#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:41:49 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/12/2241202.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241202 _cell_angle_alpha 90.000 _cell_angle_beta 91.910 _cell_angle_gamma 90.000 _cell_length_a 4.4358 _cell_length_b 12.6281 _cell_length_c 7.5588 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.7703 _cod_data_source_file wm5220Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 49.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -16 0 112.79 110.37 5.36 o 1 -16 0 122.24 117.36 6.56 o 1 -15 0 4.22 5.16 1.54 o 2 -15 0 29.12 25.29 3.56 o 0 -14 0 6.14 6.37 1.37 o 1 -14 0 4.14 4.08 1.48 o 2 -14 0 21.66 23.14 3.27 o 1 -13 0 61.31 61.67 4.21 o 2 -13 0 14.14 9.81 2.17 o 3 -13 0 34.28 44.05 4.99 o 0 -12 0 747.97 766.34 25.50 o 1 -12 0 155.27 155.42 4.22 o 2 -12 0 319.32 322.39 13.53 o 3 -12 0 31.23 27.82 3.76 o 1 -11 0 34.77 35.17 1.01 o 2 -11 0 197.57 194.71 9.23 o 3 -11 0 220.42 219.28 10.70 o 4 -11 0 70.54 68.86 5.67 o 1 -10 0 1017.58 1035.78 16.48 o 2 -10 0 0.73 -0.06 0.68 o 3 -10 0 289.59 299.93 13.13 o 4 -10 0 34.44 42.83 4.93 o 1 -9 0 94.26 87.71 2.27 o 2 -9 0 1.64 1.73 0.67 o 3 -9 0 121.92 122.38 6.94 o 4 -9 0 8.07 10.53 2.45 o 0 -8 0 26.60 24.67 2.52 o 1 -8 0 146.27 149.23 3.28 o 2 -8 0 48.42 47.32 3.93 o 3 -8 0 52.71 52.45 4.07 o 4 -8 0 40.99 40.44 4.54 o 5 -8 0 89.11 88.41 6.63 o 1 -7 0 139.64 141.58 4.22 o 2 -7 0 98.37 90.03 3.36 o 3 -7 0 214.49 199.64 9.17 o 4 -7 0 133.72 130.86 7.50 o 5 -7 0 67.39 64.21 5.48 o 0 -6 0 1615.72 1526.16 117.83 o 1 -6 0 1201.24 1200.89 27.09 o 2 -6 0 611.90 627.16 21.68 o 3 -6 0 255.73 249.41 10.62 o 4 -6 0 34.88 38.98 4.18 o 5 -6 0 12.29 11.99 2.65 o 1 -5 0 136.33 146.02 4.12 o 2 -5 0 534.35 545.35 17.89 o 3 -5 0 311.54 294.48 11.87 o 4 -5 0 260.64 243.11 10.90 o 5 -5 0 158.77 169.68 9.23 o 0 -4 0 1867.20 938.76 29.23 o 1 -4 0 575.13 564.27 13.09 o 2 -4 0 277.85 279.46 9.39 o 3 -4 0 133.96 131.24 6.41 o 4 -4 0 92.99 94.46 5.64 o 1 -3 0 494.96 494.18 11.47 o 2 -3 0 69.82 68.88 2.48 o 3 -3 0 49.29 50.30 1.36 o 4 -3 0 69.99 69.14 2.41 o 5 -3 0 12.44 11.79 1.17 o 0 -2 0 0.12 -0.29 0.29 o 1 -2 0 1703.78 1908.85 41.80 o 2 -2 0 275.71 275.01 4.69 o 3 -2 0 351.76 372.11 7.35 o 4 -2 0 73.66 70.96 2.09 o 5 -2 0 39.41 41.25 1.85 o 1 -1 0 47.06 46.82 0.95 o 2 -1 0 853.57 890.07 16.36 o 3 -1 0 420.56 420.95 10.34 o 4 -1 0 330.51 316.86 15.36 o 5 -1 0 106.98 100.60 5.01 o 1 0 0 238.19 185.91 3.67 o 2 0 0 2495.80 2637.42 40.71 o 3 0 0 125.68 119.05 2.97 o 4 0 0 216.78 228.59 6.59 o 5 0 0 60.81 58.60 3.80 o 1 1 0 43.09 41.05 0.88 o 2 1 0 848.47 886.11 14.08 o 3 1 0 433.67 430.52 8.60 o 4 1 0 321.90 311.88 8.46 o 5 1 0 107.65 109.43 5.91 o 0 2 0 0.20 -0.24 0.24 o 1 2 0 1712.58 1862.85 75.45 o 2 2 0 263.50 263.30 4.57 o 3 2 0 357.25 371.85 7.61 o 4 2 0 73.28 71.02 2.95 o 5 2 0 38.46 37.68 3.81 o 1 3 0 499.91 546.38 17.82 o 2 3 0 66.22 68.26 1.49 o 3 3 0 48.47 48.24 1.67 o 4 3 0 71.38 64.86 2.76 o 5 3 0 11.94 12.47 2.31 o 0 4 0 1881.55 2162.38 48.24 o 1 4 0 565.58 580.68 9.21 o 2 4 0 280.23 272.10 6.89 o 3 4 0 132.86 128.78 3.34 o 4 4 0 95.68 97.71 5.67 o 5 4 0 108.21 123.76 7.08 o 1 5 0 130.33 137.10 2.78 o 2 5 0 540.73 558.16 26.03 o 3 5 0 313.38 312.68 10.58 o 4 5 0 255.66 267.29 11.56 o 5 5 0 161.07 147.35 8.15 o 0 6 0 1637.46 1621.48 35.77 o 1 6 0 1187.60 1222.75 30.51 o 2 6 0 615.30 605.67 14.71 o 3 6 0 253.61 248.79 6.39 o 4 6 0 37.00 35.76 3.92 o 5 6 0 12.00 10.05 2.34 o 1 7 0 141.89 148.06 3.19 o 2 7 0 96.07 89.63 4.88 o 3 7 0 215.14 203.91 9.28 o 4 7 0 134.54 137.56 7.67 o 5 7 0 66.01 68.30 5.46 o 0 8 0 29.11 29.36 2.01 o 1 8 0 143.96 145.03 6.11 o 2 8 0 49.06 47.21 3.42 o 3 8 0 53.91 54.73 4.13 o 4 8 0 39.39 37.14 4.24 o 5 8 0 89.86 103.76 7.13 o 1 9 0 94.70 84.97 2.85 o 2 9 0 1.10 0.53 0.71 o 3 9 0 121.72 117.53 6.73 o 4 9 0 8.37 7.03 2.11 o 0 10 0 38.55 35.82 2.53 o 1 10 0 1013.54 1024.88 23.56 o 2 10 0 1.27 1.47 0.66 o 3 10 0 292.06 301.19 13.08 o 4 10 0 32.45 30.08 4.08 o 1 11 0 32.73 37.22 1.85 o 2 11 0 202.20 214.21 9.78 o 3 11 0 217.21 212.38 10.41 o 4 11 0 71.33 78.11 6.04 o 0 12 0 758.25 735.88 24.99 o 1 12 0 148.93 152.77 7.40 o 2 12 0 320.25 320.22 13.45 o 3 12 0 30.93 31.60 4.01 o 1 13 0 61.11 64.66 4.46 o 2 13 0 14.27 12.66 2.51 o 3 13 0 34.11 26.81 3.88 o -1 -16 1 10.15 11.76 2.27 o 0 -16 1 88.79 94.11 3.40 o 1 -16 1 14.29 17.38 2.82 o -2 -15 1 106.33 104.43 6.59 o -1 -15 1 83.44 84.98 5.23 o 0 -15 1 103.11 105.56 3.69 o 1 -15 1 28.73 24.63 3.11 o 2 -15 1 5.93 6.72 2.05 o -2 -14 1 16.12 16.20 2.71 o -1 -14 1 109.52 110.68 6.10 o 0 -14 1 141.88 142.14 4.52 o 1 -14 1 340.12 354.60 14.23 o 2 -14 1 145.81 130.65 7.58 o -3 -13 1 80.24 78.13 5.94 o -2 -13 1 206.42 207.48 9.98 o -1 -13 1 287.31 281.35 7.29 o 0 -13 1 44.15 43.10 3.96 o 1 -13 1 79.06 87.22 5.27 o 2 -13 1 1.73 1.59 1.17 o 3 -13 1 6.81 7.53 2.24 o -3 -12 1 58.78 55.65 4.76 o -2 -12 1 75.06 68.18 4.85 o -1 -12 1 15.48 15.43 0.73 o 0 -12 1 103.10 106.03 3.61 o 1 -12 1 12.81 9.77 1.84 o 2 -12 1 164.42 160.99 8.25 o 3 -12 1 0.17 0.55 1.01 o -4 -11 1 1.06 0.07 1.32 o -3 -11 1 13.73 14.22 2.67 o -2 -11 1 56.44 56.63 4.28 o -1 -11 1 9.37 8.97 0.96 o 0 -11 1 46.65 42.36 1.55 o 1 -11 1 54.30 48.14 1.69 o 2 -11 1 65.60 52.68 4.08 o 3 -11 1 8.75 7.65 2.04 o 4 -11 1 21.77 15.14 3.08 o -4 -10 1 95.00 99.97 6.82 o -3 -10 1 66.69 64.17 4.83 o -2 -10 1 54.61 54.70 4.00 o -1 -10 1 83.61 83.36 1.87 o 0 -10 1 164.24 154.41 3.89 o 1 -10 1 349.84 334.68 8.72 o 2 -10 1 91.04 89.31 5.38 o 3 -10 1 218.15 209.45 10.15 o 4 -10 1 31.51 27.76 3.98 o -4 -9 1 191.05 184.13 9.77 o -3 -9 1 272.58 259.50 11.61 o -2 -9 1 529.72 571.53 28.66 o -1 -9 1 361.58 356.55 7.23 o 0 -9 1 446.02 440.35 8.67 o 1 -9 1 17.21 16.63 0.54 o 2 -9 1 73.07 68.72 4.47 o 3 -9 1 86.23 77.73 5.28 o 4 -9 1 50.64 47.11 5.01 o -5 -8 1 73.73 80.96 6.30 o -4 -8 1 18.31 22.83 3.43 o -3 -8 1 46.46 43.74 3.74 o -2 -8 1 216.43 217.66 10.79 o -1 -8 1 330.93 329.83 5.66 o 0 -8 1 1082.65 1128.29 20.70 o 1 -8 1 355.64 345.35 10.00 o 2 -8 1 1219.90 1200.42 27.79 o 3 -8 1 105.58 105.62 6.18 o 4 -8 1 372.55 373.71 15.80 o -5 -7 1 72.63 72.84 5.81 o -4 -7 1 112.50 109.03 6.71 o -3 -7 1 240.64 235.10 10.42 o -2 -7 1 224.25 229.05 6.64 o -1 -7 1 501.97 503.82 11.54 o 0 -7 1 219.10 214.08 10.75 o 1 -7 1 286.95 310.07 9.16 o 2 -7 1 59.80 64.46 4.80 o 3 -7 1 103.61 92.55 5.51 o 4 -7 1 126.91 128.81 7.43 o 5 -7 1 39.86 42.73 5.01 o -5 -6 1 33.05 39.17 4.68 o -4 -6 1 263.22 259.82 11.72 o -3 -6 1 33.32 28.02 3.13 o -2 -6 1 170.94 169.48 5.18 o -1 -6 1 182.80 192.61 3.44 o 0 -6 1 109.97 110.66 2.20 o 1 -6 1 76.96 79.32 2.69 o 2 -6 1 32.37 31.62 1.72 o 3 -6 1 35.45 38.56 3.79 o 4 -6 1 8.82 9.95 2.22 o 5 -6 1 56.83 57.16 4.99 o -5 -5 1 65.70 60.95 4.99 o -4 -5 1 25.57 25.70 3.31 o -3 -5 1 116.05 106.12 5.77 o -2 -5 1 275.65 296.24 7.90 o -1 -5 1 8.35 8.17 0.45 o 0 -5 1 339.29 346.64 5.76 o 1 -5 1 107.31 111.82 4.28 o 2 -5 1 118.87 122.06 3.88 o 3 -5 1 84.42 89.69 5.11 o 4 -5 1 24.17 27.76 3.41 o -4 -4 1 26.43 27.32 1.13 o -3 -4 1 61.71 57.38 1.80 o -2 -4 1 164.20 158.07 4.71 o -1 -4 1 554.53 569.79 9.12 o 0 -4 1 1139.14 1180.65 23.52 o 1 -4 1 483.43 491.57 11.50 o 2 -4 1 1127.55 1102.30 35.79 o 3 -4 1 385.78 358.56 13.66 o 4 -4 1 178.40 176.71 8.54 o -5 -3 1 55.23 58.41 2.79 o -4 -3 1 487.70 487.19 9.56 o -3 -3 1 691.30 696.15 13.05 o -2 -3 1 1065.43 1097.30 17.32 o -1 -3 1 2327.86 2291.79 50.26 o 0 -3 1 1853.80 1909.37 61.84 o 1 -3 1 335.20 342.55 5.53 o 2 -3 1 620.11 658.41 10.52 o 3 -3 1 192.30 199.98 4.18 o 4 -3 1 56.52 55.35 1.63 o 5 -3 1 152.08 153.29 5.61 o -5 -2 1 15.30 14.71 1.75 o -4 -2 1 194.61 202.38 4.61 o -3 -2 1 10.98 10.85 0.63 o -2 -2 1 231.00 230.03 4.09 o -1 -2 1 1761.93 1814.32 39.86 o 0 -2 1 654.20 645.77 10.11 o 2 -2 1 461.47 433.02 7.13 o 3 -2 1 764.53 774.86 14.48 o 4 -2 1 110.14 112.93 3.96 o 5 -2 1 226.39 231.28 8.79 o -5 -1 1 122.17 127.83 4.21 o -4 -1 1 152.93 151.44 4.82 o -3 -1 1 148.13 147.62 4.38 o -2 -1 1 486.81 473.91 9.11 o -1 -1 1 1437.11 1639.31 35.99 o 0 -1 1 77.36 68.75 1.19 o 1 -1 1 554.88 577.85 10.54 o 2 -1 1 145.99 140.27 3.11 o 3 -1 1 84.87 80.72 2.81 o 4 -1 1 88.89 91.53 3.38 o 5 -1 1 104.23 106.47 5.25 o -5 0 1 109.53 111.23 5.69 o -4 0 1 132.86 125.04 10.25 o -3 0 1 67.47 68.73 2.06 o -2 0 1 655.58 673.73 10.92 o -1 0 1 2.57 3.18 0.27 o 1 0 1 113.18 116.50 2.09 o 2 0 1 66.24 71.78 1.58 o 3 0 1 139.03 148.35 3.49 o 4 0 1 148.17 139.34 7.94 o 5 0 1 39.69 41.17 3.19 o -5 1 1 124.08 133.03 6.70 o -4 1 1 150.14 151.60 4.87 o -3 1 1 154.63 150.73 4.24 o -2 1 1 482.25 460.06 7.67 o -1 1 1 1429.10 1567.42 25.17 o 0 1 1 82.62 73.60 1.36 o 1 1 1 560.29 576.75 9.09 o 2 1 1 145.02 142.17 2.69 o 3 1 1 86.96 85.95 3.41 o 4 1 1 84.93 92.20 4.43 o 5 1 1 106.39 103.72 5.76 o -5 2 1 16.56 16.25 2.45 o -4 2 1 192.99 199.40 5.98 o -3 2 1 12.08 11.98 0.90 o -2 2 1 226.76 228.88 4.77 o -1 2 1 1781.21 1744.16 70.23 o 0 2 1 612.51 600.12 9.42 o 2 2 1 450.63 426.20 7.04 o 3 2 1 762.10 790.16 20.17 o 4 2 1 112.09 113.80 4.00 o 5 2 1 227.88 245.84 10.76 o -5 3 1 56.75 53.76 4.15 o -4 3 1 492.87 504.19 12.70 o -3 3 1 673.16 682.29 13.21 o -2 3 1 1086.88 1135.77 17.99 o -1 3 1 2316.30 2260.60 49.63 o 0 3 1 1864.95 1903.50 87.72 o 1 3 1 321.52 329.45 5.36 o 2 3 1 621.91 674.91 10.84 o 3 3 1 194.21 197.11 4.48 o 4 3 1 57.48 56.12 2.54 o 5 3 1 151.03 148.10 7.79 o -5 4 1 125.97 134.79 7.47 o -4 4 1 28.65 26.05 3.07 o -3 4 1 61.10 57.39 1.90 o -2 4 1 167.75 175.92 3.28 o -1 4 1 548.98 545.08 8.79 o 0 4 1 1139.79 1188.98 18.53 o 1 4 1 480.27 487.43 7.83 o 2 4 1 1136.68 1145.69 18.03 o 3 4 1 379.20 383.81 7.86 o 4 4 1 179.17 168.78 8.15 o 5 4 1 52.74 53.90 4.37 o -5 5 1 63.60 53.76 4.52 o -4 5 1 27.35 27.05 3.23 o -3 5 1 116.80 113.81 3.00 o -2 5 1 271.65 297.96 5.18 o -1 5 1 9.78 9.50 0.45 o 0 5 1 342.17 356.12 7.28 o 1 5 1 105.51 112.25 2.15 o 2 5 1 122.20 124.05 2.96 o 3 5 1 82.29 89.09 2.47 o 4 5 1 24.25 19.04 2.74 o 5 5 1 70.85 72.72 5.33 o -5 6 1 33.27 38.12 4.49 o -4 6 1 264.38 260.42 11.59 o -3 6 1 30.48 27.73 1.32 o -2 6 1 173.80 167.31 4.48 o -1 6 1 179.81 191.72 3.49 o 0 6 1 113.33 116.22 2.32 o 1 6 1 75.62 84.81 3.50 o 2 6 1 32.45 28.78 2.07 o 3 6 1 35.25 33.94 1.41 o 4 6 1 8.08 7.50 1.85 o 5 6 1 58.28 50.04 5.19 o -5 7 1 73.17 76.38 5.80 o -4 7 1 113.39 114.45 6.81 o -3 7 1 239.19 232.22 6.10 o -2 7 1 226.35 221.87 4.98 o -1 7 1 496.67 489.56 9.31 o 0 7 1 225.77 234.87 4.33 o 1 7 1 282.85 290.13 5.78 o 2 7 1 58.36 60.86 3.79 o 3 7 1 107.77 93.07 5.48 o 4 7 1 124.92 122.00 7.11 o 5 7 1 39.73 39.87 4.68 o -5 8 1 71.50 79.12 6.12 o -4 8 1 19.98 26.59 3.69 o -3 8 1 45.08 34.36 3.63 o -2 8 1 214.15 214.16 10.68 o -1 8 1 346.01 352.96 8.72 o 0 8 1 1060.03 1125.14 25.40 o 1 8 1 369.88 351.70 11.08 o 2 8 1 1216.05 1109.23 36.71 o 3 8 1 105.95 111.53 6.34 o 4 8 1 372.03 364.54 15.43 o -4 9 1 192.61 188.21 9.85 o -3 9 1 271.61 262.00 11.63 o -2 9 1 527.30 541.86 13.00 o -1 9 1 363.00 352.57 8.87 o 0 9 1 449.11 451.28 11.03 o 1 9 1 15.54 14.01 1.11 o 2 9 1 72.73 67.13 4.31 o 3 9 1 86.58 89.53 5.70 o 4 9 1 49.72 45.56 4.85 o -4 10 1 98.21 111.29 7.27 o -3 10 1 63.42 61.50 4.72 o -2 10 1 56.80 63.00 4.19 o -1 10 1 82.28 80.32 2.90 o 0 10 1 164.00 157.86 9.33 o 1 10 1 352.00 345.97 11.11 o 2 10 1 88.68 88.69 3.02 o 3 10 1 219.67 209.01 10.11 o 4 10 1 30.39 31.01 4.10 o -4 11 1 1.30 0.93 1.31 o -3 11 1 14.09 13.34 2.52 o -2 11 1 55.89 53.46 4.15 o -1 11 1 10.37 9.89 1.09 o 0 11 1 45.29 46.10 2.18 o 1 11 1 54.00 56.15 3.19 o 2 11 1 66.77 61.43 4.40 o 3 11 1 8.68 8.84 2.18 o 4 11 1 20.98 17.60 3.26 o -3 12 1 57.81 61.20 5.00 o -2 12 1 77.60 78.05 5.26 o -1 12 1 14.00 16.37 2.46 o 0 12 1 103.88 106.09 3.79 o 1 12 1 11.60 13.59 2.15 o 2 12 1 164.73 172.42 8.61 o 3 12 1 0.37 0.89 1.21 o -3 13 1 81.98 87.34 6.36 o -2 13 1 200.40 203.26 9.92 o -1 13 1 294.70 283.39 11.93 o 1 13 1 79.34 71.34 4.70 o 2 13 1 1.49 1.48 1.24 o 3 13 1 7.44 6.85 2.13 o 0 -16 2 7.07 7.32 1.04 o -2 -15 2 7.91 5.17 1.66 o -1 -15 2 61.74 60.64 4.28 o 0 -15 2 114.35 125.53 4.20 o 1 -15 2 39.42 39.33 4.09 o -2 -14 2 74.36 78.90 5.51 o -1 -14 2 2.88 3.61 0.68 o 0 -14 2 16.54 15.91 1.42 o 1 -14 2 12.18 10.38 2.06 o 2 -14 2 0.85 1.68 1.27 o -3 -13 2 84.66 79.23 5.91 o -2 -13 2 22.71 18.26 2.90 o -1 -13 2 228.82 231.03 6.41 o 0 -13 2 59.29 56.58 2.45 o 1 -13 2 71.80 69.52 4.67 o 2 -13 2 88.77 89.62 5.93 o 3 -13 2 7.14 14.84 2.90 o -3 -12 2 103.77 118.04 7.32 o -2 -12 2 12.17 13.47 2.44 o -1 -12 2 65.01 62.46 2.49 o 0 -12 2 18.70 17.37 1.45 o 1 -12 2 55.83 56.58 1.47 o 2 -12 2 224.60 235.56 10.87 o 3 -12 2 105.95 114.39 7.28 o -4 -11 2 109.90 106.14 7.26 o -3 -11 2 51.69 53.25 4.54 o -2 -11 2 376.13 403.59 15.93 o -1 -11 2 336.14 325.83 8.82 o 0 -11 2 617.53 596.77 14.37 o 1 -11 2 252.98 244.31 4.98 o 2 -11 2 193.34 210.32 9.81 o 3 -11 2 66.03 67.19 5.19 o 4 -11 2 3.47 5.83 2.19 o -4 -10 2 66.25 62.18 5.24 o -3 -10 2 57.58 53.66 4.42 o -2 -10 2 124.08 116.14 6.37 o -1 -10 2 120.33 121.73 2.63 o 0 -10 2 72.61 70.31 2.31 o 1 -10 2 128.22 125.33 2.52 o 2 -10 2 78.54 79.13 5.06 o 3 -10 2 209.18 200.36 9.94 o 4 -10 2 74.36 72.77 5.78 o -4 -9 2 55.91 57.44 5.68 o -3 -9 2 58.38 58.87 4.55 o -2 -9 2 89.10 83.07 5.05 o -1 -9 2 0.52 0.80 0.25 o 0 -9 2 107.72 106.46 2.62 o 1 -9 2 68.13 67.23 1.54 o 2 -9 2 22.80 22.43 2.77 o 3 -9 2 23.31 24.79 3.37 o 4 -9 2 52.05 67.86 5.46 o -4 -8 2 42.97 43.38 4.70 o -3 -8 2 287.49 291.07 12.53 o -2 -8 2 95.45 94.30 3.68 o -1 -8 2 35.30 34.42 1.07 o 0 -8 2 89.34 94.12 2.13 o 1 -8 2 15.31 17.40 1.17 o 2 -8 2 145.33 141.87 6.93 o 3 -8 2 7.23 4.50 1.53 o 4 -8 2 42.50 36.87 4.33 o -5 -7 2 17.98 22.37 3.61 o -4 -7 2 76.88 67.94 5.13 o -3 -7 2 155.39 158.24 7.98 o -2 -7 2 277.29 264.20 15.09 o -1 -7 2 689.09 712.65 11.61 o 0 -7 2 357.49 355.70 6.13 o 1 -7 2 596.11 623.60 10.13 o 2 -7 2 113.44 120.89 6.06 o 3 -7 2 101.07 104.38 6.02 o 4 -7 2 65.34 63.54 4.96 o -5 -6 2 79.60 83.07 6.08 o -4 -6 2 386.98 374.57 15.52 o -3 -6 2 36.73 41.26 3.47 o -2 -6 2 266.49 252.05 4.48 o -1 -6 2 34.44 41.62 1.13 o 0 -6 2 359.08 366.63 6.24 o 1 -6 2 400.87 415.56 6.92 o 2 -6 2 90.58 90.05 4.83 o 3 -6 2 901.70 879.05 30.21 o 4 -6 2 104.35 99.00 6.22 o -5 -5 2 13.84 24.81 3.74 o -4 -5 2 57.79 59.51 4.53 o -3 -5 2 313.50 309.72 6.11 o -2 -5 2 960.78 975.62 18.47 o -1 -5 2 728.61 685.91 19.34 o 0 -5 2 1661.82 1678.42 26.17 o 1 -5 2 2014.60 2120.17 38.04 o 2 -5 2 689.67 716.72 21.54 o 3 -5 2 255.20 245.94 10.37 o 4 -5 2 129.92 120.68 6.87 o -4 -4 2 15.58 15.48 1.20 o -3 -4 2 392.54 402.96 7.95 o -2 -4 2 94.66 95.26 2.06 o -1 -4 2 178.87 193.23 5.26 o 0 -4 2 55.46 59.07 1.50 o 1 -4 2 41.85 40.63 1.02 o 2 -4 2 575.52 594.56 8.56 o 3 -4 2 75.84 75.35 1.80 o 4 -4 2 281.74 265.49 11.55 o -5 -3 2 182.91 176.42 6.73 o -4 -3 2 76.93 80.78 2.96 o -3 -3 2 145.70 148.02 3.46 o -2 -3 2 141.05 144.83 2.87 o -1 -3 2 179.67 186.68 4.00 o 0 -3 2 208.00 213.32 3.74 o 1 -3 2 256.18 239.51 12.13 o 2 -3 2 90.46 97.22 2.00 o 3 -3 2 74.57 78.86 2.06 o 4 -3 2 84.23 84.58 3.03 o 5 -3 2 31.50 33.45 1.97 o -5 -2 2 120.87 125.14 5.54 o -4 -2 2 60.23 64.91 2.69 o -3 -2 2 227.68 222.37 6.08 o -2 -2 2 62.80 59.74 3.08 o -1 -2 2 253.73 263.38 4.56 o 0 -2 2 184.62 199.81 3.12 o 1 -2 2 255.97 258.28 5.10 o 2 -2 2 117.53 115.65 3.06 o 3 -2 2 59.28 58.11 1.74 o 4 -2 2 173.33 172.99 5.27 o 5 -2 2 21.35 23.49 2.05 o -5 -1 2 14.80 18.08 2.19 o -4 -1 2 85.02 86.76 3.30 o -3 -1 2 667.58 675.83 13.02 o -2 -1 2 407.17 410.04 7.01 o -1 -1 2 2092.32 2134.58 38.21 o 0 -1 2 1758.18 1923.59 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