data_2241163 _cell_angle_alpha 72.825 _cell_angle_beta 75.522 _cell_angle_gamma 89.168 _cell_length_a 14.0384 _cell_length_b 15.7969 _cell_length_c 16.7235 _exptl_crystal_F_000 2820.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file hb7461Isup2.hkl _cod_data_source_block I _shelx_title ' NAPTMO IN P-1 PH 1.90' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1181.00 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 152.58 165.13 18.75 o 2 0 0 49.54 345.23 50.60 o 3 0 0 474.98 514.58 27.63 o 4 0 0 873.54 975.45 68.51 o 5 0 0 16.00 30.22 13.97 o 6 0 0 2395.02 2546.25 140.44 o 7 0 0 697.82 711.04 52.05 o 8 0 0 211781.12 211555.91 6941.32 o 9 0 0 4857.93 4719.13 268.06 o 10 0 0 9049.10 9611.59 471.16 o 11 0 0 2482.98 2176.20 182.46 o 12 0 0 51680.87 52152.92 2189.86 o 13 0 0 104.79 109.12 280.02 o 14 0 0 1793.60 1762.01 271.21 o 15 0 0 1944.07 1934.18 304.98 o 16 0 0 2562.51 3344.92 407.59 o 17 0 0 5112.15 4638.99 503.42 o -17 1 0 53684.58 53155.87 3204.90 o -16 1 0 2310.29 1757.78 314.29 o -15 1 0 2297.06 2549.20 425.85 o -14 1 0 536.87 782.81 200.94 o -13 1 0 1732.86 1930.25 268.01 o -12 1 0 2834.89 2934.37 226.53 o -11 1 0 8706.43 8387.81 435.22 o -10 1 0 194.03 417.18 86.13 o -9 1 0 300609.44 314734.44 10988.69 o -8 1 0 2501.68 2486.33 260.40 o -7 1 0 107714.80 109906.97 2983.84 o -6 1 0 276.33 335.19 28.31 o -5 1 0 30843.50 30935.89 809.40 o -4 1 0 3833.48 3549.73 108.59 o -3 1 0 146.35 566.19 127.94 o -2 1 0 846.21 717.76 27.41 o -1 1 0 315078.62 375850.66 17463.81 o 0 1 0 69.31 150.91 20.04 o 1 1 0 216244.27 162858.27 6996.66 o 2 1 0 118.45 45.65 16.21 o 3 1 0 691577.56 657029.81 24254.84 o 4 1 0 1931.00 1745.53 82.22 o 5 1 0 4973.41 4996.61 176.82 o 6 1 0 2548.27 2348.96 115.25 o 7 1 0 4111.49 3861.66 174.03 o 8 1 0 4441.76 4471.47 194.88 o 9 1 0 21896.61 21891.69 767.06 o 10 1 0 653.25 687.72 102.56 o 11 1 0 196368.97 188867.78 7623.74 o 12 1 0 1389.43 1457.03 255.53 o 13 1 0 11262.51 11133.07 881.90 o 14 1 0 485.65 769.55 197.54 o 15 1 0 1669.86 2124.67 918.79 o 16 1 0 3115.71 2710.60 360.02 o 17 1 0 2688.83 2567.02 380.13 o -17 2 0 2260.74 2116.38 381.00 o -16 2 0 41065.91 40153.40 2461.80 o -15 2 0 1217.04 971.29 231.20 o -14 2 0 3880.96 2949.90 351.11 o -13 2 0 2753.15 2456.65 301.38 o -12 2 0 908.39 1086.07 139.87 o -11 2 0 140.31 120.14 63.95 o -10 2 0 17334.54 17354.40 784.78 o -9 2 0 2376.55 2443.60 152.78 o -8 2 0 203244.64 210760.09 7347.99 o -7 2 0 1379.84 1429.70 63.51 o -6 2 0 125201.71 129624.99 3312.82 o -5 2 0 1071.71 1044.14 47.78 o -4 2 0 5533.54 4895.77 136.29 o -3 2 0 498.13 574.50 32.67 o -2 2 0 4886.42 5377.28 178.86 o -1 2 0 2388.63 2227.03 128.25 o 0 2 0 29302.47 27310.76 1653.26 o 1 2 0 38.79 66.62 7.46 o 2 2 0 257309.88 221299.67 9310.76 o 3 2 0 656.90 649.96 37.91 o 4 2 0 110590.24 110413.63 3557.90 o 5 2 0 232.39 285.79 36.30 o 6 2 0 4989.70 5353.36 196.86 o 7 2 0 2468.89 2536.97 146.18 o 8 2 0 626.94 700.77 66.72 o 9 2 0 351.81 371.34 47.68 o 10 2 0 8062.09 7700.74 306.99 o 11 2 0 4482.44 4233.56 268.35 o 12 2 0 28566.44 30291.41 1615.57 o 13 2 0 65.21 117.61 118.80 o 14 2 0 20904.51 19552.80 1261.41 o 15 2 0 1113.57 1232.01 241.52 o 16 2 0 5648.71 5378.09 522.66 o 17 2 0 84.67 6.28 291.21 o -17 3 0 23901.54 24168.88 1611.73 o -16 3 0 29.46 151.21 158.40 o -15 3 0 2265.22 2687.84 722.81 o -14 3 0 1789.32 1778.50 288.06 o -13 3 0 1684.63 1483.66 242.19 o -12 3 0 86.50 25.64 61.11 o -11 3 0 3276.96 3251.21 230.32 o -10 3 0 4893.95 4675.03 276.31 o -9 3 0 12156.71 12876.65 515.36 o -8 3 0 387.14 362.30 79.15 o -7 3 0 7236.75 7753.28 232.79 o -6 3 0 11.77 57.57 20.02 o -5 3 0 42629.59 38598.62 966.69 o -4 3 0 1183.70 1178.21 58.07 o -3 3 0 2339.28 2151.65 172.25 o -2 3 0 632.96 652.07 39.22 o -1 3 0 19007.08 19123.88 786.73 o 0 3 0 58.28 95.85 15.65 o 1 3 0 1770.17 1532.60 65.99 o 2 3 0 164.12 143.28 19.99 o 3 3 0 54847.50 53294.13 1515.49 o 4 3 0 41.78 77.77 20.33 o 5 3 0 7534.75 7798.39 266.63 o 6 3 0 1115.48 1168.41 72.29 o 7 3 0 18600.90 18535.04 666.94 o 8 3 0 24.94 29.22 31.17 o 9 3 0 5402.32 5265.76 225.88 o 10 3 0 4143.38 4130.87 190.76 o 11 3 0 832.13 869.52 82.33 o 12 3 0 1747.43 1354.75 167.22 o 13 3 0 320.36 342.09 201.62 o 14 3 0 2013.94 2033.14 283.94 o 15 3 0 6154.52 6354.94 554.51 o 16 3 0 948.59 1046.57 257.36 o -17 4 0 1724.88 2074.38 588.24 o -16 4 0 1.61 143.47 164.07 o -15 4 0 936.81 615.29 204.14 o -14 4 0 9655.65 10321.24 870.13 o -13 4 0 267.34 108.76 118.05 o -12 4 0 3.31 60.34 63.60 o -11 4 0 1067.52 872.87 121.44 o -10 4 0 1298.73 1624.18 151.07 o -9 4 0 1044.45 1039.14 100.40 o -8 4 0 139.18 313.83 130.30 o -7 4 0 1059.20 1145.69 62.92 o -6 4 0 883.70 1248.64 97.85 o -5 4 0 106.28 99.24 21.36 o -4 4 0 338.41 410.99 41.81 o -3 4 0 320.88 324.23 30.58 o -2 4 0 9226.62 7828.05 344.90 o -1 4 0 121.68 101.86 19.50 o 0 4 0 1747.86 2087.12 91.69 o 1 4 0 3039.60 2958.88 96.37 o 2 4 0 799.92 650.74 52.18 o 3 4 0 401.74 453.75 35.78 o 4 4 0 465.57 317.53 31.80 o 5 4 0 554.92 602.20 46.91 o 6 4 0 1269.01 1550.02 85.30 o 7 4 0 4776.30 4885.43 227.74 o 8 4 0 2490.66 2496.99 151.89 o 9 4 0 68.59 98.06 43.75 o 10 4 0 1481.42 1587.25 114.82 o 11 4 0 647.58 683.61 70.62 o 12 4 0 1356.18 1177.73 163.30 o 13 4 0 1803.00 1270.71 224.88 o 14 4 0 514.21 537.68 182.18 o 15 4 0 4291.79 4195.65 784.81 o 16 4 0 1830.22 1759.16 425.78 o -17 5 0 359.59 887.90 261.02 o -16 5 0 32.93 -30.72 137.08 o -15 5 0 741.18 1002.04 247.17 o -14 5 0 1780.34 1721.56 487.43 o -13 5 0 290.36 418.64 252.03 o -12 5 0 1.87 -10.26 64.02 o -11 5 0 3685.24 3420.78 295.79 o -10 5 0 436.69 336.59 100.34 o -9 5 0 5695.45 5423.89 356.55 o -8 5 0 73.74 34.25 25.23 o -7 5 0 3864.99 4181.75 227.20 o -6 5 0 1040.86 1081.87 66.83 o -5 5 0 337.18 418.99 63.37 o -4 5 0 13.83 27.73 20.87 o -3 5 0 3070.41 2834.02 123.87 o -2 5 0 2.35 -26.72 17.81 o -1 5 0 3790.47 3712.06 232.73 o 0 5 0 11.13 -22.50 15.00 o 1 5 0 9914.35 9314.87 352.26 o 2 5 0 22.24 96.53 17.97 o 3 5 0 1441.34 1527.39 85.95 o 4 5 0 90.52 115.60 34.74 o 5 5 0 6497.34 6519.82 212.54 o 6 5 0 2653.92 2627.25 117.41 o 7 5 0 2130.17 2224.16 111.87 o 8 5 0 778.90 871.11 109.52 o 9 5 0 464.43 868.42 164.19 o 10 5 0 1153.50 1153.32 128.00 o 11 5 0 12391.28 11989.83 539.56 o 12 5 0 30.27 81.72 56.13 o 13 5 0 13067.65 11876.88 842.82 o 14 5 0 4390.34 3940.24 627.88 o 15 5 0 1167.96 1691.70 392.12 o 16 5 0 186.00 212.81 257.62 o -16 6 0 6517.24 7198.02 651.30 o -15 6 0 1933.69 1713.09 298.19 o -14 6 0 891.23 780.80 212.13 o -13 6 0 244.94 425.64 158.41 o -12 6 0 280.93 403.85 184.82 o -11 6 0 1554.33 1525.39 191.01 o -10 6 0 2146.36 2169.44 218.53 o -9 6 0 3239.71 3437.84 269.66 o -8 6 0 21330.72 20577.64 683.82 o -7 6 0 86.73 27.82 31.28 o -6 6 0 141248.16 136999.47 3989.35 o -5 6 0 24.51 31.65 31.06 o -4 6 0 6021.60 6333.66 273.34 o -3 6 0 1.08 31.25 19.08 o -2 6 0 7588.69 6556.61 295.58 o -1 6 0 806.46 767.05 59.05 o 0 6 0 9036.27 8772.35 269.20 o 1 6 0 2816.27 2613.65 117.22 o 2 6 0 231806.66 223364.53 5979.33 o 3 6 0 5261.90 5089.40 160.61 o 4 6 0 93492.90 89432.40 2639.51 o 5 6 0 6122.31 6299.85 225.91 o 6 6 0 6984.21 7007.81 260.11 o 7 6 0 548.58 518.25 54.90 o 8 6 0 20916.37 20365.24 835.71 o 9 6 0 1851.00 2114.70 156.35 o 10 6 0 7174.37 7009.94 350.26 o 11 6 0 1258.43 1124.66 146.66 o 12 6 0 21156.94 21198.46 1077.16 o 13 6 0 5133.60 4407.35 583.16 o 14 6 0 26753.22 25799.52 2299.30 o 15 6 0 39.25 11.20 190.41 o 16 6 0 1706.94 1389.35 403.36 o -16 7 0 99.64 89.37 324.82 o -15 7 0 61883.45 57476.12 4162.98 o -14 7 0 1231.48 1671.61 274.23 o -13 7 0 1083.31 1364.57 239.51 o -12 7 0 1210.91 991.79 207.27 o -11 7 0 1897.84 1826.66 213.50 o -10 7 0 2367.18 2281.24 221.05 o -9 7 0 264.33 361.03 87.66 o -8 7 0 126.76 119.41 43.98 o -7 7 0 201935.66 202716.53 6863.62 o -6 7 0 1342.53 1166.06 89.27 o -5 7 0 6661.71 6907.81 273.40 o -4 7 0 7629.33 7815.98 315.36 o -3 7 0 310353.44 307381.69 10192.45 o -2 7 0 647.81 657.90 85.13 o -1 7 0 24.31 55.04 25.89 o 0 7 0 3690.01 3341.16 135.21 o 1 7 0 2284.77 2524.11 103.72 o 2 7 0 293.74 291.58 34.45 o 3 7 0 10555.41 10256.78 297.59 o 4 7 0 10872.82 10492.57 306.41 o 5 7 0 352841.69 347052.50 10720.86 o 6 7 0 2229.89 2151.71 130.22 o 7 7 0 10070.40 10737.23 452.41 o 8 7 0 4783.53 4949.26 260.63 o 9 7 0 2358.14 2277.04 166.48 o 10 7 0 1511.93 1531.83 143.25 o 11 7 0 8701.16 9309.54 529.32 o 12 7 0 1711.79 2090.96 571.47 o 13 7 0 70019.38 63635.06 5239.33 o 14 7 0 1033.01 1288.34 358.50 o 15 7 0 11036.84 11452.29 1201.37 o -16 8 0 50630.98 55051.96 4755.62 o -15 8 0 237.63 -145.61 212.82 o -14 8 0 20414.26 17975.38 1209.20 o -13 8 0 345.76 472.69 212.82 o -12 8 0 62340.77 59211.00 3427.76 o -11 8 0 1426.12 1650.28 233.86 o -10 8 0 2662.92 2878.26 326.10 o -9 8 0 764.44 771.85 67.42 o -8 8 0 4242.99 4184.53 200.33 o -7 8 0 1229.39 1122.09 91.06 o -6 8 0 12168.08 12590.54 412.43 o -5 8 0 595.07 506.44 73.83 o -4 8 0 626330.88 643691.81 21620.69 o -3 8 0 537.16 636.76 64.79 o -2 8 0 8808.32 9071.01 633.88 o -1 8 0 2414.50 2399.25 116.71 o 0 8 0 13068.54 12282.61 376.72 o 1 8 0 1102.25 1055.05 59.90 o 2 8 0 11611.30 11228.32 340.98 o 3 8 0 1802.82 1769.46 81.93 o 4 8 0 270604.28 265820.06 7150.35 o 5 8 0 7690.32 7765.34 293.55 o 6 8 0 5884.62 6766.28 358.75 o 7 8 0 4698.99 4868.10 258.74 o 8 8 0 139661.44 142890.66 5365.76 o 9 8 0 1590.19 1761.13 150.94 o 10 8 0 11749.39 12483.96 838.24 o 11 8 0 65.13 31.11 104.95 o 12 8 0 2771.35 3052.63 325.03 o 13 8 0 7302.44 7326.52 546.22 o 14 8 0 403.44 515.26 280.03 o 15 8 0 1599.24 1871.10 425.76 o -15 9 0 24764.09 26093.82 2477.62 o -14 9 0 92.32 212.81 235.21 o -13 9 0 113068.54 115486.05 9341.04 o -12 9 0 156.66 358.42 257.62 o -11 9 0 37333.08 35730.26 2126.01 o -10 9 0 1237.69 1527.80 175.56 o -9 9 0 9556.59 9827.30 517.72 o -8 9 0 3210.22 3250.25 194.00 o -7 9 0 10179.04 10509.60 460.62 o -6 9 0 273.19 389.32 71.11 o -5 9 0 207143.80 208188.89 7605.87 o -4 9 0 11985.68 11668.58 485.34 o -3 9 0 197819.61 197938.09 7109.65 o -2 9 0 124.33 9.31 38.05 o -1 9 0 236656.19 228433.53 6662.54 o 0 9 0 3458.00 3130.81 123.41 o 1 9 0 15407.19 14125.95 434.14 o 2 9 0 140.66 72.62 31.29 o 3 9 0 399.33 523.88 56.97 o 4 9 0 2285.79 2317.08 115.51 o 5 9 0 33058.37 32836.25 1178.93 o 6 9 0 3.53 37.44 44.61 o 7 9 0 136288.09 140424.16 5284.05 o 8 9 0 8409.97 8585.40 467.66 o 9 9 0 39242.97 40886.90 1852.00 o 10 9 0 15.59 -142.56 95.04 o 11 9 0 905.41 1261.75 213.88 o 12 9 0 3156.11 3406.52 339.71 o 13 9 0 10358.87 9674.14 688.49 o 14 9 0 172.60 -56.00 190.41 o -15 10 0 556.89 772.92 403.26 o -14 10 0 6439.79 7795.60 1020.72 o -13 10 0 293.55 268.83 280.03 o -12 10 0 120833.16 125139.46 10066.04 o -11 10 0 1692.21 1893.68 448.21 o -10 10 0 12951.65 13094.20 1303.80 o -9 10 0 368.41 407.04 109.94 o -8 10 0 1469.97 1377.55 173.06 o -7 10 0 992.05 890.86 95.54 o -6 10 0 186.95 340.64 65.44 o -5 10 0 88.39 190.86 55.43 o -4 10 0 222350.42 216965.78 9954.52 o -3 10 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77.29 o 3 12 0 2074.27 2193.62 218.85 o 4 12 0 16992.66 16308.66 773.11 o 5 12 0 261.33 288.37 78.69 o 6 12 0 1356.29 1420.34 162.19 o 7 12 0 1454.30 1709.90 206.53 o 8 12 0 1170.65 976.54 199.12 o 9 12 0 28.37 -21.32 122.57 o 10 12 0 1258.49 1639.48 259.99 o 11 12 0 5762.82 5980.93 526.25 o 12 12 0 2546.65 2417.10 320.86 o -13 13 0 4669.49 4137.14 717.55 o -12 13 0 48.32 156.81 246.41 o -11 13 0 2286.03 2465.39 504.28 o -10 13 0 235.95 190.42 140.01 o -9 13 0 2064.60 1962.72 236.20 o -8 13 0 38.19 44.31 88.78 o -7 13 0 574.16 560.99 140.74 o -6 13 0 26.03 -81.42 69.13 o -5 13 0 2329.19 2434.44 531.54 o -4 13 0 0.78 -17.94 67.47 o -3 13 0 1177.59 1561.84 236.11 o -2 13 0 807.82 888.88 113.89 o -1 13 0 4587.21 4341.67 253.93 o 0 13 0 2028.62 2066.06 139.24 o 1 13 0 554.99 832.23 152.21 o 2 13 0 489.78 458.88 82.13 o 3 13 0 407.45 563.71 94.46 o 4 13 0 1309.96 1096.36 139.10 o 5 13 0 4647.08 4458.27 295.67 o 6 13 0 1134.38 1134.40 175.07 o 7 13 0 17181.17 16760.02 1122.74 o 8 13 0 21.42 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9594.15 618.93 o 2 4 21 115.94 189.84 138.22 o 3 4 21 518.51 468.06 156.63 o 4 4 21 711.64 584.67 171.11 o 5 4 21 5047.46 4813.34 479.09 o 6 4 21 4378.29 4315.56 554.76 o 7 4 21 46937.67 45189.43 2132.20 o 2 5 21 2801.78 2346.01 269.38 o 3 5 21 99.41 49.64 143.70 o 4 5 21 7767.45 6836.05 470.74 o 5 5 21 34.15 -119.74 101.62 o 6 5 21 3179.60 3135.82 430.03 o 7 5 21 1643.28 1517.05 236.16 o 2 6 21 31.26 -90.75 118.42 o 3 6 21 6963.50 5927.41 556.77 o 4 6 21 1400.72 1208.01 202.26 o 5 6 21 11677.23 10355.31 609.91 o 6 6 21 864.42 799.77 196.35 o 7 6 21 1592.64 1647.74 403.35 o 2 7 21 1582.11 1202.21 259.60 o 3 7 21 425.79 453.49 155.35 o 4 7 21 13409.72 12243.25 937.95 o 5 7 21 3312.00 3153.55 350.09 o 6 7 21 1031.92 1504.11 330.48 o 7 7 21 1034.44 941.21 352.89 o 2 8 21 5633.98 5608.23 552.72 o 3 8 21 3429.14 2512.32 335.68 o 4 8 21 1727.54 1725.22 277.06 o 5 8 21 2869.81 3289.54 360.42 o 6 8 21 68.16 45.42 132.29 o 3 9 21 4188.02 4021.35 427.62 o 4 9 21 851.73 460.64 197.56 o 5 9 21 327.99 377.50 176.10 o