#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:41:49 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/12/2241290.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241290 _cell_angle_alpha 64.591 _cell_angle_beta 75.659 _cell_angle_gamma 82.262 _cell_length_a 10.2135 _cell_length_b 13.3707 _cell_length_c 14.0565 _exptl_crystal_F_000 954.00 _reflns_d_resolution_high 0.6706 _cod_data_source_file lh5780IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' GMF12038_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 355.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10004.76 10853.83 96.44 o 2 0 0 621.74 601.53 9.59 o 3 0 0 15923.54 15774.21 139.22 o 4 0 0 12774.74 13331.35 119.43 o 5 0 0 29.53 44.73 12.85 o 6 0 0 504.10 528.54 17.83 o 7 0 0 5857.72 6167.14 73.32 o 8 0 0 1457.28 1451.13 34.82 o 9 0 0 774.60 819.48 37.69 o 10 0 0 2664.79 2749.56 61.30 o 11 0 0 1254.69 1196.83 62.01 o 12 0 0 201.02 150.32 72.58 o 13 0 0 387.20 401.09 83.04 o 14 0 0 265.64 117.45 113.06 o -14 1 0 268.48 267.09 105.94 o -13 1 0 1740.51 1746.12 120.66 o -12 1 0 463.63 578.68 73.18 o -11 1 0 0.39 -42.80 42.80 o -10 1 0 1308.99 1420.92 42.20 o -9 1 0 151.53 159.02 30.14 o -8 1 0 2165.51 2325.85 41.38 o -7 1 0 301.75 338.21 23.51 o -6 1 0 1954.47 1944.48 29.13 o -5 1 0 3582.83 3998.98 44.09 o -4 1 0 2067.77 2315.86 25.97 o -3 1 0 1809.41 1692.40 17.58 o -2 1 0 22.55 68.91 5.38 o -1 1 0 323.70 334.39 5.40 o 0 1 0 318.49 445.69 7.83 o 1 1 0 516.98 669.75 11.72 o 2 1 0 2750.05 2983.72 36.80 o 3 1 0 12764.76 12951.74 122.48 o 4 1 0 0.31 -5.54 12.39 o 5 1 0 54.05 29.13 14.72 o 6 1 0 754.50 767.68 21.82 o 7 1 0 3123.24 3290.83 46.63 o 8 1 0 933.22 1030.96 35.68 o 9 1 0 1005.59 1101.31 40.54 o 10 1 0 25.78 92.85 45.36 o 11 1 0 110.87 164.03 57.85 o 12 1 0 1031.76 1024.71 85.61 o 13 1 0 1674.16 1628.97 131.66 o -14 2 0 1006.00 892.23 106.17 o -13 2 0 36.84 100.75 93.72 o -12 2 0 107.35 124.27 58.66 o -11 2 0 913.56 862.34 56.93 o -10 2 0 442.83 414.85 37.08 o -9 2 0 955.10 933.44 34.88 o -8 2 0 1112.40 1126.35 31.72 o -7 2 0 795.36 831.92 26.02 o -6 2 0 1775.35 1982.56 29.08 o -5 2 0 9200.32 9283.34 90.61 o -4 2 0 647.14 637.22 10.76 o -3 2 0 332.86 259.10 8.47 o -2 2 0 1543.52 1401.51 16.99 o -1 2 0 4867.23 4986.24 49.36 o 0 2 0 33076.29 34379.97 388.51 o 1 2 0 63.09 110.24 11.35 o 2 2 0 331.17 380.38 14.09 o 3 2 0 330.31 412.23 19.07 o 4 2 0 2241.95 2346.70 35.18 o 5 2 0 218.15 276.69 17.04 o 6 2 0 297.89 282.57 20.34 o 7 2 0 1200.93 1220.10 28.62 o 8 2 0 1235.02 1320.78 39.26 o 9 2 0 4476.94 4657.26 72.59 o 10 2 0 3758.77 3998.95 94.08 o 11 2 0 1226.91 1143.00 82.70 o 12 2 0 182.65 86.64 112.58 o 14 2 0 55.57 49.85 46.25 o -13 3 0 192.22 144.32 71.80 o -12 3 0 412.82 387.96 67.59 o -11 3 0 195.40 76.71 48.51 o -10 3 0 1034.40 1057.54 52.07 o -9 3 0 641.42 590.09 34.76 o -8 3 0 998.68 934.25 29.83 o -7 3 0 1897.44 1857.01 32.82 o -6 3 0 10094.26 10188.67 101.66 o -5 3 0 1477.21 1298.86 16.70 o -4 3 0 5516.27 5334.80 50.75 o -3 3 0 16066.48 15869.94 148.56 o -2 3 0 3518.32 3492.23 40.25 o -1 3 0 4579.33 4766.47 54.83 o 0 3 0 4577.08 4814.12 59.31 o 1 3 0 1768.80 1935.56 32.58 o 2 3 0 2695.43 2807.92 42.26 o 3 3 0 198.23 209.00 17.45 o 4 3 0 4018.38 4510.30 65.39 o 5 3 0 1.42 1.61 22.97 o 6 3 0 317.13 305.88 28.45 o 7 3 0 5905.00 6000.88 73.81 o 8 3 0 551.92 494.58 39.95 o 9 3 0 113.48 226.82 46.46 o 10 3 0 36.49 65.68 93.62 o 13 3 0 1219.24 1067.81 120.49 o -13 4 0 41.33 -48.82 93.49 o -12 4 0 45.21 -43.60 57.67 o -11 4 0 161.10 239.98 49.14 o -10 4 0 2.04 46.38 40.17 o -9 4 0 2175.15 2191.86 51.54 o -8 4 0 37.91 1.03 30.35 o -7 4 0 18.45 16.03 21.39 o -6 4 0 3803.15 3730.46 37.81 o -5 4 0 100.41 69.59 12.44 o -4 4 0 307.43 237.08 11.50 o -3 4 0 5.23 31.01 13.13 o -2 4 0 2790.53 2750.72 35.62 o -1 4 0 5466.91 4921.14 58.07 o 0 4 0 208.90 173.51 16.25 o 1 4 0 16.29 22.48 16.44 o 2 4 0 242.42 354.86 20.01 o 3 4 0 5858.09 6249.24 84.73 o 4 4 0 84.86 175.03 21.27 o 5 4 0 601.80 641.86 28.92 o 6 4 0 76.39 59.23 28.62 o 7 4 0 1775.30 1925.03 48.26 o 8 4 0 621.97 580.90 46.76 o 9 4 0 6775.35 6908.90 114.73 o 11 4 0 1050.23 1102.62 96.39 o 12 4 0 182.09 39.78 106.71 o 13 4 0 1181.51 1027.42 121.90 o 14 4 0 760.46 644.42 186.40 o -13 5 0 464.76 454.99 129.98 o -12 5 0 87.81 87.10 79.94 o -11 5 0 30.15 12.36 46.71 o -10 5 0 2805.93 2703.89 58.46 o -9 5 0 0.38 -3.41 33.89 o -8 5 0 274.84 246.29 30.64 o -7 5 0 2497.80 2420.59 44.72 o -6 5 0 4151.91 3728.27 40.24 o -5 5 0 1031.46 850.42 17.74 o -4 5 0 1334.07 1071.75 23.12 o -3 5 0 14139.86 14129.44 137.94 o -2 5 0 27.14 19.80 13.65 o -1 5 0 1723.26 1640.51 27.73 o 0 5 0 11656.67 12094.40 156.68 o 1 5 0 597.01 522.99 22.04 o 2 5 0 1018.28 971.94 28.94 o 3 5 0 1051.37 994.70 29.33 o 4 5 0 4797.24 4957.62 67.56 o 5 5 0 2091.09 2306.79 41.20 o 6 5 0 5071.64 5542.07 85.84 o 7 5 0 4864.81 5180.86 84.77 o 8 5 0 1242.30 1319.21 62.22 o 9 5 0 290.37 436.20 94.20 o 9 5 0 187.02 242.76 94.28 o 10 5 0 658.73 728.01 83.75 o 11 5 0 859.99 945.85 93.80 o 12 5 0 575.25 430.85 94.05 o 13 5 0 226.84 342.72 82.90 o -12 6 0 21.55 57.91 68.61 o -11 6 0 97.67 86.70 63.89 o -10 6 0 703.09 662.49 41.62 o -9 6 0 2444.33 2381.09 51.75 o -8 6 0 789.69 674.33 34.77 o -7 6 0 383.29 349.52 37.13 o -6 6 0 3328.27 3331.17 61.52 o -5 6 0 220.98 225.52 21.37 o -4 6 0 1447.54 1300.48 28.40 o -3 6 0 1376.95 1306.13 28.27 o -2 6 0 145.49 111.94 18.48 o -1 6 0 9978.12 9983.03 121.06 o 0 6 0 1250.25 1159.92 34.85 o 1 6 0 338.07 311.76 23.35 o 2 6 0 1638.91 1731.24 35.73 o 3 6 0 1323.17 1439.23 36.16 o 4 6 0 1677.86 1723.30 41.18 o 5 6 0 1433.15 1390.83 52.34 o 6 6 0 930.18 1034.24 42.48 o 7 6 0 2021.74 2026.26 54.84 o 8 6 0 44.55 -14.19 110.18 o 8 6 0 116.31 205.73 87.79 o 9 6 0 1334.33 1372.54 69.02 o 10 6 0 2500.90 2519.01 109.59 o 11 6 0 749.00 680.44 74.48 o 12 6 0 610.34 544.22 97.48 o 13 6 0 864.91 857.50 92.05 o -12 7 0 154.83 149.85 72.90 o -11 7 0 24.81 -31.61 66.26 o -10 7 0 137.47 120.22 38.32 o -9 7 0 7.98 -46.79 46.79 o -8 7 0 29.97 -26.49 43.21 o -7 7 0 1180.68 1265.21 48.56 o -6 7 0 2218.85 2206.88 58.11 o -5 7 0 335.61 283.35 29.29 o -4 7 0 1161.33 1105.66 29.90 o -3 7 0 9849.71 9947.84 120.55 o -2 7 0 2060.47 2169.68 37.97 o -1 7 0 336.33 302.66 23.48 o 0 7 0 7.10 -1.65 25.93 o 1 7 0 4.03 28.61 25.36 o 2 7 0 1495.63 1579.83 37.92 o 3 7 0 63.15 66.92 30.53 o 4 7 0 5080.87 5156.69 98.93 o 5 7 0 358.45 326.04 46.63 o 6 7 0 6339.97 6435.12 111.46 o 7 7 0 3373.35 3420.74 91.08 o 7 7 0 3129.29 3270.35 139.57 o 8 7 0 62.60 35.27 98.38 o 8 7 0 1201.85 1281.55 64.38 o 9 7 0 712.43 683.33 65.93 o 10 7 0 665.01 729.49 71.43 o 11 7 0 1014.13 945.10 80.70 o 12 7 0 462.81 354.97 72.09 o 13 7 0 75.71 10.88 143.33 o -12 8 0 130.29 21.15 75.10 o -11 8 0 190.87 149.99 60.83 o -10 8 0 763.41 763.63 61.16 o -9 8 0 2246.94 2237.53 68.14 o -8 8 0 380.12 324.48 48.96 o -7 8 0 317.02 333.47 46.32 o -6 8 0 6442.53 6412.86 112.99 o -5 8 0 100.38 7.73 32.47 o -4 8 0 1394.63 1295.31 41.65 o -3 8 0 348.03 327.53 34.36 o -2 8 0 196.90 222.35 33.94 o -1 8 0 3734.85 3734.11 72.41 o 0 8 0 811.01 809.25 31.80 o 1 8 0 4067.59 4313.54 66.22 o 2 8 0 555.75 609.16 38.48 o 3 8 0 475.28 493.70 39.27 o 4 8 0 5562.01 5708.03 109.76 o 5 8 0 2.95 8.32 48.57 o 6 8 0 1019.98 1082.05 78.53 o 6 8 0 638.93 550.46 83.69 o 7 8 0 75.25 67.18 107.80 o 7 8 0 356.44 363.57 89.34 o 8 8 0 300.98 432.01 60.95 o 8 8 0 111.24 -5.19 108.25 o 9 8 0 220.86 273.49 66.56 o 10 8 0 1061.92 1129.07 78.75 o 11 8 0 298.10 246.46 68.39 o 12 8 0 111.81 78.06 74.71 o -11 9 0 195.93 171.78 75.29 o -10 9 0 5.96 24.72 64.75 o -9 9 0 78.88 23.82 56.54 o -8 9 0 129.67 130.65 52.67 o -7 9 0 3565.57 3493.87 85.51 o -6 9 0 579.40 583.29 54.50 o -5 9 0 2745.35 2706.80 59.76 o -4 9 0 3514.04 3508.19 66.84 o -3 9 0 523.70 438.15 39.85 o -2 9 0 295.84 284.58 46.03 o -1 9 0 489.17 473.36 70.77 o 0 9 0 2320.19 2341.05 47.82 o 1 9 0 507.93 504.14 43.30 o 2 9 0 617.68 698.25 43.54 o 3 9 0 2127.71 2153.57 57.92 o 4 9 0 321.56 287.24 66.05 o 5 9 0 777.29 813.94 77.05 o 6 9 0 7824.80 7821.10 185.56 o 6 9 0 4293.34 4017.45 130.19 o 7 9 0 2801.25 2827.71 80.00 o 8 9 0 211.14 139.67 66.24 o 9 9 0 304.97 407.95 79.36 o 10 9 0 1688.21 1778.06 79.30 o 11 9 0 294.09 244.74 72.89 o 12 9 0 295.11 278.47 78.98 o -11 10 0 0.63 77.66 83.86 o -10 10 0 2407.95 2448.68 94.66 o -9 10 0 1146.64 1180.78 69.42 o -8 10 0 38.29 38.51 57.57 o -7 10 0 736.00 668.33 64.23 o -6 10 0 1355.69 1210.96 54.02 o -5 10 0 462.60 401.64 45.86 o -4 10 0 875.95 814.20 48.90 o -3 10 0 6.78 -27.61 52.61 o -2 10 0 545.39 563.16 84.52 o -1 10 0 49.41 42.11 21.76 o 0 10 0 1613.25 1527.84 75.68 o 1 10 0 838.30 757.68 94.70 o 2 10 0 327.86 339.71 88.06 o 3 10 0 488.18 531.45 97.12 o 4 10 0 1806.97 1736.17 126.79 o 5 10 0 288.26 307.10 110.33 o 6 10 0 351.07 315.90 73.90 o 7 10 0 11.89 8.56 52.36 o 8 10 0 355.03 361.98 73.43 o 9 10 0 816.93 880.11 86.60 o 10 10 0 887.62 914.50 76.54 o 11 10 0 25.79 -25.42 76.69 o -10 11 0 86.46 98.51 99.44 o -9 11 0 290.92 294.47 68.96 o -8 11 0 145.11 123.10 64.76 o -7 11 0 2478.96 2561.91 87.71 o -6 11 0 86.96 27.80 47.58 o -5 11 0 84.30 -20.82 54.81 o -4 11 0 2085.94 2176.22 79.83 o -3 11 0 15.97 -1.03 72.21 o -2 11 0 937.09 910.22 46.07 o -1 11 0 40.18 -68.26 92.57 o 0 11 0 812.21 831.86 106.62 o 1 11 0 1537.05 1509.78 119.75 o 2 11 0 69.70 155.21 101.01 o 3 11 0 3401.86 3285.29 161.94 o 4 11 0 545.74 285.03 116.90 o 4 11 0 879.95 826.12 125.45 o 5 11 0 285.21 220.60 74.81 o 6 11 0 1555.07 1568.20 63.21 o 7 11 0 1765.87 1724.96 86.93 o 8 11 0 231.60 214.60 70.76 o 9 11 0 50.83 -28.36 101.08 o 10 11 0 1009.10 1099.19 82.94 o 11 11 0 313.18 250.36 91.79 o -9 12 0 941.30 889.64 87.08 o -8 12 0 12.66 -16.29 68.32 o -7 12 0 1404.88 1356.56 82.42 o -6 12 0 639.04 774.08 120.99 o -5 12 0 250.44 119.05 79.48 o -4 12 0 44.33 -72.15 80.48 o -3 12 0 21.65 2.35 28.01 o -2 12 0 537.26 589.02 38.60 o -1 12 0 305.45 149.01 109.05 o 0 12 0 4015.01 3765.76 179.93 o 1 12 0 887.19 814.16 124.25 o 2 12 0 1142.68 1087.37 130.17 o 3 12 0 424.60 308.35 122.14 o 3 12 0 768.10 759.63 125.47 o 4 12 0 1242.89 1337.72 148.15 o 4 12 0 1448.14 1771.76 145.69 o 5 12 0 1286.29 1304.18 65.94 o 6 12 0 32.42 18.82 60.00 o 7 12 0 352.07 245.02 56.84 o 8 12 0 207.73 182.97 89.22 o 9 12 0 822.85 881.53 113.13 o 10 12 0 328.11 252.65 79.84 o -8 13 0 138.28 71.66 85.07 o -7 13 0 568.37 443.67 130.39 o -6 13 0 140.67 89.21 76.51 o -5 13 0 81.78 1.71 82.84 o -4 13 0 32.50 22.91 30.99 o -3 13 0 471.74 605.46 42.86 o -2 13 0 481.16 303.74 126.99 o -1 13 0 263.62 160.39 126.05 o 0 13 0 107.88 212.93 127.27 o 1 13 0 348.99 380.65 132.02 o 2 13 0 1480.63 1459.04 152.96 o 3 13 0 1034.71 1020.30 39.13 o 4 13 0 1166.01 1362.28 147.70 o 5 13 0 1038.75 920.73 88.39 o 6 13 0 1622.65 1600.88 102.35 o 7 13 0 193.28 114.06 77.10 o 8 13 0 235.31 123.77 77.92 o 9 13 0 588.80 609.89 112.42 o -8 14 0 0.43 -7.86 51.96 o -7 14 0 717.64 634.02 175.94 o -6 14 0 10.62 -152.96 152.96 o -5 14 0 200.59 263.87 38.56 o -4 14 0 40.93 24.22 32.84 o -3 14 0 51.01 51.23 32.49 o -2 14 0 5.77 -41.75 138.18 o -1 14 0 34.34 -50.65 143.31 o 0 14 0 2669.17 2857.18 191.23 o 1 14 0 220.88 316.99 151.56 o 2 14 0 46.61 -13.85 31.70 o 3 14 0 124.45 192.44 36.29 o 4 14 0 1348.07 1413.95 156.49 o 5 14 0 319.65 329.20 80.63 o 6 14 0 201.67 144.23 79.23 o 7 14 0 97.93 -56.61 79.82 o 8 14 0 234.75 157.29 100.78 o 9 14 0 0.34 -42.48 42.48 o -7 15 0 38.81 16.01 52.46 o -6 15 0 6.61 28.01 34.99 o -5 15 0 21.41 67.79 34.43 o -4 15 0 89.92 112.54 35.82 o -3 15 0 683.26 611.92 163.40 o -2 15 0 133.34 8.27 156.56 o -1 15 0 14.93 14.62 30.25 o 0 15 0 373.03 398.26 165.22 o 1 15 0 145.97 136.93 36.87 o 2 15 0 390.65 317.68 81.21 o 3 15 0 277.30 156.16 147.48 o 4 15 0 83.11 49.96 83.47 o 5 15 0 163.91 265.13 159.23 o 6 15 0 873.63 952.54 121.97 o 7 15 0 32.47 -164.68 182.58 o 7 15 0 561.43 317.88 130.80 o 8 15 0 62.63 58.63 136.49 o -5 16 0 185.22 -157.48 166.82 o -4 16 0 10.15 -68.50 163.49 o -3 16 0 927.20 889.15 176.82 o -2 16 0 17.43 -3.17 33.38 o -1 16 0 374.47 190.00 137.37 o 0 16 0 1038.79 1075.60 157.81 o 1 16 0 2.32 -31.05 32.69 o 2 16 0 389.52 274.50 153.29 o 3 16 0 985.36 937.23 168.57 o 4 16 0 827.56 953.43 174.58 o 5 16 0 195.04 215.64 172.37 o 6 16 0 236.22 379.06 193.80 o -4 17 0 37.42 83.07 50.51 o -3 17 0 554.29 579.14 52.13 o -2 17 0 6.93 -9.36 38.16 o -1 17 0 353.72 357.55 157.83 o 0 17 0 579.43 518.24 149.10 o 0 17 0 200.69 191.50 151.50 o 1 17 0 1002.59 786.22 171.15 o 2 17 0 75.37 111.37 80.00 o -4 -16 1 124.91 146.86 162.68 o -3 -16 1 611.18 409.40 167.92 o -2 -16 1 167.60 44.79 149.90 o -1 -16 1 261.78 311.00 149.69 o 0 -16 1 840.11 789.84 70.53 o 1 -16 1 326.99 418.94 61.03 o 2 -16 1 138.66 138.78 55.80 o 3 -16 1 18.89 -46.72 50.57 o 4 -16 1 698.62 823.09 54.86 o 5 -16 1 13.67 37.62 35.82 o -7 -15 1 775.05 783.39 202.44 o -6 -15 1 514.07 615.02 192.92 o -5 -15 1 272.31 255.48 176.16 o -4 -15 1 148.55 1.36 153.90 o -3 -15 1 307.87 461.02 154.32 o -2 -15 1 766.68 821.59 157.71 o -1 -15 1 1.43 30.62 49.37 o 0 -15 1 66.92 55.75 32.38 o 1 -15 1 122.39 167.94 34.01 o 2 -15 1 73.94 67.50 32.30 o 3 -15 1 1110.20 993.09 165.23 o 4 -15 1 19.62 61.11 152.90 o 5 -15 1 8.21 -152.90 152.90 o 5 -15 1 9.15 94.68 116.82 o 6 -15 1 99.59 133.33 51.86 o 7 -15 1 56.04 78.33 53.42 o -8 -14 1 234.75 313.12 191.88 o -7 -14 1 68.30 -66.98 175.82 o -6 -14 1 21.18 16.71 165.54 o -6 -14 1 9.13 26.38 167.09 o -5 -14 1 40.35 -19.45 156.43 o -5 -14 1 45.98 29.11 151.41 o -4 -14 1 86.46 67.78 43.05 o -3 -14 1 97.62 116.14 35.96 o -2 -14 1 45.22 35.57 33.35 o -1 -14 1 221.41 221.27 33.20 o 0 -14 1 1152.75 1212.23 53.31 o 1 -14 1 738.55 775.03 153.85 o 2 -14 1 218.41 35.40 143.07 o 3 -14 1 359.83 445.77 146.25 o 4 -14 1 825.09 660.00 149.65 o 5 -14 1 24.25 45.49 32.31 o 6 -14 1 18.92 10.68 32.00 o 7 -14 1 8.45 -43.88 43.88 o 8 -14 1 16.63 -1.97 51.06 o -9 -13 1 170.13 134.34 143.21 o -8 -13 1 200.20 120.08 85.31 o -7 -13 1 247.02 239.66 40.40 o -6 -13 1 47.39 11.42 33.78 o -5 -13 1 1007.56 1083.81 143.16 o -4 -13 1 597.36 737.96 142.56 o -3 -13 1 269.82 335.57 151.06 o -2 -13 1 289.22 312.79 140.84 o -1 -13 1 78.92 169.68 134.80 o 0 -13 1 3.38 6.19 131.82 o 1 -13 1 1234.03 1231.40 144.63 o 2 -13 1 15.64 9.68 122.45 o 3 -13 1 892.20 744.91 133.63 o 4 -13 1 55.65 54.35 31.26 o 5 -13 1 6.67 19.18 98.80 o 6 -13 1 106.07 45.96 143.84 o 7 -13 1 218.83 140.94 157.64 o 8 -13 1 313.33 348.21 47.56 o 9 -13 1 37.41 42.78 79.73 o -10 -12 1 159.79 109.44 47.70 o -9 -12 1 411.82 318.60 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