data_2241153 _cell_angle_alpha 90.000 _cell_angle_beta 99.363 _cell_angle_gamma 90.000 _cell_length_a 39.2739 _cell_length_b 4.3327 _cell_length_c 12.4234 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file wm5206Isup2.hkl _cod_data_source_block I _shelx_title ' gs14gs13 DCPA35K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 379.45 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 21497.48 22291.84 150.76 o 8 0 0 3959.20 4477.54 61.53 o 10 0 0 16787.10 17510.22 137.32 o 12 0 0 1067.85 1221.01 40.23 o 14 0 0 23931.19 24907.31 195.84 o 16 0 0 45977.67 46514.05 287.50 o 18 0 0 4827.09 4693.57 96.96 o 20 0 0 3939.74 3840.80 109.79 o 22 0 0 3271.46 3567.30 95.11 o 24 0 0 9.79 7.38 8.03 o 26 0 0 2415.39 2243.89 82.25 o 28 0 0 11768.19 11814.55 230.72 o 30 0 0 27891.09 27034.80 368.83 o 32 0 0 16256.98 16181.20 292.50 o 34 0 0 168.38 348.99 48.13 o 36 0 0 7838.56 7518.55 213.80 o 38 0 0 299.40 334.74 49.61 o 40 0 0 123.00 186.88 39.79 o 42 0 0 358.85 367.99 53.25 o 44 0 0 0.76 52.54 41.53 o 46 0 0 7379.51 7581.54 366.75 o 1 1 0 1323.41 1311.50 26.48 o 3 1 0 1154.69 1195.52 23.20 o 5 1 0 30.59 39.15 5.46 o 7 1 0 7943.25 7851.84 89.95 o 9 1 0 58151.27 59300.75 430.40 o 11 1 0 409.51 349.61 10.20 o 13 1 0 1764.45 1877.15 23.45 o 15 1 0 2753.83 2735.09 33.10 o 17 1 0 1614.92 1860.97 28.61 o 19 1 0 8893.31 9040.70 114.81 o 21 1 0 6133.88 6276.24 56.66 o 23 1 0 17.73 11.64 9.07 o 25 1 0 2152.99 1980.35 56.61 o 27 1 0 3971.41 4053.13 84.56 o 29 1 0 1327.17 1347.44 57.51 o 31 1 0 7065.86 6869.94 232.19 o 33 1 0 56.87 66.39 14.70 o 35 1 0 78.32 61.26 18.79 o 37 1 0 3466.41 3631.38 113.81 o 39 1 0 1766.67 1809.27 98.56 o 41 1 0 77.35 71.79 18.65 o 43 1 0 24.40 23.82 13.22 o 45 1 0 193.84 275.25 41.27 o 0 2 0 3700.98 3541.70 74.96 o 2 2 0 29493.13 28740.55 188.98 o 4 2 0 6019.56 5944.97 81.40 o 6 2 0 7410.16 7043.05 89.37 o 8 2 0 173.96 161.49 12.27 o 10 2 0 866.00 813.59 22.13 o 12 2 0 9400.09 9654.37 87.88 o 14 2 0 5266.70 5251.42 80.94 o 16 2 0 36.35 20.41 4.96 o 18 2 0 13327.03 13085.29 152.53 o 20 2 0 420.89 410.99 35.68 o 22 2 0 2566.53 2217.34 246.84 o 24 2 0 1637.44 1450.96 153.05 o 26 2 0 127.14 128.08 15.77 o 28 2 0 5111.26 4383.67 397.62 o 30 2 0 1608.75 1563.26 108.41 o 32 2 0 2661.41 2615.58 114.70 o 34 2 0 2935.18 2816.92 136.81 o 36 2 0 1259.37 1183.26 81.94 o 38 2 0 719.99 742.95 67.51 o 40 2 0 521.51 500.29 56.84 o 42 2 0 18.25 72.82 37.19 o 44 2 0 2323.70 2391.12 161.21 o 1 3 0 677.87 664.06 29.23 o 3 3 0 10428.34 10156.48 111.09 o 5 3 0 0.01 6.73 7.50 o 7 3 0 34.13 33.32 7.88 o 9 3 0 1439.60 1496.38 40.67 o 11 3 0 61.71 58.86 9.29 o 13 3 0 2243.38 2256.51 64.20 o 15 3 0 1127.15 1022.98 43.13 o 17 3 0 1391.52 1389.46 47.84 o 19 3 0 2352.05 2429.08 76.36 o 21 3 0 56.92 27.85 18.82 o 23 3 0 0.11 9.07 11.47 o 25 3 0 84.11 90.20 17.64 o 27 3 0 1297.70 1308.22 64.65 o 29 3 0 1432.92 1436.41 113.49 o 31 3 0 728.75 692.12 79.65 o 33 3 0 2529.56 2605.62 158.40 o 35 3 0 571.67 592.20 76.18 o 37 3 0 10.76 58.49 38.59 o 39 3 0 84.34 184.32 49.02 o 0 4 0 162.95 163.38 33.28 o 2 4 0 2494.25 2606.75 91.58 o 4 4 0 1879.35 1860.56 65.22 o 6 4 0 779.56 775.40 42.60 o 8 4 0 228.43 210.72 23.61 o 10 4 0 272.31 232.09 28.56 o 12 4 0 2993.58 3193.40 105.39 o 14 4 0 302.00 299.83 30.07 o 16 4 0 304.71 293.64 30.71 o 18 4 0 3613.21 3705.43 107.12 o 20 4 0 19.00 20.02 13.48 o 22 4 0 141.33 142.30 24.89 o 24 4 0 1069.18 1004.17 64.28 o 26 4 0 223.10 218.71 31.40 o 28 4 0 1040.71 1147.90 107.81 o 30 4 0 172.56 81.96 39.29 o 1 5 0 926.54 1043.96 79.25 o 3 5 0 37.99 21.66 12.96 o 5 5 0 270.35 305.20 38.30 o 7 5 0 337.96 380.92 42.76 o 9 5 0 548.64 576.49 52.39 o 11 5 0 295.99 290.16 38.06 o 13 5 0 202.14 202.39 40.47 o 15 5 0 3288.13 3269.46 149.09 o -47 1 1 1.68 11.90 26.76 o -45 1 1 208.89 255.09 35.84 o -43 1 1 110.71 116.61 22.39 o -41 1 1 93.65 171.57 28.48 o -39 1 1 3181.49 3015.49 133.58 o -37 1 1 55.54 37.88 14.46 o -35 1 1 421.14 424.49 37.68 o -33 1 1 2949.02 2921.43 78.74 o -31 1 1 6.13 0.84 7.34 o -29 1 1 1731.49 1719.94 55.76 o -27 1 1 279.86 275.47 16.57 o -25 1 1 7473.31 7123.10 116.84 o -23 1 1 5088.37 4922.70 55.50 o -21 1 1 351.39 423.01 13.96 o -19 1 1 8908.72 8500.95 81.44 o -17 1 1 2211.95 2535.96 34.50 o -15 1 1 3297.83 3560.63 47.90 o -13 1 1 6558.90 6845.87 82.04 o -11 1 1 179.83 215.55 8.07 o -9 1 1 3915.27 3398.02 90.83 o -7 1 1 1530.73 1687.10 39.55 o -5 1 1 6990.55 7287.72 77.42 o -3 1 1 9719.38 9569.95 72.87 o -1 1 1 24640.85 25322.33 120.44 o 1 1 1 4405.80 4522.56 41.86 o 3 1 1 6388.58 6750.83 60.16 o 5 1 1 206.27 332.95 13.94 o 7 1 1 27191.31 27326.26 228.71 o 9 1 1 1926.18 1926.72 26.35 o 11 1 1 58984.34 60914.86 501.45 o 13 1 1 9096.29 8942.60 105.06 o 15 1 1 1978.65 2067.16 32.77 o 17 1 1 20320.95 21409.19 202.57 o 19 1 1 355.65 297.37 13.18 o 21 1 1 3416.90 3341.81 42.53 o 23 1 1 1296.89 1179.47 28.49 o 25 1 1 0.60 8.01 4.17 o 27 1 1 2128.63 2054.28 48.90 o 29 1 1 550.55 577.88 34.73 o 31 1 1 2103.02 2256.06 70.19 o 33 1 1 172.51 196.68 22.20 o 35 1 1 1862.33 1837.10 69.02 o 37 1 1 50.87 70.77 18.27 o 39 1 1 75.17 63.81 20.76 o 41 1 1 1329.30 1263.34 84.60 o 43 1 1 3450.56 3341.11 157.18 o 45 1 1 141.62 189.75 38.32 o -44 2 1 472.16 500.48 61.15 o -42 2 1 471.79 549.10 65.55 o -40 2 1 2.08 -4.46 15.16 o -38 2 1 0.64 -8.52 16.86 o -36 2 1 56.07 52.06 21.60 o -34 2 1 6.99 15.60 23.28 o -32 2 1 121.57 117.28 30.43 o -30 2 1 2936.99 2907.33 144.94 o -28 2 1 2442.30 1748.11 520.87 o -26 2 1 82.00 69.53 25.70 o -24 2 1 126.55 102.67 18.45 o -22 2 1 2336.12 2050.61 214.67 o -20 2 1 6437.55 6607.74 110.15 o -18 2 1 451.13 516.17 20.69 o -16 2 1 10241.75 9407.32 269.27 o -14 2 1 4953.85 4667.64 254.96 o -12 2 1 12953.62 11625.65 707.66 o -10 2 1 220.29 174.51 11.48 o -8 2 1 7663.57 7131.21 228.90 o -6 2 1 4144.33 3696.24 132.67 o -4 2 1 557.83 512.76 20.18 o -2 2 1 3281.43 3289.11 59.83 o 0 2 1 3931.10 3627.22 66.57 o 2 2 1 9920.35 9883.13 156.92 o 4 2 1 2304.47 2467.15 58.46 o 6 2 1 122.91 95.37 12.24 o 8 2 1 4172.51 4092.74 67.06 o 10 2 1 371.01 337.02 21.62 o 12 2 1 579.65 513.66 23.37 o 14 2 1 235.86 286.14 20.74 o 16 2 1 12175.20 12638.06 217.14 o 18 2 1 658.32 560.47 29.36 o 20 2 1 2908.54 2816.91 67.14 o 22 2 1 27.27 19.88 7.09 o 24 2 1 867.81 884.81 45.04 o 26 2 1 249.36 285.83 31.32 o 28 2 1 8.51 16.05 18.24 o 30 2 1 1961.54 1977.92 97.14 o 32 2 1 108.11 120.21 25.75 o 34 2 1 716.23 748.07 63.81 o 36 2 1 442.69 495.70 53.59 o 38 2 1 2744.45 2849.02 130.10 o 40 2 1 129.36 176.87 43.44 o 42 2 1 553.00 582.39 106.26 o -39 3 1 599.76 610.15 103.11 o -37 3 1 2094.35 2571.14 163.71 o -35 3 1 90.08 51.84 21.19 o -33 3 1 48.45 84.93 36.98 o -31 3 1 678.15 658.42 77.42 o -29 3 1 161.85 157.09 37.61 o -27 3 1 809.98 920.09 54.28 o -25 3 1 281.53 296.61 28.07 o -23 3 1 215.37 191.14 24.60 o -21 3 1 5344.25 5241.57 123.97 o -19 3 1 66.58 71.74 13.62 o -17 3 1 3101.81 3112.87 83.39 o -15 3 1 0.14 9.05 5.94 o -13 3 1 330.01 316.20 21.82 o -11 3 1 2032.96 1945.96 53.82 o -9 3 1 448.02 391.61 25.26 o -7 3 1 4122.39 3929.98 71.07 o -5 3 1 1575.84 1489.86 38.64 o -3 3 1 838.91 892.38 34.82 o -1 3 1 3630.49 3558.47 70.49 o 1 3 1 27.06 32.39 8.10 o 3 3 1 7.97 5.27 5.15 o 5 3 1 265.19 291.71 21.58 o 7 3 1 507.89 548.14 27.74 o 9 3 1 7001.81 7077.91 98.51 o 11 3 1 104.57 104.05 13.72 o 13 3 1 3886.20 3952.44 75.26 o 15 3 1 2938.29 2992.65 70.75 o 17 3 1 321.65 305.19 23.58 o 19 3 1 891.45 878.03 39.09 o 21 3 1 238.01 250.13 28.71 o 23 3 1 107.95 99.93 18.24 o 25 3 1 2659.63 2806.06 95.08 o 27 3 1 135.09 159.47 23.17 o 29 3 1 4329.86 4403.76 196.18 o 31 3 1 189.59 243.04 54.93 o 33 3 1 905.07 904.83 93.91 o 35 3 1 21.66 28.34 55.65 o 37 3 1 15.13 25.88 60.88 o -32 4 1 112.33 102.59 27.70 o -30 4 1 116.90 50.93 69.30 o -28 4 1 9.08 0.67 41.33 o -26 4 1 1365.84 1535.35 80.58 o -24 4 1 666.76 681.72 53.06 o -22 4 1 1198.72 1300.40 65.83 o -20 4 1 168.59 192.59 24.75 o -18 4 1 2726.90 2700.48 100.41 o -16 4 1 1098.22 1092.21 63.76 o -14 4 1 145.51 178.61 26.35 o -12 4 1 540.33 566.08 44.73 o -10 4 1 870.15 968.70 57.51 o -8 4 1 151.65 174.44 19.75 o -6 4 1 2229.83 2312.73 68.76 o -4 4 1 310.38 298.47 25.09 o -2 4 1 453.82 442.80 27.27 o 0 4 1 49.19 40.65 12.00 o 2 4 1 1161.28 1203.67 51.41 o 4 4 1 1207.60 1249.45 52.67 o 6 4 1 1741.00 1737.31 56.20 o 8 4 1 1372.01 1435.21 51.54 o 10 4 1 1051.51 1041.27 47.65 o 12 4 1 13.81 6.84 16.74 o 14 4 1 3362.53 3670.22 115.45 o 16 4 1 52.53 35.47 23.77 o 18 4 1 342.34 303.04 33.41 o 20 4 1 71.82 80.09 17.74 o 22 4 1 1.66 16.60 13.83 o 24 4 1 903.59 881.61 60.69 o 26 4 1 396.28 392.75 40.36 o 28 4 1 64.43 100.36 35.92 o 30 4 1 14.00 66.00 32.84 o -17 5 1 313.49 278.53 39.21 o -15 5 1 493.09 543.92 53.73 o -13 5 1 266.98 292.97 36.97 o -11 5 1 0.29 -20.06 12.06 o -9 5 1 61.46 58.97 20.44 o -7 5 1 175.30 177.26 31.39 o -5 5 1 179.77 147.15 32.07 o -3 5 1 41.62 30.13 19.16 o -1 5 1 463.93 551.17 71.56 o 1 5 1 190.29 239.77 54.44 o 3 5 1 216.01 266.50 52.67 o 5 5 1 404.66 482.49 54.97 o 7 5 1 30.22 18.88 14.55 o 9 5 1 90.67 139.89 34.32 o 11 5 1 999.94 997.35 89.94 o 13 5 1 5.08 11.50 18.66 o 15 5 1 288.89 320.84 46.21 o -48 0 2 3180.03 3565.19 249.18 o -46 0 2 42.13 167.54 60.23 o -44 0 2 3364.17 3634.10 235.75 o -42 0 2 2594.14 2505.10 190.53 o -40 0 2 218.32 290.66 50.18 o -38 0 2 5583.74 5655.10 223.02 o -36 0 2 1.14 1.78 10.26 o -34 0 2 595.61 630.43 50.40 o -32 0 2 9844.61 9866.23 221.85 o -30 0 2 77.39 110.98 22.46 o -28 0 2 16555.88 16342.54 224.77 o -26 0 2 285.08 273.43 29.92 o -24 0 2 8596.48 7907.17 242.23 o -22 0 2 21661.92 21945.54 416.46 o -20 0 2 5033.27 5038.43 81.16 o -18 0 2 41626.25 44527.36 293.45 o -16 0 2 11099.29 11127.88 152.35 o -14 0 2 10159.55 9958.74 99.62 o -12 0 2 86027.66 83489.19 267.25 o -10 0 2 9679.69 9713.44 84.95 o -8 0 2 68718.50 67706.49 1341.38 o -6 0 2 2735.94 3046.54 77.47 o -4 0 2 593.81 556.68 34.22 o -2 0 2 3963.76 4296.87 98.60 o 0 0 2 12722.03 14069.39 185.43 o 2 0 2 203.17 200.83 24.10 o 4 0 2 9009.74 10187.29 177.86 o 6 0 2 2856.72 3063.78 103.65 o 8 0 2 93038.74 96073.99 1232.29 o 10 0 2 2960.98 3267.11 71.88 o 12 0 2 164.48 254.87 36.98 o 14 0 2 8502.33 9578.88 166.12 o 16 0 2 811.62 868.50 34.43 o 18 0 2 47791.02 48739.90 253.38 o 20 0 2 11.55 22.89 7.45 o 22 0 2 16680.45 15486.09 538.96 o 24 0 2 15529.87 15410.02 265.45 o 26 0 2 562.04 566.28 55.27 o 28 0 2 3918.60 3717.47 141.38 o 30 0 2 7324.25 7208.16 202.89 o 32 0 2 2807.54 2699.01 130.07 o 34 0 2 155.02 235.96 44.92 o 36 0 2 4484.90 4354.02 175.09 o 38 0 2 6027.63 5936.70 219.40 o 40 0 2 74.28 172.68 43.90 o 42 0 2 422.79 430.87 60.53 o 44 0 2 137.42 111.87 31.99 o 46 0 2 88.07 113.32 56.56 o -47 1 2 1415.37 1419.57 97.39 o -45 1 2 274.09 334.35 45.95 o -43 1 2 523.64 573.55 49.34 o -41 1 2 115.20 109.47 21.58 o -39 1 2 823.88 950.14 59.20 o -37 1 2 1005.08 1090.77 62.22 o -35 1 2 2388.45 2295.95 85.55 o -33 1 2 1828.41 1863.04 74.76 o -31 1 2 2057.94 2104.75 62.68 o -29 1 2 6000.00 5744.38 77.70 o -27 1 2 0.68 12.22 5.09 o -25 1 2 282.34 268.30 13.76 o -23 1 2 2204.43 2084.24 43.03 o -21 1 2 1047.85 898.19 20.23 o -19 1 2 10549.51 9538.01 126.66 o -17 1 2 9541.11 9487.73 140.28 o -15 1 2 1171.58 1295.40 37.85 o -13 1 2 1105.24 1120.38 33.25 o -11 1 2 1266.05 1288.44 32.55 o -9 1 2 11039.45 10589.81 640.86 o -7 1 2 402.93 470.96 32.41 o -5 1 2 12450.63 12838.28 71.92 o -3 1 2 19838.07 19779.71 243.89 o -1 1 2 117565.25 119300.17 619.66 o 1 1 2 11909.95 11818.22 180.56 o 3 1 2 1.12 3.31 6.94 o 5 1 2 1694.98 1786.22 39.22 o 7 1 2 2629.21 2509.09 43.38 o 9 1 2 4459.95 4864.97 76.44 o 11 1 2 7375.01 7605.67 98.55 o 13 1 2 6442.50 6886.28 96.72 o 15 1 2 10137.84 10408.84 121.62 o 17 1 2 8258.02 8552.00 141.53 o 19 1 2 829.99 829.10 33.44 o 21 1 2 1381.18 1410.79 39.04 o 23 1 2 853.63 804.14 28.75 o 25 1 2 326.86 304.28 17.01 o 27 1 2 16271.58 15624.77 149.95 o 29 1 2 3482.36 3466.15 87.17 o 31 1 2 8.53 40.41 13.70 o 33 1 2 1334.19 1325.71 58.27 o 35 1 2 79.94 84.04 20.93 o 37 1 2 119.40 145.10 29.47 o 39 1 2 365.84 387.60 45.49 o 41 1 2 238.90 302.14 55.41 o 43 1 2 1319.90 1239.15 109.36 o 45 1 2 3053.49 3043.64 198.61 o -44 2 2 1836.26 1783.64 145.39 o -42 2 2 1218.27 1274.89 92.53 o -40 2 2 1808.21 1782.97 107.45 o -38 2 2 28.70 52.02 21.93 o -36 2 2 343.96 278.71 39.38 o -34 2 2 453.72 513.83 65.23 o -32 2 2 1565.92 1375.03 101.99 o -30 2 2 6076.40 6222.20 211.08 o -28 2 2 340.24 194.87 81.13 o -26 2 2 4865.02 4906.64 127.05 o -24 2 2 1483.15 1416.82 67.52 o -22 2 2 742.93 727.89 48.63 o -20 2 2 33.85 37.81 10.06 o -18 2 2 1895.98 1888.83 63.38 o -16 2 2 119.45 120.49 15.85 o -14 2 2 12673.01 12507.24 156.56 o -12 2 2 9426.06 8749.22 368.27 o -10 2 2 25543.54 24072.51 495.91 o -8 2 2 2779.03 2781.24 42.97 o -6 2 2 1660.74 1454.35 35.26 o -4 2 2 8013.15 8102.18 215.46 o -2 2 2 2400.43 2355.98 46.36 o 0 2 2 2594.58 2647.54 49.58 o 2 2 2 7380.95 7582.94 167.79 o 4 2 2 1378.76 1327.96 45.16 o 6 2 2 5620.07 5593.50 109.46 o 8 2 2 142.51 160.09 18.15 o 10 2 2 1949.47 1957.61 59.53 o 12 2 2 5311.03 5299.75 116.43 o 14 2 2 503.17 497.58 37.19 o 16 2 2 945.72 910.34 44.04 o 18 2 2 856.50 904.62 39.18 o 20 2 2 8949.63 9062.61 126.63 o 22 2 2 1755.80 1747.37 56.08 o 24 2 2 1971.86 1882.05 58.67 o 26 2 2 303.82 340.19 25.45 o 28 2 2 153.28 112.28 19.84 o 30 2 2 1541.68 1460.06 81.42 o 32 2 2 1366.48 1419.25 91.46 o 34 2 2 7.80 24.74 14.98 o 36 2 2 1713.92 1986.78 173.95 o 38 2 2 29.24 70.20 31.95 o 40 2 2 1252.48 1284.03 114.30 o 42 2 2 56.26 91.13 37.71 o -39 3 2 67.84 121.18 42.79 o -37 3 2 18.11 79.29 76.76 o -35 3 2 0.64 -6.37 19.75 o -33 3 2 23.77 11.26 16.06 o -31 3 2 40.22 77.33 30.31 o -29 3 2 0.30 7.07 11.45 o -27 3 2 128.02 97.66 21.21 o -25 3 2 2960.14 3079.18 98.15 o -23 3 2 366.91 364.78 29.71 o -21 3 2 239.29 241.97 24.18 o -19 3 2 16.42 17.75 10.93 o -17 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92.06 o -18 4 2 102.40 163.94 23.80 o -16 4 2 4264.00 4264.56 117.12 o -14 4 2 1.67 27.07 15.06 o -12 4 2 413.24 393.38 34.71 o -10 4 2 4047.57 4097.92 106.84 o -8 4 2 134.41 140.92 20.00 o -6 4 2 24.42 43.08 12.05 o -4 4 2 1762.38 1730.94 59.24 o -2 4 2 1193.82 1161.79 49.04 o 0 4 2 3449.25 3441.14 104.09 o 2 4 2 106.86 107.33 17.11 o 4 4 2 911.47 919.55 50.26 o 6 4 2 1595.62 1559.55 65.67 o 8 4 2 792.36 834.29 42.95 o 10 4 2 787.05 814.67 42.63 o 12 4 2 1289.97 1283.71 54.19 o 14 4 2 3289.28 3066.11 95.82 o 16 4 2 34.20 54.73 16.65 o 18 4 2 175.03 174.46 26.94 o 20 4 2 1712.69 1777.51 84.58 o 22 4 2 266.65 267.54 41.08 o 24 4 2 45.66 31.52 17.40 o 26 4 2 1101.48 1175.56 83.96 o 28 4 2 114.92 174.11 45.31 o 30 4 2 729.31 745.57 90.12 o -15 5 2 191.57 190.22 38.50 o -13 5 2 162.97 157.62 31.83 o -11 5 2 12.13 27.39 16.66 o -9 5 2 146.26 194.16 38.14 o -7 5 2 2324.21 2362.48 122.75 o -5 5 2 644.83 706.36 67.96 o -3 5 2 185.15 209.62 37.06 o -1 5 2 639.74 698.69 65.84 o 1 5 2 16.98 46.04 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