#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:39:57 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181912 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/11/2241136.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241136 _cell_angle_alpha 90.000 _cell_angle_beta 100.578 _cell_angle_gamma 90.000 _cell_length_a 9.8539 _cell_length_b 9.8671 _cell_length_c 18.1633 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.6948 _cod_data_source_file lh5784Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -12 0 437.48 578.60 54.02 o 1 -11 0 56.12 58.06 20.77 o 1 -10 0 389.15 409.34 40.19 o 2 -10 0 176.95 176.20 27.78 o 1 -9 0 790.17 855.64 51.61 o 2 -9 0 104.16 126.48 22.42 o 3 -9 0 117.03 135.46 21.92 o 4 -9 0 263.74 265.27 27.57 o 1 -8 0 1828.64 1991.17 72.19 o 2 -8 0 555.02 594.76 39.58 o 3 -8 0 407.58 426.06 31.89 o 4 -8 0 29.16 22.62 11.32 o 5 -8 0 21.74 11.08 15.61 o 6 -8 0 251.01 229.41 29.08 o 7 -8 0 6.33 29.53 20.88 o 2 -7 0 889.49 893.90 43.36 o 3 -7 0 419.14 422.33 29.35 o 4 -7 0 857.80 847.48 30.87 o 5 -7 0 333.20 306.25 18.61 o 6 -7 0 31.68 40.18 19.04 o 7 -7 0 229.47 259.68 33.42 o 2 -6 0 71.26 66.58 13.84 o 3 -6 0 533.95 561.88 30.26 o 4 -6 0 92.09 77.14 10.33 o 5 -6 0 165.86 154.38 13.27 o 6 -6 0 204.81 219.58 30.01 o 7 -6 0 446.58 476.82 42.21 o 2 -5 0 96.02 89.76 13.87 o 3 -5 0 616.86 634.70 21.45 o 4 -5 0 179.80 179.61 12.75 o 5 -5 0 135.44 128.90 12.01 o 6 -5 0 237.70 291.62 31.28 o 7 -5 0 425.26 480.57 43.08 o 12 -5 0 7.33 53.03 29.87 o 2 -4 0 869.55 1006.87 32.52 o 3 -4 0 2122.31 2207.31 29.30 o 4 -4 0 648.55 685.21 17.62 o 5 -4 0 557.18 584.10 36.92 o 6 -4 0 88.07 138.76 25.85 o 7 -4 0 298.58 266.63 22.16 o 8 -4 0 350.35 339.00 25.99 o 11 -4 0 61.30 113.73 34.36 o 12 -4 0 120.57 171.76 40.62 o 1 -3 0 1874.78 1857.84 29.11 o 2 -3 0 227.04 237.08 11.01 o 3 -3 0 618.82 570.16 14.16 o 4 -3 0 899.56 951.47 40.13 o 5 -3 0 402.33 520.83 36.06 o 6 -3 0 854.20 794.24 33.67 o 7 -3 0 186.42 169.29 18.40 o 10 -3 0 127.75 162.53 35.35 o 11 -3 0 65.19 125.76 34.11 o 12 -3 0 57.43 69.60 29.63 o 0 -2 0 7508.91 8001.65 76.64 o 1 -2 0 95.20 72.94 5.37 o 2 -2 0 190.47 193.30 6.58 o 3 -2 0 1996.45 2017.50 48.77 o 4 -2 0 630.18 641.93 34.22 o 5 -2 0 265.90 283.84 36.00 o 6 -2 0 672.87 697.47 32.36 o 9 -2 0 153.26 188.65 34.62 o 10 -2 0 45.34 52.63 25.83 o 11 -2 0 21.87 37.25 25.63 o 12 -2 0 51.28 71.38 30.83 o 1 -1 0 2494.39 269.81 122.90 o 2 -1 0 15338.06 16067.32 376.52 o 3 -1 0 168.66 200.18 10.85 o 4 -1 0 1049.22 1046.99 32.81 o 5 -1 0 2082.86 1942.92 49.67 o 7 -1 0 45.96 74.15 23.68 o 8 -1 0 207.10 232.48 33.12 o 9 -1 0 323.49 334.01 40.82 o 10 -1 0 153.72 141.13 31.94 o 11 -1 0 1.22 10.90 21.90 o 12 -1 0 11.52 25.53 23.15 o 1 0 0 1743.76 1717.13 26.24 o 2 0 0 1851.79 1810.84 22.07 o 3 0 0 3130.67 3157.91 39.69 o 4 0 0 251.85 297.71 15.72 o 5 0 0 429.79 420.41 32.54 o 6 0 0 222.47 255.31 29.12 o 7 0 0 1107.60 1143.73 61.24 o 8 0 0 106.70 124.35 26.07 o 9 0 0 0.05 7.77 19.30 o 10 0 0 106.53 128.59 31.43 o 11 0 0 5.03 -13.16 21.63 o 12 0 0 23.01 21.42 22.00 o 1 1 0 2480.45 2431.30 35.55 o 2 1 0 15490.38 15977.62 159.89 o 3 1 0 177.91 193.50 9.50 o 4 1 0 1057.73 1042.38 42.45 o 5 1 0 2069.05 1963.44 65.98 o 6 1 0 1053.26 1026.65 52.28 o 7 1 0 46.89 34.06 16.56 o 8 1 0 206.59 190.08 30.46 o 9 1 0 319.65 335.12 40.08 o 10 1 0 153.54 129.87 29.98 o 11 1 0 1.31 -26.22 26.22 o 12 1 0 11.28 -9.27 24.92 o 0 2 0 7624.95 8163.57 76.26 o 1 2 0 101.15 84.49 8.16 o 2 2 0 189.71 186.96 9.58 o 3 2 0 1953.58 1947.08 42.46 o 4 2 0 623.85 621.14 21.66 o 5 2 0 258.68 227.29 24.16 o 6 2 0 678.50 659.64 42.98 o 7 2 0 511.70 477.70 40.41 o 8 2 0 87.73 84.30 21.62 o 9 2 0 154.30 137.47 28.36 o 10 2 0 45.31 50.62 15.72 o 11 2 0 23.51 33.57 17.06 o 12 2 0 51.76 73.70 28.84 o 1 3 0 1872.34 1857.57 32.71 o 2 3 0 212.03 215.38 22.39 o 3 3 0 619.91 578.49 16.51 o 4 3 0 904.93 943.17 22.48 o 5 3 0 390.39 405.23 33.04 o 6 3 0 861.69 788.78 48.92 o 7 3 0 183.83 149.27 26.06 o 8 3 0 164.18 162.35 20.10 o 9 3 0 89.08 96.36 17.82 o 10 3 0 127.45 145.23 22.15 o 11 3 0 67.21 87.19 19.58 o 12 3 0 58.58 51.37 28.63 o 0 4 0 712.71 853.60 37.01 o 1 4 0 161.88 172.53 13.87 o 2 4 0 867.40 959.63 28.08 o 3 4 0 2122.57 2169.57 69.58 o 4 4 0 665.70 691.52 20.73 o 5 4 0 562.43 578.76 28.68 o 6 4 0 95.52 104.01 16.15 o 7 4 0 299.81 298.62 24.99 o 8 4 0 342.11 358.05 28.57 o 9 4 0 0.37 -9.40 14.07 o 10 4 0 63.84 44.95 16.82 o 11 4 0 62.93 88.49 21.23 o 12 4 0 121.06 118.88 22.89 o 1 5 0 607.68 636.82 25.63 o 2 5 0 92.77 84.72 12.10 o 3 5 0 617.28 666.41 43.34 o 4 5 0 180.14 197.71 27.78 o 5 5 0 133.57 136.60 17.30 o 6 5 0 234.37 226.91 22.06 o 7 5 0 418.60 422.70 30.38 o 8 5 0 24.32 27.16 14.34 o 9 5 0 7.18 11.55 13.90 o 10 5 0 34.32 45.69 17.04 o 11 5 0 12.35 3.93 15.17 o 12 5 0 6.80 4.25 16.04 o 0 6 0 527.77 482.97 35.82 o 1 6 0 17.86 20.87 10.92 o 2 6 0 67.90 63.19 12.37 o 3 6 0 524.94 545.65 43.16 o 4 6 0 95.66 89.22 24.13 o 5 6 0 169.99 170.82 30.05 o 6 6 0 200.89 194.00 33.07 o 7 6 0 445.65 430.92 32.01 o 8 6 0 49.26 52.42 15.61 o 9 6 0 55.32 53.83 17.12 o 10 6 0 9.56 12.22 17.06 o 11 6 0 47.71 45.45 18.14 o 12 6 0 61.00 62.96 31.60 o 1 7 0 1012.92 987.50 38.37 o 2 7 0 878.46 885.06 35.87 o 3 7 0 417.12 423.09 42.23 o 4 7 0 865.98 826.44 58.69 o 5 7 0 324.03 379.41 43.29 o 6 7 0 35.12 26.22 23.32 o 7 7 0 224.01 249.71 39.91 o 8 7 0 28.49 26.75 24.47 o 9 7 0 147.75 172.58 36.83 o 10 7 0 25.33 21.90 16.71 o 11 7 0 57.83 52.83 20.46 o 0 8 0 1405.63 1479.33 70.05 o 1 8 0 1843.79 1820.49 55.06 o 2 8 0 577.53 548.98 31.76 o 3 8 0 395.59 410.51 45.15 o 4 8 0 30.49 25.08 22.90 o 5 8 0 21.24 32.67 24.91 o 6 8 0 249.60 268.09 42.14 o 7 8 0 6.94 7.63 23.75 o 8 8 0 5.74 2.77 24.36 o 9 8 0 130.62 129.35 37.45 o 10 8 0 64.72 59.73 33.37 o 1 9 0 803.70 812.27 40.55 o 2 9 0 102.58 106.31 18.93 o 3 9 0 120.69 156.41 33.87 o 4 9 0 254.26 247.74 40.26 o 5 9 0 310.79 269.38 42.40 o 6 9 0 243.38 282.96 45.48 o 7 9 0 163.58 171.95 37.94 o 8 9 0 26.49 41.00 29.33 o 9 9 0 11.92 32.86 29.57 o 0 10 0 235.74 213.95 34.80 o 1 10 0 389.39 378.15 31.17 o 2 10 0 174.91 170.66 22.90 o 3 10 0 368.63 337.98 45.30 o 4 10 0 97.71 84.54 30.15 o 5 10 0 28.04 5.83 24.51 o 6 10 0 32.57 75.33 33.82 o 7 10 0 122.67 147.94 38.96 o 8 10 0 88.18 95.60 36.35 o 1 11 0 58.49 60.60 19.13 o 2 11 0 181.94 213.61 39.66 o 3 11 0 90.30 92.63 31.70 o 4 11 0 22.27 30.99 29.44 o 5 11 0 117.01 101.56 33.57 o 6 11 0 229.69 234.26 46.47 o 7 11 0 360.90 447.35 60.86 o 0 12 0 429.10 563.82 57.97 o 1 12 0 213.36 249.46 30.02 o 2 12 0 143.20 150.78 36.02 o 3 12 0 33.37 40.56 30.94 o 4 12 0 93.56 102.41 36.45 o 5 12 0 204.11 234.16 48.21 o 1 13 0 57.89 67.80 21.90 o 2 13 0 63.99 91.81 36.11 o 3 13 0 56.89 76.26 34.69 o -2 -13 1 38.71 60.66 29.26 o -1 -13 1 33.60 60.24 27.02 o -1 -12 1 1.88 -22.77 23.14 o 0 -12 1 30.60 25.46 15.03 o -1 -11 1 470.71 522.90 45.80 o 0 -11 1 117.59 121.17 29.11 o 1 -11 1 5.48 4.35 16.96 o -2 -10 1 40.61 39.36 16.78 o -1 -10 1 3.61 -6.12 17.80 o 0 -10 1 59.46 90.31 23.86 o 1 -10 1 193.82 201.09 30.68 o 2 -10 1 99.22 100.72 22.88 o 3 -10 1 111.41 100.68 21.97 o -6 -9 1 41.50 25.27 16.96 o -5 -9 1 107.98 71.14 17.16 o -4 -9 1 440.81 380.44 33.81 o -3 -9 1 537.99 559.56 37.60 o -2 -9 1 313.10 312.95 30.79 o -1 -9 1 1334.06 1338.65 63.15 o 1 -9 1 347.69 374.38 36.46 o 2 -9 1 222.80 188.62 26.82 o 3 -9 1 237.79 216.15 17.37 o 4 -9 1 671.63 655.76 41.92 o -8 -8 1 57.98 126.26 29.34 o -7 -8 1 124.10 141.71 27.70 o -6 -8 1 28.81 13.52 15.69 o -5 -8 1 117.04 92.23 18.49 o -4 -8 1 259.50 237.91 17.01 o -3 -8 1 1.11 -1.32 10.78 o -2 -8 1 95.84 99.19 18.95 o 1 -8 1 305.15 288.14 30.93 o 2 -8 1 482.20 477.00 36.68 o 3 -8 1 494.55 484.84 23.40 o 4 -8 1 98.04 99.17 12.25 o 5 -8 1 57.59 32.86 10.44 o 6 -8 1 44.92 54.16 20.06 o -8 -7 1 12.18 49.35 26.63 o -7 -7 1 7.22 35.08 20.44 o -6 -7 1 108.63 108.64 22.45 o -5 -7 1 156.67 158.74 15.58 o -4 -7 1 10.05 6.28 10.26 o -3 -7 1 116.55 97.64 15.42 o -2 -7 1 422.60 415.16 29.36 o 1 -7 1 285.61 289.46 29.11 o 2 -7 1 71.93 56.96 15.02 o 3 -7 1 123.06 131.88 12.73 o 4 -7 1 455.14 435.07 21.12 o 5 -7 1 29.05 33.34 9.89 o 6 -7 1 90.64 102.81 17.45 o -8 -6 1 42.15 104.88 30.68 o -7 -6 1 55.82 70.15 24.88 o -6 -6 1 177.11 191.26 26.44 o -5 -6 1 294.75 286.87 15.97 o -4 -6 1 144.19 148.18 11.96 o -3 -6 1 562.38 578.19 28.65 o -2 -6 1 966.69 997.08 39.45 o 1 -6 1 578.01 591.63 35.93 o 2 -6 1 36.49 33.78 12.21 o 3 -6 1 461.15 471.16 20.15 o 4 -6 1 149.26 142.74 12.62 o 5 -6 1 174.91 173.02 14.82 o 6 -6 1 124.80 185.14 27.95 o -12 -5 1 25.23 48.03 27.86 o -7 -5 1 102.51 148.20 27.88 o -6 -5 1 151.00 118.04 23.16 o -5 -5 1 377.74 347.80 29.24 o -4 -5 1 11.16 1.77 5.83 o -3 -5 1 93.98 89.96 11.83 o -2 -5 1 1951.38 2054.21 50.02 o 1 -5 1 902.17 976.67 39.90 o 2 -5 1 311.77 344.49 24.97 o 3 -5 1 560.35 557.00 20.23 o 4 -5 1 1091.04 1098.69 30.20 o 5 -5 1 110.71 115.69 16.23 o 6 -5 1 712.04 786.04 45.29 o 12 -5 1 69.37 136.29 38.72 o -12 -4 1 5.82 48.60 28.83 o -11 -4 1 57.31 121.39 33.39 o -7 -4 1 734.39 679.20 25.41 o -6 -4 1 37.84 40.10 7.79 o -5 -4 1 705.19 682.12 22.50 o -4 -4 1 217.19 226.79 21.16 o -3 -4 1 1416.03 1493.18 25.97 o -2 -4 1 590.66 653.57 18.59 o 1 -4 1 1336.65 1433.03 43.56 o 2 -4 1 1144.68 1320.35 40.42 o 3 -4 1 438.08 422.24 24.50 o 4 -4 1 151.04 174.32 13.04 o 5 -4 1 433.29 472.75 33.64 o 7 -4 1 83.10 77.47 15.11 o 8 -4 1 186.84 177.66 21.40 o 11 -4 1 65.76 133.83 37.86 o 12 -4 1 51.50 69.48 32.21 o -12 -3 1 6.23 12.63 22.18 o -11 -3 1 80.16 117.50 33.04 o -10 -3 1 165.60 225.81 38.82 o -7 -3 1 307.00 278.38 20.13 o -6 -3 1 254.40 240.33 15.20 o -5 -3 1 166.54 220.51 27.55 o -4 -3 1 2068.71 2156.22 43.57 o -3 -3 1 999.54 985.06 16.33 o -2 -3 1 554.41 537.94 13.90 o -1 -3 1 93.81 108.59 12.46 o 0 -3 1 2018.22 2179.09 49.82 o 1 -3 1 2218.53 2287.59 28.20 o 2 -3 1 1679.58 1737.78 23.46 o 3 -3 1 1449.12 1474.99 28.95 o 4 -3 1 503.24 546.75 21.20 o 6 -3 1 174.07 190.07 19.16 o 7 -3 1 359.60 380.17 28.15 o 8 -3 1 189.19 178.16 21.18 o 11 -3 1 6.67 65.23 30.15 o 12 -3 1 109.26 134.91 36.93 o -12 -2 1 101.37 46.54 25.38 o -11 -2 1 131.33 140.33 33.80 o -10 -2 1 105.26 130.37 32.27 o -9 -2 1 6.94 17.81 20.61 o -6 -2 1 290.66 417.47 37.83 o -5 -2 1 998.46 919.04 24.83 o -4 -2 1 294.14 278.23 12.78 o -3 -2 1 2757.98 2763.97 58.11 o -2 -2 1 53.49 44.87 3.76 o -1 -2 1 1611.91 1639.27 83.89 o 0 -2 1 5699.64 6415.09 69.91 o 1 -2 1 903.23 910.80 12.11 o 2 -2 1 403.28 409.58 11.23 o 3 -2 1 4335.92 4417.44 48.46 o 5 -2 1 42.47 44.24 11.06 o 6 -2 1 813.41 806.74 37.65 o 7 -2 1 31.65 29.69 11.53 o 9 -2 1 132.32 178.03 34.59 o 10 -2 1 289.71 319.51 44.78 o 11 -2 1 84.06 151.28 36.30 o 12 -2 1 20.22 39.96 27.76 o -13 -1 1 43.06 61.00 29.60 o -12 -1 1 52.05 52.80 24.75 o -11 -1 1 60.20 75.17 27.46 o -10 -1 1 29.63 34.48 22.55 o -9 -1 1 173.93 173.38 31.84 o -8 -1 1 28.84 39.41 21.05 o -7 -1 1 13.08 38.87 19.77 o -4 -1 1 186.61 278.12 29.04 o -3 -1 1 3880.12 3782.60 55.40 o -2 -1 1 29069.22 30772.70 850.84 o -1 -1 1 3413.71 2627.97 945.25 o 0 -1 1 360.49 128.42 78.10 o 1 -1 1 3073.57 1228.57 123.72 o 2 -1 1 2607.99 2785.05 27.82 o 3 -1 1 1201.95 1251.82 40.57 o 4 -1 1 70.33 89.51 13.06 o 5 -1 1 607.22 624.77 31.37 o 6 -1 1 528.33 550.14 32.42 o 8 -1 1 39.47 52.68 23.19 o 9 -1 1 152.62 192.64 33.88 o 10 -1 1 22.15 20.19 21.71 o 11 -1 1 19.06 22.73 24.64 o 12 -1 1 172.02 218.20 42.46 o -13 0 1 11.31 -10.28 27.47 o -12 0 1 52.21 41.03 25.66 o -11 0 1 280.85 236.25 38.88 o -10 0 1 79.45 96.35 27.60 o -9 0 1 3.82 8.60 17.09 o -8 0 1 830.81 801.79 56.05 o -7 0 1 63.38 58.27 18.64 o -6 0 1 7.36 6.21 13.61 o -5 0 1 176.00 211.32 14.88 o -4 0 1 1454.69 1511.99 30.88 o -3 0 1 34139.52 33688.09 197.70 o -2 0 1 6125.69 6090.57 39.16 o 1 0 1 3419.79 3054.38 37.44 o 2 0 1 598.05 596.15 15.39 o 3 0 1 2340.75 2466.28 86.84 o 4 0 1 1005.99 941.85 36.09 o 5 0 1 955.09 1099.60 48.84 o 6 0 1 235.40 272.67 30.33 o 7 0 1 532.98 556.24 43.85 o 8 0 1 87.50 84.10 23.85 o 9 0 1 6.22 0.90 16.86 o 10 0 1 352.43 360.94 44.95 o 11 0 1 27.71 36.24 22.36 o 12 0 1 13.60 -4.13 24.29 o -13 1 1 45.04 71.01 31.75 o -12 1 1 50.64 65.90 29.09 o -11 1 1 61.38 61.45 26.57 o -10 1 1 30.02 30.79 19.20 o -9 1 1 173.61 178.70 31.85 o -8 1 1 29.00 29.95 18.33 o -7 1 1 13.80 5.50 15.05 o -6 1 1 1541.32 1521.72 62.99 o -5 1 1 1679.89 1750.83 61.01 o -4 1 1 179.81 191.62 20.24 o -3 1 1 3838.10 3694.67 104.75 o -2 1 1 29036.11 30317.27 177.77 o -1 1 1 3448.41 3556.65 31.12 o 0 1 1 382.21 361.59 12.87 o 1 1 1 3163.82 3114.89 38.77 o 2 1 1 2590.15 2721.42 32.17 o 3 1 1 1188.49 1223.30 22.02 o 4 1 1 76.58 81.02 16.30 o 5 1 1 614.53 630.52 38.15 o 6 1 1 522.71 546.31 38.96 o 7 1 1 180.19 171.29 27.23 o 8 1 1 37.92 28.52 18.24 o 9 1 1 154.22 156.71 30.35 o 10 1 1 21.94 -2.46 20.25 o 11 1 1 19.77 -26.72 26.72 o 12 1 1 172.41 174.98 38.18 o -12 2 1 102.33 96.97 31.35 o -11 2 1 130.07 128.47 21.04 o -10 2 1 103.33 98.87 17.60 o -9 2 1 7.16 15.25 12.09 o -8 2 1 984.56 1029.30 40.80 o -7 2 1 679.20 674.26 31.16 o -6 2 1 301.06 244.08 28.22 o -5 2 1 959.76 908.99 77.62 o -4 2 1 287.85 295.49 16.94 o -3 2 1 2754.27 2745.46 36.07 o -2 2 1 59.00 45.29 4.93 o -1 2 1 1622.69 1605.68 73.39 o 0 2 1 5766.60 6320.89 62.96 o 1 2 1 895.76 862.60 18.45 o 2 2 1 395.79 391.23 11.21 o 3 2 1 4236.89 4298.10 40.82 o 4 2 1 147.98 113.45 14.73 o 5 2 1 41.29 41.78 12.69 o 6 2 1 799.95 792.31 47.34 o 7 2 1 27.53 20.64 14.54 o 8 2 1 254.75 254.61 33.84 o 9 2 1 129.21 120.14 26.83 o 10 2 1 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