data_2241282 _cell_angle_alpha 90.000 _cell_angle_beta 100.538 _cell_angle_gamma 90.000 _cell_length_a 6.6833 _cell_length_b 12.2817 _cell_length_c 14.6134 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.5713 _cod_data_source_file pj20251sup2.hkl _cod_data_source_block 1 _shelx_title ' brocr01 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 469.26 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2101.28 2484.19 50.08 o 4 0 0 5922.39 6236.67 119.47 o 6 0 0 17861.10 18646.65 327.51 o 8 0 0 11225.36 11666.75 264.42 o 10 0 0 3224.63 3459.31 157.05 o 1 1 0 48558.21 51479.56 489.59 o 2 1 0 740.66 860.31 20.18 o 3 1 0 463.99 484.87 15.75 o 4 1 0 19581.45 19849.94 245.65 o 5 1 0 31803.41 32065.68 343.52 o 6 1 0 2292.60 2292.18 45.29 o 7 1 0 9631.20 9875.22 143.69 o 8 1 0 733.18 806.16 42.43 o 9 1 0 13.06 16.70 33.58 o 10 1 0 254.01 251.60 57.11 o 11 1 0 2151.08 2164.95 124.51 o 0 2 0 28191.78 29729.64 403.75 o 1 2 0 37714.76 40336.49 385.73 o 2 2 0 23604.25 24887.50 232.13 o 3 2 0 12765.19 12929.88 142.25 o 4 2 0 8130.36 8248.78 100.48 o 5 2 0 2394.31 2477.46 47.64 o 6 2 0 18725.00 18854.47 215.06 o 7 2 0 377.26 432.74 32.72 o 8 2 0 126.50 183.90 30.95 o 9 2 0 6490.39 6920.35 137.95 o 10 2 0 110.68 55.53 43.73 o 11 2 0 395.09 324.22 76.82 o 1 3 0 11822.90 12509.81 121.01 o 2 3 0 32316.34 32360.92 287.76 o 3 3 0 5109.57 4870.88 56.68 o 4 3 0 22293.36 23188.20 236.42 o 5 3 0 727.24 776.09 26.69 o 6 3 0 363.01 402.96 24.01 o 7 3 0 2387.80 2413.12 59.09 o 8 3 0 8245.36 8619.76 149.53 o 9 3 0 3.51 36.04 35.59 o 10 3 0 5312.35 5756.63 133.16 o 11 3 0 1174.96 1228.49 112.64 o 0 4 0 5311.81 5599.65 83.41 o 1 4 0 1300.13 1347.02 22.05 o 2 4 0 34.41 43.45 6.81 o 3 4 0 79694.22 79645.84 728.70 o 4 4 0 41.42 60.20 11.00 o 5 4 0 11273.06 11512.48 131.47 o 6 4 0 46.54 53.23 15.24 o 7 4 0 6192.71 6316.22 124.33 o 8 4 0 244.71 306.12 41.42 o 9 4 0 7031.93 7306.89 146.02 o 10 4 0 130.58 134.04 50.43 o 11 4 0 1908.01 1957.98 127.68 o 1 5 0 5619.63 5511.27 66.74 o 2 5 0 31667.18 31691.52 299.57 o 3 5 0 3903.85 3847.80 47.37 o 4 5 0 26435.58 26552.46 258.16 o 5 5 0 644.17 634.53 23.10 o 6 5 0 19.77 39.90 20.78 o 7 5 0 3655.86 3597.31 91.74 o 8 5 0 7191.89 7269.55 137.90 o 9 5 0 3.25 -33.78 35.58 o 10 5 0 6086.43 6215.46 172.64 o 11 5 0 480.04 429.29 94.44 o 0 6 0 15205.18 15360.04 275.23 o 1 6 0 25477.72 24558.30 249.49 o 2 6 0 4883.10 4761.95 59.23 o 3 6 0 13853.08 13877.59 144.14 o 4 6 0 3054.26 3133.76 44.30 o 5 6 0 2995.78 3110.12 53.00 o 6 6 0 8231.58 8404.93 117.88 o 7 6 0 129.04 129.84 33.21 o 8 6 0 316.52 357.10 42.86 o 9 6 0 10114.75 10226.71 222.60 o 10 6 0 240.53 235.17 61.14 o 1 7 0 20151.12 20162.78 222.61 o 2 7 0 536.63 504.24 18.90 o 3 7 0 3134.26 2980.04 60.45 o 4 7 0 14894.25 14788.14 157.76 o 5 7 0 25191.07 24898.91 297.83 o 6 7 0 1751.49 1763.63 48.19 o 7 7 0 5413.66 5495.42 112.97 o 8 7 0 1384.39 1440.03 70.53 o 9 7 0 3.73 65.69 49.47 o 10 7 0 597.30 563.69 75.83 o 0 8 0 93904.90 92112.09 1146.32 o 1 8 0 1006.42 961.44 27.30 o 2 8 0 2277.14 2238.99 41.28 o 3 8 0 2272.53 2173.94 39.55 o 4 8 0 6237.79 6171.74 87.03 o 5 8 0 697.92 784.77 34.91 o 6 8 0 11649.93 11653.29 166.16 o 7 8 0 670.53 768.82 57.14 o 8 8 0 5634.53 5539.31 168.31 o 9 8 0 6.52 25.29 49.68 o 10 8 0 1662.55 1567.80 103.45 o 1 9 0 31901.62 30868.98 302.77 o 2 9 0 720.26 678.33 26.21 o 3 9 0 354.83 373.13 25.84 o 4 9 0 8479.38 8249.59 110.25 o 5 9 0 11227.64 10951.56 157.72 o 6 9 0 1245.24 1145.13 48.62 o 7 9 0 10464.65 10408.83 218.63 o 8 9 0 32.11 18.96 46.40 o 9 9 0 7.59 -5.69 47.61 o 10 9 0 27.03 -45.20 59.62 o 0 10 0 10775.67 10756.33 163.77 o 1 10 0 1325.32 1382.59 34.29 o 2 10 0 10325.17 10494.85 128.27 o 3 10 0 7706.97 7439.46 116.71 o 4 10 0 4571.97 4484.19 92.89 o 5 10 0 198.38 208.86 30.03 o 6 10 0 12889.49 12832.51 187.11 o 7 10 0 265.17 286.72 55.76 o 8 10 0 212.52 147.75 55.06 o 9 10 0 1827.26 1985.09 124.78 o 10 10 0 257.90 4.42 154.69 o 1 11 0 8608.60 8528.16 128.40 o 2 11 0 18843.56 18554.38 237.37 o 3 11 0 1655.25 1672.54 83.84 o 4 11 0 4537.18 4379.75 95.24 o 5 11 0 1662.41 1630.80 62.34 o 6 11 0 942.27 924.38 70.42 o 7 11 0 2108.62 2111.61 118.23 o 8 11 0 3830.23 3907.82 138.79 o 9 11 0 9.31 -27.46 57.76 o 0 12 0 4542.16 4502.35 103.56 o 1 12 0 855.73 819.98 37.64 o 2 12 0 1.82 -18.73 19.93 o 3 12 0 22688.75 22351.72 285.05 o 4 12 0 204.56 181.42 35.33 o 5 12 0 4557.42 4594.73 117.47 o 6 12 0 527.17 576.64 82.00 o 7 12 0 3105.25 3069.07 139.50 o 8 12 0 108.60 150.44 58.77 o 9 12 0 3730.41 3678.06 165.89 o 1 13 0 529.55 578.62 38.68 o 2 13 0 11131.98 11175.01 153.54 o 3 13 0 700.54 681.60 43.83 o 4 13 0 15064.08 15168.17 256.08 o 5 13 0 538.05 617.42 58.37 o 6 13 0 26.33 74.31 49.13 o 7 13 0 593.83 547.76 106.85 o 8 13 0 3442.37 3377.63 189.04 o 9 13 0 35.07 81.76 205.52 o 0 14 0 3699.58 3744.56 138.70 o 1 14 0 7774.00 7716.15 137.68 o 2 14 0 187.34 164.97 29.71 o 3 14 0 6329.49 6346.34 117.94 o 4 14 0 96.89 107.65 41.54 o 5 14 0 1441.44 1509.92 99.40 o 6 14 0 2182.72 2105.39 103.74 o 7 14 0 326.84 324.23 78.71 o 8 14 0 261.54 168.07 64.27 o 1 15 0 4259.92 4289.45 111.16 o 2 15 0 3319.17 3186.67 96.36 o 3 15 0 1334.65 1226.60 70.76 o 4 15 0 2810.77 2862.24 90.94 o 5 15 0 7669.25 7601.72 173.17 o 6 15 0 20.32 -14.57 50.98 o 7 15 0 1702.82 1425.09 121.26 o 8 15 0 1922.04 1788.02 237.56 o 0 16 0 17326.14 17760.59 406.80 o 1 16 0 423.46 423.08 50.58 o 2 16 0 921.98 1068.81 81.47 o 3 16 0 2249.03 2386.25 148.02 o 4 16 0 1351.34 1269.95 92.52 o 5 16 0 213.26 226.81 54.55 o 6 16 0 4843.82 4850.31 141.83 o 7 16 0 630.34 532.68 81.69 o 1 17 0 9497.36 9959.24 216.15 o 2 17 0 146.70 126.19 49.75 o 3 17 0 176.28 193.17 51.79 o 4 17 0 314.83 312.63 63.30 o 5 17 0 3025.95 3185.41 133.08 o 6 17 0 106.31 66.87 57.44 o 0 18 0 3149.81 3335.49 194.86 o 1 18 0 231.32 255.10 55.40 o 2 18 0 3008.63 3206.87 123.42 o 3 18 0 1041.44 1067.13 89.92 o 4 18 0 1545.06 1526.54 101.71 o 5 18 0 144.09 145.74 64.53 o 6 18 0 4562.76 4259.10 241.33 o 1 19 0 2781.84 2919.32 190.10 o 2 19 0 3143.60 3439.72 128.00 o 3 19 0 36.43 45.24 54.79 o 4 19 0 1417.60 1328.89 98.86 o 5 19 0 1692.54 1726.52 148.81 o 0 20 0 2032.89 2119.49 175.87 o 1 20 0 600.58 552.42 81.44 o 2 20 0 4.30 29.17 57.58 o 3 20 0 4792.78 5048.00 163.71 o 4 20 0 298.40 352.10 104.77 o 1 21 0 16.74 76.71 72.29 o -11 0 1 1843.23 1975.41 172.34 o -9 0 1 1696.51 1716.79 153.42 o -7 0 1 10590.38 10967.04 219.93 o -5 0 1 53442.05 54268.81 843.66 o -3 0 1 4352.18 4830.50 81.59 o -1 0 1 21492.36 23933.09 325.58 o 1 0 1 84188.16 86400.77 1311.76 o 3 0 1 8743.24 8942.44 170.68 o 5 0 1 36633.67 36347.04 584.35 o 7 0 1 7364.65 7728.94 154.06 o 9 0 1 2747.59 2879.36 158.84 o 11 0 1 1668.34 1680.20 164.60 o -11 1 1 99.90 164.53 79.52 o -10 1 1 2932.99 3224.87 116.79 o -9 1 1 2415.12 2497.40 78.84 o -8 1 1 2097.94 2059.19 56.30 o -7 1 1 109.42 140.88 25.10 o -6 1 1 20224.14 20631.89 234.52 o -5 1 1 1890.32 1903.52 41.56 o -4 1 1 15844.16 15978.55 177.18 o -3 1 1 8043.62 8239.15 90.85 o -2 1 1 56.54 102.75 8.32 o -1 1 1 5694.59 6128.83 62.29 o 0 1 1 119386.70 113758.59 1044.28 o 1 1 1 1839.75 2023.32 23.95 o 2 1 1 16561.72 17367.32 172.57 o 3 1 1 132.53 194.32 11.51 o 4 1 1 800.91 837.27 23.21 o 5 1 1 3491.57 3605.15 55.27 o 6 1 1 14011.52 14115.00 173.73 o 7 1 1 0.20 23.97 20.13 o 8 1 1 9624.12 9819.16 143.25 o 9 1 1 2742.35 2883.31 92.35 o 10 1 1 760.94 657.90 69.74 o 11 1 1 2.25 -2.17 58.73 o -11 2 1 3707.20 3881.05 144.16 o -10 2 1 1011.91 1093.10 74.00 o -9 2 1 33.08 57.09 34.11 o -8 2 1 5028.19 5116.74 96.49 o -7 2 1 2413.17 2497.13 59.67 o -6 2 1 1906.48 2021.37 46.48 o -5 2 1 9767.98 9914.02 121.32 o -4 2 1 20848.96 21096.59 227.67 o -3 2 1 10836.22 10760.50 114.16 o -2 2 1 5594.30 5782.57 63.20 o -1 2 1 59212.05 62272.77 591.82 o 0 2 1 3064.12 3266.39 37.16 o 1 2 1 11530.44 12243.99 116.76 o 2 2 1 2998.63 2989.54 41.45 o 3 2 1 15.31 69.90 13.30 o 4 2 1 35658.61 36737.47 425.86 o 5 2 1 1392.93 1480.61 33.28 o 6 2 1 449.87 488.87 30.56 o 7 2 1 16631.10 16925.80 220.96 o 8 2 1 938.52 934.59 45.38 o 9 2 1 7.85 52.49 35.82 o 10 2 1 3141.00 3252.45 108.11 o 11 2 1 882.89 833.98 86.32 o -11 3 1 434.10 471.96 82.58 o -10 3 1 309.30 312.24 46.50 o -9 3 1 8120.95 8448.68 168.99 o -8 3 1 476.76 517.33 43.26 o -7 3 1 6665.07 6601.35 113.85 o -6 3 1 13701.25 13795.15 156.42 o -5 3 1 5082.69 5240.52 72.33 o -4 3 1 211.62 239.49 14.37 o -3 3 1 28107.29 28781.47 299.36 o -2 3 1 20.96 80.48 12.48 o -1 3 1 24707.43 26249.66 286.66 o 0 3 1 1639.33 1897.11 35.09 o 1 3 1 1586.88 1699.89 22.81 o 2 3 1 16800.78 17421.61 184.55 o 3 3 1 62645.68 62884.52 606.24 o 4 3 1 2636.14 2632.96 41.09 o 5 3 1 10109.71 10331.16 126.09 o 6 3 1 2694.39 2779.68 59.41 o 7 3 1 597.70 616.84 38.03 o 8 3 1 118.28 140.04 33.15 o 9 3 1 5970.14 6243.47 131.80 o 10 3 1 107.42 65.99 41.51 o 11 3 1 2235.61 2364.25 135.78 o -11 4 1 1.07 32.49 56.19 o -10 4 1 7929.34 8274.58 180.56 o -9 4 1 56.01 85.63 36.68 o -8 4 1 5789.11 5771.06 125.55 o -7 4 1 11.77 31.61 25.57 o -6 4 1 314.26 394.82 22.82 o -5 4 1 427.27 478.34 21.34 o -4 4 1 8789.24 9131.16 95.26 o -3 4 1 565.13 616.27 15.37 o -2 4 1 99987.76 101032.69 1014.20 o -1 4 1 66.29 112.61 11.85 o 0 4 1 145.22 210.07 16.03 o 1 4 1 10.98 44.49 7.42 o 2 4 1 22721.85 23002.41 209.90 o 3 4 1 501.26 550.55 16.83 o 4 4 1 27853.20 27689.17 280.97 o 5 4 1 1584.04 1608.30 34.61 o 6 4 1 8228.47 8339.53 120.35 o 7 4 1 60.75 71.93 23.12 o 8 4 1 10348.62 10620.89 192.80 o 9 4 1 47.88 60.92 37.74 o 10 4 1 6267.36 6720.36 139.63 o 11 4 1 9.52 26.87 66.46 o -11 5 1 386.56 439.85 66.86 o -10 5 1 99.38 165.74 57.36 o -9 5 1 9558.04 9989.26 215.99 o -8 5 1 298.00 408.89 46.66 o -7 5 1 5634.67 5704.00 110.02 o -6 5 1 6247.50 6240.97 94.41 o -5 5 1 3888.84 4015.87 56.51 o -4 5 1 275.54 336.23 15.55 o -3 5 1 25068.90 24688.63 238.93 o -2 5 1 174.11 223.08 13.78 o -1 5 1 36493.75 37506.91 349.25 o 0 5 1 1063.10 1170.48 21.54 o 1 5 1 306.71 314.45 17.52 o 2 5 1 14973.97 14970.67 142.70 o 3 5 1 43562.72 43454.39 407.06 o 4 5 1 4365.04 4359.57 57.93 o 5 5 1 14035.16 14109.19 150.95 o 6 5 1 1352.16 1334.90 38.99 o 7 5 1 578.57 666.71 45.37 o 8 5 1 15.73 73.95 41.43 o 9 5 1 7184.99 7539.78 150.88 o 10 5 1 180.81 196.29 54.31 o -11 6 1 1243.12 868.83 144.23 o -10 6 1 837.71 739.94 85.85 o -9 6 1 42.03 74.06 48.09 o -8 6 1 7346.24 7410.38 181.28 o -7 6 1 1610.67 1667.82 59.78 o -6 6 1 616.25 663.39 32.74 o -5 6 1 10622.09 10628.37 135.48 o -4 6 1 17179.61 17035.59 174.97 o -3 6 1 1619.37 1633.48 29.23 o -2 6 1 4828.39 4866.99 62.05 o -1 6 1 11985.25 11673.30 120.03 o 0 6 1 6929.05 6666.21 71.42 o 1 6 1 11104.34 10905.79 109.46 o 2 6 1 5770.85 5529.64 67.14 o 3 6 1 260.39 294.79 14.47 o 4 6 1 37919.86 37184.94 355.90 o 5 6 1 1387.22 1449.37 49.78 o 6 6 1 672.95 663.03 37.31 o 7 6 1 6212.62 6365.85 139.41 o 8 6 1 1220.48 1143.73 60.53 o 9 6 1 111.94 105.82 43.82 o 10 6 1 3922.21 4148.48 180.85 o -10 7 1 1925.51 1827.12 104.57 o -9 7 1 2591.67 2504.25 109.44 o -8 7 1 2224.60 2287.80 109.35 o -7 7 1 182.17 219.76 35.00 o -6 7 1 7313.70 7427.08 109.64 o -5 7 1 444.28 482.60 27.02 o -4 7 1 11800.65 11475.31 135.35 o -3 7 1 8311.13 7990.97 98.86 o -2 7 1 537.32 524.17 20.63 o -1 7 1 10224.64 10219.26 109.39 o 0 7 1 62203.55 61493.54 545.17 o 1 7 1 4343.87 4194.72 64.09 o 2 7 1 2165.53 2092.82 36.86 o 3 7 1 873.54 912.19 26.75 o 4 7 1 28.93 83.21 17.90 o 5 7 1 5187.63 5064.07 81.73 o 6 7 1 14155.87 14241.31 193.92 o 7 7 1 13.86 14.42 31.14 o 8 7 1 5266.86 5293.29 128.86 o 9 7 1 3213.25 3257.14 121.80 o 10 7 1 518.93 451.30 71.60 o -10 8 1 339.45 273.83 75.27 o -9 8 1 1261.44 1421.24 91.71 o -8 8 1 10.68 18.82 46.65 o -7 8 1 9975.22 9949.34 183.99 o -6 8 1 32.45 26.78 22.56 o -5 8 1 25061.16 24749.17 284.34 o -4 8 1 177.54 189.82 20.14 o -3 8 1 84.98 110.02 17.14 o -2 8 1 1869.83 1763.21 34.75 o -1 8 1 11037.97 10865.87 117.57 o 0 8 1 65.30 75.69 12.28 o 1 8 1 44805.82 43663.82 421.48 o 2 8 1 136.76 171.28 16.03 o 3 8 1 3855.17 3677.80 58.74 o 4 8 1 387.71 432.53 27.76 o 5 8 1 15904.71 16126.85 197.45 o 6 8 1 370.57 389.00 34.85 o 7 8 1 7514.49 7422.37 153.07 o 8 8 1 1028.79 1130.22 71.11 o 9 8 1 1099.19 1210.43 90.80 o 10 8 1 27.03 27.61 55.58 o -10 9 1 1699.78 1722.67 120.65 o -9 9 1 1035.83 1066.47 139.45 o -8 9 1 588.93 584.14 71.30 o -7 9 1 768.98 807.49 61.02 o -6 9 1 15867.21 15608.01 216.33 o -5 9 1 1406.44 1412.62 54.24 o -4 9 1 8884.11 8651.54 129.29 o -3 9 1 1605.79 1637.57 46.71 o -2 9 1 1673.33 1704.60 36.30 o -1 9 1 3298.17 3192.96 74.02 o 0 9 1 38629.31 37547.35 344.92 o 1 9 1 8012.19 7767.11 92.91 o 2 9 1 12344.92 12125.53 142.27 o 3 9 1 1134.44 1164.87 33.51 o 4 9 1 1588.25 1663.68 63.45 o 5 9 1 1289.45 1308.70 47.29 o 6 9 1 10648.87 10577.15 172.35 o 7 9 1 1.42 26.00 35.39 o 8 9 1 5245.33 5251.01 152.41 o 9 9 1 1074.44 1199.34 97.06 o 10 9 1 128.89 93.90 59.78 o -10 10 1 533.50 308.40 115.20 o -9 10 1 11.43 1.76 58.69 o -8 10 1 2780.02 2811.81 132.96 o -7 10 1 3063.21 3060.83 129.92 o -6 10 1 291.13 292.12 40.96 o -5 10 1 6756.57 6475.79 140.68 o -4 10 1 4010.94 3839.06 78.86 o -3 10 1 5208.44 4980.16 89.39 o -2 10 1 5984.50 5832.15 96.35 o -1 10 1 18879.14 18922.28 197.14 o 0 10 1 453.21 485.19 23.66 o 1 10 1 14198.82 13952.46 152.78 o 2 10 1 1559.97 1665.65 40.56 o 3 10 1 6.69 10.62 18.81 o 4 10 1 7083.97 6871.07 113.76 o 5 10 1 938.68 905.36 47.71 o 6 10 1 40.91 51.06 30.83 o 7 10 1 11196.64 11233.80 236.19 o 8 10 1 601.44 687.12 119.54 o 9 10 1 47.67 69.03 56.01 o -9 11 1 2236.09 2246.67 147.36 o -8 11 1 5.91 12.88 75.91 o -7 11 1 4880.57 4923.36 143.23 o -6 11 1 5408.53 5396.00 127.95 o -5 11 1 3044.86 2852.46 88.32 o -4 11 1 2311.24 2136.78 61.17 o -3 11 1 11799.85 11394.21 163.61 o -2 11 1 1036.56 1026.96 39.42 o -1 11 1 2656.88 2674.28 51.51 o 0 11 1 2958.20 2899.60 50.32 o 1 11 1 474.40 534.92 27.59 o 2 11 1 6407.84 6508.69 102.12 o 3 11 1 26039.62 25232.72 334.87 o 4 11 1 1074.94 963.95 49.30 o 5 11 1 2966.20 2991.42 75.25 o 6 11 1 2686.09 2588.99 82.46 o 7 11 1 725.01 814.57 77.50 o 8 11 1 500.03 530.23 81.38 o 9 11 1 1670.86 1588.95 122.39 o -9 12 1 128.76 140.03 75.04 o -8 12 1 3649.81 3679.63 160.62 o -7 12 1 99.15 124.07 50.94 o -6 12 1 455.07 494.99 59.30 o -5 12 1 1561.39 1441.83 71.60 o -4 12 1 6187.18 5790.68 119.08 o -3 12 1 409.18 394.34 35.16 o -2 12 1 26724.54 26766.66 308.29 o -1 12 1 10.24 49.57 19.84 o 0 12 1 367.66 432.23 31.93 o 1 12 1 1711.91 1679.18 42.95 o 2 12 1 8584.74 8447.12 130.88 o 3 12 1 162.85 183.46 32.40 o 4 12 1 11585.60 11593.24 186.78 o 5 12 1 1482.75 1413.06 63.85 o 6 12 1 2376.09 2360.18 99.52 o 7 12 1 16.03 -11.73 58.34 o 8 12 1 3366.23 3466.10 152.94 o 9 12 1 116.86 18.73 66.55 o -9 13 1 5973.73 6143.39 517.11 o -8 13 1 92.55 29.69 66.18 o -7 13 1 1033.40 1212.62 109.41 o -6 13 1 1371.85 1422.84 79.93 o -5 13 1 228.25 249.15 57.48 o -4 13 1 776.00 756.56 54.41 o -3 13 1 15667.00 15369.15 200.32 o -2 13 1 76.48 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