data_2241229 _cell_angle_alpha 90.000 _cell_angle_beta 98.921 _cell_angle_gamma 90.000 _cell_length_a 11.9518 _cell_length_b 12.1291 _cell_length_c 19.5901 _exptl_crystal_F_000 1484.00 _reflns_d_resolution_high 0.5846 _cod_data_source_file gw2154Isup2.hkl _cod_data_source_block I _shelx_title ' 9233sad in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 315.43 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10557.46 8710.52 120.34 o 4 0 0 45495.66 44000.49 567.82 o 6 0 0 3591.46 3554.13 54.51 o 8 0 0 26057.80 25520.76 383.98 o 10 0 0 5140.93 4877.09 84.96 o 12 0 0 917.59 1109.98 48.15 o 14 0 0 180.08 189.77 29.86 o 16 0 0 14.26 3.68 29.66 o 18 0 0 437.21 411.26 53.20 o 2 1 0 1610.56 1587.18 20.98 o 3 1 0 311.12 485.59 11.52 o 4 1 0 11340.11 10562.41 108.33 o 5 1 0 2165.85 2039.13 25.69 o 6 1 0 617.90 723.33 13.86 o 7 1 0 545.56 719.93 23.34 o 8 1 0 61.95 136.07 43.63 o 9 1 0 444.78 486.50 14.84 o 10 1 0 4610.09 4462.88 58.07 o 11 1 0 23.92 75.20 10.72 o 12 1 0 1789.52 1790.54 41.15 o 13 1 0 66.27 89.84 17.08 o 14 1 0 36.74 50.68 18.32 o 15 1 0 1641.31 1704.84 45.87 o 16 1 0 23.13 52.24 22.38 o 17 1 0 62.31 69.45 26.13 o 18 1 0 641.62 580.49 40.96 o 19 1 0 485.93 506.10 40.49 o 0 2 0 90.90 112.42 4.94 o 1 2 0 501.09 518.68 15.18 o 2 2 0 3752.75 5325.23 123.23 o 3 2 0 46953.85 47681.61 595.24 o 4 2 0 787.80 651.57 13.84 o 5 2 0 6590.73 6027.96 66.68 o 6 2 0 10692.19 10660.89 111.95 o 7 2 0 3369.52 3407.97 52.56 o 8 2 0 4344.66 3890.98 45.65 o 9 2 0 1487.14 1469.27 24.41 o 10 2 0 388.32 406.87 15.21 o 11 2 0 51.17 155.63 13.29 o 12 2 0 697.71 825.01 24.15 o 13 2 0 539.27 616.28 26.54 o 14 2 0 1051.23 1114.81 36.48 o 15 2 0 110.34 119.76 22.41 o 16 2 0 1746.20 1759.85 49.53 o 17 2 0 2.77 2.23 22.74 o 18 2 0 332.45 318.04 30.95 o 19 2 0 166.17 218.37 34.53 o 1 3 0 366.03 318.04 11.80 o 2 3 0 41543.13 42765.29 536.64 o 3 3 0 1433.73 1303.51 26.87 o 4 3 0 99496.06 100971.15 1205.74 o 5 3 0 355.77 391.19 10.58 o 6 3 0 19201.31 18194.72 188.76 o 7 3 0 747.55 706.59 14.68 o 8 3 0 7754.78 7159.93 82.16 o 9 3 0 22.80 52.08 9.33 o 10 3 0 198.20 260.59 13.85 o 11 3 0 267.36 264.21 15.45 o 12 3 0 877.54 947.32 27.33 o 13 3 0 70.19 65.52 17.28 o 14 3 0 595.69 642.66 28.91 o 15 3 0 29.57 18.79 19.68 o 16 3 0 460.30 494.54 29.89 o 17 3 0 12.26 20.23 23.23 o 18 3 0 6.13 19.16 26.21 o 19 3 0 2.17 29.57 31.23 o 0 4 0 4900.58 5986.64 163.27 o 1 4 0 2522.18 3105.61 85.96 o 2 4 0 74.91 151.51 9.65 o 3 4 0 252.97 342.10 38.33 o 4 4 0 399.40 1212.38 103.27 o 5 4 0 1720.26 1911.09 28.51 o 6 4 0 2523.96 3004.53 39.40 o 7 4 0 1271.42 1100.09 19.01 o 8 4 0 1681.05 1638.06 39.32 o 9 4 0 1477.27 1538.20 32.00 o 10 4 0 198.69 250.99 14.20 o 11 4 0 2143.58 2227.02 49.88 o 12 4 0 282.21 348.39 17.98 o 13 4 0 248.86 299.54 21.31 o 14 4 0 2604.60 2879.01 59.49 o 15 4 0 8.95 10.79 19.09 o 16 4 0 895.81 896.24 36.56 o 17 4 0 27.28 -15.05 23.73 o 18 4 0 268.20 192.52 32.30 o 19 4 0 112.05 68.24 33.20 o 1 5 0 41553.45 47760.85 1272.45 o 2 5 0 3298.16 4120.58 111.94 o 3 5 0 2039.07 1984.56 48.20 o 4 5 0 1237.44 1288.08 31.07 o 5 5 0 409.04 417.37 14.09 o 6 5 0 3.07 148.44 18.40 o 7 5 0 5804.44 5640.21 69.23 o 8 5 0 181.22 165.65 10.20 o 9 5 0 304.52 295.12 11.98 o 10 5 0 2551.59 2617.36 42.47 o 11 5 0 1678.63 1611.44 33.24 o 12 5 0 3814.44 3767.20 60.78 o 13 5 0 222.59 234.77 20.49 o 14 5 0 66.89 75.96 19.07 o 15 5 0 30.35 74.21 20.58 o 16 5 0 0.60 18.52 22.32 o 17 5 0 84.67 15.81 26.90 o 18 5 0 222.23 220.97 34.26 o 19 5 0 11.76 -8.48 47.48 o 0 6 0 13447.11 14825.25 415.74 o 1 6 0 13.61 21.14 7.37 o 2 6 0 31578.69 36752.04 998.81 o 3 6 0 5644.70 5967.47 76.72 o 4 6 0 3279.58 3589.07 55.52 o 5 6 0 2490.24 2753.95 114.59 o 6 6 0 46.78 82.52 12.41 o 7 6 0 471.01 456.09 15.50 o 8 6 0 4894.85 4684.56 58.82 o 9 6 0 7.18 87.04 10.41 o 10 6 0 900.18 996.57 27.78 o 11 6 0 130.61 164.80 14.66 o 12 6 0 4362.12 4301.95 67.22 o 13 6 0 75.35 100.86 18.57 o 14 6 0 315.42 304.69 24.92 o 15 6 0 0.76 -19.38 19.38 o 16 6 0 0.34 0.41 30.14 o 17 6 0 84.22 11.98 29.60 o 18 6 0 80.45 97.55 31.63 o 19 6 0 85.16 4.28 50.43 o 1 7 0 103.09 123.71 11.70 o 2 7 0 1592.77 1858.52 50.18 o 3 7 0 814.23 815.86 33.93 o 4 7 0 817.26 786.60 20.52 o 5 7 0 2060.64 2066.35 35.37 o 6 7 0 278.50 283.62 13.84 o 7 7 0 2330.84 2294.33 36.94 o 8 7 0 483.00 513.87 17.96 o 9 7 0 1517.22 1361.38 26.66 o 10 7 0 335.88 428.27 30.66 o 11 7 0 13.57 24.44 12.94 o 12 7 0 1464.89 1733.80 44.46 o 13 7 0 1782.55 1658.85 46.21 o 14 7 0 2.62 -4.66 19.49 o 15 7 0 127.01 90.80 25.81 o 16 7 0 4.97 12.83 26.39 o 17 7 0 725.31 728.21 42.98 o 18 7 0 283.26 256.56 35.29 o 0 8 0 29.54 186.97 42.59 o 1 8 0 3344.77 3747.39 70.93 o 2 8 0 173.12 330.91 15.32 o 3 8 0 12022.24 12708.83 367.81 o 4 8 0 792.75 793.40 20.60 o 5 8 0 9543.44 9258.99 133.13 o 6 8 0 26.94 56.08 11.14 o 7 8 0 5711.94 5473.06 85.11 o 8 8 0 336.24 358.90 16.07 o 9 8 0 994.74 898.57 23.51 o 10 8 0 290.52 355.60 31.51 o 11 8 0 463.35 496.78 27.14 o 12 8 0 777.76 791.40 30.19 o 13 8 0 34.62 38.06 19.29 o 14 8 0 997.21 1126.81 41.27 o 15 8 0 543.82 540.49 35.18 o 16 8 0 530.02 618.26 45.63 o 17 8 0 62.47 53.54 40.56 o 18 8 0 407.50 344.58 58.12 o 1 9 0 9745.42 10262.63 153.02 o 2 9 0 2968.25 3587.31 80.79 o 3 9 0 4.55 81.12 20.69 o 4 9 0 304.70 434.40 36.43 o 5 9 0 683.32 777.25 23.73 o 6 9 0 3228.76 3709.70 61.91 o 7 9 0 2854.13 2590.92 52.04 o 8 9 0 1679.89 1706.63 36.99 o 9 9 0 1130.94 1185.15 29.32 o 10 9 0 664.56 760.09 26.93 o 11 9 0 36.20 61.36 19.55 o 12 9 0 7.01 172.55 22.61 o 13 9 0 11.01 14.72 22.43 o 14 9 0 72.93 93.64 23.95 o 15 9 0 313.68 251.58 31.34 o 16 9 0 259.96 248.41 33.81 o 17 9 0 5.29 -0.75 30.55 o 0 10 0 15.14 39.56 13.34 o 1 10 0 332.71 339.49 17.38 o 2 10 0 1994.79 2094.66 39.72 o 3 10 0 108.13 277.15 49.52 o 4 10 0 320.78 440.15 40.06 o 5 10 0 4.47 10.93 12.52 o 6 10 0 74.72 88.26 23.21 o 7 10 0 206.60 237.01 17.16 o 8 10 0 181.51 222.42 17.33 o 9 10 0 1224.14 1240.32 31.12 o 10 10 0 7.65 4.39 14.65 o 11 10 0 1916.73 1808.38 49.17 o 12 10 0 1516.63 1619.59 52.08 o 13 10 0 1016.22 932.45 51.87 o 14 10 0 244.23 250.97 37.68 o 15 10 0 117.81 123.83 37.43 o 16 10 0 648.36 577.62 40.53 o 17 10 0 470.72 356.01 85.14 o 1 11 0 5032.83 5181.79 96.85 o 2 11 0 2357.04 2611.06 86.56 o 3 11 0 1658.94 2260.64 92.75 o 4 11 0 1112.17 1315.50 84.72 o 5 11 0 0.34 53.30 14.88 o 6 11 0 1207.19 1251.01 35.83 o 7 11 0 1196.37 1222.34 39.80 o 8 11 0 731.26 769.90 31.43 o 9 11 0 2543.15 2416.39 46.38 o 10 11 0 253.34 263.15 21.64 o 11 11 0 1610.80 1536.87 50.91 o 12 11 0 56.58 47.65 26.60 o 13 11 0 390.75 446.29 41.40 o 14 11 0 513.20 422.04 43.98 o 15 11 0 11.47 50.59 36.16 o 16 11 0 72.06 56.41 46.47 o 0 12 0 3171.85 3279.49 103.12 o 1 12 0 2462.72 2527.98 61.83 o 2 12 0 50.87 204.85 18.83 o 3 12 0 700.44 796.66 41.87 o 4 12 0 706.37 823.52 58.53 o 5 12 0 1568.77 1663.83 50.75 o 6 12 0 483.67 569.29 32.26 o 7 12 0 627.21 694.45 35.80 o 8 12 0 144.02 163.17 19.47 o 9 12 0 1.03 35.48 16.12 o 10 12 0 90.01 90.77 18.84 o 11 12 0 1065.53 1014.34 43.29 o 12 12 0 31.89 38.06 27.44 o 13 12 0 163.42 166.14 35.00 o 14 12 0 1548.02 1442.98 80.00 o 15 12 0 9.20 60.64 44.70 o 16 12 0 271.86 171.59 80.40 o 1 13 0 2172.31 2138.77 75.86 o 2 13 0 7.10 2.80 17.84 o 3 13 0 1.63 44.26 19.91 o 4 13 0 1935.11 2064.53 117.39 o 5 13 0 1574.70 1585.32 88.46 o 6 13 0 423.77 415.27 37.33 o 7 13 0 161.91 175.44 28.59 o 8 13 0 66.07 70.32 22.92 o 9 13 0 485.33 545.87 30.72 o 10 13 0 160.37 225.07 37.72 o 11 13 0 76.49 47.96 29.57 o 12 13 0 6.79 44.99 36.64 o 13 13 0 395.73 377.17 50.08 o 14 13 0 258.96 158.69 68.44 o 15 13 0 791.66 449.77 126.73 o 0 14 0 5454.56 5892.11 199.13 o 1 14 0 13.66 5.48 19.96 o 2 14 0 1827.02 2069.76 66.43 o 3 14 0 2837.36 2971.08 84.27 o 4 14 0 290.87 285.91 27.19 o 5 14 0 2259.16 2497.70 198.94 o 6 14 0 577.99 611.72 54.19 o 7 14 0 988.16 1097.72 67.82 o 8 14 0 1175.23 1116.38 54.29 o 9 14 0 76.40 78.96 24.28 o 10 14 0 284.02 336.79 52.03 o 11 14 0 5.67 -43.28 43.28 o 12 14 0 20.83 13.50 45.02 o 13 14 0 455.98 503.80 80.79 o 14 14 0 0.81 79.26 63.38 o 1 15 0 1746.71 1673.50 72.87 o 2 15 0 11.01 36.76 23.58 o 3 15 0 120.04 214.31 28.12 o 4 15 0 9.12 -0.31 32.51 o 5 15 0 15.24 7.68 35.02 o 6 15 0 6.68 -0.91 37.00 o 7 15 0 1042.59 1196.56 82.52 o 8 15 0 82.31 110.39 43.11 o 9 15 0 285.84 263.56 51.39 o 10 15 0 960.44 915.92 91.59 o 11 15 0 251.56 232.50 55.13 o 12 15 0 373.18 333.47 58.10 o 13 15 0 3.52 -21.81 90.37 o 0 16 0 4001.25 3984.84 171.91 o 1 16 0 3.68 45.14 29.39 o 2 16 0 505.85 605.72 43.14 o 3 16 0 91.72 88.57 27.28 o 4 16 0 202.96 196.44 29.65 o 5 16 0 593.35 681.42 47.08 o 6 16 0 232.18 236.99 46.12 o 7 16 0 74.01 80.87 45.58 o 8 16 0 522.81 527.74 51.42 o 9 16 0 883.60 877.81 96.61 o 10 16 0 1339.38 1137.16 99.12 o 11 16 0 567.13 303.60 77.85 o 12 16 0 157.26 93.51 96.08 o 1 17 0 512.10 638.57 56.30 o 2 17 0 651.82 758.86 67.19 o 3 17 0 111.19 141.49 52.86 o 4 17 0 2138.54 2204.10 198.36 o 5 17 0 731.93 762.13 65.76 o 6 17 0 938.55 887.67 71.34 o 7 17 0 119.10 30.68 46.74 o 8 17 0 369.76 409.50 50.61 o 9 17 0 1043.63 841.15 70.89 o 10 17 0 75.20 121.52 68.53 o 11 17 0 217.58 108.09 73.08 o 0 18 0 401.64 508.99 171.91 o 1 18 0 2.65 27.51 39.44 o 2 18 0 443.07 477.76 43.57 o 3 18 0 293.23 332.90 39.52 o 4 18 0 3.56 -28.88 28.88 o 5 18 0 293.37 290.05 48.73 o 6 18 0 458.41 379.04 58.68 o 7 18 0 72.28 74.17 38.79 o 8 18 0 99.16 92.27 39.32 o 9 18 0 57.39 182.23 71.70 o 1 19 0 555.80 571.79 48.79 o 2 19 0 547.52 549.16 47.93 o 3 19 0 421.09 409.87 44.33 o 4 19 0 945.52 931.58 56.80 o 5 19 0 198.13 131.78 53.37 o 6 19 0 840.22 730.70 73.51 o 7 19 0 1.72 51.09 50.56 o 0 20 0 1566.16 1712.09 278.90 o 1 20 0 982.36 922.74 65.81 o 2 20 0 148.04 55.05 123.61 o -19 0 1 16.99 -2.25 43.36 o -17 0 1 1118.65 1138.24 60.41 o -15 0 1 175.69 175.93 32.04 o -13 0 1 1808.78 1973.09 62.15 o -11 0 1 132.91 100.91 16.92 o -9 0 1 2257.46 1990.12 36.54 o -7 0 1 22827.42 21825.79 303.81 o -5 0 1 7577.50 6161.09 88.54 o -3 0 1 333.56 410.73 8.05 o 3 0 1 3927.17 3353.49 46.38 o 5 0 1 4941.16 3984.87 60.43 o 7 0 1 6777.85 6295.89 101.26 o 9 0 1 1674.33 1649.92 37.25 o 11 0 1 1070.69 959.47 31.32 o 13 0 1 10.27 -13.54 22.48 o 15 0 1 158.23 148.70 32.26 o 17 0 1 22.37 -3.27 32.92 o 19 0 1 26.34 -41.13 43.07 o -20 1 1 214.31 29.08 87.25 o -19 1 1 244.64 241.86 32.87 o -18 1 1 359.69 436.61 34.78 o -17 1 1 350.68 391.03 31.49 o -16 1 1 364.63 429.16 29.53 o -15 1 1 47.54 131.82 20.97 o -14 1 1 1241.06 1276.13 41.38 o -13 1 1 41.25 85.16 17.50 o -12 1 1 359.13 437.49 23.34 o -11 1 1 415.53 408.22 15.67 o -10 1 1 558.15 804.06 36.24 o -9 1 1 3028.64 2913.78 36.54 o -8 1 1 10574.50 9883.74 108.58 o -7 1 1 2966.63 2950.52 33.51 o -6 1 1 217.54 224.70 7.24 o -5 1 1 271.87 374.30 23.68 o -4 1 1 13169.21 12768.54 129.39 o -3 1 1 342.25 310.71 6.15 o -2 1 1 3039.69 3164.58 42.18 o 2 1 1 1125.32 1376.11 19.30 o 3 1 1 23921.19 23362.09 236.81 o 4 1 1 3610.24 3185.06 34.05 o 5 1 1 5182.96 4792.14 54.43 o 6 1 1 2719.76 2731.89 32.69 o 7 1 1 3600.80 3400.21 40.16 o 8 1 1 16576.13 15996.09 172.99 o 9 1 1 3699.38 3434.78 44.37 o 10 1 1 1712.36 1825.52 37.03 o 11 1 1 1472.11 1513.08 40.98 o 12 1 1 928.73 1015.68 26.60 o 13 1 1 391.22 457.81 23.62 o 14 1 1 285.03 322.09 23.56 o 15 1 1 635.27 755.05 32.87 o 16 1 1 1003.78 929.17 39.51 o 17 1 1 841.34 914.61 54.09 o 18 1 1 266.00 269.62 32.10 o 19 1 1 19.14 29.39 33.80 o -20 2 1 325.62 326.16 102.84 o -19 2 1 238.70 295.64 38.14 o -18 2 1 28.96 33.66 25.19 o -17 2 1 6.10 -22.20 22.20 o -16 2 1 73.88 147.20 24.85 o -15 2 1 136.79 132.53 21.59 o -14 2 1 354.81 440.84 25.15 o -13 2 1 1191.71 1279.00 36.56 o -12 2 1 3014.03 3013.10 54.29 o -11 2 1 1008.07 992.97 28.46 o -10 2 1 5499.02 5391.16 68.91 o -9 2 1 66.56 93.51 7.90 o -8 2 1 2296.48 2177.66 31.01 o -7 2 1 950.81 1069.56 24.68 o -6 2 1 421.09 570.63 45.12 o -5 2 1 2415.00 2453.34 31.43 o -4 2 1 352.02 356.65 10.26 o -3 2 1 47053.54 47011.80 557.49 o -2 2 1 79885.53 85129.67 1125.44 o -1 2 1 4370.03 4983.48 96.13 o 0 2 1 5025.45 5530.35 139.78 o 1 2 1 6814.85 7271.86 138.57 o 2 2 1 87592.98 89337.04 1127.25 o 3 2 1 32762.15 34323.62 406.57 o 4 2 1 1402.94 1470.48 20.50 o 5 2 1 10320.73 10431.44 108.39 o 6 2 1 17.26 80.22 9.32 o 7 2 1 9972.08 9542.38 101.03 o 8 2 1 831.29 871.66 16.58 o 9 2 1 3849.55 3768.28 50.03 o 10 2 1 819.06 836.57 20.98 o 11 2 1 3568.57 3633.08 51.16 o 12 2 1 3355.48 3265.65 51.03 o 13 2 1 1124.25 1118.26 34.53 o 14 2 1 124.61 166.13 21.55 o 15 2 1 228.29 231.20 23.42 o 16 2 1 424.77 405.98 28.49 o 17 2 1 24.58 0.61 23.33 o 18 2 1 20.13 -22.09 26.64 o 19 2 1 551.20 485.89 37.67 o -19 3 1 113.05 169.54 31.25 o -18 3 1 42.55 53.19 25.62 o -17 3 1 2.64 -8.09 22.62 o -16 3 1 50.01 95.73 22.96 o -15 3 1 23.80 -17.92 18.62 o -14 3 1 91.37 88.27 19.29 o -13 3 1 1784.32 1778.40 44.57 o -12 3 1 92.79 165.92 18.52 o -11 3 1 6345.16 6228.07 82.22 o -10 3 1 381.16 404.62 16.70 o -9 3 1 5286.19 5088.44 59.26 o -8 3 1 2.89 18.82 9.08 o -7 3 1 606.28 429.22 11.77 o -6 3 1 1344.64 1624.41 89.24 o -5 3 1 2374.92 2612.71 33.65 o -4 3 1 5454.12 6632.73 238.23 o -3 3 1 16892.99 16276.45 206.68 o -2 3 1 4727.43 5396.20 106.26 o -1 3 1 4107.51 4267.48 92.34 o 0 3 1 1264.47 1496.68 40.80 o 1 3 1 8087.99 7938.11 158.03 o 2 3 1 5678.54 5953.05 78.43 o 3 3 1 16195.39 15944.39 204.78 o 4 3 1 5647.86 5551.43 68.14 o 5 3 1 2.14 34.21 6.27 o 6 3 1 682.34 872.82 33.03 o 7 3 1 49.19 78.26 8.09 o 8 3 1 120.35 124.88 9.10 o 9 3 1 1695.75 1596.17 26.55 o 10 3 1 1581.13 1485.90 29.33 o 11 3 1 32.29 32.22 11.21 o 12 3 1 864.36 833.86 24.55 o 13 3 1 668.91 753.05 28.82 o 14 3 1 202.25 217.10 21.30 o 15 3 1 170.01 131.05 21.67 o 16 3 1 0.64 19.07 21.72 o 17 3 1 1.83 24.57 24.77 o 18 3 1 13.99 45.58 26.75 o 19 3 1 72.30 45.14 31.41 o -19 4 1 18.51 -9.78 30.01 o -18 4 1 52.40 63.01 28.35 o -17 4 1 1.25 8.82 22.76 o -16 4 1 979.70 1053.29 41.72 o -15 4 1 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