#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:39:57 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181912 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/11/2241177.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241177 _cell_angle_alpha 90.000 _cell_angle_beta 95.315 _cell_angle_gamma 90.000 _cell_length_a 10.8177 _cell_length_b 28.5680 _cell_length_c 26.1639 _exptl_crystal_F_000 3944.00 _reflns_d_resolution_high 0.8366 _cod_data_source_file lh5785Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Prosp14AN020_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 963.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 109328.38 105614.93 7932.38 o 4 0 0 11976.36 11418.62 724.68 o 6 0 0 11960.11 12867.99 1817.28 o 8 0 0 586.78 425.01 139.70 o 10 0 0 41585.11 40238.51 1662.22 o 12 0 0 9584.25 8682.24 549.16 o 1 1 0 60130.47 61846.76 1954.20 o 2 1 0 28819.53 26281.08 897.10 o 3 1 0 8630.30 7757.80 276.85 o 4 1 0 21421.21 24557.91 839.59 o 5 1 0 22164.08 22251.63 795.84 o 6 1 0 585.88 496.68 39.37 o 7 1 0 79471.64 77598.26 2641.70 o 8 1 0 1663.19 1759.78 118.64 o 9 1 0 3552.13 3675.86 255.98 o 10 1 0 374.22 901.95 96.99 o 11 1 0 12479.61 12535.91 413.00 o 12 1 0 760.16 1011.14 134.66 o 0 2 0 189475.05 167219.09 7454.20 o 1 2 0 134651.36 145647.22 3928.64 o 2 2 0 34491.34 34717.01 1069.78 o 3 2 0 56680.06 54874.85 1694.99 o 4 2 0 39991.06 40302.22 1249.52 o 5 2 0 20649.15 23381.15 729.52 o 6 2 0 7891.64 8034.88 302.42 o 7 2 0 145.97 157.47 53.36 o 8 2 0 809.80 992.34 67.49 o 9 2 0 2418.35 2311.88 135.59 o 10 2 0 2348.14 2668.70 222.32 o 11 2 0 2183.44 2605.62 230.84 o 12 2 0 3588.55 3925.18 233.09 o 1 3 0 1330.83 1189.20 50.62 o 2 3 0 5093.15 5988.20 223.63 o 3 3 0 97232.17 99817.13 3045.72 o 4 3 0 61003.63 68557.98 2112.09 o 5 3 0 29306.61 28133.40 879.48 o 6 3 0 586.35 632.30 48.74 o 7 3 0 11488.29 11402.54 422.29 o 8 3 0 33613.88 30481.54 710.81 o 9 3 0 3521.86 3241.74 151.94 o 10 3 0 1840.26 1881.84 128.85 o 11 3 0 4522.83 4396.39 314.60 o 12 3 0 159.37 310.26 109.98 o 0 4 0 59.10 -37.62 37.62 o 1 4 0 19235.45 20759.22 533.80 o 2 4 0 37900.06 38239.27 1049.84 o 3 4 0 1000.10 570.16 147.94 o 4 4 0 85088.33 92480.94 2843.31 o 5 4 0 395.89 212.59 70.38 o 6 4 0 148.09 160.15 30.79 o 7 4 0 12.22 23.33 46.87 o 8 4 0 4567.97 4519.93 143.80 o 9 4 0 45.50 190.48 90.66 o 10 4 0 453.91 746.16 123.61 o 11 4 0 103.63 277.05 116.92 o 12 4 0 54.15 158.43 106.49 o 1 5 0 95285.57 98191.18 2305.70 o 2 5 0 238370.14 250760.42 6836.42 o 3 5 0 3870.96 3135.46 143.84 o 4 5 0 15361.66 17752.52 497.12 o 5 5 0 7394.51 7332.90 274.72 o 6 5 0 1398.10 1157.21 72.98 o 7 5 0 95.97 58.29 33.34 o 8 5 0 25900.13 23015.47 620.28 o 9 5 0 1577.93 1642.80 137.43 o 10 5 0 85.42 259.07 104.44 o 11 5 0 6513.58 6801.83 342.41 o 12 5 0 150.00 203.13 109.29 o 0 6 0 51609.79 57483.82 2305.97 o 1 6 0 73980.88 73194.27 1816.50 o 2 6 0 24823.67 28237.00 811.90 o 3 6 0 318.98 484.22 75.03 o 4 6 0 8.82 84.29 47.54 o 5 6 0 9380.97 9266.45 340.85 o 6 6 0 5235.60 5980.65 234.98 o 7 6 0 8376.73 7515.09 244.79 o 8 6 0 871.72 738.10 88.74 o 9 6 0 62.04 224.80 95.28 o 10 6 0 2857.81 2805.49 246.51 o 11 6 0 727.22 1180.56 148.23 o 12 6 0 537.13 714.24 124.75 o 1 7 0 2326.99 2240.50 130.43 o 2 7 0 121424.56 121946.93 3467.67 o 3 7 0 86597.16 97865.42 2668.71 o 4 7 0 724.58 661.83 47.64 o 5 7 0 4707.46 4852.15 195.03 o 6 7 0 5161.70 5298.29 237.43 o 7 7 0 1568.30 1615.95 96.72 o 8 7 0 714.83 599.85 59.58 o 9 7 0 4478.35 4663.36 240.21 o 10 7 0 1528.64 1912.82 155.59 o 11 7 0 2296.52 2594.42 174.28 o 12 7 0 8836.20 9266.28 613.91 o 0 8 0 120388.67 120958.94 4854.26 o 1 8 0 131964.56 134349.77 3636.10 o 2 8 0 71502.10 71920.53 2042.54 o 3 8 0 18123.33 19158.73 603.91 o 4 8 0 2145.86 1426.71 130.92 o 5 8 0 1163.07 1231.33 105.12 o 6 8 0 41110.60 42561.67 1647.00 o 7 8 0 5568.79 5418.96 172.03 o 8 8 0 3276.14 3216.96 139.48 o 9 8 0 1698.11 1814.98 142.20 o 10 8 0 27431.58 28443.38 959.27 o 11 8 0 177.59 664.29 141.10 o 12 8 0 72.02 169.24 110.77 o 1 9 0 1272.43 1039.24 164.12 o 2 9 0 43818.61 49868.30 1680.15 o 3 9 0 13960.67 15504.75 924.99 o 4 9 0 9511.69 9769.34 351.52 o 5 9 0 165.97 346.43 75.48 o 6 9 0 72.59 26.72 49.13 o 7 9 0 6548.33 5912.24 166.54 o 8 9 0 6154.40 5551.80 239.37 o 9 9 0 2740.29 2590.03 166.49 o 10 9 0 13973.54 14680.20 494.96 o 11 9 0 3010.73 4636.86 247.02 o 12 9 0 5842.87 5180.66 436.78 o 0 10 0 41233.18 48191.42 2303.59 o 1 10 0 59088.93 63056.18 2111.95 o 2 10 0 1566.71 1656.98 117.94 o 3 10 0 154686.95 155355.39 5931.94 o 4 10 0 43447.57 42930.99 1458.60 o 5 10 0 198.54 202.80 56.04 o 6 10 0 14987.31 16063.70 652.11 o 7 10 0 58777.73 52112.93 1196.91 o 8 10 0 4406.94 4345.29 210.03 o 9 10 0 4156.79 4325.78 222.08 o 10 10 0 3155.62 3633.98 262.02 o 11 10 0 8929.93 9597.03 471.23 o 12 10 0 797.02 766.03 148.78 o 1 11 0 24083.18 27268.37 930.77 o 2 11 0 71790.78 72610.02 3822.61 o 3 11 0 1428.61 1710.50 193.08 o 4 11 0 9304.93 10067.07 415.32 o 5 11 0 37330.94 36955.52 1442.09 o 6 11 0 47.98 186.17 58.30 o 7 11 0 13924.20 13005.24 336.87 o 8 11 0 4218.46 4097.43 224.82 o 9 11 0 661.88 666.78 117.08 o 10 11 0 13227.44 13300.90 459.00 o 11 11 0 13677.35 14040.08 576.54 o 12 11 0 2726.63 1465.35 271.81 o 0 12 0 49736.54 52363.49 2627.79 o 1 12 0 84840.62 87513.41 3502.50 o 2 12 0 10324.90 10132.26 388.85 o 3 12 0 7477.73 5886.37 528.77 o 4 12 0 64269.33 65482.18 3160.62 o 5 12 0 68.61 41.86 65.44 o 6 12 0 72734.91 64815.80 1484.26 o 7 12 0 1441.58 1485.11 91.58 o 8 12 0 177.71 250.69 89.82 o 9 12 0 91.06 133.40 75.37 o 10 12 0 1072.31 1279.52 116.19 o 11 12 0 25.35 487.17 143.96 o 1 13 0 122958.46 128960.06 5146.84 o 2 13 0 3141.73 2483.07 158.60 o 3 13 0 5353.79 4944.33 241.35 o 4 13 0 534.76 613.76 184.77 o 5 13 0 789.25 922.02 140.37 o 6 13 0 3810.59 3541.96 148.44 o 7 13 0 10634.99 9988.54 250.73 o 8 13 0 28.11 -27.17 65.92 o 9 13 0 298.82 319.42 83.05 o 10 13 0 683.63 803.94 138.78 o 11 13 0 17167.00 18200.03 1217.16 o 0 14 0 22492.03 19883.42 1290.40 o 1 14 0 1460.25 1053.81 96.18 o 2 14 0 14510.84 14859.44 632.18 o 3 14 0 8046.94 7894.44 661.72 o 4 14 0 17268.36 18832.45 1227.09 o 5 14 0 2180.40 2030.68 151.18 o 6 14 0 18921.72 17081.78 492.08 o 7 14 0 1459.32 1232.09 88.09 o 8 14 0 6155.35 5650.98 202.13 o 9 14 0 1642.67 1646.62 117.43 o 10 14 0 429.30 171.19 122.77 o 11 14 0 1433.18 1659.83 208.55 o 1 15 0 33415.36 36329.59 1477.94 o 2 15 0 65132.62 64031.20 2739.08 o 3 15 0 78.40 6.05 68.22 o 4 15 0 441.51 232.10 88.81 o 5 15 0 70.96 -39.20 50.36 o 6 15 0 2038.19 1858.80 95.94 o 7 15 0 5606.09 5331.57 180.88 o 8 15 0 4852.78 4535.05 180.87 o 9 15 0 234.76 69.06 99.04 o 10 15 0 31.81 -148.64 173.22 o 11 15 0 5415.85 5012.67 351.43 o 0 16 0 8086.66 9768.49 808.13 o 1 16 0 3366.86 2858.48 175.79 o 2 16 0 3651.99 4593.09 241.53 o 3 16 0 883.64 932.28 132.21 o 4 16 0 33245.31 25099.26 1803.85 o 5 16 0 310.43 215.36 67.57 o 6 16 0 567.70 481.45 78.54 o 7 16 0 1854.86 1912.90 124.09 o 8 16 0 2477.52 2096.57 139.57 o 9 16 0 6154.66 5969.09 371.94 o 10 16 0 29.87 -104.41 104.41 o 11 16 0 56.32 -38.08 82.56 o 1 17 0 6858.24 8440.94 512.36 o 2 17 0 630.42 569.87 89.59 o 3 17 0 7626.96 6487.30 478.13 o 4 17 0 7589.54 6996.40 202.95 o 5 17 0 1348.89 1362.30 88.17 o 6 17 0 346.14 174.30 89.07 o 7 17 0 5474.67 4723.19 275.33 o 8 17 0 1943.32 1797.33 178.31 o 9 17 0 3582.62 3835.34 380.49 o 10 17 0 181.41 -85.48 93.69 o 11 17 0 24.40 7.03 131.31 o 0 18 0 40915.41 42948.04 3215.01 o 1 18 0 21335.71 21748.37 1189.10 o 2 18 0 10341.91 9836.34 738.14 o 3 18 0 9927.85 9268.78 271.46 o 4 18 0 2732.12 2740.18 102.71 o 5 18 0 9383.16 8963.52 372.16 o 6 18 0 2630.54 2331.04 237.08 o 7 18 0 3166.18 3136.60 238.42 o 8 18 0 1514.52 1569.10 234.36 o 9 18 0 1831.89 2209.00 128.20 o 10 18 0 33.68 -58.81 58.81 o 1 19 0 1830.97 2235.38 298.54 o 2 19 0 2037.73 2300.06 94.23 o 3 19 0 17215.23 16621.45 360.20 o 4 19 0 4224.83 4219.60 137.04 o 5 19 0 1112.09 941.99 70.40 o 6 19 0 2075.04 1975.45 156.87 o 7 19 0 445.19 506.64 82.18 o 8 19 0 391.39 371.75 106.76 o 9 19 0 11078.42 10744.61 358.14 o 10 19 0 370.40 412.07 113.85 o 0 20 0 80595.92 79166.77 2322.42 o 1 20 0 21670.53 20074.40 444.45 o 2 20 0 20916.79 20413.43 417.80 o 3 20 0 5410.32 5653.27 166.48 o 4 20 0 23561.21 22978.01 478.48 o 5 20 0 1436.95 1554.64 83.24 o 6 20 0 1060.98 1213.66 95.74 o 7 20 0 142.26 17.60 85.94 o 8 20 0 3228.61 4117.12 252.68 o 9 20 0 194.72 451.88 93.64 o 10 20 0 45.72 66.56 52.15 o 1 21 0 2018.28 1892.45 75.24 o 2 21 0 1485.15 1513.95 72.79 o 3 21 0 25902.46 26075.02 580.77 o 4 21 0 7529.03 7426.83 201.35 o 5 21 0 873.13 982.73 74.38 o 6 21 0 113.94 68.38 72.28 o 7 21 0 144.15 136.66 75.70 o 8 21 0 12561.49 12402.91 382.59 o 9 21 0 10064.67 10537.08 323.76 o 10 21 0 2310.21 2201.10 196.30 o 0 22 0 48.47 752.48 127.20 o 1 22 0 81720.16 79915.76 1555.92 o 2 22 0 8966.90 9442.30 229.22 o 3 22 0 3713.08 3745.20 177.90 o 4 22 0 12299.40 12835.03 351.93 o 5 22 0 3776.23 3868.81 137.19 o 6 22 0 6161.75 6153.85 187.83 o 7 22 0 2410.40 2588.57 135.16 o 8 22 0 2286.04 2824.57 179.05 o 9 22 0 3401.10 3533.39 162.42 o 1 23 0 7374.29 7834.77 210.11 o 2 23 0 47.43 19.74 50.08 o 3 23 0 1681.66 1783.93 109.35 o 4 23 0 13533.29 14241.26 351.57 o 5 23 0 10946.63 11347.48 278.85 o 6 23 0 78.45 128.71 63.42 o 7 23 0 2993.19 3356.56 149.39 o 8 23 0 12985.04 13609.18 402.01 o 9 23 0 596.66 766.97 72.74 o 0 24 0 32719.50 32544.36 997.86 o 1 24 0 38501.16 38413.47 815.19 o 2 24 0 542.73 654.03 61.58 o 3 24 0 438.79 446.96 67.36 o 4 24 0 217.11 126.86 62.40 o 5 24 0 519.04 624.85 66.98 o 6 24 0 7976.41 8102.26 232.79 o 7 24 0 251.94 331.81 73.30 o 8 24 0 71.40 188.71 65.88 o 9 24 0 1411.12 1812.43 137.92 o 1 25 0 5.45 81.16 62.27 o 2 25 0 662.30 477.03 71.15 o 3 25 0 1078.33 1169.44 88.26 o 4 25 0 37.21 -64.64 64.64 o 5 25 0 7712.70 8266.89 275.29 o 6 25 0 595.58 586.78 82.11 o 7 25 0 5721.36 6131.74 245.72 o 8 25 0 402.02 549.97 95.70 o 0 26 0 10323.96 10698.42 376.61 o 1 26 0 2056.02 1977.56 97.72 o 2 26 0 2194.33 2422.86 112.67 o 3 26 0 1054.50 1041.01 83.65 o 4 26 0 2.08 -62.89 62.89 o 5 26 0 1700.69 1632.51 127.55 o 6 26 0 442.34 389.26 67.83 o 7 26 0 3744.69 4009.68 193.35 o 8 26 0 821.22 818.86 86.93 o 1 27 0 327.35 322.58 69.96 o 2 27 0 815.12 820.22 95.12 o 3 27 0 4164.51 4531.45 188.79 o 4 27 0 57.31 -57.05 60.91 o 5 27 0 208.91 163.63 68.04 o 6 27 0 600.29 726.87 71.39 o 7 27 0 699.43 703.59 89.74 o 0 28 0 228.29 242.19 95.86 o 1 28 0 3484.72 3605.08 141.35 o 2 28 0 1434.90 1881.26 116.85 o 3 28 0 4379.73 5123.98 200.58 o 4 28 0 3.41 -50.20 74.36 o 5 28 0 268.37 214.85 70.14 o 6 28 0 3563.63 3659.96 140.57 o 7 28 0 1227.80 1146.89 89.50 o 1 29 0 16.31 -63.84 63.84 o 2 29 0 18883.76 19523.57 512.49 o 3 29 0 15.33 517.11 124.90 o 4 29 0 629.66 579.45 71.30 o 5 29 0 300.04 325.61 67.81 o 6 29 0 46.02 -59.46 59.46 o 0 30 0 2502.25 2369.86 158.60 o 1 30 0 487.88 524.43 71.20 o 2 30 0 4983.05 6230.31 216.06 o 3 30 0 1194.95 1554.00 123.04 o 4 30 0 93.08 122.27 67.91 o 5 30 0 2337.22 2227.96 134.93 o 1 31 0 2739.22 2724.31 112.75 o 2 31 0 1000.27 1374.40 106.18 o 3 31 0 11518.72 12237.58 317.43 o 4 31 0 3.09 55.88 70.27 o 5 31 0 99.09 10.09 69.08 o 0 32 0 3718.08 4187.91 249.50 o 1 32 0 1517.25 1617.71 102.83 o 2 32 0 11105.56 11616.74 303.12 o 3 32 0 434.38 644.41 68.94 o 4 32 0 24.49 47.10 97.56 o 1 33 0 529.58 701.57 76.58 o 2 33 0 3463.67 3810.31 216.67 o 3 33 0 4808.75 5192.39 290.97 o 0 34 0 194.41 153.95 141.48 o -11 0 1 1231.79 1491.89 165.30 o -9 0 1 52010.11 48245.93 1968.60 o -7 0 1 21612.04 21067.65 1055.26 o -5 0 1 9796.69 8108.50 421.73 o -3 0 1 30389.66 30965.83 2378.39 o -1 0 1 408269.59 357097.50 26779.00 o 1 0 1 928193.56 935124.75 37106.98 o 3 0 1 40732.83 40918.33 1976.47 o 5 0 1 63642.12 66606.39 5866.28 o 7 0 1 5412.01 5877.23 742.13 o 9 0 1 5105.19 4416.55 276.16 o 11 0 1 28.05 129.68 115.34 o -12 1 1 4345.92 4216.28 241.29 o -11 1 1 781.34 1024.43 105.07 o -10 1 1 7190.05 6974.78 267.13 o -9 1 1 1631.27 1632.76 113.46 o -8 1 1 46162.60 40866.02 997.65 o -7 1 1 2307.14 1921.90 104.19 o -6 1 1 11442.38 11600.25 420.03 o -5 1 1 3343.08 2943.52 122.92 o -4 1 1 471.98 411.77 30.95 o -3 1 1 15665.94 15072.88 840.75 o -2 1 1 145.50 210.35 86.42 o -1 1 1 9084.97 7943.34 248.78 o 0 1 1 5227.26 6538.31 196.29 o 1 1 1 34040.87 37962.12 865.53 o 2 1 1 75152.98 79646.21 2682.14 o 3 1 1 80693.39 79998.38 2713.82 o 4 1 1 264464.66 279791.06 9433.83 o 5 1 1 18115.21 18872.09 658.90 o 6 1 1 160.61 160.88 30.52 o 7 1 1 50023.03 48508.26 1671.30 o 8 1 1 41933.11 36891.45 904.09 o 9 1 1 6867.62 6888.32 274.18 o 10 1 1 7736.08 7665.87 340.22 o 11 1 1 557.85 750.24 112.62 o 12 1 1 1795.39 2207.27 169.66 o -12 2 1 7350.74 7211.61 333.67 o -11 2 1 3416.96 3308.80 166.75 o -10 2 1 13239.36 13076.46 429.37 o -9 2 1 57.17 220.72 75.35 o -8 2 1 1417.87 1341.68 124.86 o -7 2 1 2133.98 1826.80 183.62 o -6 2 1 98.38 27.13 21.16 o -5 2 1 1846.26 2055.97 106.73 o -4 2 1 1409.38 2397.08 211.61 o -3 2 1 7706.89 9743.48 343.13 o -2 2 1 15948.78 14800.88 461.99 o -1 2 1 193505.47 198029.25 5546.15 o 0 2 1 314296.09 335311.06 9861.82 o 1 2 1 120199.82 130202.21 3131.45 o 2 2 1 110314.63 109022.46 3338.83 o 3 2 1 18092.14 19521.88 605.49 o 4 2 1 16072.65 16066.86 503.34 o 5 2 1 20661.54 19557.69 685.05 o 6 2 1 22295.29 22964.57 806.40 o 7 2 1 2168.98 2508.15 127.69 o 8 2 1 7166.78 6831.05 190.93 o 9 2 1 8409.39 7844.39 285.61 o 10 2 1 4825.30 5404.87 257.20 o 11 2 1 131.87 312.39 101.76 o 12 2 1 4111.25 3699.26 269.61 o -12 3 1 1000.21 1397.29 139.02 o -11 3 1 375.72 478.18 120.41 o -10 3 1 68.70 338.97 92.72 o -9 3 1 9996.12 9051.03 294.23 o -8 3 1 38279.77 33879.18 785.46 o -7 3 1 43726.73 43569.41 1507.35 o -6 3 1 15965.63 16787.52 595.64 o -5 3 1 55735.86 58362.46 1800.43 o -4 3 1 7969.96 10150.42 326.87 o -3 3 1 754.13 1186.42 73.49 o -2 3 1 294.72 195.54 25.83 o -1 3 1 6733.04 6851.95 179.04 o 0 3 1 27025.93 24323.78 661.77 o 1 3 1 21628.19 22560.34 595.54 o 2 3 1 34369.51 36786.86 1234.70 o 3 3 1 1987.28 2419.02 91.22 o 4 3 1 4372.77 4263.83 288.30 o 5 3 1 45864.44 48051.42 1642.16 o 6 3 1 15144.80 15105.25 541.24 o 7 3 1 35663.59 35116.78 1223.19 o 8 3 1 2312.83 2198.29 91.21 o 9 3 1 3910.12 4012.00 191.93 o 10 3 1 3260.71 3619.58 254.54 o 11 3 1 608.94 794.63 137.58 o 12 3 1 726.04 914.39 150.49 o -12 4 1 5997.12 5465.96 476.05 o -11 4 1 192.50 109.86 122.71 o -10 4 1 4904.12 4877.64 234.54 o -9 4 1 3247.28 2954.03 158.23 o -8 4 1 17465.20 16469.60 425.38 o -7 4 1 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