data_2241247 _cell_angle_alpha 84.920 _cell_angle_beta 85.370 _cell_angle_gamma 83.700 _cell_length_a 8.9000 _cell_length_b 13.1430 _cell_length_c 20.7780 _exptl_crystal_F_000 1608.00 _reflns_d_resolution_high 0.7196 _cod_data_source_file wm5221Isup2.hkl _cod_data_source_block I _shelx_title ' femorphmoo6_1_100_00_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 603.63 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23136.97 24560.33 433.69 o 3 0 0 10890.55 9932.70 206.47 o 4 0 0 459.59 640.81 29.89 o 5 0 0 726.55 629.06 33.73 o 6 0 0 3369.77 2962.52 89.82 o 7 0 0 100.32 91.51 34.02 o 8 0 0 1357.93 1129.39 135.14 o 9 0 0 969.52 719.24 91.75 o 10 0 0 3041.56 2832.88 188.37 o 11 0 0 1843.21 2080.40 179.04 o -12 1 0 1662.00 1808.00 229.54 o -11 1 0 7950.89 8522.65 488.70 o -10 1 0 516.07 514.06 147.65 o -9 1 0 4618.11 4498.25 190.64 o -8 1 0 7602.07 7494.36 181.80 o -7 1 0 923.39 787.67 101.37 o -6 1 0 57.35 52.27 23.81 o -5 1 0 2505.22 2574.04 90.85 o -4 1 0 3502.62 3279.09 69.40 o -3 1 0 139.61 165.60 20.36 o -2 1 0 4318.61 5005.80 77.77 o -1 1 0 11965.63 11871.99 539.46 o 2 1 0 364371.97 383814.09 9516.61 o 3 1 0 175.83 184.90 16.44 o 4 1 0 1343.65 1043.43 35.12 o 5 1 0 22290.63 20377.44 784.25 o 6 1 0 345.99 390.56 43.41 o 7 1 0 3222.45 3176.47 125.97 o 8 1 0 213.01 285.41 60.20 o 9 1 0 486.37 492.21 76.12 o 10 1 0 1076.12 770.29 168.32 o 11 1 0 259.95 524.82 97.89 o -12 2 0 325.88 601.27 150.88 o -11 2 0 44.08 5.31 90.39 o -10 2 0 859.35 789.15 115.45 o -9 2 0 306.63 282.68 62.57 o -8 2 0 155.70 132.35 41.31 o -7 2 0 1835.66 1805.02 93.16 o -6 2 0 3813.15 3491.62 104.54 o -5 2 0 0.40 -18.24 18.24 o -4 2 0 2261.34 2347.48 60.64 o -3 2 0 8021.73 8369.01 115.18 o -2 2 0 3488.35 3468.13 69.15 o 0 2 0 163.26 112.78 36.70 o 1 2 0 4900.37 4597.03 103.19 o 2 2 0 590.87 585.95 38.41 o 3 2 0 133.82 86.47 17.16 o 4 2 0 7931.08 6119.06 101.80 o 5 2 0 4.09 25.95 16.20 o 6 2 0 9155.17 9428.17 195.23 o 7 2 0 10672.60 10803.87 278.32 o 8 2 0 144.06 229.87 63.35 o 9 2 0 742.41 730.67 89.84 o 10 2 0 11.40 -6.06 60.97 o 11 2 0 201.62 4.23 55.71 o -11 3 0 1693.60 2018.14 243.00 o -10 3 0 276.45 220.77 61.72 o -9 3 0 849.00 1012.28 95.73 o -8 3 0 1562.72 1480.34 114.05 o -7 3 0 73.98 54.89 35.36 o -6 3 0 87.49 62.37 31.04 o -5 3 0 4482.45 4235.44 98.19 o -4 3 0 410.61 446.78 22.52 o -3 3 0 333.31 163.31 17.23 o -2 3 0 12165.80 12877.05 232.34 o -1 3 0 23592.52 26766.52 323.10 o 0 3 0 196.36 184.64 17.02 o 1 3 0 7113.09 7827.39 294.08 o 2 3 0 22.03 34.72 27.41 o 3 3 0 18453.41 17152.54 336.13 o 4 3 0 413.69 314.94 31.56 o 5 3 0 5664.91 5089.91 93.09 o 6 3 0 514.69 421.96 31.65 o 7 3 0 792.95 690.75 55.98 o 8 3 0 1169.19 777.07 113.38 o 9 3 0 525.55 414.65 74.48 o 10 3 0 0.63 87.53 60.58 o 11 3 0 0.63 71.16 60.59 o -11 4 0 30.08 -48.84 99.42 o -10 4 0 334.03 491.58 80.20 o -9 4 0 187.70 260.02 76.30 o -8 4 0 905.60 719.86 94.17 o -7 4 0 247.23 283.49 47.25 o -6 4 0 3216.24 3125.89 87.32 o -5 4 0 101.74 91.99 16.31 o -4 4 0 1450.81 1372.29 60.22 o -3 4 0 3929.22 3990.65 88.33 o -2 4 0 2937.10 3445.01 85.65 o -1 4 0 3.93 47.49 16.53 o 0 4 0 2574.34 2529.14 104.49 o 1 4 0 14047.79 13078.03 247.23 o 2 4 0 579.16 480.27 59.22 o 3 4 0 2324.21 2273.04 76.27 o 4 4 0 6221.27 6064.28 302.98 o 5 4 0 1784.57 1788.07 72.76 o 6 4 0 3.34 22.94 26.08 o 7 4 0 1702.47 1688.87 60.51 o 8 4 0 1962.02 1820.64 122.61 o 9 4 0 636.28 539.56 103.15 o 10 4 0 242.08 231.04 61.37 o 11 4 0 346.82 326.81 127.38 o -10 5 0 63.76 194.13 65.58 o -9 5 0 44.80 143.57 101.04 o -8 5 0 2451.37 2230.88 160.72 o -7 5 0 1124.57 1073.39 62.20 o -6 5 0 2195.94 1918.16 61.29 o -5 5 0 491.77 470.77 33.82 o -4 5 0 1855.98 1709.95 53.68 o -3 5 0 229.14 295.28 29.49 o -2 5 0 7477.64 7803.65 328.35 o -1 5 0 4008.67 3432.45 108.47 o 0 5 0 8766.74 8199.97 199.48 o 1 5 0 80.09 87.05 23.98 o 2 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0 332.86 251.67 37.09 o -6 7 0 605.21 483.76 44.08 o -5 7 0 2024.92 1913.37 81.04 o -4 7 0 17845.50 16596.03 247.98 o -3 7 0 24091.07 22529.39 343.41 o -2 7 0 9879.23 10320.46 205.06 o -1 7 0 80564.43 79923.77 914.47 o 0 7 0 30430.75 29306.62 514.55 o 1 7 0 3638.15 3563.42 87.71 o 2 7 0 2486.24 2320.23 99.84 o 3 7 0 3314.01 3455.57 95.27 o 4 7 0 0.67 33.49 28.95 o 5 7 0 1523.73 1384.10 89.06 o 6 7 0 175.39 225.92 55.45 o 7 7 0 57.54 52.72 34.18 o 8 7 0 116.10 96.88 33.99 o 9 7 0 4227.65 4154.34 170.58 o 10 7 0 6932.75 7268.14 267.12 o 11 7 0 926.33 1054.62 194.83 o -9 8 0 2630.28 2920.78 223.47 o -8 8 0 101.46 104.62 136.54 o -7 8 0 1154.63 1165.68 101.00 o -6 8 0 3487.44 3383.28 113.24 o -5 8 0 1467.79 1371.33 71.69 o -4 8 0 155.10 122.41 31.35 o -3 8 0 1478.03 1498.33 59.02 o -2 8 0 51128.26 48754.91 628.81 o -1 8 0 13595.36 13395.08 258.55 o 0 8 0 43296.16 41041.20 594.99 o 1 8 0 121785.12 119309.05 1317.25 o 2 8 0 20362.23 20051.16 332.62 o 3 8 0 11163.77 10157.86 335.94 o 4 8 0 3047.25 3144.04 104.01 o 5 8 0 118.66 173.62 52.73 o 6 8 0 2.50 17.43 38.69 o 7 8 0 52.24 60.45 28.24 o 8 8 0 600.55 560.80 42.95 o 9 8 0 112.03 -4.77 56.78 o 10 8 0 1046.47 984.81 105.30 o 11 8 0 3467.88 3477.90 327.61 o -9 9 0 328.57 550.45 167.88 o -8 9 0 2279.48 2518.36 188.96 o -7 9 0 4585.10 4991.99 401.38 o -6 9 0 46.04 31.21 35.79 o -5 9 0 286.31 254.02 38.94 o -4 9 0 5924.92 5660.82 152.37 o -3 9 0 7770.51 7444.60 172.60 o -2 9 0 21.35 18.58 26.83 o -1 9 0 9271.90 8962.44 222.26 o 0 9 0 35068.09 35810.84 642.95 o 1 9 0 0.48 30.27 21.48 o 2 9 0 15564.70 15345.79 282.00 o 3 9 0 35532.28 36272.00 675.70 o 4 9 0 2383.39 2076.36 148.04 o 5 9 0 5975.26 5587.00 188.27 o 6 9 0 4386.46 4501.64 145.05 o 7 9 0 46.02 151.86 37.95 o 8 9 0 964.78 914.02 62.32 o 9 9 0 67.92 76.73 58.91 o 10 9 0 619.71 579.19 119.07 o -9 10 0 579.15 920.24 194.74 o -8 10 0 787.93 1147.19 142.40 o -7 10 0 28.14 14.62 68.72 o -6 10 0 1623.54 1521.73 123.40 o -5 10 0 591.56 580.09 59.35 o -4 10 0 1298.34 1289.14 89.36 o -3 10 0 598.95 630.98 54.10 o -2 10 0 6836.97 6867.77 152.13 o -1 10 0 1097.27 1163.04 57.04 o 0 10 0 678.33 676.33 67.83 o 1 10 0 535.94 481.75 40.62 o 2 10 0 672.48 626.28 47.59 o 3 10 0 1896.41 1722.32 84.99 o 4 10 0 177.68 130.66 26.02 o 5 10 0 1637.25 1415.26 216.26 o 6 10 0 46.74 86.57 43.67 o 7 10 0 7114.57 6993.55 176.63 o 8 10 0 3662.45 3611.75 140.11 o 9 10 0 114.30 234.21 81.72 o 10 10 0 22.15 -13.88 115.70 o -8 11 0 1163.17 1564.79 239.48 o -7 11 0 457.29 443.45 89.95 o -6 11 0 176.97 148.01 45.44 o -5 11 0 33.08 -21.53 55.42 o -4 11 0 45.97 1.53 50.43 o -3 11 0 596.57 478.22 43.74 o -2 11 0 730.45 666.43 48.89 o -1 11 0 2111.43 2090.18 128.09 o 0 11 0 4494.75 4810.90 180.65 o 1 11 0 387.50 490.49 48.09 o 2 11 0 5591.68 5696.03 159.82 o 3 11 0 6001.50 6145.60 171.94 o 4 11 0 2755.48 2735.83 115.32 o 5 11 0 736.16 598.84 64.32 o 6 11 0 637.64 652.66 75.92 o 7 11 0 79.37 72.96 38.17 o 8 11 0 407.35 489.47 73.65 o 9 11 0 1174.25 1500.00 207.95 o 10 11 0 3.70 -54.16 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