data_2241188 _cell_angle_alpha 90.000 _cell_angle_beta 107.185 _cell_angle_gamma 90.000 _cell_length_a 9.2597 _cell_length_b 15.6485 _cell_length_c 10.3574 _exptl_crystal_F_000 780.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file cv5498Isup2.hkl _cod_data_source_block I _shelx_title ' 3N4AgBF4 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 225.93 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1352.57 1550.41 27.07 o 4 0 0 594.00 588.39 34.43 o 6 0 0 2897.99 2676.21 81.71 o 8 0 0 574.17 565.66 55.80 o 10 0 0 4.37 12.35 44.14 o 1 1 0 5631.26 8095.79 282.05 o 2 1 0 202.05 209.31 11.78 o 3 1 0 17624.69 15447.68 357.37 o 4 1 0 129.49 151.88 8.25 o 5 1 0 2261.30 2349.32 76.83 o 6 1 0 49.40 68.07 10.05 o 7 1 0 224.33 255.86 17.46 o 8 1 0 36.69 39.89 23.89 o 9 1 0 780.53 744.08 47.40 o 10 1 0 11.34 -6.85 28.12 o 0 2 0 12826.41 14059.01 89.12 o 1 2 0 13.10 30.26 4.49 o 2 2 0 21195.63 23698.68 1008.66 o 3 2 0 1607.90 1422.55 49.93 o 4 2 0 401.98 427.87 13.37 o 5 2 0 2945.95 2911.15 65.14 o 6 2 0 2919.62 2690.44 68.43 o 7 2 0 436.33 507.56 23.12 o 8 2 0 360.96 371.76 32.27 o 9 2 0 77.21 26.80 29.43 o 10 2 0 4.54 7.79 29.41 o 1 3 0 63.89 42.31 9.19 o 2 3 0 25195.93 29272.86 806.33 o 3 3 0 12380.70 13067.73 704.17 o 4 3 0 2948.49 3058.60 67.36 o 5 3 0 370.73 325.52 17.59 o 6 3 0 172.06 180.58 14.32 o 7 3 0 278.88 299.30 20.10 o 8 3 0 137.82 133.29 21.36 o 9 3 0 464.70 525.19 55.59 o 10 3 0 291.48 297.81 37.22 o 0 4 0 53.28 38.21 10.86 o 1 4 0 404.44 468.21 26.87 o 2 4 0 3933.09 5421.22 337.63 o 3 4 0 769.90 1073.70 23.10 o 4 4 0 26.27 63.28 12.66 o 5 4 0 3146.61 3131.08 81.96 o 6 4 0 557.34 493.55 46.74 o 7 4 0 2782.69 2645.38 40.52 o 8 4 0 295.49 291.81 21.55 o 9 4 0 28.20 -13.35 25.59 o 10 4 0 13.96 -3.28 28.03 o 1 5 0 494.35 490.51 16.41 o 2 5 0 5662.78 4802.95 363.63 o 3 5 0 34.81 74.89 11.50 o 4 5 0 19214.98 18516.53 759.45 o 5 5 0 978.41 962.33 28.44 o 6 5 0 30.53 13.14 17.04 o 7 5 0 0.04 5.55 16.04 o 8 5 0 759.79 725.78 36.16 o 9 5 0 8.05 5.25 18.58 o 10 5 0 164.49 172.72 34.12 o 0 6 0 215.12 177.08 16.50 o 1 6 0 8271.27 7477.56 559.44 o 2 6 0 336.01 330.81 10.66 o 3 6 0 314.45 342.04 15.11 o 4 6 0 472.58 533.35 49.15 o 5 6 0 4406.40 4131.18 268.28 o 6 6 0 35.24 7.45 17.23 o 7 6 0 3052.89 2901.45 117.52 o 8 6 0 59.74 64.98 18.17 o 9 6 0 5.31 -10.66 22.61 o 10 6 0 1.42 -14.02 43.45 o 1 7 0 505.73 434.16 28.99 o 2 7 0 4087.36 3922.30 157.40 o 3 7 0 43.23 143.32 14.75 o 4 7 0 4462.51 3934.44 242.48 o 5 7 0 909.91 786.75 34.87 o 6 7 0 429.93 433.03 27.41 o 7 7 0 151.00 185.53 32.90 o 8 7 0 363.62 391.72 29.18 o 9 7 0 111.69 116.48 29.44 o 10 7 0 271.86 298.59 55.53 o 0 8 0 7911.41 7873.18 1151.66 o 1 8 0 6651.25 6481.26 443.56 o 2 8 0 4173.33 4754.12 203.02 o 3 8 0 362.77 432.69 18.55 o 4 8 0 34.05 29.10 12.65 o 5 8 0 2345.32 2138.33 163.73 o 6 8 0 1685.07 1593.28 61.08 o 7 8 0 853.32 1005.66 109.38 o 8 8 0 8.63 3.66 20.64 o 9 8 0 105.55 91.87 25.69 o 1 9 0 1091.19 1107.34 83.83 o 2 9 0 3341.90 3256.88 100.02 o 3 9 0 2988.52 2886.98 134.81 o 4 9 0 1607.55 1614.16 78.80 o 5 9 0 527.99 476.44 36.56 o 6 9 0 137.66 169.55 31.01 o 7 9 0 70.38 83.79 28.78 o 8 9 0 85.22 65.68 24.44 o 9 9 0 292.14 331.90 39.62 o 0 10 0 7595.33 7844.64 1167.28 o 1 10 0 1057.16 1221.01 63.63 o 2 10 0 1507.22 1495.53 75.46 o 3 10 0 8.49 14.67 17.73 o 4 10 0 349.44 381.97 25.89 o 5 10 0 63.78 61.31 27.89 o 6 10 0 525.65 465.09 38.16 o 7 10 0 40.36 46.64 28.23 o 8 10 0 298.58 316.89 31.97 o 9 10 0 119.80 124.08 28.44 o 1 11 0 1340.42 1220.61 80.40 o 2 11 0 71.93 102.73 20.47 o 3 11 0 7527.54 7402.91 476.42 o 4 11 0 102.66 102.43 20.23 o 5 11 0 53.61 22.80 26.07 o 6 11 0 63.82 24.83 27.84 o 7 11 0 136.18 165.82 34.29 o 8 11 0 22.80 6.02 22.87 o 0 12 0 5582.52 5412.85 686.64 o 1 12 0 146.63 178.02 17.39 o 2 12 0 1328.10 1266.29 80.50 o 3 12 0 7.88 21.26 20.44 o 4 12 0 69.59 80.71 20.33 o 5 12 0 24.69 33.63 27.65 o 6 12 0 1341.22 1217.07 104.18 o 7 12 0 2.99 12.35 22.89 o 8 12 0 181.72 227.50 30.38 o 1 13 0 1091.17 976.22 48.03 o 2 13 0 1339.49 1096.90 49.83 o 3 13 0 1417.29 1303.86 106.21 o 4 13 0 3.01 11.90 26.73 o 5 13 0 694.26 688.65 45.10 o 6 13 0 17.29 7.85 30.55 o 7 13 0 50.63 14.65 23.27 o 8 13 0 18.81 40.09 25.70 o 0 14 0 2268.85 1914.84 248.89 o 1 14 0 1027.26 846.42 74.71 o 2 14 0 893.70 793.98 34.35 o 3 14 0 16.47 43.02 21.73 o 4 14 0 56.94 53.08 28.94 o 5 14 0 475.32 525.40 68.43 o 6 14 0 247.21 294.47 40.17 o 7 14 0 126.82 145.52 50.46 o 1 15 0 0.27 30.11 21.67 o 2 15 0 234.85 209.45 25.48 o 3 15 0 272.02 325.26 28.99 o 4 15 0 894.75 847.02 87.59 o 5 15 0 340.19 375.77 47.89 o 6 15 0 43.51 29.05 40.74 o 0 16 0 10.60 73.99 44.28 o 1 16 0 985.27 855.02 59.63 o 2 16 0 323.14 279.17 33.08 o 3 16 0 9.82 -20.91 22.32 o 4 16 0 10.30 -6.92 29.04 o 5 16 0 460.92 449.53 66.35 o 6 16 0 31.45 87.10 36.78 o 1 17 0 8.58 -7.33 22.58 o 2 17 0 818.45 751.75 50.01 o 3 17 0 0.24 13.92 30.73 o 4 17 0 851.10 752.94 98.21 o 5 17 0 0.93 -3.40 31.10 o 0 18 0 213.86 101.19 49.42 o 1 18 0 300.94 255.84 38.50 o 2 18 0 135.28 139.22 27.89 o 3 18 0 31.26 45.17 32.49 o 1 19 0 108.82 141.30 39.69 o -11 0 1 228.28 234.87 56.91 o -9 0 1 1483.13 1425.06 78.71 o -7 0 1 897.73 813.11 33.81 o -5 0 1 2103.28 1912.50 108.84 o -3 0 1 5276.46 6766.49 309.93 o -1 0 1 7837.68 5607.16 355.50 o 1 0 1 362.92 901.45 18.88 o 3 0 1 6405.27 9413.76 76.62 o 5 0 1 4524.56 4442.58 418.94 o 7 0 1 19.82 13.75 19.18 o 9 0 1 653.68 723.36 60.38 o -11 1 1 75.40 36.50 31.02 o -10 1 1 68.34 48.54 36.23 o -9 1 1 0.29 -12.41 27.38 o -8 1 1 329.62 314.06 42.96 o -7 1 1 135.40 123.00 16.40 o -6 1 1 5017.13 4744.38 152.80 o -5 1 1 112.03 119.55 8.68 o -4 1 1 4366.30 4315.43 119.29 o -3 1 1 210.57 184.38 7.39 o -2 1 1 1174.73 1314.06 55.58 o -1 1 1 984.00 1041.19 43.37 o 0 1 1 35546.21 41930.88 939.50 o 1 1 1 10397.87 10428.15 455.69 o 2 1 1 35409.44 36893.56 191.13 o 3 1 1 420.30 530.24 14.65 o 4 1 1 115.08 123.95 11.22 o 5 1 1 2746.35 2903.50 88.46 o 6 1 1 1729.48 1550.49 82.29 o 7 1 1 1.54 12.34 12.88 o 8 1 1 743.42 735.76 40.78 o 9 1 1 45.10 39.50 27.55 o 10 1 1 12.64 9.39 27.83 o -11 2 1 19.70 20.80 32.88 o -10 2 1 165.93 174.83 33.22 o -9 2 1 1152.45 1046.36 47.21 o -8 2 1 397.09 438.72 27.06 o -7 2 1 895.06 902.07 29.41 o -6 2 1 221.33 234.03 11.86 o -5 2 1 1126.82 1229.21 39.79 o -4 2 1 1335.72 1252.24 32.63 o -3 2 1 5169.33 5276.20 174.47 o -2 2 1 5061.39 5171.89 188.89 o -1 2 1 11048.83 10532.94 481.87 o 0 2 1 561.19 481.62 7.96 o 1 2 1 1257.59 1248.68 65.96 o 2 2 1 12406.22 11781.26 212.40 o 3 2 1 14702.96 17577.76 244.40 o 4 2 1 2564.89 2723.80 131.36 o 5 2 1 3899.78 3683.00 130.28 o 6 2 1 71.73 58.49 13.09 o 7 2 1 29.72 33.30 13.48 o 8 2 1 1.03 -2.47 18.22 o 9 2 1 296.71 324.71 34.77 o 10 2 1 39.40 44.99 30.87 o -11 3 1 170.15 155.10 38.94 o -10 3 1 68.95 72.05 31.69 o -9 3 1 15.72 -12.90 24.63 o -8 3 1 363.67 327.75 25.11 o -7 3 1 1137.12 1163.01 30.72 o -6 3 1 1336.24 1290.23 60.94 o -5 3 1 3575.54 3366.31 119.46 o -4 3 1 2131.56 1659.71 48.34 o -3 3 1 927.20 1221.01 36.09 o -2 3 1 31721.42 28690.18 1186.07 o -1 3 1 18078.69 18230.07 534.12 o 0 3 1 3973.42 4944.56 159.37 o 1 3 1 1030.98 640.24 30.15 o 2 3 1 4900.67 4844.90 45.81 o 3 3 1 470.43 641.86 98.06 o 4 3 1 453.03 475.76 22.62 o 5 3 1 1848.40 1840.29 110.86 o 6 3 1 1073.92 957.82 36.45 o 7 3 1 1395.12 1281.07 34.16 o 8 3 1 356.81 425.15 23.75 o 9 3 1 48.45 89.30 28.70 o 10 3 1 0.17 7.29 30.34 o -10 4 1 127.34 108.51 37.76 o -9 4 1 39.77 37.63 21.09 o -8 4 1 991.71 1144.27 39.89 o -7 4 1 773.53 779.30 27.48 o -6 4 1 253.73 245.61 18.17 o -5 4 1 0.46 11.43 13.64 o -4 4 1 2856.90 2923.11 105.52 o -3 4 1 5017.79 4450.67 250.39 o -2 4 1 51043.90 48609.65 2673.96 o -1 4 1 1938.53 2301.51 63.15 o 0 4 1 2223.91 2453.28 110.98 o 1 4 1 10536.10 11550.69 529.13 o 2 4 1 5899.41 5793.96 210.25 o 3 4 1 281.00 223.66 13.60 o 4 4 1 5716.00 5122.86 286.92 o 5 4 1 1539.85 1618.23 96.76 o 6 4 1 555.49 552.92 40.01 o 7 4 1 42.60 37.21 17.77 o 8 4 1 192.87 274.06 27.30 o 9 4 1 106.18 74.17 29.29 o 10 4 1 189.04 154.56 33.52 o -10 5 1 0.04 -11.42 29.78 o -9 5 1 45.47 20.92 21.14 o -8 5 1 1.84 -3.61 16.44 o -7 5 1 2620.20 2388.55 94.11 o -6 5 1 413.13 379.31 21.06 o -5 5 1 7631.13 6507.01 357.62 o -3 5 1 1.07 15.44 6.18 o -2 5 1 1061.90 1103.48 58.88 o -1 5 1 1519.06 1320.60 54.10 o 1 5 1 10493.84 11476.41 470.00 o 2 5 1 318.85 339.56 18.54 o 3 5 1 64.68 46.21 10.59 o 4 5 1 3.96 22.33 11.97 o 5 5 1 1504.02 1409.18 74.68 o 6 5 1 137.05 144.07 19.10 o 7 5 1 2342.47 2241.40 84.12 o 8 5 1 62.01 50.92 20.36 o 9 5 1 145.25 147.57 28.43 o 10 5 1 0.05 -19.43 38.59 o -10 6 1 228.82 255.14 54.00 o -9 6 1 6.41 -8.64 24.63 o -8 6 1 399.90 401.86 24.49 o -7 6 1 27.76 35.12 17.76 o -6 6 1 179.27 196.28 19.06 o -5 6 1 19.87 6.41 13.86 o -4 6 1 13263.90 13502.65 886.01 o -3 6 1 861.51 754.13 19.13 o -2 6 1 12031.27 11015.94 491.90 o -1 6 1 162.02 194.43 13.75 o 0 6 1 153.15 122.91 10.27 o 1 6 1 162.01 213.51 11.69 o 2 6 1 2261.61 2597.77 180.05 o 3 6 1 35.61 64.07 9.95 o 4 6 1 5756.46 5819.18 256.68 o 5 6 1 288.18 281.46 21.93 o 6 6 1 989.19 1001.92 76.96 o 7 6 1 21.40 -1.96 19.26 o 8 6 1 153.01 196.06 30.91 o 9 6 1 37.95 44.43 26.34 o 10 6 1 256.42 248.06 52.75 o -10 7 1 16.23 37.13 29.18 o -9 7 1 2.54 -15.26 25.91 o -8 7 1 3.58 7.11 17.33 o -7 7 1 256.77 210.97 20.58 o -6 7 1 663.71 716.34 42.58 o -5 7 1 6419.94 5815.10 317.85 o -4 7 1 2278.97 2253.48 123.30 o -3 7 1 1617.93 1442.56 53.30 o -2 7 1 732.92 481.17 18.69 o -1 7 1 7086.19 6989.15 453.85 o 0 7 1 1061.97 1007.20 60.75 o 1 7 1 13019.10 13752.76 413.10 o 2 7 1 1653.70 1541.92 49.55 o 3 7 1 326.74 279.28 21.76 o 4 7 1 51.91 54.60 15.61 o 5 7 1 780.68 749.11 29.26 o 6 7 1 201.85 206.81 29.54 o 7 7 1 1566.68 1471.91 144.92 o 8 7 1 45.92 18.00 25.61 o 9 7 1 187.61 173.27 26.03 o -10 8 1 149.24 140.89 33.17 o -9 8 1 272.30 358.29 37.49 o -8 8 1 598.85 634.75 34.14 o -7 8 1 817.45 815.05 54.33 o -6 8 1 408.25 400.63 34.12 o -5 8 1 1922.64 1708.32 97.60 o -4 8 1 3455.02 3498.76 209.66 o -3 8 1 663.13 588.04 22.30 o -2 8 1 5749.44 5978.47 377.42 o -1 8 1 1383.29 1428.50 113.24 o 0 8 1 3204.73 3115.76 175.48 o 1 8 1 2.58 1.69 9.53 o 2 8 1 1589.79 1664.32 23.84 o 3 8 1 1245.52 1181.06 80.18 o 4 8 1 3174.64 3251.13 152.30 o 5 8 1 432.21 477.77 35.69 o 6 8 1 373.03 386.74 34.62 o 7 8 1 18.99 -18.22 27.41 o 8 8 1 98.46 62.20 28.74 o 9 8 1 138.87 129.65 26.55 o -9 9 1 12.21 9.61 29.01 o -8 9 1 78.77 95.14 28.35 o -7 9 1 1319.70 1229.17 54.51 o -6 9 1 1710.13 1667.52 90.36 o -5 9 1 541.27 547.73 29.57 o -4 9 1 2210.08 2150.39 95.57 o -3 9 1 946.08 1000.05 55.73 o -2 9 1 1041.44 907.95 73.31 o -1 9 1 219.87 275.81 18.91 o 0 9 1 5700.20 4725.25 352.15 o 1 9 1 2499.37 2852.75 127.77 o 2 9 1 2792.96 2703.44 42.04 o 3 9 1 557.53 550.90 26.66 o 4 9 1 84.30 79.64 18.75 o 5 9 1 759.65 741.31 66.56 o 6 9 1 852.61 899.02 44.52 o 7 9 1 76.87 67.62 32.90 o 8 9 1 276.97 277.12 35.92 o 9 9 1 57.79 39.77 25.91 o -9 10 1 496.57 540.06 36.23 o -8 10 1 74.84 58.00 24.05 o -7 10 1 199.09 212.99 27.16 o -6 10 1 243.71 250.76 25.82 o -5 10 1 84.49 100.91 21.76 o -4 10 1 351.81 456.51 30.94 o -3 10 1 5655.03 5271.57 337.39 o -2 10 1 1787.99 1795.45 122.02 o -1 10 1 2692.60 2456.45 198.52 o 0 10 1 1153.98 1148.72 67.28 o 1 10 1 749.43 648.14 22.05 o 2 10 1 493.42 594.52 36.58 o 3 10 1 4360.78 4195.48 97.63 o 4 10 1 268.56 288.18 24.61 o 5 10 1 1317.92 1415.08 126.32 o 6 10 1 15.74 12.88 26.55 o 7 10 1 1.16 -22.32 31.86 o 8 10 1 13.16 12.06 29.39 o 9 10 1 236.71 256.69 31.33 o -9 11 1 40.27 28.11 25.85 o -8 11 1 387.27 419.23 33.05 o -7 11 1 0.16 -15.38 21.01 o -6 11 1 1498.14 1459.36 68.67 o -5 11 1 345.44 374.11 29.22 o -4 11 1 9.41 20.36 18.53 o -3 11 1 5.03 -1.62 17.87 o -2 11 1 364.58 289.96 19.11 o -1 11 1 41.86 64.09 15.09 o 0 11 1 6124.47 5071.31 351.53 o 1 11 1 0.47 64.17 17.10 o 2 11 1 3985.27 3972.32 157.78 o 3 11 1 1.14 0.68 18.12 o 4 11 1 0.36 9.57 18.68 o 5 11 1 1.92 12.39 26.77 o 6 11 1 1000.54 1035.58 99.11 o 7 11 1 21.75 28.45 29.04 o 8 11 1 206.27 173.05 36.29 o -8 12 1 71.14 35.44 32.55 o -7 12 1 338.84 397.08 32.40 o -6 12 1 11.54 -10.68 20.15 o -5 12 1 16.37 5.87 20.19 o -4 12 1 43.67 45.67 19.75 o -3 12 1 1477.84 1282.31 104.19 o -2 12 1 461.01 491.87 50.14 o -1 12 1 2592.70 2360.82 147.99 o 0 12 1 88.95 71.17 15.63 o 1 12 1 127.41 117.33 16.59 o 2 12 1 352.38 448.61 27.55 o 3 12 1 3856.41 3761.03 222.19 o 4 12 1 42.20 61.48 21.06 o 5 12 1 973.20 935.62 68.92 o 6 12 1 0.69 11.87 28.48 o 7 12 1 1.35 28.05 31.34 o 8 12 1 40.49 41.52 33.09 o -8 13 1 41.71 42.28 26.29 o -7 13 1 17.12 11.50 23.76 o -6 13 1 729.27 768.36 153.87 o -5 13 1 321.84 355.54 40.53 o -4 13 1 627.38 614.37 74.47 o -3 13 1 114.33 116.19 22.86 o -2 13 1 296.04 296.58 26.05 o -1 13 1 481.50 506.82 24.02 o 0 13 1 3435.15 2991.64 205.51 o 1 13 1 323.44 318.09 26.15 o 2 13 1 1971.58 2057.70 117.15 o 3 13 1 0.72 23.61 19.39 o 4 13 1 20.07 17.76 20.51 o 5 13 1 211.53 154.81 54.76 o 6 13 1 422.03 426.55 42.57 o 7 13 1 50.09 24.60 32.10 o -7 14 1 280.84 265.09 39.32 o -6 14 1 37.71 32.48 46.99 o -5 14 1 89.35 128.20 33.35 o -4 14 1 773.41 730.97 86.97 o -3 14 1 1138.57 1063.17 75.51 o -2 14 1 305.60 347.48 41.50 o -1 14 1 184.39 173.85 23.72 o 0 14 1 291.77 277.74 21.20 o 1 14 1 279.65 317.38 28.97 o 2 14 1 910.42 998.49 36.78 o 3 14 1 239.61 264.85 26.56 o 4 14 1 533.89 550.80 42.74 o 5 14 1 496.73 556.87 46.16 o 6 14 1 0.89 -11.01 46.50 o 7 14 1 18.08 -11.31 31.71 o -7 15 1 126.21 120.22 36.74 o -6 15 1 78.38 50.31 44.63 o -5 15 1 876.22 916.84 133.95 o -4 15 1 260.59 278.37 70.31 o -3 15 1 101.31 107.10 29.71 o -2 15 1 564.30 611.94 32.92 o -1 15 1 465.52 499.27 51.36 o 0 15 1 405.34 414.56 32.11 o 1 15 1 2124.81 1761.86 153.56 o 2 15 1 364.37 370.03 28.66 o 3 15 1 25.24 21.33 22.02 o 4 15 1 5.20 8.17 28.25 o 5 15 1 327.45 377.57 43.86 o 6 15 1 46.11 120.34 34.88 o -6 16 1 2.84 9.02 33.21 o -5 16 1 51.05 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