data_2241000 _cell_angle_alpha 94.913 _cell_angle_beta 90.583 _cell_angle_gamma 91.316 _cell_length_a 8.6776 _cell_length_b 13.7435 _cell_length_c 18.9994 _exptl_crystal_F_000 1066.00 _reflns_d_resolution_high 0.8282 _cod_data_source_file pk2553Isup2.hkl _cod_data_source_block I _shelx_title ' apx865 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 314.85 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 157.67 85.36 65.58 o 2 0 0 2053.00 2234.68 192.96 o 3 0 0 467.25 500.76 46.81 o 4 0 0 536.74 455.54 55.57 o 5 0 0 688.30 880.24 107.43 o 6 0 0 1082.26 1128.99 75.35 o 7 0 0 648.61 753.31 177.17 o 8 0 0 3386.72 3864.86 320.81 o 9 0 0 3.02 38.08 95.81 o 10 0 0 739.02 779.16 535.80 o -10 1 0 220.82 148.15 123.43 o -9 1 0 1068.58 1437.29 205.07 o -8 1 0 850.42 1023.33 260.09 o -7 1 0 62.35 15.39 47.04 o -6 1 0 1997.29 1811.80 145.04 o -5 1 0 321.98 257.84 57.91 o -4 1 0 593.26 544.32 59.92 o -3 1 0 1431.25 1215.89 140.53 o -2 1 0 925.46 875.18 89.81 o -1 1 0 5196.21 4882.75 250.69 o 1 1 0 4570.77 4622.03 116.46 o 2 1 0 66989.57 64190.22 2067.95 o 3 1 0 8373.47 8125.82 155.55 o 4 1 0 1230.50 1181.49 112.96 o 5 1 0 389.34 413.09 74.93 o 6 1 0 7.60 10.94 32.29 o 7 1 0 155.50 159.26 90.50 o 8 1 0 548.64 549.99 114.56 o 9 1 0 347.42 232.02 165.73 o 10 1 0 1535.10 1810.30 248.65 o -10 2 0 43.88 108.40 116.08 o -9 2 0 650.39 814.51 162.51 o -8 2 0 11.48 4.28 70.21 o -7 2 0 596.33 762.83 118.84 o -6 2 0 999.54 938.80 126.38 o -5 2 0 441.81 435.00 72.68 o -4 2 0 3632.50 3320.70 118.28 o -3 2 0 1039.30 830.21 66.32 o -2 2 0 3.77 12.52 23.01 o -1 2 0 6549.23 8145.29 831.67 o 0 2 0 3768.86 4470.65 74.86 o 1 2 0 142.97 56.27 42.31 o 2 2 0 26216.52 26027.79 838.31 o 3 2 0 2246.23 2309.44 118.56 o 4 2 0 7084.97 7763.05 289.51 o 5 2 0 2697.50 2612.23 80.53 o 6 2 0 27.84 17.08 35.59 o 7 2 0 3936.55 3538.23 445.62 o 8 2 0 1150.03 1405.78 199.52 o 9 2 0 541.23 563.19 320.19 o 10 2 0 364.05 308.25 134.55 o -10 3 0 1.36 48.72 88.30 o -9 3 0 641.27 639.47 167.61 o -8 3 0 10.41 53.06 83.73 o -7 3 0 3010.79 3144.67 291.69 o -6 3 0 1724.15 1688.76 146.19 o -5 3 0 1825.21 1702.31 168.22 o -4 3 0 2497.37 2324.64 165.85 o -3 3 0 764.98 755.54 115.30 o -2 3 0 1149.97 1016.31 83.77 o -1 3 0 28859.80 27445.01 849.68 o 0 3 0 242.47 172.79 50.73 o 1 3 0 236.58 308.21 73.89 o 2 3 0 1624.80 1500.84 77.13 o 3 3 0 611.21 889.36 86.04 o 4 3 0 10855.67 11405.54 315.81 o 5 3 0 472.39 717.49 99.54 o 6 3 0 1872.36 2240.22 150.20 o 7 3 0 100.86 84.38 47.81 o 8 3 0 134.35 215.11 92.52 o 9 3 0 824.89 955.05 188.17 o 10 3 0 48.83 59.28 114.84 o -10 4 0 1023.91 1021.42 279.30 o -9 4 0 397.69 442.99 156.22 o -8 4 0 85.43 34.66 83.79 o -7 4 0 1141.38 1101.53 158.03 o -6 4 0 293.56 301.11 68.74 o -5 4 0 8080.48 8910.14 391.04 o -4 4 0 3732.11 3875.88 230.01 o -3 4 0 503.14 438.37 62.15 o -2 4 0 5688.66 5594.99 201.94 o -1 4 0 12429.76 13570.01 569.22 o 0 4 0 199.12 243.10 36.73 o 1 4 0 2041.52 1907.75 157.76 o 2 4 0 996.56 995.97 70.16 o 3 4 0 4756.67 4816.11 170.58 o 4 4 0 1001.37 899.16 54.10 o 5 4 0 158.41 127.50 59.95 o 6 4 0 3319.55 3839.47 282.92 o 7 4 0 503.67 477.37 91.18 o 8 4 0 1025.81 906.68 356.20 o 9 4 0 310.63 360.90 123.51 o 10 4 0 65.09 9.64 117.59 o -10 5 0 399.99 471.46 183.89 o -9 5 0 189.55 277.13 113.98 o -8 5 0 922.84 1143.23 162.37 o -7 5 0 175.40 162.28 73.28 o -6 5 0 1719.43 1738.74 171.30 o -5 5 0 3885.31 3963.34 204.61 o -4 5 0 1012.27 1001.45 96.46 o -3 5 0 1950.54 2070.17 106.88 o -2 5 0 3144.04 2806.61 166.95 o -1 5 0 164.22 115.35 37.56 o 0 5 0 3611.78 3842.39 175.26 o 1 5 0 190.71 171.55 89.53 o 2 5 0 86.78 118.30 40.56 o 3 5 0 2371.01 2318.13 134.95 o 4 5 0 2.48 11.12 26.41 o 5 5 0 14.43 18.44 36.12 o 6 5 0 924.24 897.22 105.24 o 7 5 0 32.37 103.44 128.40 o 8 5 0 2023.20 2264.38 243.15 o 9 5 0 56.00 1.65 289.99 o -9 6 0 6.55 32.72 117.97 o -8 6 0 926.62 1262.21 170.51 o -7 6 0 41.79 26.37 56.08 o -6 6 0 947.67 906.28 115.51 o -5 6 0 222.96 237.66 67.26 o -4 6 0 63.33 60.46 45.80 o -3 6 0 3545.57 3858.47 232.55 o -2 6 0 111.07 132.15 41.18 o -1 6 0 2312.42 2161.49 95.75 o 0 6 0 2295.35 2187.08 184.37 o 1 6 0 244.58 227.23 37.25 o 2 6 0 2084.82 2276.37 119.45 o 3 6 0 1827.16 1909.14 74.27 o 4 6 0 249.26 246.71 53.03 o 5 6 0 1702.82 1907.46 144.68 o 6 6 0 1058.38 1157.47 119.82 o 7 6 0 491.64 592.80 288.46 o 8 6 0 1434.63 1406.47 247.77 o 9 6 0 1.27 3.41 256.86 o -9 7 0 290.84 239.69 130.04 o -8 7 0 43.71 46.32 77.70 o -7 7 0 89.46 73.65 71.55 o -6 7 0 866.75 942.36 138.70 o -5 7 0 4.78 11.62 41.68 o -4 7 0 331.13 343.24 53.45 o -3 7 0 2282.99 2319.24 149.09 o -2 7 0 49.37 41.38 27.70 o -1 7 0 8360.80 8401.40 250.13 o 0 7 0 3072.79 3095.71 126.28 o 1 7 0 2272.66 2351.64 183.17 o 2 7 0 11341.34 12750.17 1141.17 o 3 7 0 351.47 421.50 103.88 o 4 7 0 843.02 926.58 119.14 o 5 7 0 701.98 726.80 118.06 o 6 7 0 241.20 229.21 87.60 o 7 7 0 1263.22 975.06 182.42 o 8 7 0 235.83 311.55 153.31 o 9 7 0 70.46 5.78 151.45 o -9 8 0 867.26 989.77 223.99 o -8 8 0 333.93 281.45 106.44 o -7 8 0 567.11 800.06 137.65 o -6 8 0 271.14 218.79 97.27 o -5 8 0 2.09 6.61 41.86 o -4 8 0 601.14 620.64 88.48 o -3 8 0 249.16 399.37 73.72 o -2 8 0 9.29 32.96 39.96 o -1 8 0 1649.22 1854.96 121.25 o 0 8 0 1375.93 1613.93 154.44 o 1 8 0 3619.43 3677.63 397.17 o 2 8 0 1366.17 1375.40 117.29 o 3 8 0 1911.81 2113.18 200.61 o 4 8 0 1201.62 1328.43 127.11 o 5 8 0 114.85 61.23 59.04 o 6 8 0 486.55 639.04 305.38 o 7 8 0 522.20 708.02 289.46 o 8 8 0 7.10 65.69 128.51 o 9 8 0 157.19 153.67 173.79 o -8 9 0 0.44 9.45 93.27 o -7 9 0 347.71 347.94 149.80 o -6 9 0 15.50 32.42 63.50 o -5 9 0 365.14 490.93 91.60 o -4 9 0 47.24 11.87 42.08 o -3 9 0 1269.76 1165.62 157.17 o -2 9 0 3069.18 3479.28 230.39 o -1 9 0 275.30 264.02 73.19 o 0 9 0 168.38 68.50 65.26 o 1 9 0 314.63 279.59 95.80 o 2 9 0 1098.15 1093.58 110.88 o 3 9 0 2524.53 2218.40 210.84 o 4 9 0 3276.78 3392.22 486.50 o 5 9 0 154.84 162.20 69.86 o 6 9 0 439.53 690.12 185.38 o 7 9 0 261.95 273.51 162.91 o 8 9 0 332.00 435.14 177.64 o -8 10 0 272.81 298.32 130.16 o -7 10 0 1054.24 1185.06 196.58 o -6 10 0 197.68 80.63 70.38 o -5 10 0 504.59 152.85 116.27 o -4 10 0 134.80 44.91 85.79 o -3 10 0 1768.53 1821.18 463.83 o -2 10 0 347.68 267.56 95.99 o -1 10 0 146.42 170.47 88.90 o 0 10 0 884.79 967.66 128.02 o 1 10 0 481.45 382.08 94.61 o 2 10 0 28.79 67.11 52.98 o 3 10 0 964.46 1033.87 133.55 o 4 10 0 2077.02 1906.83 188.55 o 5 10 0 134.93 93.49 102.41 o 6 10 0 748.14 556.80 167.95 o 7 10 0 100.24 10.81 131.67 o 8 10 0 295.67 382.60 203.61 o -7 11 0 52.66 22.42 132.92 o -6 11 0 185.99 228.32 154.80 o -5 11 0 1387.74 1479.68 484.40 o -4 11 0 4.06 21.39 87.96 o -3 11 0 190.13 152.21 102.06 o -2 11 0 404.55 721.85 158.95 o -1 11 0 1603.01 1795.86 156.32 o 0 11 0 978.48 919.77 206.15 o 1 11 0 165.71 135.51 77.91 o 2 11 0 497.72 438.15 114.30 o 3 11 0 1170.02 1449.24 196.13 o 4 11 0 330.98 373.45 120.17 o 5 11 0 607.14 577.23 325.71 o 6 11 0 1147.39 864.21 202.23 o 7 11 0 477.95 375.29 173.88 o -7 12 0 1.75 8.52 149.05 o -6 12 0 497.95 797.86 441.63 o -5 12 0 145.60 259.95 179.51 o -4 12 0 147.72 196.72 129.81 o -3 12 0 2902.41 3354.31 524.46 o -2 12 0 30.71 57.26 108.94 o -1 12 0 590.78 647.98 135.90 o 0 12 0 1.41 34.25 73.10 o 1 12 0 504.56 364.87 134.40 o 2 12 0 850.70 1089.35 164.25 o 3 12 0 260.71 302.10 93.92 o 4 12 0 1.50 12.01 73.21 o 5 12 0 417.41 556.83 180.45 o 6 12 0 216.02 208.12 160.12 o -6 13 0 70.04 105.99 157.72 o -5 13 0 18.28 37.95 146.23 o -4 13 0 1159.42 1499.17 279.70 o -3 13 0 1518.48 1671.73 458.49 o -2 13 0 37.86 133.20 123.59 o -1 13 0 2090.22 2096.48 360.21 o 0 13 0 1.09 21.47 89.97 o 1 13 0 1504.67 1318.54 179.04 o 2 13 0 3.62 18.31 81.81 o 3 13 0 166.19 335.57 100.61 o 4 13 0 15.67 50.58 90.74 o 5 13 0 84.96 195.20 122.14 o 6 13 0 120.82 156.10 142.99 o -5 14 0 714.19 617.40 234.88 o -4 14 0 264.43 137.95 163.86 o -3 14 0 9.69 19.43 122.06 o 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