data_2241117 _cell_angle_alpha 90.000 _cell_angle_beta 94.534 _cell_angle_gamma 90.000 _cell_length_a 5.4012 _cell_length_b 8.2178 _cell_length_c 10.2713 _exptl_crystal_F_000 200.00 _reflns_d_resolution_high 0.8528 _cod_data_source_file tk5365Isup2.hkl _cod_data_source_block I _shelx_title ' 111_m in P21 No4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 76.39 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -9 0 143.24 137.44 8.54 o 2 -9 0 172.14 169.59 10.58 o 0 -8 0 79.67 76.70 5.75 o 1 -8 0 36.48 34.10 3.08 o 2 -8 0 8.54 10.70 1.42 o 3 -8 0 22.99 25.71 2.24 o 1 -7 0 516.89 522.36 27.89 o 2 -7 0 366.25 347.52 20.97 o 3 -7 0 19.86 21.46 2.13 o 4 -7 0 212.93 193.00 11.42 o 0 -6 0 706.18 640.31 35.90 o 1 -6 0 557.07 562.43 31.30 o 2 -6 0 205.58 220.67 14.03 o 3 -6 0 637.70 638.94 49.66 o 4 -6 0 62.27 57.33 2.91 o 1 -5 0 10.75 14.20 1.56 o 2 -5 0 29.91 28.65 1.30 o 3 -5 0 3.61 4.38 0.55 o 4 -5 0 63.02 65.74 2.81 o 5 -5 0 4.67 5.35 0.91 o 1 -4 0 76.06 63.73 5.67 o 2 -4 0 490.84 463.55 11.66 o 3 -4 0 647.71 689.79 17.07 o 4 -4 0 172.92 178.45 5.55 o 5 -4 0 181.33 172.37 6.53 o 1 -3 0 1934.76 2025.20 104.25 o 2 -3 0 428.25 406.37 19.96 o 3 -3 0 115.76 121.90 4.62 o 4 -3 0 258.70 254.27 7.82 o 5 -3 0 187.57 205.14 6.29 o 1 -2 0 346.41 397.27 21.52 o 2 -2 0 213.42 210.52 7.90 o 3 -2 0 1135.79 1302.10 73.22 o 4 -2 0 4.04 4.51 0.45 o 5 -2 0 66.68 73.31 2.61 o 6 -2 0 38.69 36.51 2.54 o 1 -1 0 215.34 228.95 14.91 o 2 -1 0 754.09 805.41 55.38 o 3 -1 0 223.36 218.97 7.52 o 4 -1 0 672.51 745.13 18.07 o 5 -1 0 9.35 10.50 0.70 o 1 0 0 279.21 347.13 25.67 o 2 0 0 188.61 208.10 16.05 o 3 0 0 579.75 557.05 16.91 o 4 0 0 129.81 136.55 4.63 o 5 0 0 465.13 502.54 13.34 o 6 0 0 844.53 880.44 43.45 o 1 1 0 159.78 166.86 10.22 o 2 1 0 733.04 685.91 57.20 o 3 1 0 233.39 222.34 5.96 o 4 1 0 629.24 672.40 21.24 o 5 1 0 10.80 10.79 0.80 o 6 1 0 5.02 4.22 0.79 o 0 2 0 616.44 557.19 43.27 o 1 2 0 345.45 382.12 21.56 o 2 2 0 193.07 191.65 9.20 o 3 2 0 1129.79 1249.04 36.73 o 4 2 0 4.77 5.62 0.69 o 5 2 0 66.60 73.32 2.76 o 6 2 0 42.77 40.47 2.92 o 1 3 0 1904.66 1815.17 167.57 o 2 3 0 374.93 331.30 28.93 o 3 3 0 108.27 114.66 3.92 o 4 3 0 298.25 294.96 15.77 o 5 3 0 190.96 210.34 12.48 o 1 4 0 72.86 53.84 5.82 o 2 4 0 523.81 458.72 38.58 o 3 4 0 637.47 619.65 37.16 o 4 4 0 178.51 181.01 11.05 o 5 4 0 179.06 179.45 10.62 o 1 5 0 11.35 14.65 1.45 o 2 5 0 34.37 34.50 2.40 o 3 5 0 2.31 2.84 0.46 o 4 5 0 56.08 54.19 4.40 o 0 6 0 675.67 611.21 33.27 o 1 6 0 553.67 533.50 20.60 o 2 6 0 234.16 243.02 13.01 o 3 6 0 680.58 657.34 33.88 o 1 7 0 503.52 452.86 29.33 o 2 7 0 336.39 359.28 19.26 o 3 7 0 19.04 19.43 1.59 o 0 8 0 85.41 87.42 5.53 o 1 8 0 35.50 34.57 2.05 o 2 8 0 6.77 8.83 1.15 o 1 9 0 128.26 133.33 7.83 o 2 9 0 179.52 184.35 9.72 o -2 -9 1 38.37 39.91 2.98 o -1 -9 1 49.22 46.86 3.70 o 1 -9 1 154.25 149.39 9.56 o 2 -9 1 99.95 97.42 6.08 o -3 -8 1 404.41 412.62 23.70 o -2 -8 1 3.93 5.59 1.08 o -1 -8 1 426.88 434.84 24.53 o 0 -8 1 294.35 278.65 11.90 o 1 -8 1 20.71 21.04 2.35 o 2 -8 1 288.16 304.43 18.67 o 3 -8 1 262.19 259.39 15.23 o -4 -7 1 43.06 38.38 2.83 o -3 -7 1 26.71 29.71 2.65 o -2 -7 1 169.43 162.85 10.79 o -1 -7 1 5.12 5.69 1.16 o 0 -7 1 199.17 189.01 8.35 o 1 -7 1 454.75 486.30 27.30 o 2 -7 1 63.35 64.20 5.03 o 3 -7 1 56.33 63.00 4.65 o 4 -7 1 28.17 26.04 2.12 o -4 -6 1 235.95 221.08 11.15 o -3 -6 1 78.37 73.93 3.40 o -2 -6 1 350.61 360.99 21.66 o -1 -6 1 176.14 171.11 9.93 o 0 -6 1 186.41 180.88 7.89 o 1 -6 1 104.86 107.45 7.36 o 2 -6 1 432.33 444.22 15.89 o 3 -6 1 170.41 185.06 7.00 o 4 -6 1 47.39 44.77 3.36 o -5 -5 1 119.63 107.34 6.53 o -4 -5 1 307.91 301.37 17.22 o -3 -5 1 198.58 202.80 6.38 o -2 -5 1 1655.21 1673.80 48.99 o -1 -5 1 313.59 306.63 18.42 o 0 -5 1 221.03 207.27 9.12 o 1 -5 1 701.09 629.14 24.21 o 2 -5 1 263.98 256.97 7.83 o 3 -5 1 324.20 322.81 9.74 o 4 -5 1 610.95 636.85 18.49 o -5 -4 1 50.87 48.42 3.46 o -4 -4 1 134.70 145.20 5.73 o -3 -4 1 151.73 156.34 4.17 o -2 -4 1 26.68 26.03 1.06 o -1 -4 1 186.99 144.28 7.91 o 1 -4 1 557.14 529.90 42.01 o 2 -4 1 266.59 240.48 6.30 o 3 -4 1 82.11 86.89 2.64 o 4 -4 1 1.99 2.00 0.43 o 5 -4 1 107.42 113.05 4.42 o -5 -3 1 178.19 162.36 5.13 o -4 -3 1 213.83 233.95 9.34 o -3 -3 1 114.10 113.05 3.74 o -2 -3 1 520.02 542.14 18.27 o -1 -3 1 623.87 635.77 32.64 o 0 -3 1 246.09 247.05 14.00 o 1 -3 1 315.12 332.89 25.99 o 2 -3 1 140.39 132.09 7.51 o 3 -3 1 100.71 107.98 5.42 o 4 -3 1 68.09 67.06 2.37 o 5 -3 1 2.78 2.82 0.50 o -5 -2 1 124.47 120.85 3.94 o -4 -2 1 177.01 198.69 5.85 o -3 -2 1 694.80 672.71 22.07 o -2 -2 1 521.99 521.72 23.43 o -1 -2 1 1506.71 1564.64 117.31 o 0 -2 1 3049.77 2867.87 151.20 o 1 -2 1 276.04 309.78 23.55 o 2 -2 1 649.46 611.61 25.53 o 3 -2 1 685.02 708.26 50.61 o 4 -2 1 92.81 103.14 3.38 o 5 -2 1 560.17 615.79 17.70 o 6 -2 1 245.27 223.32 11.59 o -6 -1 1 5.57 5.82 0.64 o -5 -1 1 673.83 758.65 20.04 o -4 -1 1 93.99 97.76 2.94 o -3 -1 1 512.38 533.16 17.27 o -2 -1 1 2657.28 2849.30 205.41 o -1 -1 1 997.07 1169.65 60.44 o 1 -1 1 5611.58 4205.29 321.31 o 2 -1 1 108.67 115.82 6.70 o 3 -1 1 134.84 134.18 4.38 o 4 -1 1 895.81 1037.16 30.40 o 5 -1 1 80.77 87.01 2.55 o 6 -1 1 175.18 170.11 8.45 o -6 0 1 9.03 8.90 0.66 o -5 0 1 92.97 111.43 3.97 o -4 0 1 78.49 76.64 2.82 o -3 0 1 85.85 93.79 4.00 o -2 0 1 527.63 664.53 49.37 o -1 0 1 3115.94 3205.06 232.79 o 0 0 1 414.04 289.64 22.49 o 1 0 1 1484.33 1347.60 85.11 o 2 0 1 863.69 853.97 65.73 o 3 0 1 35.31 38.48 3.55 o 4 0 1 6.73 6.90 0.61 o 5 0 1 351.50 368.16 9.95 o 6 0 1 17.88 15.20 1.42 o -5 1 1 701.52 781.70 23.06 o -4 1 1 100.00 107.46 3.82 o -3 1 1 508.77 516.26 16.06 o -2 1 1 2511.04 2731.26 211.36 o -1 1 1 961.93 1101.11 61.34 o 0 1 1 675.71 573.58 39.97 o 1 1 1 5836.02 4721.69 344.78 o 2 1 1 132.27 123.54 9.80 o 3 1 1 137.11 132.22 3.76 o 4 1 1 870.90 980.35 25.92 o 5 1 1 62.26 66.27 4.91 o 6 1 1 160.62 140.85 8.21 o -6 2 1 154.35 132.32 7.99 o -5 2 1 123.91 120.13 5.27 o -4 2 1 167.07 179.44 7.72 o -3 2 1 681.69 646.46 20.55 o -2 2 1 547.04 551.24 29.63 o -1 2 1 1510.07 1508.04 83.07 o 0 2 1 2950.88 2602.98 211.18 o 1 2 1 265.25 293.25 16.67 o 2 2 1 528.06 541.58 44.50 o 3 2 1 720.52 746.26 21.49 o 4 2 1 90.06 99.10 3.56 o 5 2 1 576.40 626.25 23.22 o -5 3 1 183.01 169.62 10.26 o -4 3 1 216.81 244.01 9.50 o -3 3 1 126.50 130.02 5.49 o -2 3 1 516.60 514.10 41.67 o -1 3 1 579.57 541.61 32.35 o 0 3 1 267.82 249.60 16.13 o 1 3 1 336.70 323.74 18.61 o 3 3 1 108.45 120.74 4.77 o 4 3 1 58.04 60.00 3.10 o 5 3 1 4.25 3.53 0.60 o -5 4 1 46.51 47.55 3.75 o -4 4 1 154.96 157.23 9.50 o -3 4 1 129.08 124.42 9.00 o -2 4 1 21.50 19.08 1.27 o -1 4 1 171.79 137.40 12.44 o 2 4 1 274.00 241.72 12.98 o 3 4 1 91.63 91.26 3.12 o 4 4 1 1.87 2.68 0.56 o 5 4 1 106.31 110.61 7.15 o -5 5 1 121.16 111.32 6.86 o -4 5 1 334.09 320.54 18.18 o -3 5 1 217.36 199.66 8.10 o -2 5 1 1645.83 1799.21 87.78 o -1 5 1 330.15 325.06 17.18 o 0 5 1 243.11 227.44 8.62 o 1 5 1 672.43 595.74 22.97 o 2 5 1 258.59 256.81 13.96 o 3 5 1 348.34 307.82 17.04 o 4 5 1 637.68 602.37 34.86 o -3 6 1 62.33 58.24 4.10 o -2 6 1 349.92 376.02 20.06 o -1 6 1 157.41 146.84 6.44 o 0 6 1 189.09 178.49 7.38 o 1 6 1 113.99 114.60 4.97 o 2 6 1 407.30 428.91 23.53 o 3 6 1 167.67 170.44 9.94 o -3 7 1 26.18 29.67 2.12 o -2 7 1 173.30 179.27 9.96 o -1 7 1 6.51 6.45 0.81 o 0 7 1 206.43 187.72 7.82 o 1 7 1 460.91 454.51 17.95 o 2 7 1 64.69 72.09 4.60 o 3 7 1 58.14 62.93 3.91 o -2 8 1 3.44 5.74 0.91 o -1 8 1 400.94 407.76 16.08 o 0 8 1 265.78 273.06 10.98 o 1 8 1 22.56 23.67 1.60 o 2 8 1 299.64 328.63 17.24 o -2 9 1 36.82 39.07 2.57 o -1 9 1 53.21 55.67 3.55 o 0 9 1 24.66 27.48 1.62 o 1 9 1 153.28 160.02 8.84 o 2 9 1 90.45 91.84 5.58 o -1 -9 2 89.03 78.08 5.47 o 1 -9 2 226.62 208.40 13.40 o -3 -8 2 40.20 40.94 3.10 o -2 -8 2 125.91 132.04 8.43 o -1 -8 2 81.54 85.06 5.98 o 0 -8 2 114.54 102.55 6.85 o 1 -8 2 83.66 89.85 6.41 o 2 -8 2 88.42 87.74 6.14 o 3 -8 2 28.67 26.25 2.26 o -4 -7 2 108.07 96.86 6.05 o -3 -7 2 94.56 106.46 6.87 o -2 -7 2 477.97 471.58 28.13 o -1 -7 2 146.93 140.05 9.54 o 0 -7 2 372.28 364.41 15.06 o 1 -7 2 142.35 164.57 10.66 o 2 -7 2 36.51 40.83 3.48 o 3 -7 2 157.49 158.71 10.11 o -4 -6 2 301.97 283.58 11.41 o -3 -6 2 132.83 139.64 6.11 o -2 -6 2 298.53 301.79 17.97 o -1 -6 2 265.89 272.23 16.06 o 0 -6 2 331.05 326.28 13.56 o 1 -6 2 321.02 348.87 20.86 o 2 -6 2 958.68 975.29 33.85 o 3 -6 2 9.96 12.45 0.99 o 4 -6 2 88.95 87.09 3.62 o -5 -5 2 36.40 30.02 2.31 o -4 -5 2 152.89 149.24 8.87 o -3 -5 2 385.49 380.06 15.17 o -2 -5 2 255.99 251.92 10.73 o -1 -5 2 473.13 455.80 25.98 o 0 -5 2 1.89 2.37 0.51 o 1 -5 2 25.89 24.86 2.33 o 2 -5 2 209.90 220.51 8.31 o 3 -5 2 118.62 116.61 3.97 o 4 -5 2 31.06 30.82 1.38 o 5 -5 2 37.72 37.94 2.33 o -5 -4 2 63.98 64.22 4.35 o -3 -4 2 238.58 231.79 7.26 o -2 -4 2 40.38 40.19 2.99 o -1 -4 2 1439.82 1329.87 49.05 o 2 -4 2 125.14 113.99 3.04 o 3 -4 2 383.21 386.66 9.92 o 4 -4 2 103.76 101.33 3.47 o 5 -4 2 331.70 330.74 9.59 o -5 -3 2 394.48 391.12 21.70 o -4 -3 2 61.97 60.48 2.18 o -3 -3 2 448.26 462.74 12.77 o -2 -3 2 1355.27 1398.37 47.21 o 0 -3 2 645.27 650.82 50.46 o 1 -3 2 1449.97 1497.97 111.34 o 2 -3 2 193.70 174.38 6.37 o 3 -3 2 631.04 628.04 19.03 o 4 -3 2 546.93 622.84 18.22 o 5 -3 2 17.49 17.20 0.95 o -6 -2 2 151.19 136.86 7.52 o -5 -2 2 23.07 24.68 1.54 o -4 -2 2 96.11 93.59 2.91 o -3 -2 2 363.25 367.81 11.20 o -2 -2 2 638.70 631.14 33.19 o 0 -2 2 322.66 335.34 26.10 o 2 -2 2 172.30 156.55 7.05 o 3 -2 2 290.69 297.05 10.55 o 4 -2 2 92.09 91.62 4.19 o 5 -2 2 143.56 155.78 5.07 o -6 -1 2 62.68 63.14 3.84 o -5 -1 2 171.52 182.61 5.14 o -4 -1 2 744.55 823.77 21.85 o -3 -1 2 327.06 333.39 10.72 o -2 -1 2 366.89 350.28 18.23 o -1 -1 2 916.78 1014.94 70.95 o 0 -1 2 2748.40 2904.47 207.09 o 2 -1 2 343.00 373.16 19.28 o 3 -1 2 29.99 26.99 1.21 o 4 -1 2 157.28 169.78 5.80 o 5 -1 2 131.85 132.41 4.27 o 6 -1 2 188.11 171.08 8.83 o -6 0 2 123.62 103.95 5.57 o -5 0 2 30.54 29.54 1.46 o -4 0 2 1278.37 1460.08 33.97 o -3 0 2 12.06 8.96 0.61 o -2 0 2 104.53 123.63 7.01 o 0 0 2 6.60 14.64 1.56 o 1 0 2 147.70 155.71 9.89 o 2 0 2 887.45 651.38 50.63 o 3 0 2 348.85 372.71 11.53 o 4 0 2 639.71 680.87 20.78 o 5 0 2 671.62 710.38 28.81 o 6 0 2 1.19 1.20 0.46 o -6 1 2 57.82 56.03 2.72 o -5 1 2 160.34 168.46 7.34 o -4 1 2 760.20 821.16 25.52 o -3 1 2 307.63 303.57 10.09 o -2 1 2 352.04 320.13 18.45 o -1 1 2 864.62 936.74 52.19 o 0 1 2 2711.57 2472.48 205.48 o 1 1 2 1360.55 1182.75 91.46 o 2 1 2 347.05 342.84 16.09 o 3 1 2 25.18 21.84 1.12 o 4 1 2 169.33 179.97 5.85 o 5 1 2 128.31 131.31 5.61 o 6 1 2 180.38 159.87 8.76 o -6 2 2 143.49 127.68 7.94 o -5 2 2 24.90 26.61 1.69 o -4 2 2 112.43 111.63 4.55 o -3 2 2 325.32 327.87 10.97 o -2 2 2 591.62 594.98 46.91 o -1 2 2 1890.33 1790.16 97.39 o 0 2 2 345.07 327.52 26.19 o 1 2 2 42.43 45.55 2.48 o 2 2 2 162.17 142.44 12.44 o 3 2 2 248.18 259.54 10.62 o 4 2 2 98.05 103.15 4.40 o 5 2 2 154.11 170.28 6.73 o -5 3 2 412.30 399.47 22.71 o -4 3 2 53.90 55.39 2.93 o -3 3 2 414.37 415.86 16.74 o -1 3 2 646.81 610.23 33.91 o 0 3 2 748.70 657.37 36.64 o 1 3 2 1421.58 1407.72 78.34 o 2 3 2 202.57 184.63 9.59 o 3 3 2 598.66 608.26 22.96 o 4 3 2 579.38 665.70 24.07 o 5 3 2 16.99 16.87 1.23 o -5 4 2 63.42 65.50 4.71 o -4 4 2 207.23 218.97 13.27 o -3 4 2 248.70 247.17 13.98 o -2 4 2 46.96 43.57 2.10 o -1 4 2 1351.60 1174.60 65.54 o 1 4 2 361.06 322.73 17.28 o 2 4 2 141.60 127.76 6.62 o 3 4 2 393.52 378.52 11.84 o 4 4 2 111.75 107.62 4.60 o -5 5 2 29.98 26.71 2.41 o -4 5 2 160.76 148.38 9.32 o -3 5 2 406.66 381.48 14.80 o -2 5 2 277.72 295.02 14.73 o -1 5 2 464.85 445.61 24.07 o 1 5 2 26.82 26.15 1.57 o 2 5 2 231.20 226.36 12.34 o 3 5 2 125.86 120.99 4.83 o 4 5 2 31.31 28.22 2.56 o -3 6 2 131.16 141.50 7.93 o -2 6 2 288.50 300.91 16.57 o -1 6 2 278.10 265.52 10.92 o 0 6 2 335.86 323.23 12.67 o 1 6 2 343.04 356.74 13.83 o 2 6 2 928.83 938.63 50.28 o -3 7 2 94.36 100.01 5.89 o -2 7 2 453.19 496.31 26.03 o -1 7 2 163.15 152.76 6.40 o 0 7 2 357.92 351.56 14.00 o 1 7 2 146.96 166.09 7.02 o 2 7 2 37.08 41.43 3.06 o 3 7 2 164.85 165.58 9.01 o -2 8 2 123.99 130.35 7.68 o -1 8 2 83.73 85.59 5.57 o 0 8 2 102.00 101.76 4.62 o 1 8 2 85.02 93.84 4.24 o 2 8 2 83.84 94.46 5.64 o -1 9 2 87.16 89.85 5.20 o 0 9 2 62.89 57.76 2.74 o 1 9 2 239.11 244.71 12.56 o -1 -9 3 67.92 56.66 4.31 o -3 -8 3 81.76 76.65 5.01 o -2 -8 3 65.39 67.98 4.66 o -1 -8 3 185.85 193.84 12.29 o 1 -8 3 326.14 352.43 20.76 o 2 -8 3 259.08 286.57 17.76 o 3 -8 3 3.79 3.56 0.81 o -3 -7 3 235.83 246.59 14.74 o -2 -7 3 108.51 113.38 7.70 o -1 -7 3 565.58 582.01 32.64 o 1 -7 3 58.34 64.83 4.63 o 2 -7 3 119.41 126.30 8.43 o 3 -7 3 101.83 108.74 7.20 o -4 -6 3 73.54 67.30 3.17 o -3 -6 3 280.42 284.90 11.55 o -2 -6 3 185.26 183.37 8.10 o -1 -6 3 53.57 49.32 4.03 o 0 -6 3 128.09 128.73 6.32 o 1 -6 3 237.95 245.92 14.32 o 2 -6 3 140.97 137.20 5.57 o 3 -6 3 372.11 386.66 15.54 o 4 -6 3 53.06 47.41 2.19 o -4 -5 3 19.79 17.36 1.85 o -3 -5 3 472.36 483.85 17.74 o -2 -5 3 89.33 91.36 4.02 o -1 -5 3 37.19 36.19 2.96 o 0 -5 3 525.08 507.35 20.60 o 1 -5 3 495.55 504.45 26.58 o 2 -5 3 182.05 183.75 7.02 o 3 -5 3 341.45 357.20 10.26 o 4 -5 3 48.10 51.82 2.04 o -5 -4 3 68.91 66.93 4.56 o -4 -4 3 62.68 63.47 4.60 o -3 -4 3 446.76 449.95 17.98 o -2 -4 3 602.67 607.95 23.37 o -1 -4 3 1130.13 1123.79 43.37 o 0 -4 3 658.39 603.50 23.83 o 1 -4 3 19.88 17.55 1.83 o 2 -4 3 239.98 221.47 9.03 o 3 -4 3 88.94 89.20 3.18 o 4 -4 3 440.46 452.73 11.77 o 5 -4 3 297.22 290.59 8.51 o -5 -3 3 174.24 176.47 9.97 o -4 -3 3 335.89 330.35 18.69 o -3 -3 3 62.96 63.16 3.87 o -2 -3 3 476.87 482.51 26.34 o -1 -3 3 152.80 140.23 7.06 o 1 -3 3 184.72 193.04 15.92 o 2 -3 3 194.66 165.58 7.31 o 3 -3 3 85.67 87.94 3.11 o 4 -3 3 265.17 276.78 10.41 o 5 -3 3 103.77 108.23 3.58 o -5 -2 3 21.46 22.83 1.31 o -4 -2 3 683.02 684.99 20.95 o -3 -2 3 349.05 367.04 14.10 o -2 -2 3 684.89 715.78 34.25 o -1 -2 3 1855.61 1702.14 130.58 o 1 -2 3 612.17 579.14 34.26 o 2 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