 1 4 0 0 -0.1903 0.33392 5 -5 0 0 903.922 39.8750 8 -5 0 0 916.765 40.1276 3 -5 0 0 905.965 39.8145 2 -5 0 0 869.796 40.0100 4 5 0 0 896.873 40.5509 9 5 0 0 921.522 40.2250 6 5 0 0 890.494 40.1933 1 5 0 0 895.294 40.0257 4 5 0 0 912.937 40.0522 5 -6 0 0 86.9720 5.04617 8 -6 0 0 87.9956 5.00308 2 -6 0 0 92.5869 5.37802 3 -6 0 0 89.4008 5.22521 4 6 0 0 96.2209 5.28318 4 6 0 0 87.8976 5.75463 9 6 0 0 89.6946 5.43562 1 6 0 0 89.6183 5.22968 5 6 0 0 97.7939 5.50930 6 -7 0 0 -0.8967 0.63043 4 -7 0 0 0.37052 0.77358 3 -7 0 0 2.04097 0.96533 8 -7 0 0 0.71540 0.87628 2 7 0 0 0.96449 0.84917 4 7 0 0 1.85306 0.98427 5 7 0 0 -0.5919 0.62691 1 7 0 0 -0.7107 0.80167 6 7 0 0 0.37537 0.88502 9 -8 0 0 1.87736 0.91699 2 -8 0 0 0.55265 0.95002 8 -8 0 0 0.79278 1.02189 3 8 0 0 -0.0878 1.00143 9 8 0 0 1.64701 1.21513 4 8 0 0 0.10855 1.20068 1 8 0 0 1.32797 1.03202 6 -9 0 0 0.52067 1.15069 3 -9 0 0 0.90047 0.99448 8 -9 0 0 2.72633 1.26373 2 9 0 0 1.97276 1.55982 1 9 0 0 -0.5835 1.29835 6 -10 0 0 6.11337 1.61048 2 -10 0 0 5.42366 1.72833 8 10 0 0 4.68417 1.85366 1 10 0 0 5.99742 1.88956 6 -11 0 0 6.95669 2.28704 8 11 0 0 6.05588 2.44163 1 11 0 0 6.93044 2.35022 6 11 -1 0 0.97350 1.36818 6 11 -1 0 1.82231 1.72577 1 -11 1 0 3.23215 1.80941 8 10 -1 0 13.6228 2.85443 1 10 -1 0 13.4765 2.77872 6 -10 1 0 12.1826 2.24474 8 -10 1 0 13.5505 2.33299 2 9 -1 0 11.9414 2.75319 1 9 -1 0 17.1996 2.74162 6 -9 1 0 18.8313 2.51698 2 -9 1 0 15.5533 3.00425 3 -9 1 0 14.6859 2.49608 8 8 -1 0 1.34164 1.25400 5 8 -1 0 2.96406 1.81843 9 8 -1 0 0.53928 0.88840 6 8 -1 0 2.42314 1.66730 1 -8 1 0 5.46866 1.47866 3 -8 1 0 4.76044 1.41708 2 -8 1 0 2.75256 1.12484 8 7 -1 0 109.133 7.08639 9 7 -1 0 113.541 6.63545 5 7 -1 0 107.648 6.70765 1 7 -1 0 115.346 6.54936 6 -7 1 0 98.8208 6.03255 2 -7 1 0 101.916 6.04367 8 -7 1 0 114.786 6.43692 3 6 -1 0 -0.3292 0.53562 4 6 -1 0 0.84059 0.61975 7 6 -1 0 0.42861 0.74539 6 6 -1 0 0.93965 0.87667 5 6 -1 0 0.31530 0.90123 1 6 -1 0 0.15687 0.70478 9 -6 1 0 0.21027 0.51763 7 -6 1 0 0.10563 0.58516 4 -6 1 0 -0.1294 0.56447 8 -6 1 0 0.75638 0.82176 2 -6 1 0 -0.1578 0.75470 3 5 -1 0 157.901 7.32060 7 5 -1 0 157.312 7.94570 1 5 -1 0 142.092 7.80312 5 5 -1 0 149.759 7.37300 4 5 -1 0 148.343 7.68061 6 5 -1 0 145.176 8.19337 9 -5 1 0 142.348 7.41616 2 -5 1 0 154.850 7.48094 8 -5 1 0 145.924 7.23534 7 -5 1 0 157.280 7.61517 3 -5 1 0 138.737 7.32111 4 4 -1 0 226.944 10.7569 1 4 -1 0 220.341 10.5557 6 4 -1 0 217.085 11.0107 9 4 -1 0 231.486 10.3257 4 4 -1 0 223.508 10.3096 7 4 -1 0 217.658 10.7438 5 -4 1 0 217.755 10.2767 7 -4 1 0 213.459 10.3486 8 -4 1 0 217.171 10.2880 4 -4 1 0 228.606 10.4639 3 -4 1 0 222.369 10.4280 2 3 -1 0 623.657 27.2799 6 3 -1 0 625.522 27.7179 9 3 -1 0 618.137 27.0344 4 3 -1 0 617.781 27.4376 1 3 -1 0 595.905 27.1339 7 3 -1 0 592.011 27.4660 5 -3 1 0 617.307 27.2083 2 -3 1 0 603.812 27.1279 8 -3 1 0 659.535 27.1984 3 -3 1 0 597.607 27.0182 4 2 -1 0 576.788 25.7878 1 2 -1 0 563.598 25.8686 5 2 -1 0 596.812 25.6461 6 2 -1 0 549.575 25.6410 7 2 -1 0 586.388 25.9897 9 -2 1 0 581.915 25.6525 2 -2 1 0 589.006 25.9533 9 -2 1 0 584.988 25.4356 4 -2 1 0 626.865 25.5858 3 -2 1 0 576.343 25.5821 8 1 -1 0 1067.47 45.9209 6 1 -1 0 1050.57 46.0754 1 1 -1 0 1088.47 46.2154 9 1 -1 0 1046.97 46.1966 5 1 -1 0 1033.59 46.0843 7 -1 1 0 1046.84 45.9610 8 -1 1 0 1087.16 46.1978 9 -1 1 0 1073.44 45.9227 3 -1 1 0 1047.65 46.0274 2 0 -1 0 320.620 14.0318 9 0 -1 0 316.473 14.0893 7 0 -1 0 323.538 13.9688 4 0 -1 0 327.688 14.0104 8 0 -1 0 345.038 13.9032 6 0 -1 0 327.793 14.0575 2 0 -1 0 314.254 14.0990 5 0 -1 0 306.847 13.9652 1 0 1 0 317.051 13.9995 8 0 1 0 317.779 13.9593 4 0 1 0 320.396 14.0323 9 0 1 0 303.971 14.0205 3 -1 -1 0 316.897 13.6772 9 -1 -1 0 309.832 13.5484 5 -1 -1 0 326.821 13.6996 2 -1 -1 0 315.792 13.7141 8 -1 -1 0 313.714 13.6251 7 -1 -1 0 316.438 13.8617 4 -1 -1 0 305.030 13.8538 3 1 1 0 295.966 13.5478 5 1 1 0 309.733 13.6668 9 1 1 0 305.838 13.6159 1 1 1 0 308.619 13.8375 4 1 1 0 320.247 13.7680 6 -2 -1 0 3612.75 150.176 2 -2 -1 0 3602.54 149.595 9 -2 -1 0 3345.52 149.494 8 -2 -1 0 3476.96 149.756 4 -2 -1 0 3408.60 149.713 3 2 1 0 3385.84 149.578 9 2 1 0 3448.16 149.731 4 2 1 0 3459.68 149.667 6 2 1 0 3413.91 149.478 1 -3 -1 0 2436.87 99.7357 2 -3 -1 0 2227.40 100.012 3 -3 -1 0 2237.00 100.053 4 -3 -1 0 2295.41 99.7756 8 -3 -1 0 2433.93 100.006 9 3 1 0 2261.17 99.9915 6 3 1 0 2290.46 99.8200 1 3 1 0 2310.80 99.5695 5 3 1 0 2268.35 99.9842 9 3 1 0 2257.70 100.039 4 -4 -1 0 240.254 11.1360 9 -4 -1 0 240.975 10.8248 8 -4 -1 0 224.904 10.6822 2 -4 -1 0 231.701 10.2645 7 -4 -1 0 223.289 11.0907 4 -4 -1 0 237.663 11.1125 3 4 1 0 230.728 10.8973 1 4 1 0 237.423 11.1284 4 4 1 0 222.607 10.6033 5 4 1 0 227.828 11.0534 6 4 1 0 236.619 11.1684 9 -5 -1 0 0.03620 0.57231 3 -5 -1 0 0.14109 0.24710 7 -5 -1 0 0.33832 0.45023 8 -5 -1 0 -0.1317 0.44954 2 -5 -1 0 0.19615 0.41679 4 5 1 0 -0.4052 0.41350 6 5 1 0 -0.4046 0.53126 9 5 1 0 0.01137 0.39515 4 5 1 0 -0.5850 0.45933 1 5 1 0 -1.2447 0.44895 5 -6 -1 0 250.189 11.4457 2 -6 -1 0 225.204 11.8373 3 -6 -1 0 232.693 11.8839 4 -6 -1 0 245.582 11.5627 8 6 1 0 232.499 11.8536 4 6 1 0 242.447 11.7935 1 6 1 0 231.731 12.0860 9 6 1 0 240.784 11.4102 5 6 1 0 249.184 12.0148 6 -7 -1 0 4.47613 1.15180 8 -7 -1 0 1.80157 1.02612 3 -7 -1 0 3.83324 1.36127 4 -7 -1 0 3.37454 0.95528 2 7 1 0 5.39685 1.41103 6 7 1 0 2.04302 1.15654 4 7 1 0 5.63624 1.64647 9 7 1 0 5.01097 1.46380 1 7 1 0 4.02387 1.14713 5 -8 -1 0 19.8934 2.54691 8 -8 -1 0 16.6223 2.18865 2 -8 -1 0 17.0129 2.59028 3 8 1 0 17.5905 2.80057 9 8 1 0 17.3447 2.56050 6 8 1 0 18.4434 2.72254 1 8 1 0 18.2604 2.54364 4 -9 -1 0 10.9858 2.32978 3 -9 -1 0 11.7067 1.98455 2 -9 -1 0 12.6517 2.26349 8 9 1 0 9.32061 2.00696 4 9 1 0 13.7805 2.56518 6 9 1 0 9.59517 2.19139 1 -10 -1 0 -2.4955 1.12656 8 -10 -1 0 3.09704 1.64223 3 -10 -1 0 4.03048 1.45316 2 10 1 0 3.96545 1.86495 1 10 1 0 1.15310 1.23264 6 -11 -1 0 2.22181 1.80923 8 11 1 0 -0.6857 1.21837 1 11 1 0 0.28460 1.75497 6 10 -2 0 6.06555 2.52064 1 -10 2 0 9.44415 2.07851 2 -10 2 0 13.6718 2.57795 8 9 -2 0 4.69092 1.55459 6 9 -2 0 5.19727 2.23675 1 -9 2 0 4.61350 1.42823 2 -9 2 0 2.84387 1.57281 8 8 -2 0 31.9943 3.88561 5 8 -2 0 27.5845 3.29778 6 8 -2 0 23.0327 3.52968 1 -8 2 0 23.5868 2.93272 2 -8 2 0 27.0843 3.08579 8 -8 2 0 29.7759 3.31885 3 7 -2 0 22.3220 2.70368 6 7 -2 0 20.8345 2.95302 5 7 -2 0 20.1909 3.22607 9 7 -2 0 23.7584 3.09159 1 -7 2 0 19.8388 2.51354 3 -7 2 0 23.3524 2.61776 8 -7 2 0 25.5539 2.75577 2 6 -2 0 244.374 11.4240 7 6 -2 0 249.753 12.6693 9 6 -2 0 231.640 11.6297 6 6 -2 0 224.914 12.1040 5 6 -2 0 242.449 12.1126 1 -6 2 0 236.739 11.5150 3 -6 2 0 234.925 11.5328 2 -6 2 0 241.624 11.4814 8 -6 2 0 208.124 11.1815 7 5 -2 0 25.1949 2.71301 1 5 -2 0 22.4105 1.58152 4 5 -2 0 18.2305 2.01193 7 5 -2 0 21.5940 1.94188 6 5 -2 0 22.0019 2.59749 5 5 -2 0 21.4365 2.75207 9 -5 2 0 18.5380 1.75094 7 -5 2 0 19.0302 1.81679 3 -5 2 0 21.3480 2.17992 8 -5 2 0 20.7460 1.86638 2 4 -2 0 7.32267 1.10770 6 4 -2 0 7.33975 1.18410 7 4 -2 0 8.20186 1.44698 5 4 -2 0 7.96597 1.42438 1 4 -2 0 6.65913 0.81582 4 4 -2 0 5.91044 1.27661 9 -4 2 0 8.37165 1.19890 8 -4 2 0 7.52664 1.09927 3 -4 2 0 7.09183 0.83113 4 -4 2 0 6.06807 1.11317 2 3 -2 0 -0.5689 0.18759 4 3 -2 0 0.12560 0.56618 5 3 -2 0 0.51097 0.48870 9 3 -2 0 0.05337 0.34921 1 3 -2 0 -0.9942 0.34422 7 3 -2 0 0.20010 0.33750 6 -3 2 0 0.63991 0.47754 2 -3 2 0 0.34291 0.18460 4 -3 2 0 1.03427 0.43933 3 -3 2 0 -0.1025 0.26714 8 2 -2 0 331.677 14.4044 6 2 -2 0 309.563 14.9353 5 2 -2 0 332.015 14.7655 7 2 -2 0 329.172 14.0088 4 2 -2 0 326.837 14.9843 9 2 -2 0 314.001 14.7158 1 -2 2 0 307.064 14.5882 2 -2 2 0 315.231 13.9993 4 -2 2 0 318.905 14.4903 8 -2 2 0 329.840 14.9246 9 -2 2 0 333.922 14.4225 3 1 -2 0 373.278 16.8438 7 1 -2 0 376.945 16.9732 5 1 -2 0 364.404 16.3766 6 1 -2 0 376.036 16.7039 1 1 -2 0 379.840 16.8814 9 1 -2 0 372.996 16.7279 2 -1 2 0 377.807 16.6010 8 -1 2 0 376.916 16.8515 9 -1 2 0 375.809 16.5461 3 -1 2 0 366.667 16.7058 2 -1 2 0 376.063 16.1945 4 0 -2 0 5496.32 215.942 1 0 -2 0 4530.00 215.055 7 0 -2 0 5424.38 215.838 6 0 -2 0 4967.57 216.292 9 0 -2 0 4414.99 215.063 5 0 2 0 5287.14 216.230 4 0 2 0 4931.37 216.059 9 0 2 0 4812.11 215.757 3 -1 -2 0 199.057 8.59670 6 -1 -2 0 198.012 8.45530 1 -1 -2 0 186.886 8.78847 4 -1 -2 0 196.145 8.52397 9 -1 -2 0 189.208 8.67744 7 -1 -2 0 190.788 8.64668 8 -1 -2 0 184.217 8.66912 2 -1 -2 0 184.744 8.60450 5 -1 -2 0 185.029 8.85002 3 1 2 0 183.757 8.75241 4 1 2 0 192.012 8.60708 6 1 2 0 191.062 8.54865 9 1 2 0 191.173 8.53523 9 -2 -2 0 247.692 11.9507 4 -2 -2 0 284.309 11.6643 9 -2 -2 0 255.582 11.5239 7 -2 -2 0 244.773 11.9583 3 -2 -2 0 266.560 11.3613 5 -2 -2 0 255.042 11.6951 8 -2 -2 0 251.708 11.6452 2 2 2 0 265.086 11.5154 1 2 2 0 257.961 11.7966 6 2 2 0 266.144 11.6114 9 2 2 0 253.774 11.3611 5 2 2 0 251.900 11.9303 4 -3 -2 0 645.828 30.2502 3 -3 -2 0 663.425 29.9124 8 -3 -2 0 671.443 30.3102 4 -3 -2 0 678.817 29.8491 2 -3 -2 0 709.064 29.9678 9 -3 -2 0 706.742 29.5472 7 3 2 0 668.581 30.1222 6 3 2 0 661.013 30.2568 4 3 2 0 726.411 29.4435 5 3 2 0 643.293 29.9022 9 3 2 0 678.660 29.7912 1 -4 -2 0 23.0557 2.11836 3 -4 -2 0 27.3005 1.87872 8 -4 -2 0 24.0402 1.90937 9 -4 -2 0 28.0765 1.40585 7 -4 -2 0 24.8618 1.76935 2 -4 -2 0 25.5052 2.14389 4 4 2 0 26.5056 1.47856 5 4 2 0 23.9032 1.99205 6 4 2 0 26.9519 2.02449 9 4 2 0 25.5940 1.84107 1 4 2 0 22.0169 2.02627 4 -5 -2 0 4.89048 1.04738 8 -5 -2 0 3.54253 0.43869 7 -5 -2 0 3.08247 1.06164 3 -5 -2 0 3.13408 0.72884 2 -5 -2 0 2.75347 0.98265 4 5 2 0 4.71002 1.18830 4 5 2 0 4.03597 1.19326 6 5 2 0 3.45175 0.91037 1 5 2 0 3.98442 0.67368 5 5 2 0 2.55194 0.93931 9 -6 -2 0 0.74823 0.88652 4 -6 -2 0 0.48942 0.60471 8 -6 -2 0 1.15866 0.97206 3 -6 -2 0 0.31592 0.63595 2 6 2 0 0.51841 0.89266 6 6 2 0 0.41411 0.76295 1 6 2 0 0.61322 0.93030 4 6 2 0 -0.2626 0.42827 5 6 2 0 -0.4948 0.44389 9 -7 -2 0 7.93141 1.71874 3 -7 -2 0 4.24515 1.31151 8 -7 -2 0 1.88364 1.18565 4 -7 -2 0 6.44862 1.23494 2 7 2 0 6.82105 1.58192 6 7 2 0 5.37899 1.43265 9 7 2 0 7.15919 1.60321 1 7 2 0 8.57206 1.79813 4 -8 -2 0 94.7636 6.29444 4 -8 -2 0 94.4191 5.76492 8 -8 -2 0 90.6144 6.28625 3 -8 -2 0 103.621 5.69158 2 8 2 0 93.4170 6.05637 1 8 2 0 100.905 6.33097 4 8 2 0 98.1057 6.25129 6 8 2 0 91.7143 6.27873 9 -9 -2 0 2.50473 1.39773 8 -9 -2 0 2.90266 1.15181 2 -9 -2 0 -0.1992 1.31175 3 9 2 0 1.93068 1.27362 1 9 2 0 0.39856 1.07310 9 9 2 0 -0.9507 1.14900 6 9 2 0 -0.3591 0.74202 4 -10 -2 0 -0.3100 1.45492 3 -10 -2 0 1.30048 1.08094 2 -10 -2 0 -0.1170 0.87787 8 10 2 0 -0.3755 1.19914 4 10 2 0 0.47622 1.23217 1 10 2 0 -1.2850 1.27038 6 -11 -2 0 9.00348 2.12660 8 -11 -2 0 12.0648 2.86441 3 11 2 0 8.04079 2.51792 1 11 2 0 9.86654 2.44724 6 10 -3 0 0.23555 1.66873 1 -10 3 0 2.94370 1.40862 8 -10 3 0 0.10533 1.49264 2 9 -3 0 4.55463 2.12297 5 9 -3 0 2.68381 1.91168 1 -9 3 0 4.13728 1.51390 2 -9 3 0 7.23452 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1.49790 6 2 3 14 1.09544 1.83501 7 2 3 14 1.39647 2.07180 5 2 3 14 2.50435 1.86084 1 -3 -3 -14 -0.1711 1.13815 4 -3 -3 -14 -0.4415 1.80737 1 -3 -3 -14 -0.8365 1.71117 6 3 3 14 -0.2619 1.93998 5 3 3 14 -0.0590 1.70858 7 3 3 14 1.02238 1.58099 1 -4 -3 -14 -1.2564 1.14896 4 -4 -3 -14 -0.9752 1.71326 6 4 3 14 -1.6620 1.83130 5 4 3 14 2.04695 1.91012 1 -5 -3 -14 -1.1229 1.24562 4 -5 -3 -14 2.48130 2.21370 6 5 3 14 -2.7437 1.84606 5 5 3 14 0.83016 1.27925 1 -6 -3 -14 -1.4625 1.27386 4 -6 -3 -14 -0.4741 1.85249 6 6 3 14 -0.3786 2.19468 5 6 3 14 1.76021 1.98379 1 2 -4 -14 -3.7937 1.80089 1 -2 4 14 -0.2820 1.98219 5 1 -4 -14 -0.9482 2.05132 6 1 -4 -14 -1.7703 1.80929 1 -1 4 14 -2.0699 2.05340 5 -1 4 14 -2.1432 1.88753 7 0 -4 -14 0.39330 1.93259 1 0 -4 -14 -1.4885 1.05192 4 0 -4 -14 1.85038 2.25263 6 0 4 14 3.26490 2.19013 1 0 4 14 -0.1518 1.95124 5 0 4 14 0.55528 1.94831 7 -1 -4 -14 1.30458 1.67660 4 -1 -4 -14 4.49251 1.98879 6 -1 -4 -14 -1.2340 1.89495 1 1 4 14 -0.7556 1.39162 7 1 4 14 1.49422 1.70914 5 1 4 14 -1.0398 1.70129 1 -2 -4 -14 -1.3036 1.34583 4 -2 -4 -14 -0.4816 1.40076 6 -2 -4 -14 0.21593 1.65028 1 2 4 14 1.89920 2.29287 5 2 4 14 -0.9903 2.00409 7 2 4 14 -1.0322 1.57921 1 -3 -4 -14 0.82655 1.29245 4 -3 -4 -14 0.33550 1.29522 1 -3 -4 -14 2.01674 1.72806 6 3 4 14 1.98182 1.48927 1 3 4 14 -0.0506 2.12479 5 3 4 14 1.82891 1.82106 7 -4 -4 -14 4.17275 2.27917 4 -4 -4 -14 4.85487 2.42855 6 4 4 14 5.83153 2.31952 1 4 4 14 6.62897 2.79495 5 -5 -4 -14 -1.2714 1.66577 4 -5 -4 -14 0.06439 1.96944 6 5 4 14 1.07656 2.19868 5 5 4 14 2.06934 2.03483 1 -6 -4 -14 2.30156 2.30447 6 6 4 14 -0.4769 2.40761 5 6 4 14 2.06457 1.59005 1 0 -5 -14 2.90229 2.52478 6 0 -5 -14 4.37584 2.45888 1 0 5 14 3.07833 2.00970 5 0 5 14 3.30267 2.38197 7 0 5 14 0.77890 2.07480 1 -1 -5 -14 0.55806 1.59479 1 -1 -5 -14 -1.6249 1.39014 4 -1 -5 -14 0.81569 2.20581 6 1 5 14 -0.4360 1.82516 7 1 5 14 -0.4144 1.49198 1 1 5 14 -0.0689 2.02338 5 -2 -5 -14 0.78462 1.38064 4 -2 -5 -14 0.02460 1.89933 1 -2 -5 -14 1.13554 1.75916 6 2 5 14 -2.4201 1.67846 1 2 5 14 0.85670 1.51639 5 2 5 14 0.61501 1.79116 7 -3 -5 -14 2.79599 2.00712 4 -3 -5 -14 2.42069 1.81222 1 -3 -5 -14 2.80327 1.75910 6 3 5 14 2.49475 2.10912 7 3 5 14 1.62712 1.92055 1 3 5 14 4.77656 2.60313 5 -4 -5 -14 3.42404 1.98187 6 -4 -5 -14 5.59144 2.35680 1 -4 -5 -14 2.44313 2.21302 4 4 5 14 3.81325 2.57095 5 4 5 14 2.63510 2.08219 1 -5 -5 -14 3.66524 2.31511 6 -5 -5 -14 4.13723 2.26164 4 5 5 14 0.43014 1.53146 1 5 5 14 1.67677 2.43672 5 -2 -6 -14 12.2704 3.66118 1 -2 -6 -14 7.40408 2.50645 4 2 6 14 7.38782 3.23866 1 2 6 14 10.2858 3.07214 7 -3 -6 -14 -0.5228 1.72377 4 -3 -6 -14 1.39761 1.55625 1 3 6 14 -0.3531 1.42285 1 3 6 14 4.53559 2.32756 7 -4 -6 -14 0.51470 1.50620 4 0 2 -15 1.50629 2.34667 4 0 -2 15 -0.5194 1.80025 5 0 -2 15 1.26809 1.72483 7 -1 2 -15 1.42867 2.28083 4 1 -2 15 2.72908 2.35121 7 1 -2 15 2.69598 2.03375 5 2 -2 15 0.31440 1.53377 7 2 -2 15 -0.3999 1.78019 5 2 1 -15 -3.7260 2.09093 6 1 1 -15 -0.8290 2.15550 6 1 1 -15 -0.7391 2.00369 4 -1 -1 15 1.88190 2.32748 7 0 1 -15 5.90170 2.32906 4 0 1 -15 0.21905 1.99096 6 0 -1 15 0.36525 1.98121 5 0 -1 15 -1.9221 2.18230 7 -1 1 -15 4.31878 2.68269 4 1 -1 15 -0.2430 1.86031 5 1 -1 15 2.35701 2.25272 7 -2 1 -15 1.86553 2.41956 4 2 -1 15 4.97388 2.23516 5 2 -1 15 5.16027 2.55209 7 -3 1 -15 -2.6881 1.87446 4 3 -1 15 -0.5171 1.80000 5 3 -1 15 0.75960 2.02070 7 2 0 -15 -1.5126 2.15750 4 2 0 -15 -1.4691 2.41792 6 1 0 -15 -0.7137 2.28202 6 1 0 -15 0.62099 1.88790 4 -1 0 15 2.80797 2.10255 5 -1 0 15 1.50206 1.70895 7 0 0 -15 0.41570 1.56447 6 0 0 -15 1.21250 1.73868 4 0 0 15 0.36350 1.53440 7 0 0 15 -0.7432 1.81844 5 -1 0 -15 0.85517 1.55251 6 -1 0 -15 1.90839 2.20553 4 1 0 15 0.39203 1.48687 7 1 0 15 -0.7359 1.88715 5 -2 0 -15 20.0533 3.99643 4 -2 0 -15 21.7802 3.48042 6 2 0 15 20.8482 3.71164 5 2 0 15 22.8465 3.90272 7 -3 0 -15 3.52446 2.46975 4 3 0 15 0.96421 1.98540 7 3 0 15 3.17923 2.35105 5 4 0 15 0.03140 1.61159 7 1 -1 -15 23.2754 4.43181 6 1 -1 -15 30.2719 4.50449 4 -1 1 15 25.7454 4.14759 5 -1 1 15 45.6077 5.38945 7 0 -1 -15 9.61669 3.07373 4 0 -1 -15 11.1952 2.87281 6 0 1 15 11.5956 3.14876 7 0 1 15 8.40222 2.51725 5 -1 -1 -15 2.58337 2.38306 6 -1 -1 -15 2.35202 1.85860 4 1 1 15 3.55601 2.36082 7 1 1 15 4.64164 2.05348 5 -2 -1 -15 4.98687 2.47528 4 -2 -1 -15 -1.9061 1.77350 6 2 1 15 0.43158 1.42776 7 2 1 15 -1.3682 1.76872 5 -3 -1 -15 -0.6302 1.99572 4 -3 -1 -15 3.82267 2.24573 6 3 1 15 -0.6771 1.32117 5 3 1 15 -0.3136 1.42385 7 -4 -1 -15 4.44386 2.33335 6 -4 -1 -15 5.63446 3.21993 4 4 1 15 5.67629 2.52320 5 1 -2 -15 17.9200 3.36064 4 1 -2 -15 26.3979 4.37530 6 -1 2 15 16.4222 3.85308 7 -1 2 15 13.8094 3.34584 5 0 -2 -15 4.46740 2.76316 6 0 -2 -15 1.54831 2.21514 4 0 2 15 2.37388 1.64005 7 0 2 15 0.67856 2.00431 5 -1 -2 -15 3.02481 2.04171 1 -1 -2 -15 6.90781 2.71618 6 -1 -2 -15 2.56425 2.25285 4 1 2 15 3.45844 2.20300 1 1 2 15 7.57057 2.71401 5 1 2 15 7.96193 2.45856 7 -2 -2 -15 -4.7732 1.70762 6 -2 -2 -15 -1.3497 1.76812 4 -2 -2 -15 0.53658 1.82296 1 2 2 15 -0.1196 1.80301 1 2 2 15 -0.3862 1.87943 5 2 2 15 -1.1788 1.82405 7 -3 -2 -15 -0.0750 1.83958 6 -3 -2 -15 0.06571 1.57171 4 3 2 15 0.96466 1.75647 1 3 2 15 -0.7306 1.67712 7 3 2 15 -1.3019 1.20662 5 -4 -2 -15 5.70451 2.44311 4 -4 -2 -15 7.62284 2.69646 6 4 2 15 8.80101 3.63359 5 4 2 15 6.24996 1.97243 1 0 -3 -15 7.41273 2.75489 6 0 -3 -15 3.63047 2.49673 4 0 -3 -15 0.51959 1.56024 1 0 3 15 3.71862 1.95379 7 0 3 15 2.23472 1.72845 1 0 3 15 9.00752 2.95079 5 -1 -3 -15 -2.9502 1.65994 4 -1 -3 -15 3.70134 2.10317 6 -1 -3 -15 1.14710 1.92218 1 1 3 15 3.54172 2.15854 1 1 3 15 1.05159 1.71935 7 1 3 15 2.11571 2.38007 5 -2 -3 -15 6.88354 2.36560 4 -2 -3 -15 3.70777 1.71504 1 -2 -3 -15 3.71509 2.63917 6 2 3 15 6.00782 2.33468 5 2 3 15 5.96480 2.18196 1 2 3 15 12.2684 3.13141 7 -3 -3 -15 12.9360 3.20215 4 -3 -3 -15 7.85648 2.51098 6 3 3 15 11.8243 3.43412 5 3 3 15 5.63274 2.35164 1 3 3 15 11.3851 2.60360 7 -4 -3 -15 0.43280 1.55042 6 4 3 15 -0.3336 1.17456 1 -1 -4 -15 2.11726 2.13533 4 -1 -4 -15 1.73399 1.83717 1 1 4 15 3.43162 1.92129 1 -2 -4 -15 -0.1141 1.42691 4 -2 -4 -15 0.47704 1.87930 6 -2 -4 -15 -0.6106 2.08503 1 2 4 15 0.53972 1.63007 7 2 4 15 -1.2855 1.75956 1 -3 -4 -15 1.65238 2.63010 6 -3 -4 -15 0.51011 2.13811 4 -3 -4 -15 0.04123 1.37238 1 3 4 15 0.85659 2.08301 7 3 4 15 0.35469 1.39586 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 43695 _shelx_res_file ; mo_o2a_0m.res created by SHELXL-2014/7 TITL mo_o2a_0m in P-1 (RT) CELL 0.71073 8.54340 8.74770 11.05300 86.1868 83.3739 73.8746 ZERR 2.00 0.00040 0.00040 0.00050 0.0013 0.0013 0.0013 LATT 1 SFAC C H N O S UNIT 32 34 6 2 2 TEMP 23.000 SIZE 0.224 0.424 0.532 L.S. 10 BOND $H FMAP 2 1 60 PLAN 20 ACTA CONF WGHT 0.051500 0.234200 FVAR 0.96379 S1 5 0.298580 1.051787 -0.144836 11.00000 0.05652 0.04744 = 0.05187 0.01618 -0.00764 -0.00366 O1 4 0.464153 0.621592 0.109451 11.00000 0.06923 0.03692 = 0.04460 0.00379 0.00175 0.00607 N1 3 0.324174 0.876217 0.058029 11.00000 0.03955 0.03090 = 0.03604 0.00103 -0.00318 -0.00432 N2 3 0.477184 0.754032 -0.113373 11.00000 0.04625 0.03837 = 0.03552 0.00259 -0.00162 -0.00956 N3 3 0.873381 0.818196 -0.155977 11.00000 0.04833 0.03954 = 0.05863 -0.00520 -0.00051 -0.00787 C1 1 0.351457 0.724378 0.366360 11.00000 0.06414 0.04145 = 0.04054 0.00543 -0.01030 -0.01664 C2 1 0.252208 0.737904 0.476814 11.00000 0.09942 0.06266 = 0.03550 0.00494 -0.00799 -0.02526 AFIX 43 H2A 2 0.301228 0.708279 0.548804 11.00000 -1.20000 AFIX 0 C3 1 0.084741 0.793431 0.482817 11.00000 0.08860 0.06949 = 0.05234 -0.00272 0.02006 -0.01786 AFIX 43 H3A 2 0.022557 0.799861 0.558070 11.00000 -1.20000 AFIX 0 C4 1 0.008822 0.839323 0.378895 11.00000 0.06006 0.05920 = 0.06354 -0.00322 0.01401 -0.00996 AFIX 43 H4A 2 -0.104647 0.876908 0.382808 11.00000 -1.20000 AFIX 0 C5 1 0.102955 0.829064 0.268199 11.00000 0.05063 0.04357 = 0.04580 -0.00084 -0.00151 -0.00858 AFIX 43 H5A 2 0.052181 0.861851 0.197248 11.00000 -1.20000 AFIX 0 C6 1 0.272241 0.770646 0.260746 11.00000 0.04995 0.03097 = 0.03574 0.00062 -0.00379 -0.00987 C7 1 0.364893 0.747773 0.137282 11.00000 0.04304 0.03313 = 0.03681 0.00058 -0.00539 -0.00671 C8 1 0.375066 0.883505 -0.065954 11.00000 0.03450 0.03747 = 0.03690 0.00283 -0.00719 -0.01114 C9 1 0.527483 0.737914 -0.242797 11.00000 0.05592 0.04882 = 0.03596 -0.00565 -0.00247 -0.01765 AFIX 23 H9A 2 0.434790 0.790599 -0.287497 11.00000 -1.20000 H9B 2 0.558932 0.625858 -0.260982 11.00000 -1.20000 AFIX 0 C10 1 0.669785 0.807641 -0.287089 11.00000 0.05983 0.04829 = 0.03742 0.00121 0.00167 -0.01709 AFIX 23 H10A 2 0.692639 0.797374 -0.374642 11.00000 -1.20000 H10B 2 0.637130 0.920328 -0.270864 11.00000 -1.20000 AFIX 0 C11 1 0.823394 0.730093 -0.228893 11.00000 0.04742 0.03798 = 0.04492 -0.00090 0.01116 -0.01312 C12 1 0.911238 0.573767 -0.250794 11.00000 0.06329 0.04277 = 0.08833 -0.01578 0.00887 -0.01158 AFIX 43 H12A 2 0.874502 0.513807 -0.301931 11.00000 -1.20000 AFIX 0 C13 1 1.051735 0.508418 -0.196979 11.00000 0.05815 0.04237 = 0.12850 -0.00765 0.01054 0.00000 AFIX 43 H13A 2 1.110542 0.403199 -0.210158 11.00000 -1.20000 AFIX 0 C14 1 1.105618 0.599201 -0.123221 11.00000 0.04366 0.06609 = 0.11452 0.00837 -0.00508 -0.00318 AFIX 43 H14A 2 1.202123 0.558183 -0.086679 11.00000 -1.20000 AFIX 0 C15 1 1.012253 0.752320 -0.105335 11.00000 0.05341 0.06122 = 0.08712 -0.00620 -0.01261 -0.01092 AFIX 43 H15A 2 1.047668 0.814157 -0.054897 11.00000 -1.20000 AFIX 0 C16 1 0.533501 0.668579 0.364770 11.00000 0.07022 0.07084 = 0.06066 0.01741 -0.02613 -0.02175 AFIX 137 H16A 2 0.580832 0.749352 0.326440 11.00000 -1.50000 H16B 2 0.574280 0.572776 0.320015 11.00000 -1.50000 H16C 2 0.562406 0.647743 0.446831 11.00000 -1.50000 AFIX 0 H1N2 2 0.507630 0.676046 -0.064667 11.00000 0.04853 H1N1 2 0.264875 0.966798 0.087559 11.00000 0.04938 HKLF 4 REM mo_o2a_0m in P-1 (RT) REM R1 = 0.0447 for 3412 Fo > 4sig(Fo) and 0.0664 for all 4698 data REM 199 parameters refined using 0 restraints END WGHT 0.0499 0.2393 REM Highest difference peak 0.373, deepest hole -0.216, 1-sigma level 0.044 Q1 1 0.3389 0.9571 -0.0996 11.00000 0.05 0.37 Q2 1 0.3561 0.8141 0.0969 11.00000 0.05 0.28 Q3 1 0.3205 0.7643 0.2018 11.00000 0.05 0.27 Q4 1 0.1997 0.8252 0.2752 11.00000 0.05 0.25 Q5 1 0.0803 0.8245 0.4177 11.00000 0.05 0.24 Q6 1 0.5117 0.8187 -0.0999 11.00000 0.05 0.23 Q7 1 0.7499 0.7610 -0.2526 11.00000 0.05 0.23 Q8 1 0.3205 0.7540 0.3014 11.00000 0.05 0.22 Q9 1 0.3803 0.6267 0.0940 11.00000 0.05 0.21 Q10 1 0.9955 0.5646 -0.2419 11.00000 0.05 0.21 Q11 1 0.2095 1.1602 -0.1111 11.00000 0.05 0.20 Q12 1 0.1777 0.8104 0.4922 11.00000 0.05 0.18 Q13 1 0.3264 0.8683 0.0003 11.00000 0.05 0.18 Q14 1 0.4327 0.7084 0.3570 11.00000 0.05 0.18 Q15 1 0.5982 0.7793 -0.2632 11.00000 0.05 0.18 Q16 1 0.4018 0.7962 -0.0869 11.00000 0.05 0.17 Q17 1 1.0618 0.5383 -0.1195 11.00000 0.05 0.17 Q18 1 0.2548 0.9768 -0.1555 11.00000 0.05 0.17 Q19 1 0.8526 0.6549 -0.2282 11.00000 0.05 0.17 Q20 1 0.4464 0.7020 0.1247 11.00000 0.05 0.16 ; _shelx_res_checksum 77343 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy S S1 0.29858(5) 1.05179(5) -0.14484(4) 0.05473(14) Uani d 1 O O1 0.46415(15) 0.62159(12) 0.10945(10) 0.0552(3) Uani d 1 N N1 0.32417(14) 0.87622(13) 0.05803(10) 0.0367(2) Uani d 1 N N2 0.47718(15) 0.75403(15) -0.11337(11) 0.0408(3) Uani d 1 N N3 0.87338(16) 0.81820(15) -0.15598(13) 0.0499(3) Uani d 1 C C1 0.3515(2) 0.72438(18) 0.36636(14) 0.0482(3) Uani d 1 C C2 0.2522(3) 0.7379(2) 0.47681(15) 0.0654(5) Uani d 1 H H2A 0.3012 0.7083 0.5488 0.079 Uiso calc 1 C C3 0.0847(3) 0.7934(3) 0.48282(18) 0.0731(6) Uani d 1 H H3A 0.0226 0.7999 0.5581 0.088 Uiso calc 1 C C4 0.0088(2) 0.8393(2) 0.37890(18) 0.0638(5) Uani d 1 H H4A -0.1046 0.8769 0.3828 0.077 Uiso calc 1 C C5 0.10295(19) 0.82906(18) 0.26820(15) 0.0478(3) Uani d 1 H H5A 0.0522 0.8619 0.1972 0.057 Uiso calc 1 C C6 0.27224(18) 0.77065(15) 0.26075(12) 0.0392(3) Uani d 1 C C7 0.36489(17) 0.74777(16) 0.13728(12) 0.0384(3) Uani d 1 C C8 0.37507(16) 0.88350(16) -0.06595(12) 0.0359(3) Uani d 1 C C9 0.5275(2) 0.73791(19) -0.24280(13) 0.0462(3) Uani d 1 H H9A 0.4348 0.7906 -0.2875 0.055 Uiso calc 1 H H9B 0.5589 0.6259 -0.2610 0.055 Uiso calc 1 C C10 0.6698(2) 0.80764(19) -0.28709(14) 0.0487(3) Uani d 1 H H10A 0.6926 0.7974 -0.3746 0.058 Uiso calc 1 H H10B 0.6371 0.9203 -0.2709 0.058 Uiso calc 1 C C11 0.82339(18) 0.73009(17) -0.22889(14) 0.0445(3) Uani d 1 C C12 0.9112(2) 0.5738(2) -0.2508(2) 0.0661(5) Uani d 1 H H12A 0.8745 0.5138 -0.3019 0.079 Uiso calc 1 C C13 1.0517(3) 0.5084(2) -0.1970(3) 0.0805(7) Uani d 1 H H13A 1.1105 0.4032 -0.2102 0.097 Uiso calc 1 C C14 1.1056(2) 0.5992(3) -0.1232(2) 0.0779(6) Uani d 1 H H14A 1.2021 0.5582 -0.0867 0.093 Uiso calc 1 C C15 1.0123(2) 0.7523(2) -0.1053(2) 0.0676(5) Uani d 1 H H15A 1.0477 0.8142 -0.0549 0.081 Uiso calc 1 C C16 0.5335(2) 0.6686(3) 0.36477(18) 0.0661(5) Uani d 1 H H16A 0.5808 0.7494 0.3264 0.099 Uiso calc 1 H H16B 0.5743 0.5728 0.3200 0.099 Uiso calc 1 H H16C 0.5624 0.6477 0.4468 0.099 Uiso calc 1 H H1N2 0.508(2) 0.676(2) -0.0647(16) 0.049(5) Uiso d 1 H H1N1 0.265(2) 0.967(2) 0.0876(16) 0.049(5) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0565(2) 0.0474(2) 0.0519(2) -0.00366(17) -0.00764(18) 0.01618(17) O1 0.0692(7) 0.0369(5) 0.0446(6) 0.0061(5) 0.0018(5) 0.0038(4) N1 0.0395(6) 0.0309(5) 0.0360(6) -0.0043(4) -0.0032(4) 0.0010(4) N2 0.0463(6) 0.0384(6) 0.0355(6) -0.0096(5) -0.0016(5) 0.0026(5) N3 0.0483(7) 0.0395(6) 0.0586(8) -0.0079(5) -0.0005(6) -0.0052(6) C1 0.0641(9) 0.0415(7) 0.0405(7) -0.0166(7) -0.0103(7) 0.0054(6) C2 0.0994(15) 0.0627(11) 0.0355(8) -0.0253(10) -0.0080(9) 0.0049(7) C3 0.0886(15) 0.0695(12) 0.0523(10) -0.0179(11) 0.0201(10) -0.0027(9) C4 0.0601(10) 0.0592(10) 0.0635(11) -0.0100(8) 0.0140(9) -0.0032(8) C5 0.0506(8) 0.0436(8) 0.0458(8) -0.0086(6) -0.0015(6) -0.0008(6) C6 0.0499(8) 0.0310(6) 0.0357(7) -0.0099(5) -0.0038(6) 0.0006(5) C7 0.0430(7) 0.0331(6) 0.0368(7) -0.0067(5) -0.0054(5) 0.0006(5) C8 0.0345(6) 0.0375(6) 0.0369(6) -0.0111(5) -0.0072(5) 0.0028(5) C9 0.0559(9) 0.0488(8) 0.0360(7) -0.0176(7) -0.0025(6) -0.0056(6) C10 0.0598(9) 0.0483(8) 0.0374(7) -0.0171(7) 0.0017(6) 0.0012(6) C11 0.0474(8) 0.0380(7) 0.0449(8) -0.0131(6) 0.0112(6) -0.0009(6) C12 0.0633(11) 0.0428(9) 0.0883(14) -0.0116(8) 0.0089(10) -0.0158(9) C13 0.0581(11) 0.0424(9) 0.128(2) 0.0000(8) 0.0105(12) -0.0077(11) C14 0.0437(9) 0.0661(12) 0.1145(18) -0.0032(9) -0.0051(10) 0.0084(12) C15 0.0534(10) 0.0612(11) 0.0871(14) -0.0109(8) -0.0126(9) -0.0062(10) C16 0.0702(12) 0.0708(12) 0.0607(11) -0.0217(9) -0.0261(9) 0.0174(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C7 N1 C8 127.33(12) C7 N1 H1N1 118.0(12) C8 N1 H1N1 114.5(12) C8 N2 C9 123.54(13) C8 N2 H1N2 116.3(12) C9 N2 H1N2 120.0(12) C11 N3 C15 118.03(15) C2 C1 C6 116.77(16) C2 C1 C16 120.27(16) C6 C1 C16 122.91(15) C3 C2 C1 122.25(17) C3 C2 H2A 118.9 C1 C2 H2A 118.9 C4 C3 C2 120.40(17) C4 C3 H3A 119.8 C2 C3 H3A 119.8 C3 C4 C5 118.99(18) C3 C4 H4A 120.5 C5 C4 H4A 120.5 C4 C5 C6 121.16(16) C4 C5 H5A 119.4 C6 C5 H5A 119.4 C5 C6 C1 120.41(14) C5 C6 C7 118.19(13) C1 C6 C7 121.25(13) O1 C7 N1 123.59(13) O1 C7 C6 121.89(12) N1 C7 C6 114.47(11) N2 C8 N1 117.23(12) N2 C8 S1 124.66(11) N1 C8 S1 118.08(10) N2 C9 C10 113.56(12) N2 C9 H9A 108.9 C10 C9 H9A 108.9 N2 C9 H9B 108.9 C10 C9 H9B 108.9 H9A C9 H9B 107.7 C11 C10 C9 113.91(13) C11 C10 H10A 108.8 C9 C10 H10A 108.8 C11 C10 H10B 108.8 C9 C10 H10B 108.8 H10A C10 H10B 107.7 N3 C11 C12 121.26(16) N3 C11 C10 117.10(13) C12 C11 C10 121.64(16) C13 C12 C11 119.68(19) C13 C12 H12A 120.2 C11 C12 H12A 120.2 C12 C13 C14 119.45(18) C12 C13 H13A 120.3 C14 C13 H13A 120.3 C15 C14 C13 117.6(2) C15 C14 H14A 121.2 C13 C14 H14A 121.2 N3 C15 C14 123.9(2) N3 C15 H15A 118.0 C14 C15 H15A 118.0 C1 C16 H16A 109.5 C1 C16 H16B 109.5 H16A C16 H16B 109.5 C1 C16 H16C 109.5 H16A C16 H16C 109.5 H16B C16 H16C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance S1 C8 1.6675(13) O1 C7 1.2236(16) N1 C7 1.3686(17) N1 C8 1.3919(17) N1 H1N1 0.874(18) N2 C8 1.3203(18) N2 C9 1.4499(18) N2 H1N2 0.841(19) N3 C11 1.331(2) N3 C15 1.336(2) C1 C2 1.396(2) C1 C6 1.397(2) C1 C16 1.494(3) C2 C3 1.372(3) C2 H2A 0.9300 C3 C4 1.366(3) C3 H3A 0.9300 C4 C5 1.378(2) C4 H4A 0.9300 C5 C6 1.388(2) C5 H5A 0.9300 C6 C7 1.4926(19) C9 C10 1.525(2) C9 H9A 0.9700 C9 H9B 0.9700 C10 C11 1.496(2) C10 H10A 0.9700 C10 H10B 0.9700 C11 C12 1.387(2) C12 C13 1.364(3) C12 H12A 0.9300 C13 C14 1.372(3) C13 H13A 0.9300 C14 C15 1.369(3) C14 H14A 0.9300 C15 H15A 0.9300 C16 H16A 0.9600 C16 H16B 0.9600 C16 H16C 0.9600 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N2 H1N2 O1 . 0.842(17) 1.971(18) 2.6550(16) 137.8(16) N1 H1N1 N3 2_675 0.875(17) 2.061(17) 2.9366(17) 180(3) C16 H16A S1 2_675 0.96 2.86 3.782(2) 162 C12 H12A Cg2 2_665 0.93 2.92 3.7724(19) 153 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C6 C1 C2 C3 0.1(3) C16 C1 C2 C3 177.89(19) C1 C2 C3 C4 -0.6(3) C2 C3 C4 C5 0.0(3) C3 C4 C5 C6 1.1(3) C4 C5 C6 C1 -1.6(2) C4 C5 C6 C7 174.02(15) C2 C1 C6 C5 0.9(2) C16 C1 C6 C5 -176.76(16) C2 C1 C6 C7 -174.53(14) C16 C1 C6 C7 7.8(2) C8 N1 C7 O1 5.5(2) C8 N1 C7 C6 -171.85(12) C5 C6 C7 O1 -128.16(16) C1 C6 C7 O1 47.4(2) C5 C6 C7 N1 49.22(18) C1 C6 C7 N1 -135.22(14) C9 N2 C8 N1 173.37(12) C9 N2 C8 S1 -4.5(2) C7 N1 C8 N2 -1.7(2) C7 N1 C8 S1 176.26(11) C8 N2 C9 C10 84.03(18) N2 C9 C10 C11 61.39(18) C15 N3 C11 C12 0.8(2) C15 N3 C11 C10 -178.50(15) C9 C10 C11 N3 -113.16(15) C9 C10 C11 C12 67.54(19) N3 C11 C12 C13 -0.1(3) C10 C11 C12 C13 179.20(17) C11 C12 C13 C14 -1.0(3) C12 C13 C14 C15 1.2(3) C11 N3 C15 C14 -0.5(3) C13 C14 C15 N3 -0.5(4) _cod_database_fobs_code 2240993