data_2241289 _cell_angle_alpha 77.610 _cell_angle_beta 78.927 _cell_angle_gamma 69.938 _cell_length_a 7.3584 _cell_length_b 10.4470 _cell_length_c 15.7436 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.6971 _cod_data_source_file lh5780Isup2.hkl _cod_data_source_block I _shelx_title ' IN492-DG in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 221.93 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12557.65 13303.97 201.82 o 2 0 0 3.40 -1.92 10.46 o 3 0 0 70.97 42.91 13.06 o 4 0 0 4665.70 4358.86 65.52 o 5 0 0 1240.11 1186.38 49.72 o 6 0 0 328.57 374.50 35.61 o 7 0 0 3.30 -20.51 29.01 o 8 0 0 448.78 494.68 113.04 o 9 0 0 207.93 320.07 51.96 o -9 1 0 26.63 7.36 33.54 o -8 1 0 62.20 66.87 34.61 o -7 1 0 340.01 358.39 41.83 o -6 1 0 34.83 185.19 40.12 o -5 1 0 37.07 66.96 25.33 o -4 1 0 73.09 37.05 13.69 o -3 1 0 646.41 633.52 35.12 o -2 1 0 75.95 44.11 16.59 o -1 1 0 667.12 772.81 19.67 o 0 1 0 4781.66 5577.57 110.75 o 1 1 0 20704.29 20724.20 281.45 o 2 1 0 369.29 322.89 22.66 o 3 1 0 5587.54 5479.82 72.93 o 4 1 0 1468.24 1459.78 45.40 o 5 1 0 3028.78 2750.11 54.03 o 6 1 0 3795.43 3759.43 89.03 o 7 1 0 741.53 789.61 53.39 o 8 1 0 6.17 -33.86 33.86 o 9 1 0 20.96 10.84 40.24 o 10 1 0 68.75 221.50 146.10 o -9 2 0 82.25 65.68 41.75 o -8 2 0 76.93 170.10 79.80 o -7 2 0 1075.03 1302.95 66.11 o -6 2 0 2420.50 2356.03 73.13 o -5 2 0 946.00 993.00 61.79 o -4 2 0 446.16 410.77 23.51 o -3 2 0 155.81 150.34 17.56 o -2 2 0 6.30 7.48 11.17 o -1 2 0 1377.88 1519.76 31.37 o 0 2 0 93.49 103.54 12.61 o 1 2 0 1898.92 1922.35 58.24 o 2 2 0 2503.36 2782.35 42.65 o 3 2 0 204.82 171.37 15.47 o 4 2 0 1557.05 1451.57 35.69 o 5 2 0 35.51 35.32 14.48 o 6 2 0 208.92 251.56 32.58 o 7 2 0 1788.04 1679.67 64.33 o 8 2 0 1892.67 1942.46 77.84 o 9 2 0 149.93 278.64 48.77 o 10 2 0 112.00 4.14 76.45 o -8 3 0 759.76 734.71 57.28 o -7 3 0 8.50 125.16 33.91 o -6 3 0 12.72 -19.11 29.99 o -5 3 0 3335.37 3432.51 83.63 o -4 3 0 3066.33 3005.40 61.61 o -3 3 0 2952.17 2719.18 50.44 o -2 3 0 48.10 29.28 13.75 o -1 3 0 2300.91 2351.42 58.03 o 0 3 0 509.52 497.14 21.50 o 1 3 0 6486.82 7397.51 152.89 o 2 3 0 0.12 14.49 14.57 o 3 3 0 152.10 178.94 17.19 o 4 3 0 827.60 946.21 31.10 o 5 3 0 371.34 414.22 25.07 o 6 3 0 1.37 30.12 24.94 o 7 3 0 370.86 434.49 40.60 o 8 3 0 176.12 209.47 43.58 o 9 3 0 696.03 601.69 58.35 o 10 3 0 710.07 772.95 75.66 o -8 4 0 809.04 877.15 139.35 o -7 4 0 695.91 798.74 57.03 o -6 4 0 429.16 416.44 42.74 o -5 4 0 547.75 646.04 52.48 o -4 4 0 1265.40 1345.89 40.63 o -3 4 0 1743.99 1566.75 40.30 o -2 4 0 1479.60 1432.54 44.75 o -1 4 0 12.64 11.67 19.49 o 0 4 0 167.68 172.30 19.87 o 1 4 0 10543.28 11218.48 192.86 o 2 4 0 5100.09 5156.81 79.66 o 3 4 0 2882.12 2725.94 49.47 o 4 4 0 2274.35 2246.83 46.77 o 5 4 0 375.60 425.84 26.38 o 6 4 0 828.42 892.89 49.76 o 7 4 0 69.91 78.28 31.78 o 8 4 0 1.18 -7.29 55.76 o 9 4 0 0.17 -16.33 45.04 o 10 4 0 58.28 147.66 126.35 o -7 5 0 262.34 309.89 102.95 o -6 5 0 101.60 124.40 59.96 o -5 5 0 309.83 328.08 35.78 o -4 5 0 413.24 424.15 28.82 o -3 5 0 1294.13 1231.16 37.73 o -2 5 0 460.15 383.99 23.70 o -1 5 0 6921.61 7009.68 151.30 o 0 5 0 5667.88 6566.70 100.93 o 1 5 0 156.57 164.85 25.36 o 2 5 0 2433.09 2346.74 45.05 o 3 5 0 9334.45 9258.32 133.78 o 4 5 0 3782.47 3515.86 61.31 o 5 5 0 330.21 332.52 25.36 o 6 5 0 62.42 74.60 21.91 o 7 5 0 635.19 720.18 66.53 o 8 5 0 154.35 154.17 55.70 o 9 5 0 232.26 273.20 88.65 o 10 5 0 3.90 -1.01 50.69 o -7 6 0 108.32 103.47 93.59 o -6 6 0 243.16 271.41 90.99 o -5 6 0 9.78 -3.64 60.31 o -4 6 0 31.98 22.04 17.62 o -3 6 0 1784.06 1610.00 43.34 o -2 6 0 879.46 922.49 32.98 o -1 6 0 891.21 879.04 36.80 o 0 6 0 4176.68 4514.18 126.47 o 1 6 0 1579.57 1631.79 45.60 o 2 6 0 248.45 224.90 23.65 o 3 6 0 244.05 222.27 24.48 o 4 6 0 4223.45 4003.78 69.08 o 5 6 0 721.43 674.70 33.48 o 6 6 0 2512.52 2509.99 59.84 o 7 6 0 0.02 31.91 35.13 o 8 6 0 205.77 194.61 85.53 o 9 6 0 267.79 183.86 56.59 o 10 6 0 319.90 402.44 118.55 o -6 7 0 128.96 215.26 90.47 o -5 7 0 0.93 17.68 72.79 o -4 7 0 238.89 266.73 72.27 o -3 7 0 1030.71 952.83 40.10 o -2 7 0 69.17 88.59 14.87 o -1 7 0 78.52 91.28 20.64 o 0 7 0 2.80 13.74 20.38 o 1 7 0 206.50 195.21 22.89 o 2 7 0 51.94 37.04 18.52 o 3 7 0 247.99 272.46 26.11 o 4 7 0 236.72 251.82 27.66 o 5 7 0 686.10 688.91 36.07 o 6 7 0 708.85 694.89 45.35 o 7 7 0 1062.55 1099.83 59.33 o 8 7 0 6.05 21.74 47.33 o 9 7 0 70.73 15.49 95.93 o 10 7 0 238.39 226.70 93.07 o -6 8 0 700.69 835.03 139.87 o -5 8 0 535.36 367.60 99.83 o -4 8 0 308.59 291.69 78.51 o -3 8 0 408.61 420.70 48.09 o -2 8 0 2214.25 2232.99 82.32 o -1 8 0 118.64 155.39 29.22 o 0 8 0 379.36 424.17 38.21 o 1 8 0 117.88 121.81 25.25 o 2 8 0 3135.57 2907.76 66.58 o 3 8 0 107.57 117.28 24.59 o 4 8 0 289.48 277.94 39.77 o 5 8 0 69.67 46.32 33.73 o 6 8 0 226.14 211.90 36.45 o 7 8 0 237.58 221.86 39.83 o 8 8 0 499.65 466.40 89.69 o 9 8 0 61.12 131.32 59.22 o -5 9 0 51.30 133.11 98.79 o -4 9 0 398.46 382.68 98.79 o -3 9 0 803.07 708.69 98.79 o -2 9 0 9.96 33.61 60.05 o -1 9 0 1704.62 1742.89 75.07 o 0 9 0 266.70 241.34 43.97 o 1 9 0 1118.03 1152.55 50.30 o 2 9 0 106.73 80.22 25.78 o 3 9 0 180.91 212.14 29.38 o 4 9 0 44.66 120.29 35.41 o 5 9 0 368.06 316.73 43.68 o 6 9 0 117.19 132.51 34.59 o 7 9 0 148.32 163.61 40.64 o 8 9 0 22.86 -19.87 45.60 o 9 9 0 9.34 58.94 80.33 o -4 10 0 34.15 75.39 92.55 o -3 10 0 657.97 556.34 102.43 o -2 10 0 599.36 688.93 61.50 o -1 10 0 394.82 436.03 53.07 o 0 10 0 599.62 681.46 58.83 o 1 10 0 1681.97 1598.31 74.91 o 2 10 0 3763.97 3756.00 108.22 o 3 10 0 688.13 750.14 57.52 o 4 10 0 34.45 55.44 35.73 o 5 10 0 954.90 1008.89 68.57 o 6 10 0 616.51 577.73 58.91 o 7 10 0 1061.06 1142.52 70.02 o 8 10 0 377.83 405.14 66.69 o 9 10 0 97.77 106.11 60.84 o -3 11 0 1.42 4.68 87.87 o -2 11 0 9.39 -5.26 41.46 o -1 11 0 171.80 226.26 65.51 o 0 11 0 103.51 86.54 44.34 o 1 11 0 0.07 -5.24 46.34 o 2 11 0 502.89 538.14 92.55 o 3 11 0 1499.78 1418.41 117.51 o 4 11 0 931.98 924.98 103.99 o 5 11 0 689.19 722.85 67.13 o 6 11 0 279.20 352.00 56.76 o 7 11 0 881.04 881.66 66.25 o 8 11 0 616.33 774.14 136.75 o -2 12 0 38.54 72.79 91.51 o -1 12 0 56.05 56.74 46.06 o 0 12 0 113.54 194.98 68.63 o 1 12 0 7.74 31.72 59.27 o 2 12 0 42.49 36.92 80.07 o 3 12 0 16.95 15.08 58.23 o 4 12 0 172.30 188.22 76.95 o 5 12 0 332.23 349.40 92.55 o 6 12 0 110.00 55.11 82.67 o 7 12 0 7.14 17.40 79.81 o 8 12 0 20.24 -6.24 74.35 o -1 13 0 361.52 264.13 78.51 o 0 13 0 25.75 102.43 66.55 o 1 13 0 503.71 433.63 84.23 o 3 13 0 132.26 35.88 83.19 o 4 13 0 39.61 -36.40 82.67 o 5 13 0 21.99 87.35 88.91 o 6 13 0 0.13 -9.36 85.27 o 7 13 0 123.03 78.51 112.83 o 1 14 0 16.94 48.87 54.59 o 2 14 0 58.34 148.70 73.31 o 3 14 0 373.05 404.00 135.71 o 4 14 0 497.56 585.46 129.47 o -3 -14 1 26.46 -11.96 69.15 o -7 -13 1 12.81 -7.28 119.59 o -6 -13 1 1.12 55.63 95.15 o -5 -13 1 5.69 80.07 89.43 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390.68 98.27 o -1 -10 1 286.75 328.71 48.22 o 0 -10 1 816.19 776.98 87.09 o 1 -10 1 487.17 401.37 51.74 o 2 -10 1 0.38 16.30 38.48 o 3 -10 1 117.49 107.11 90.99 o 4 -10 1 244.98 280.77 98.79 o -9 -9 1 50.58 7.61 51.15 o -8 -9 1 607.27 588.09 74.84 o -7 -9 1 951.04 1053.64 64.32 o -6 -9 1 401.34 366.69 50.90 o -5 -9 1 79.90 91.78 31.92 o -4 -9 1 2094.06 2067.06 64.76 o -3 -9 1 2421.69 2429.79 65.92 o -2 -9 1 863.01 902.30 45.92 o -1 -9 1 6.57 33.97 34.23 o 0 -9 1 8.19 25.01 32.54 o 1 -9 1 1345.82 1326.99 72.24 o 2 -9 1 931.66 917.87 64.98 o 3 -9 1 646.41 654.56 57.12 o 4 -9 1 12.73 69.67 78.51 o 5 -9 1 200.13 100.87 98.27 o -9 -8 1 8.50 52.99 56.74 o -8 -8 1 140.29 62.04 69.67 o -7 -8 1 38.88 37.70 42.13 o -6 -8 1 334.56 346.19 39.35 o -5 -8 1 1686.24 1549.60 72.10 o -4 -8 1 23.18 29.42 24.09 o -3 -8 1 30.99 67.66 23.92 o -2 -8 1 252.57 239.91 28.16 o -1 -8 1 1320.59 1313.31 47.75 o 0 -8 1 936.77 993.62 80.07 o 1 -8 1 271.43 228.91 38.52 o 2 -8 1 829.73 935.20 61.28 o 3 -8 1 2020.30 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147.14 108.15 o -10 -5 1 281.47 341.08 109.19 o -9 -5 1 162.45 245.76 61.56 o -8 -5 1 18.52 18.13 40.21 o -7 -5 1 80.39 63.32 34.58 o -6 -5 1 2266.18 2052.86 55.39 o -5 -5 1 2556.56 2485.43 58.76 o -4 -5 1 1517.07 1402.13 41.09 o -3 -5 1 1183.86 1142.56 82.17 o -2 -5 1 1659.15 1523.72 40.53 o -1 -5 1 1150.27 1034.88 38.19 o 0 -5 1 361.60 250.87 21.96 o 1 -5 1 0.45 16.44 17.97 o 2 -5 1 4424.47 4256.27 68.26 o 3 -5 1 934.97 948.80 38.62 o 4 -5 1 126.79 167.28 25.70 o 5 -5 1 2.56 -23.54 33.54 o 7 -5 1 80.59 54.59 96.19 o -10 -4 1 12.25 -42.64 85.27 o -9 -4 1 93.31 48.62 41.86 o -8 -4 1 15.01 -20.04 35.37 o -7 -4 1 92.56 115.66 35.35 o -6 -4 1 138.53 126.14 33.38 o -5 -4 1 1733.88 1608.88 43.77 o -4 -4 1 11051.35 10829.38 136.97 o -3 -4 1 6945.21 6572.81 99.82 o -2 -4 1 2.99 -8.70 14.22 o -1 -4 1 672.87 633.87 46.56 o 0 -4 1 5188.13 4946.41 77.09 o 1 -4 1 4973.47 4814.25 78.42 o 2 -4 1 28.39 44.01 14.58 o 3 -4 1 846.97 861.97 41.65 o 4 -4 1 7.28 -2.16 17.24 o 5 -4 1 7.30 21.06 29.72 o 6 -4 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