#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:38:30 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181911 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/10/2241011.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241011 _cell_angle_alpha 90.000 _cell_angle_beta 113.514 _cell_angle_gamma 90.000 _cell_length_a 24.0780 _cell_length_b 8.5585 _cell_length_c 26.6841 _exptl_crystal_F_000 2544.00 _reflns_d_resolution_high 0.7306 _cod_data_source_file tk5379Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' RG in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 645.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 369119.16 356434.66 16500.85 o 4 0 0 6414.78 7237.89 95.22 o 5 0 0 10388.90 10736.57 117.66 o 6 0 0 36216.36 37593.61 387.91 o 7 0 0 3537.57 3704.91 94.80 o 8 0 0 30465.35 31388.45 376.59 o 9 0 0 1925.98 2417.94 87.88 o 10 0 0 418.63 393.32 46.10 o 11 0 0 4.27 30.75 29.52 o 12 0 0 782.72 712.92 84.82 o 13 0 0 1828.47 2303.40 146.66 o 14 0 0 29631.62 29223.62 517.65 o 15 0 0 5253.22 5871.44 270.11 o 16 0 0 6365.69 6552.62 216.89 o 17 0 0 19651.13 19875.80 384.74 o 18 0 0 2401.38 2996.74 161.62 o 19 0 0 8828.26 8597.74 272.30 o 20 0 0 774.68 928.48 110.77 o 21 0 0 2.09 89.28 64.85 o 22 0 0 4835.79 5471.96 327.76 o 23 0 0 2115.62 2478.54 231.90 o 24 0 0 525.82 556.04 131.89 o 25 0 0 1648.51 1992.44 223.46 o 26 0 0 536.45 532.17 167.72 o 27 0 0 748.58 816.82 194.20 o 28 0 0 32.05 357.50 225.09 o 29 0 0 17.56 -4.41 163.30 o 1 1 0 25.99 19.75 5.47 o 2 1 0 98.68 57.65 12.16 o 3 1 0 10437.39 10600.92 384.28 o 4 1 0 6727.37 7360.66 63.63 o 5 1 0 9116.09 9594.22 79.58 o 6 1 0 2525.97 2671.61 49.28 o 7 1 0 4461.81 4735.88 91.53 o 8 1 0 33834.05 33906.43 329.77 o 9 1 0 548.72 550.03 31.73 o 10 1 0 286.84 464.45 32.91 o 11 1 0 72355.34 72108.64 370.07 o 12 1 0 10782.22 10567.82 163.86 o 13 1 0 16434.79 16064.59 238.64 o 14 1 0 28911.12 28546.84 489.61 o 15 1 0 532.62 789.60 73.48 o 16 1 0 11051.01 10809.98 275.36 o 17 1 0 1156.70 1418.58 91.52 o 18 1 0 620.93 617.46 69.64 o 19 1 0 3455.03 3429.70 141.49 o 20 1 0 335.59 343.27 70.70 o 21 1 0 1256.21 1063.15 102.90 o 22 1 0 1.99 38.74 56.21 o 23 1 0 1204.66 1201.47 124.07 o 24 1 0 314.20 400.31 94.65 o 25 1 0 137.20 145.99 68.99 o 26 1 0 1959.64 2049.56 177.65 o 27 1 0 698.42 636.30 110.82 o 28 1 0 98.33 141.03 88.47 o 29 1 0 297.15 548.22 173.90 o 0 2 0 100330.77 106479.51 885.78 o 1 2 0 2034.21 2171.21 38.27 o 2 2 0 1398.00 1475.78 33.77 o 3 2 0 3401.95 3446.50 57.81 o 4 2 0 146.54 149.52 19.55 o 5 2 0 576.52 636.23 28.64 o 6 2 0 2830.20 3061.57 98.28 o 7 2 0 2144.85 2309.31 70.68 o 8 2 0 304.92 360.81 34.42 o 9 2 0 2165.65 2373.38 83.25 o 10 2 0 527.16 602.98 53.95 o 11 2 0 305.63 304.22 42.33 o 12 2 0 6914.23 7479.03 174.08 o 13 2 0 654.41 667.48 60.59 o 14 2 0 0.98 35.26 40.46 o 15 2 0 908.45 888.14 102.50 o 16 2 0 93.47 135.61 65.20 o 17 2 0 372.27 451.95 72.83 o 18 2 0 81.72 115.87 56.42 o 19 2 0 0.43 120.95 63.01 o 20 2 0 5.99 161.15 74.23 o 21 2 0 105.86 344.43 87.61 o 22 2 0 0.37 58.07 65.97 o 23 2 0 39.20 182.35 80.91 o 24 2 0 43.83 97.70 73.96 o 25 2 0 52.30 -20.61 69.86 o 26 2 0 11.77 105.59 70.08 o 27 2 0 193.38 315.19 113.25 o 28 2 0 30.04 24.62 96.26 o 1 3 0 1440.55 1535.83 46.98 o 2 3 0 54.32 95.49 15.70 o 3 3 0 3313.39 3271.30 64.70 o 4 3 0 6678.41 7067.07 99.68 o 5 3 0 6333.51 6551.74 102.55 o 6 3 0 19149.66 19667.24 209.57 o 7 3 0 4244.92 4232.91 107.55 o 8 3 0 40854.21 42237.72 415.09 o 9 3 0 3670.99 3851.94 104.67 o 10 3 0 6.22 99.76 24.68 o 11 3 0 18730.25 18502.11 250.76 o 12 3 0 707.46 647.82 61.30 o 13 3 0 7014.90 6581.75 181.37 o 14 3 0 1227.05 1268.97 116.99 o 15 3 0 427.75 497.13 82.43 o 16 3 0 6891.27 7052.18 415.58 o 17 3 0 58.53 54.86 66.22 o 18 3 0 56.56 178.82 79.73 o 19 3 0 3900.35 4000.84 235.82 o 20 3 0 17.26 170.64 87.48 o 21 3 0 1131.99 1460.69 160.73 o 22 3 0 25.92 124.93 81.75 o 23 3 0 2.84 -72.77 90.90 o 24 3 0 127.34 74.25 105.11 o 25 3 0 555.54 466.75 96.68 o 26 3 0 83.26 103.19 107.66 o 27 3 0 62.55 86.79 101.71 o 28 3 0 265.50 303.46 165.32 o 0 4 0 137996.56 139133.33 1662.29 o 1 4 0 704.98 616.04 40.50 o 2 4 0 2091.16 1843.87 64.23 o 3 4 0 102513.03 103361.14 453.06 o 4 4 0 10149.80 10040.83 146.45 o 5 4 0 65621.37 65512.38 397.88 o 6 4 0 8069.15 8551.86 150.45 o 7 4 0 1397.24 1489.94 74.46 o 8 4 0 28566.42 28807.66 319.66 o 9 4 0 2352.72 2245.39 63.08 o 10 4 0 109.33 147.88 33.97 o 11 4 0 27.06 15.52 18.45 o 12 4 0 219.60 207.26 44.68 o 13 4 0 87.57 250.56 63.40 o 14 4 0 7904.35 7904.47 295.54 o 15 4 0 1075.42 1081.19 121.86 o 16 4 0 4605.59 4557.79 243.06 o 17 4 0 3878.01 3914.24 228.22 o 18 4 0 1663.98 1904.53 172.98 o 19 4 0 6698.11 6749.06 318.52 o 20 4 0 89.71 114.86 88.21 o 21 4 0 6.29 -67.05 117.85 o 22 4 0 6398.13 6813.88 343.64 o 23 4 0 467.80 398.75 137.80 o 24 4 0 516.70 616.29 111.07 o 25 4 0 1057.47 1072.31 143.03 o 26 4 0 212.48 44.58 82.17 o 27 4 0 633.46 166.08 123.11 o 28 4 0 6.38 127.99 203.03 o 1 5 0 1536.63 1325.51 61.86 o 2 5 0 30.92 -5.70 30.59 o 3 5 0 6319.19 6476.40 127.14 o 4 5 0 8971.31 8809.66 159.93 o 5 5 0 932.25 914.46 46.14 o 6 5 0 8854.68 8905.79 174.03 o 7 5 0 13572.49 13973.72 214.85 o 8 5 0 25941.46 25914.01 338.64 o 9 5 0 492.20 435.58 46.51 o 10 5 0 810.24 882.08 95.21 o 11 5 0 27474.72 28004.47 490.38 o 12 5 0 7243.56 7139.78 255.89 o 13 5 0 377.57 364.11 106.15 o 14 5 0 18035.65 18070.74 429.30 o 15 5 0 404.09 525.57 95.81 o 16 5 0 4867.77 4820.64 236.87 o 17 5 0 1049.38 1170.20 129.63 o 18 5 0 974.61 908.93 128.46 o 19 5 0 956.37 1027.62 130.23 o 20 5 0 30.82 -41.63 80.62 o 21 5 0 2136.96 2302.78 191.13 o 22 5 0 44.27 165.28 75.50 o 23 5 0 164.00 241.62 79.72 o 24 5 0 286.56 214.22 107.64 o 25 5 0 191.33 137.09 114.65 o 26 5 0 850.15 753.37 201.06 o 27 5 0 313.93 383.98 203.03 o 0 6 0 25627.39 26114.62 418.94 o 1 6 0 1156.79 1044.52 65.55 o 2 6 0 356.02 295.13 39.06 o 3 6 0 9213.35 8757.03 158.33 o 4 6 0 3041.86 2954.77 105.10 o 5 6 0 450.42 450.50 39.83 o 6 6 0 99.88 96.40 31.18 o 7 6 0 3.66 -19.57 29.56 o 8 6 0 11.88 7.97 47.83 o 9 6 0 684.69 659.27 65.66 o 10 6 0 1019.61 979.19 88.56 o 11 6 0 13.51 20.70 67.89 o 12 6 0 1192.05 1216.24 119.96 o 13 6 0 427.49 324.81 81.95 o 14 6 0 1738.74 1845.63 150.17 o 15 6 0 1095.52 1102.81 123.29 o 16 6 0 1626.16 1905.59 192.98 o 17 6 0 80.55 77.28 69.64 o 18 6 0 515.45 653.36 108.67 o 19 6 0 364.39 245.15 77.41 o 20 6 0 187.23 168.11 87.63 o 21 6 0 15.60 110.95 106.43 o 22 6 0 173.35 178.03 85.73 o 23 6 0 235.02 262.55 168.18 o 24 6 0 10.50 45.00 132.41 o 1 7 0 1986.90 1872.05 89.60 o 2 7 0 845.68 870.92 63.15 o 3 7 0 3432.99 3481.52 133.40 o 4 7 0 65.45 26.60 39.18 o 5 7 0 1121.47 955.40 70.00 o 6 7 0 1703.77 1700.09 93.46 o 7 7 0 131.91 58.33 49.66 o 8 7 0 4989.73 5227.19 189.07 o 9 7 0 1481.40 1450.40 121.21 o 10 7 0 151.80 166.15 59.77 o 11 7 0 1569.80 1618.30 138.93 o 12 7 0 4.74 -58.35 59.93 o 13 7 0 521.42 580.63 95.01 o 14 7 0 73.93 205.05 73.44 o 15 7 0 0.33 84.88 69.05 o 16 7 0 2318.79 2295.55 199.09 o 17 7 0 61.41 98.07 81.92 o 18 7 0 295.13 379.73 102.05 o 19 7 0 991.53 935.34 147.86 o 20 7 0 276.37 529.54 128.23 o 21 7 0 194.68 84.46 102.15 o 22 7 0 49.13 -0.22 123.79 o 0 8 0 5215.11 5217.28 266.02 o 1 8 0 603.42 549.07 76.95 o 2 8 0 4410.65 4222.79 154.93 o 3 8 0 1701.86 1727.04 102.60 o 4 8 0 1025.46 1014.19 88.49 o 5 8 0 12955.23 13114.51 295.46 o 6 8 0 978.58 981.03 108.08 o 7 8 0 84.72 97.79 61.72 o 8 8 0 4890.92 4823.88 256.45 o 9 8 0 329.84 345.97 87.83 o 10 8 0 1049.54 1105.19 150.91 o 11 8 0 61.36 65.21 71.12 o 12 8 0 675.88 573.59 108.67 o 13 8 0 725.17 670.45 118.07 o 14 8 0 602.40 860.59 130.85 o 15 8 0 194.61 243.71 91.62 o 16 8 0 77.54 -26.66 81.53 o 17 8 0 419.00 339.54 180.55 o 18 8 0 515.43 447.49 119.00 o 19 8 0 1797.82 1880.76 349.16 o 1 9 0 0.87 -57.83 57.83 o 2 9 0 35.33 60.40 67.16 o 3 9 0 1520.58 1395.30 118.52 o 4 9 0 2342.01 2092.41 143.94 o 5 9 0 917.86 985.46 101.02 o 6 9 0 1987.35 2011.67 195.92 o 7 9 0 2546.62 2627.53 199.62 o 8 9 0 6485.60 6791.18 350.15 o 9 9 0 42.19 17.72 103.84 o 10 9 0 256.01 325.58 108.54 o 11 9 0 4521.33 5102.80 319.66 o 12 9 0 888.94 1152.42 166.78 o 13 9 0 300.88 522.01 155.09 o 14 9 0 660.26 525.79 131.62 o 15 9 0 311.66 398.69 101.72 o 16 9 0 608.69 723.83 295.71 o 17 9 0 117.41 600.25 273.64 o 0 10 0 1816.53 1752.77 212.19 o 1 10 0 367.22 275.72 80.08 o 2 10 0 0.15 -40.83 70.37 o 3 10 0 1029.75 944.12 107.31 o 4 10 0 378.64 288.06 73.39 o 5 10 0 329.62 334.84 98.57 o 6 10 0 466.35 271.36 95.24 o 7 10 0 145.04 136.57 104.48 o 8 10 0 78.74 -49.03 114.67 o 9 10 0 9.42 17.37 73.48 o 10 10 0 113.89 56.87 98.66 o 11 10 0 93.87 48.55 229.51 o 14 10 0 71.17 79.44 123.58 o 15 10 0 278.20 304.54 216.27 o 1 11 0 678.33 719.24 147.79 o 2 11 0 320.42 569.87 168.41 o 3 11 0 181.85 -24.43 95.77 o 4 11 0 755.72 920.79 339.85 o 5 11 0 17.82 -115.61 191.99 o 6 11 0 194.35 -153.71 344.26 o 7 11 0 290.83 763.55 278.06 o -29 1 1 85.32 246.09 344.26 o -28 1 1 42.97 238.59 105.25 o -27 1 1 1392.34 1602.00 183.17 o -26 1 1 0.26 150.76 83.72 o -25 1 1 115.44 185.72 84.27 o -24 1 1 1721.70 1772.38 146.96 o -23 1 1 87.61 172.64 78.40 o -22 1 1 547.72 430.99 71.27 o -21 1 1 876.42 832.06 99.63 o -20 1 1 450.01 492.78 85.29 o -19 1 1 17.59 91.24 43.87 o -18 1 1 294.70 403.62 60.63 o -17 1 1 4099.04 4118.03 143.34 o -16 1 1 1213.51 1273.39 83.65 o -15 1 1 574.00 705.89 54.47 o -14 1 1 9412.81 9383.65 181.83 o -13 1 1 4047.32 3881.79 91.73 o -12 1 1 665.75 784.08 42.99 o -11 1 1 29031.42 28511.65 234.66 o -10 1 1 182.69 190.64 26.24 o -9 1 1 2421.28 2555.66 59.18 o -8 1 1 75100.64 75121.10 579.91 o -7 1 1 6165.67 5833.06 93.21 o -6 1 1 58.69 122.56 18.36 o -5 1 1 57546.68 60778.38 461.84 o -4 1 1 1156.18 1362.40 35.58 o -3 1 1 16881.56 14423.80 1110.58 o -2 1 1 48248.00 34330.11 5646.55 o -1 1 1 10860.02 8807.76 1593.77 o 0 1 1 11516.15 9387.35 1677.23 o 1 1 1 291.82 151.33 42.23 o 2 1 1 1483.63 1426.89 111.34 o 3 1 1 5961.10 5936.64 70.03 o 4 1 1 148.45 188.51 13.50 o 5 1 1 12.39 52.63 12.28 o 6 1 1 4595.03 4816.57 75.18 o 7 1 1 788.89 924.48 37.19 o 8 1 1 690.29 663.05 31.10 o 9 1 1 19419.41 18978.33 174.50 o 10 1 1 1493.51 1509.06 54.71 o 11 1 1 589.64 587.73 42.26 o 12 1 1 13681.82 13277.84 228.29 o 13 1 1 11616.16 11242.46 227.29 o 14 1 1 7913.50 7744.84 167.01 o 15 1 1 783.23 1065.54 79.08 o 16 1 1 3.25 90.44 50.46 o 17 1 1 11216.38 10746.38 237.64 o 18 1 1 375.63 500.77 66.06 o 19 1 1 1180.51 1195.71 80.89 o 20 1 1 4991.52 5137.91 229.29 o 21 1 1 416.51 569.25 74.89 o 22 1 1 1142.09 1150.61 95.52 o 23 1 1 75.30 179.56 58.78 o 24 1 1 19.23 96.70 77.12 o 25 1 1 289.81 303.70 93.04 o 26 1 1 75.11 110.36 82.09 o 27 1 1 35.16 28.63 86.27 o 28 1 1 22.36 -60.88 112.35 o 29 1 1 4.20 -19.16 191.99 o -28 2 1 76.33 298.40 118.42 o -27 2 1 229.09 304.15 127.64 o -26 2 1 60.66 69.91 108.94 o -25 2 1 61.78 44.57 93.90 o -24 2 1 1628.47 1639.67 153.84 o -23 2 1 281.72 273.03 76.16 o -22 2 1 2989.68 3111.79 194.89 o -21 2 1 2988.61 3131.90 190.82 o -20 2 1 962.18 1210.49 126.35 o -19 2 1 10340.51 10092.61 316.77 o -18 2 1 903.41 966.67 107.89 o -17 2 1 2405.41 2341.08 151.66 o -16 2 1 17381.62 17131.75 371.35 o -15 2 1 4630.05 4193.55 182.66 o -14 2 1 7.74 -28.02 36.52 o -13 2 1 20588.04 19900.35 279.51 o -12 2 1 6831.10 6326.55 151.84 o -11 2 1 18837.98 18514.77 243.47 o -10 2 1 6136.44 5762.75 137.79 o -9 2 1 20996.25 21005.59 225.13 o -8 2 1 27583.48 28381.29 262.85 o -7 2 1 24.17 89.63 16.75 o -6 2 1 11548.53 12031.51 138.88 o -5 2 1 1014.23 1294.80 39.89 o -4 2 1 48.20 76.69 13.57 o -3 2 1 27750.60 28837.01 141.85 o -2 2 1 1237.41 1142.49 27.57 o -1 2 1 17593.44 17841.60 156.91 o 0 2 1 4086.11 3826.31 50.57 o 1 2 1 76441.46 77302.97 326.80 o 2 2 1 50.97 144.56 14.20 o 3 2 1 66240.11 65544.94 411.23 o 4 2 1 257.59 256.49 22.83 o 5 2 1 487.69 525.93 30.89 o 6 2 1 127011.05 121843.48 547.59 o 7 2 1 361.72 642.86 40.86 o 8 2 1 5532.10 5271.88 107.69 o 9 2 1 96553.40 94299.38 581.41 o 10 2 1 42.43 177.32 33.78 o 11 2 1 13662.55 13405.44 209.16 o 12 2 1 6819.65 6224.75 150.58 o 13 2 1 1324.87 1338.74 88.35 o 14 2 1 1778.79 1717.17 101.38 o 15 2 1 815.49 776.07 61.74 o 16 2 1 3.46 29.08 34.98 o 17 2 1 19.70 21.10 46.56 o 18 2 1 1686.88 1487.82 128.39 o 19 2 1 977.76 1045.28 114.87 o 20 2 1 4199.96 3871.09 207.20 o 21 2 1 3133.57 3195.71 196.75 o 22 2 1 5342.97 5288.02 258.15 o 23 2 1 3028.26 2780.03 178.91 o 24 2 1 728.76 732.90 99.60 o 25 2 1 4911.47 5122.81 274.97 o 26 2 1 20.44 372.13 98.95 o 27 2 1 0.09 220.77 113.68 o 28 2 1 1635.16 1786.01 281.81 o -28 3 1 70.22 -32.16 225.09 o -27 3 1 1052.46 1313.80 180.30 o -26 3 1 40.88 44.40 83.55 o -25 3 1 209.90 147.43 79.77 o -24 3 1 2239.16 2277.33 214.69 o -23 3 1 523.45 476.34 121.68 o -22 3 1 739.26 598.33 142.62 o -21 3 1 3036.25 3171.19 227.28 o -20 3 1 2850.56 2848.04 222.97 o -19 3 1 91.92 34.97 74.77 o -18 3 1 1090.14 1061.12 128.11 o -17 3 1 2720.27 2576.55 179.50 o -16 3 1 160.32 221.90 74.53 o -15 3 1 1123.65 1002.61 112.62 o -14 3 1 5366.73 5466.86 233.83 o -13 3 1 3762.50 3287.33 119.30 o -12 3 1 429.01 432.43 35.94 o -11 3 1 19685.96 18615.52 278.83 o -10 3 1 1535.11 1365.16 54.39 o -9 3 1 4177.36 4083.18 99.42 o -8 3 1 88836.90 86711.90 432.06 o -7 3 1 12577.76 12999.19 131.81 o -6 3 1 47.90 80.45 18.44 o -5 3 1 127455.67 126375.00 584.39 o -4 3 1 55.94 98.12 17.78 o -3 3 1 2115.30 2385.03 55.29 o -2 3 1 6488.62 6090.87 89.46 o -1 3 1 948.65 855.82 36.55 o 0 3 1 113.65 154.13 18.49 o 1 3 1 233.95 276.58 23.70 o 2 3 1 1234.01 1085.20 38.30 o 3 3 1 2448.77 2407.00 64.58 o 4 3 1 385.11 389.51 29.17 o 5 3 1 2393.60 2589.90 68.03 o 6 3 1 12586.02 12953.02 186.00 o 7 3 1 61.81 128.73 31.62 o 8 3 1 15800.79 16258.59 242.32 o 9 3 1 25903.45 24700.10 268.88 o 10 3 1 36.99 68.44 27.96 o 11 3 1 8988.72 8693.35 178.58 o 12 3 1 9425.50 9269.54 219.73 o 13 3 1 6518.65 6473.76 247.88 o 14 3 1 4859.34 4576.91 217.66 o 15 3 1 1514.99 1304.10 128.05 o 16 3 1 410.54 460.22 93.34 o 17 3 1 3582.77 3475.53 211.17 o 18 3 1 1327.98 1446.35 145.06 o 19 3 1 965.97 826.58 124.64 o 20 3 1 6300.15 6288.52 307.53 o 21 3 1 341.97 425.60 111.27 o 22 3 1 220.13 314.45 89.97 o 23 3 1 523.54 395.01 115.41 o 24 3 1 172.65 211.24 84.08 o 25 3 1 265.45 298.25 125.09 o 26 3 1 65.54 16.78 128.30 o 27 3 1 80.62 308.95 220.68 o 28 3 1 4.14 -127.99 150.06 o -28 4 1 6.94 -54.49 117.45 o -27 4 1 152.57 183.56 126.59 o -26 4 1 151.03 202.64 91.40 o -25 4 1 0.14 221.79 93.27 o -24 4 1 16.78 -37.00 89.78 o -23 4 1 404.26 377.41 112.78 o -22 4 1 181.64 167.33 122.31 o 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