#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:41:49 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/12/2241266.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241266 _cell_angle_alpha 90.000 _cell_angle_beta 103.591 _cell_angle_gamma 90.000 _cell_length_a 12.3282 _cell_length_b 5.8935 _cell_length_c 18.9202 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8543 _cod_data_source_file gk2647Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.74 -0.67 0.67 o 4 0 0 7239.03 4683.66 335.66 o 6 0 0 1922.23 2078.26 105.74 o 8 0 0 40.83 40.88 2.01 o 10 0 0 17.22 17.73 1.75 o 12 0 0 7.51 8.67 1.02 o 1 1 0 12.70 20.10 1.13 o 2 1 0 13340.01 12999.86 656.73 o 3 1 0 7880.48 8150.29 412.40 o 4 1 0 2178.00 2231.31 138.11 o 5 1 0 69.94 70.34 9.88 o 6 1 0 512.35 530.55 17.27 o 7 1 0 115.32 114.97 2.68 o 8 1 0 64.61 69.69 2.38 o 9 1 0 55.51 55.28 1.81 o 10 1 0 0.48 0.31 0.47 o 11 1 0 17.32 15.88 1.03 o 12 1 0 18.64 18.98 1.21 o 13 1 0 4.91 6.11 1.13 o 1 2 0 758.17 649.11 47.07 o 2 2 0 38.33 33.88 1.63 o 3 2 0 11.56 11.75 1.05 o 4 2 0 51.35 49.62 2.72 o 5 2 0 238.70 245.32 7.04 o 6 2 0 66.17 74.52 2.03 o 7 2 0 163.70 176.80 4.59 o 8 2 0 180.00 195.51 5.34 o 9 2 0 0.01 -0.25 0.39 o 10 2 0 595.46 560.61 39.11 o 11 2 0 373.60 395.96 13.43 o 12 2 0 63.61 74.26 5.37 o 13 2 0 37.21 36.87 2.56 o 1 3 0 91.33 87.42 5.65 o 2 3 0 630.89 600.65 22.12 o 3 3 0 94.05 102.68 3.83 o 4 3 0 589.56 619.87 22.80 o 5 3 0 13.09 12.69 0.91 o 6 3 0 57.31 57.22 2.41 o 7 3 0 17.48 18.65 1.07 o 8 3 0 2077.07 1485.47 53.91 o 9 3 0 243.23 254.74 9.80 o 10 3 0 9.39 8.16 0.87 o 11 3 0 1.46 1.25 0.73 o 12 3 0 28.93 27.55 1.78 o 0 4 0 270.05 265.40 14.56 o 1 4 0 9.10 7.63 0.72 o 2 4 0 329.14 338.97 10.46 o 3 4 0 41.92 42.28 2.04 o 4 4 0 64.62 62.55 2.97 o 5 4 0 63.79 60.77 4.62 o 6 4 0 294.80 249.85 11.44 o 7 4 0 5.82 4.61 0.69 o 8 4 0 76.00 61.94 4.13 o 9 4 0 102.78 100.73 4.35 o 10 4 0 69.48 61.96 4.19 o 11 4 0 19.30 15.22 1.55 o 1 5 0 40.89 42.46 2.46 o 2 5 0 9.58 11.13 1.24 o 3 5 0 165.86 149.69 11.06 o 4 5 0 10.54 8.77 1.24 o 5 5 0 53.46 38.33 6.66 o 6 5 0 21.76 24.20 1.94 o 7 5 0 21.53 19.27 1.38 o 8 5 0 10.00 11.09 1.02 o 9 5 0 4.76 4.34 0.71 o 0 6 0 277.20 287.55 15.70 o 1 6 0 111.96 103.00 6.93 o 2 6 0 83.93 78.82 5.51 o 3 6 0 17.93 17.17 1.91 o 4 6 0 2.14 2.15 0.94 o 5 6 0 18.60 15.74 1.88 o 6 6 0 0.01 -0.13 0.67 o -13 0 1 3.22 2.45 0.82 o -11 0 1 4.41 3.74 0.78 o -9 0 1 22.07 29.14 1.71 o -7 0 1 1296.06 1389.29 50.04 o -5 0 1 1206.66 864.55 62.81 o -3 0 1 992.16 1079.71 77.72 o -1 0 1 0.40 -0.13 0.13 o 1 0 1 3952.37 1873.92 134.61 o 3 0 1 109.38 85.52 6.72 o 5 0 1 0.12 -0.13 0.81 o 7 0 1 10.06 11.32 0.88 o 9 0 1 43.35 38.44 3.24 o 11 0 1 6.85 7.51 1.33 o 13 0 1 5.21 3.48 1.03 o -13 1 1 102.71 107.00 4.40 o -12 1 1 75.51 83.68 3.24 o -11 1 1 1.10 0.23 0.51 o -10 1 1 10.49 10.14 0.73 o -9 1 1 4.02 7.44 0.62 o -8 1 1 304.45 325.41 7.39 o -7 1 1 173.48 184.57 4.27 o -6 1 1 697.75 744.86 24.40 o -5 1 1 438.34 489.18 25.90 o -4 1 1 586.75 639.96 33.18 o -3 1 1 10239.35 10770.76 545.00 o -1 1 1 685.97 642.62 26.55 o 0 1 1 1394.82 1248.02 51.58 o 1 1 1 2072.96 2103.98 106.60 o 2 1 1 167.47 195.68 10.22 o 3 1 1 2404.81 2464.92 125.04 o 4 1 1 120.13 119.84 8.20 o 5 1 1 114.07 126.00 7.08 o 6 1 1 215.98 219.44 7.38 o 7 1 1 177.21 172.05 4.15 o 8 1 1 0.05 0.20 0.33 o 9 1 1 288.22 303.29 9.32 o 10 1 1 10.15 11.19 0.88 o 11 1 1 7.86 8.46 0.95 o 12 1 1 26.60 24.86 1.62 o 13 1 1 47.36 50.14 3.28 o -13 2 1 21.61 18.20 1.71 o -12 2 1 4.86 3.55 0.72 o -11 2 1 134.02 143.87 5.35 o -10 2 1 325.18 277.49 18.38 o -9 2 1 38.93 32.28 3.24 o -8 2 1 32.60 33.45 2.02 o -7 2 1 419.82 451.09 11.72 o -6 2 1 2348.10 2440.21 58.32 o -5 2 1 2636.30 2724.80 79.94 o -4 2 1 1246.65 1392.21 58.28 o -3 2 1 230.92 241.51 10.64 o -2 2 1 42.73 45.10 4.24 o -1 2 1 583.75 441.89 32.41 o 0 2 1 309.53 295.98 21.52 o 1 2 1 1768.76 1697.22 86.10 o 2 2 1 8.68 10.57 0.79 o 3 2 1 2309.60 2485.49 103.11 o 4 2 1 60.00 76.11 3.89 o 5 2 1 1338.36 1306.48 33.28 o 6 2 1 386.97 392.90 9.20 o 7 2 1 484.52 517.82 12.68 o 8 2 1 9.42 10.41 0.67 o 9 2 1 199.41 199.19 7.11 o 10 2 1 0.05 0.33 0.51 o 11 2 1 1.91 1.90 0.63 o 12 2 1 21.03 24.31 4.40 o 13 2 1 0.28 1.21 1.08 o -12 3 1 9.39 11.00 1.13 o -11 3 1 3.22 2.98 0.80 o -10 3 1 12.91 15.66 1.07 o -9 3 1 161.76 141.49 13.51 o -8 3 1 548.32 490.48 23.04 o -7 3 1 172.36 164.20 5.14 o -6 3 1 18.26 15.95 0.98 o -5 3 1 5.19 6.55 0.71 o -4 3 1 43.79 44.82 1.92 o -3 3 1 20.57 21.51 1.24 o -2 3 1 1.67 3.49 0.70 o -1 3 1 38.56 46.68 3.51 o 0 3 1 96.20 90.10 5.80 o 1 3 1 476.55 465.93 24.87 o 2 3 1 210.34 206.74 8.05 o 3 3 1 260.07 258.33 8.84 o 4 3 1 125.44 126.56 4.55 o 5 3 1 83.25 90.18 3.11 o 6 3 1 223.21 235.24 6.86 o 7 3 1 352.74 355.99 11.46 o 8 3 1 265.44 278.02 8.74 o 9 3 1 108.43 110.19 5.99 o 10 3 1 1.35 1.50 0.76 o 11 3 1 3.25 2.64 0.93 o 12 3 1 6.04 6.87 1.03 o -11 4 1 3.33 2.41 0.87 o -10 4 1 7.74 7.24 0.88 o -9 4 1 10.11 11.05 0.96 o -8 4 1 24.80 22.65 2.12 o -7 4 1 194.32 191.79 7.80 o -6 4 1 36.07 36.75 4.72 o -5 4 1 268.33 264.59 11.57 o -4 4 1 1.05 1.35 0.59 o -3 4 1 0.55 0.93 0.57 o -2 4 1 136.05 132.76 4.43 o -1 4 1 67.31 70.07 2.88 o 0 4 1 81.51 92.25 4.06 o 1 4 1 68.10 81.14 3.22 o 2 4 1 208.75 196.32 6.29 o 3 4 1 16.86 16.70 1.12 o 4 4 1 138.41 142.83 5.87 o 5 4 1 662.78 584.28 30.14 o 6 4 1 741.80 459.06 28.76 o 7 4 1 66.63 67.49 4.21 o 8 4 1 2.13 2.05 0.67 o 9 4 1 73.00 73.64 3.38 o 10 4 1 0.07 -0.24 0.74 o 11 4 1 2.73 3.61 0.84 o -9 5 1 2.51 3.23 0.66 o -8 5 1 4.56 5.18 0.79 o -7 5 1 4.41 4.99 0.77 o -6 5 1 47.94 47.30 2.43 o -5 5 1 128.74 120.50 13.44 o -4 5 1 16.49 17.34 2.22 o -3 5 1 290.39 206.15 15.87 o -2 5 1 35.02 36.87 2.79 o -1 5 1 77.32 82.59 3.87 o 0 5 1 371.53 379.40 14.52 o 1 5 1 64.47 69.06 3.39 o 2 5 1 440.10 464.88 15.64 o 3 5 1 321.13 339.44 14.95 o 4 5 1 108.27 107.22 8.61 o 5 5 1 46.62 52.79 3.14 o 6 5 1 39.72 36.51 1.98 o 7 5 1 5.76 6.30 0.82 o 8 5 1 1.43 1.23 0.61 o 9 5 1 0.00 0.99 0.64 o -7 6 1 1.15 1.34 1.08 o -6 6 1 0.20 0.13 0.81 o -5 6 1 0.69 -0.13 0.81 o -4 6 1 0.17 1.08 0.94 o -3 6 1 39.02 40.70 3.27 o -2 6 1 38.65 41.75 3.30 o -1 6 1 41.92 37.90 4.03 o 0 6 1 41.85 41.72 2.56 o 1 6 1 15.86 15.22 1.45 o 2 6 1 15.59 15.36 1.79 o 3 6 1 0.44 1.24 1.41 o 4 6 1 0.10 0.54 0.81 o 5 6 1 4.16 2.72 0.79 o 6 6 1 18.42 18.16 2.02 o -12 0 2 22.26 22.16 1.95 o -10 0 2 24.21 29.11 2.50 o -8 0 2 0.13 1.26 0.45 o -6 0 2 90.45 117.66 9.68 o -4 0 2 460.31 332.97 24.61 o -2 0 2 8057.10 9005.05 644.41 o 0 0 2 577.04 594.12 43.17 o 2 0 2 3197.47 3244.24 232.51 o 4 0 2 965.01 668.75 48.82 o 6 0 2 465.72 504.91 21.38 o 8 0 2 525.49 626.26 22.96 o 10 0 2 32.69 33.19 2.50 o 12 0 2 18.58 18.79 1.75 o -13 1 2 15.99 16.22 1.32 o -12 1 2 8.00 7.97 0.79 o -11 1 2 7.98 6.11 0.68 o -10 1 2 1.20 0.62 0.46 o -9 1 2 120.34 132.64 3.47 o -8 1 2 197.98 215.16 5.01 o -7 1 2 69.27 92.05 2.41 o -6 1 2 377.09 393.56 13.16 o -5 1 2 1.97 5.48 0.89 o -4 1 2 13.72 14.21 2.23 o -3 1 2 26.46 39.01 3.36 o -2 1 2 341.24 372.17 19.21 o -1 1 2 1016.60 877.21 62.87 o 0 1 2 1729.87 1708.77 70.55 o 1 1 2 5904.92 6005.33 303.86 o 2 1 2 123.80 162.93 8.56 o 3 1 2 2609.74 2734.87 138.74 o 4 1 2 235.17 246.53 13.03 o 5 1 2 18.28 25.54 2.56 o 6 1 2 1.57 1.16 0.31 o 7 1 2 0.31 0.74 0.32 o 8 1 2 164.17 175.55 5.22 o 9 1 2 12.02 10.99 1.17 o 10 1 2 80.18 80.00 5.73 o 11 1 2 189.73 201.60 6.52 o 12 1 2 6.33 7.11 0.78 o 13 1 2 11.12 11.60 1.10 o -13 2 2 3.12 1.45 0.70 o -12 2 2 2.36 1.77 0.97 o -11 2 2 37.45 45.93 3.00 o -10 2 2 2.36 2.94 0.62 o -9 2 2 8.13 9.81 1.07 o -8 2 2 63.75 69.27 3.00 o -7 2 2 12.36 15.77 0.83 o -6 2 2 842.93 830.43 20.16 o -5 2 2 1655.66 1718.11 50.55 o -4 2 2 127.92 124.60 5.93 o -3 2 2 574.10 603.17 25.46 o -2 2 2 109.70 113.01 6.70 o -1 2 2 682.77 536.02 39.67 o 0 2 2 0.78 0.54 0.45 o 1 2 2 33.21 37.73 1.89 o 2 2 2 82.47 83.10 3.42 o 3 2 2 223.09 183.41 8.25 o 4 2 2 320.50 370.79 16.21 o 5 2 2 149.43 153.58 3.77 o 6 2 2 62.18 66.91 1.87 o 7 2 2 46.22 47.95 2.03 o 8 2 2 126.57 135.32 3.69 o 9 2 2 121.41 125.85 5.31 o 10 2 2 5.61 5.41 0.68 o 11 2 2 35.98 38.55 1.98 o 12 2 2 3.01 2.40 0.94 o -12 3 2 3.60 2.67 1.05 o -11 3 2 0.39 -0.13 0.55 o -10 3 2 252.11 259.63 10.19 o -9 3 2 0.10 0.73 0.45 o -8 3 2 878.22 851.40 30.91 o -7 3 2 45.60 38.44 2.13 o -6 3 2 581.26 586.09 19.11 o -5 3 2 29.90 30.09 1.49 o -4 3 2 268.70 243.55 7.47 o -3 3 2 55.05 46.95 1.83 o -2 3 2 177.85 177.89 8.13 o -1 3 2 65.35 68.38 4.61 o 0 3 2 430.48 448.82 23.96 o 1 3 2 1305.43 1374.73 70.84 o 2 3 2 0.71 0.75 0.42 o 3 3 2 787.10 796.25 23.61 o 4 3 2 45.79 51.30 2.18 o 5 3 2 13.27 10.55 0.78 o 6 3 2 28.18 33.34 1.52 o 7 3 2 529.77 561.45 15.75 o 8 3 2 4.47 4.94 0.68 o 9 3 2 52.94 56.29 2.50 o 10 3 2 0.01 -0.45 0.65 o 11 3 2 1.18 2.31 0.75 o 12 3 2 0.34 -0.27 0.94 o -11 4 2 22.22 16.61 1.57 o -10 4 2 121.28 112.00 5.59 o -9 4 2 47.40 41.09 2.02 o -8 4 2 67.02 52.91 6.07 o -7 4 2 215.38 223.98 10.39 o -6 4 2 32.05 29.53 4.04 o -5 4 2 235.91 226.96 10.04 o -4 4 2 48.38 41.10 2.43 o -3 4 2 5.26 3.01 0.69 o -2 4 2 76.90 81.01 3.70 o -1 4 2 233.03 216.60 8.54 o 0 4 2 410.91 394.56 13.21 o 1 4 2 129.04 126.83 4.67 o 2 4 2 299.12 319.32 10.86 o 3 4 2 53.13 51.08 2.47 o 4 4 2 11.81 14.27 1.16 o 5 4 2 2.13 2.67 0.60 o 6 4 2 167.45 102.59 5.89 o 7 4 2 1.62 2.58 0.62 o 8 4 2 22.57 25.07 1.96 o 9 4 2 10.77 12.08 1.24 o 10 4 2 8.88 9.14 1.19 o -9 5 2 0.56 1.03 0.56 o -8 5 2 2.83 2.55 0.83 o -7 5 2 24.86 25.13 1.66 o -6 5 2 1.49 1.66 0.74 o -5 5 2 142.82 150.00 7.33 o -4 5 2 90.61 97.08 5.09 o -3 5 2 35.40 28.20 10.29 o -2 5 2 1.51 0.28 0.91 o -1 5 2 23.39 22.47 1.69 o 0 5 2 1.95 2.29 0.78 o 1 5 2 14.06 16.89 1.44 o 2 5 2 78.97 85.86 3.77 o 3 5 2 375.46 402.06 17.61 o 4 5 2 52.84 54.70 7.59 o 5 5 2 30.09 26.67 4.30 o 6 5 2 0.04 -0.43 0.54 o 7 5 2 17.48 17.23 1.23 o 8 5 2 1.75 1.73 0.63 o 9 5 2 16.47 17.48 2.15 o -7 6 2 1.48 0.40 0.94 o -6 6 2 24.96 24.64 1.85 o -5 6 2 16.78 15.26 1.43 o -4 6 2 8.28 8.39 1.51 o -3 6 2 0.38 0.71 0.88 o -2 6 2 0.91 0.65 2.35 o -1 6 2 180.47 181.22 10.47 o 0 6 2 204.13 208.80 9.48 o 1 6 2 15.06 17.48 1.61 o 2 6 2 27.18 26.76 2.82 o 3 6 2 0.44 1.48 0.81 o 4 6 2 9.22 10.06 1.48 o 5 6 2 0.13 0.54 0.94 o 6 6 2 45.26 47.21 4.03 o -13 0 3 6.81 5.25 1.19 o -11 0 3 5.85 4.01 0.80 o -9 0 3 0.13 1.14 0.51 o -7 0 3 1378.00 1562.81 56.16 o -5 0 3 1666.90 1187.29 86.06 o -3 0 3 10.10 15.33 1.88 o 1 0 3 3417.01 3529.60 252.81 o 3 0 3 321.29 232.51 17.35 o 5 0 3 357.16 196.74 15.20 o 7 0 3 72.18 84.12 3.50 o 9 0 3 142.46 167.92 7.53 o 11 0 3 81.34 92.86 5.08 o 13 0 3 1.09 0.04 0.94 o -13 1 3 76.01 81.88 3.42 o -12 1 3 67.23 78.76 2.93 o -11 1 3 0.00 0.24 0.52 o -10 1 3 5.95 5.93 0.62 o -9 1 3 87.99 94.68 2.64 o -8 1 3 68.95 68.13 2.06 o -7 1 3 145.69 144.41 3.61 o -6 1 3 599.25 684.74 22.50 o -5 1 3 515.90 569.29 29.81 o -4 1 3 582.54 432.61 32.14 o -3 1 3 5358.73 5369.79 346.81 o -2 1 3 2904.91 2624.37 145.70 o -1 1 3 5031.85 4444.24 301.97 o 0 1 3 1774.13 1802.32 91.38 o 1 1 3 7049.20 7566.55 382.69 o 2 1 3 1759.35 1814.91 92.19 o 3 1 3 245.88 250.93 13.22 o 4 1 3 143.68 153.38 8.42 o 5 1 3 639.61 731.54 37.80 o 6 1 3 816.68 894.29 21.54 o 7 1 3 2.37 3.86 0.41 o 8 1 3 17.22 19.57 0.95 o 9 1 3 22.96 20.91 2.27 o 10 1 3 104.68 102.67 6.89 o 11 1 3 84.85 87.89 3.19 o 12 1 3 4.12 3.45 0.72 o 13 1 3 0.08 0.49 0.80 o -13 2 3 15.16 15.16 1.12 o -12 2 3 93.12 101.18 3.92 o -11 2 3 125.72 139.12 5.52 o -10 2 3 164.83 176.78 5.81 o -9 2 3 56.69 58.91 2.11 o -8 2 3 4.45 6.85 0.60 o -7 2 3 1.72 2.14 0.40 o -6 2 3 739.32 744.35 19.18 o -5 2 3 361.14 370.69 9.75 o -4 2 3 16.88 17.37 1.65 o -3 2 3 376.76 395.00 21.16 o -2 2 3 1166.19 1063.27 54.81 o -1 2 3 33.96 32.47 2.41 o 0 2 3 68.53 65.05 3.89 o 1 2 3 1181.13 1162.43 48.37 o 2 2 3 55.87 60.65 2.67 o 3 2 3 4653.20 4985.41 310.91 o 4 2 3 45.84 58.16 2.13 o 5 2 3 0.26 1.12 0.54 o 6 2 3 134.04 136.13 3.45 o 7 2 3 635.12 680.05 15.82 o 8 2 3 7.56 9.81 0.74 o 9 2 3 318.03 354.51 12.14 o 10 2 3 3.16 3.46 0.72 o 11 2 3 37.35 36.71 3.20 o 12 2 3 55.45 52.73 3.46 o -12 3 3 12.07 12.98 1.26 o -11 3 3 2.45 2.24 0.61 o -10 3 3 110.78 102.29 6.90 o -9 3 3 95.64 91.69 3.34 o -8 3 3 23.61 19.06 1.05 o -7 3 3 150.02 143.06 4.55 o -6 3 3 0.00 0.22 0.34 o -5 3 3 20.45 26.22 1.16 o -4 3 3 0.00 -0.20 0.31 o -3 3 3 59.86 59.53 2.22 o -2 3 3 51.21 47.42 2.09 o -1 3 3 15.17 23.11 2.44 o 0 3 3 0.00 0.19 0.80 o 1 3 3 462.57 493.83 18.25 o 2 3 3 101.21 96.42 3.00 o 3 3 3 0.07 0.26 0.35 o 4 3 3 0.13 0.74 0.37 o 5 3 3 19.02 20.03 1.09 o 6 3 3 6.31 8.43 0.82 o 7 3 3 11.49 11.95 0.91 o 8 3 3 17.79 22.81 1.57 o 9 3 3 131.04 130.11 4.45 o 10 3 3 6.48 7.93 1.02 o 11 3 3 0.36 1.09 0.76 o -11 4 3 60.41 53.50 3.41 o -10 4 3 73.68 65.92 3.16 o -9 4 3 183.55 184.99 6.56 o -8 4 3 164.22 98.54 5.89 o -7 4 3 183.60 190.89 8.97 o -6 4 3 50.51 49.30 6.48 o -5 4 3 52.62 53.08 2.92 o -4 4 3 28.02 27.64 1.77 o -3 4 3 2.04 2.29 0.52 o -2 4 3 118.00 107.31 6.54 o -1 4 3 143.49 143.51 5.66 o 0 4 3 10.91 10.73 1.08 o 1 4 3 415.28 403.30 13.47 o 2 4 3 367.92 381.63 12.87 o 3 4 3 58.31 62.89 2.91 o 4 4 3 15.37 15.70 0.98 o 5 4 3 98.89 94.78 8.66 o 6 4 3 18.98 19.10 2.42 o 7 4 3 2.21 1.77 0.57 o 8 4 3 6.05 6.01 0.78 o 9 4 3 1.97 1.67 0.72 o 10 4 3 31.71 26.77 2.04 o -9 5 3 1.30 0.40 0.60 o -8 5 3 0.01 -0.45 0.52 o -7 5 3 11.13 13.53 1.06 o -6 5 3 10.97 10.35 1.11 o -5 5 3 20.78 19.08 2.61 o -4 5 3 32.38 26.75 2.57 o -3 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