data_2241321 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.9247 _cell_length_b 11.5487 _cell_length_c 28.1106 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.7574 _cod_data_source_file tk5406Isup2.hkl _cod_data_source_block I _shelx_title ' 4jey in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 216.63 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' '-x, y, z+1/2' 'x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -14 0 141.87 108.96 63.92 o 2 -14 0 54.61 45.40 55.49 o 0 -12 0 150.65 110.06 38.68 o 1 -12 0 6.10 46.29 39.45 o 2 -12 0 185.62 226.45 46.23 o 3 -12 0 38.23 2.44 43.33 o 0 -10 0 4033.98 4013.30 143.47 o 1 -10 0 58.58 63.50 20.84 o 2 -10 0 46.79 50.13 24.51 o 3 -10 0 201.10 200.83 73.24 o 0 -8 0 2001.31 1981.74 81.18 o 1 -8 0 505.98 576.78 61.31 o 2 -8 0 226.43 281.29 35.74 o 3 -8 0 486.72 475.42 37.56 o 4 -8 0 58.87 39.05 44.73 o 0 -6 0 9517.59 11086.44 293.17 o 1 -6 0 4340.52 4641.43 96.44 o 2 -6 0 2301.03 2221.19 58.25 o 3 -6 0 143.58 139.69 23.52 o 4 -6 0 115.63 65.82 45.46 o 0 -4 0 5983.51 6777.90 248.10 o 1 -4 0 8473.64 9096.59 187.95 o 2 -4 0 4159.78 4033.85 79.15 o 3 -4 0 242.34 199.31 26.45 o 4 -4 0 86.80 62.69 30.31 o 0 -2 0 46103.84 59174.13 1954.89 o 1 -2 0 1500.66 1521.98 32.96 o 2 -2 0 4156.71 4155.30 72.16 o 3 -2 0 1731.61 1501.95 44.43 o 4 -2 0 75.23 47.26 25.08 o 5 -2 0 124.79 73.51 59.40 o 1 0 0 771.89 759.63 27.76 o 2 0 0 1435.54 1708.71 44.94 o 3 0 0 2666.35 2704.49 85.10 o 4 0 0 8.44 64.75 54.42 o 5 0 0 99.39 80.53 46.78 o 0 2 0 46927.23 54577.97 1519.42 o 1 2 0 1776.47 1671.33 44.54 o 2 2 0 3807.23 3809.51 161.45 o 3 2 0 1912.81 1807.60 81.13 o 4 2 0 92.24 188.91 39.19 o 5 2 0 121.01 132.50 45.73 o 0 4 0 6088.03 6504.92 282.72 o 1 4 0 8308.32 8785.33 259.26 o 2 4 0 4222.00 4139.81 110.53 o 3 4 0 305.27 366.35 45.14 o 4 4 0 82.97 142.60 112.78 o 0 6 0 10448.09 11059.55 313.81 o 1 6 0 4506.32 4689.76 122.55 o 2 6 0 2372.56 2301.35 75.73 o 3 6 0 114.88 149.97 39.88 o 4 6 0 97.40 141.12 52.65 o 0 8 0 1839.82 2116.49 128.39 o 1 8 0 549.61 500.47 34.02 o 2 8 0 283.48 386.01 35.33 o 3 8 0 439.54 507.44 56.52 o 4 8 0 49.73 77.06 73.64 o 0 10 0 3968.76 3838.53 208.81 o 1 10 0 46.00 47.32 36.91 o 2 10 0 25.66 16.90 28.22 o 3 10 0 188.44 124.36 77.73 o 0 12 0 180.45 219.62 71.50 o 1 12 0 4.42 39.05 42.57 o 2 12 0 175.62 180.64 66.00 o 3 12 0 47.90 38.62 56.28 o 0 14 0 26.52 6.54 67.89 o 1 14 0 137.48 145.72 51.03 o 1 -14 1 9.41 17.86 39.14 o 2 -14 1 8.07 36.97 59.64 o 1 -13 1 19.33 92.90 34.95 o 2 -13 1 3.55 36.65 27.77 o 1 -12 1 112.17 140.06 28.14 o 2 -12 1 64.57 30.03 25.22 o 3 -12 1 1.90 70.95 58.54 o 1 -11 1 8.59 44.49 21.42 o 2 -11 1 5.63 -15.45 21.92 o 3 -11 1 1.04 15.24 22.03 o 1 -10 1 150.34 191.14 18.22 o 2 -10 1 43.96 78.35 19.57 o 3 -10 1 29.10 30.28 25.32 o 1 -9 1 341.57 376.29 18.74 o 2 -9 1 55.63 80.23 19.83 o 3 -9 1 77.96 80.03 19.59 o 4 -9 1 34.69 57.59 27.17 o 1 -8 1 978.43 953.50 24.98 o 2 -8 1 401.24 431.66 22.90 o 3 -8 1 28.97 35.90 15.97 o 4 -8 1 80.42 64.18 21.69 o 1 -7 1 1030.92 1000.97 22.19 o 2 -7 1 185.57 157.45 16.84 o 3 -7 1 91.21 88.87 17.21 o 4 -7 1 69.18 74.06 33.33 o 1 -6 1 1934.01 2030.08 36.32 o 2 -6 1 488.20 485.23 19.26 o 3 -6 1 150.22 144.04 16.82 o 4 -6 1 198.87 217.18 25.89 o 1 -5 1 878.49 955.43 21.89 o 2 -5 1 352.35 369.88 16.07 o 3 -5 1 92.49 55.43 11.09 o 4 -5 1 22.34 14.23 18.41 o 1 -4 1 4188.42 4463.23 62.17 o 2 -4 1 675.02 616.92 17.09 o 3 -4 1 437.16 411.86 20.53 o 4 -4 1 273.60 261.90 27.43 o 1 -3 1 1667.13 1776.52 27.85 o 2 -3 1 512.46 503.03 14.92 o 3 -3 1 319.50 286.32 20.17 o 4 -3 1 125.97 86.46 22.01 o 5 -3 1 2.46 22.79 35.87 o 1 -2 1 7343.68 8522.00 100.54 o 2 -2 1 2034.02 2026.39 32.45 o 3 -2 1 129.70 160.12 15.16 o 4 -2 1 322.57 305.20 27.96 o 5 -2 1 0.68 4.00 47.70 o 1 -1 1 2870.96 3126.70 40.73 o 2 -1 1 493.01 508.49 14.53 o 3 -1 1 163.13 156.13 14.19 o 4 -1 1 184.28 193.85 26.08 o 5 -1 1 0.19 67.42 31.58 o 1 0 1 101.86 98.43 7.09 o 2 0 1 439.59 368.43 13.04 o 3 0 1 544.29 519.32 25.16 o 4 0 1 727.41 719.31 44.99 o 5 0 1 3.62 -3.15 33.72 o 1 1 1 2499.26 2734.86 56.00 o 2 1 1 474.85 466.36 17.96 o 3 1 1 126.20 95.28 19.99 o 4 1 1 178.70 58.43 49.74 o 5 1 1 0.09 36.24 28.49 o 1 2 1 7738.62 8476.54 149.84 o 2 2 1 1836.15 1906.14 51.55 o 3 2 1 149.36 195.72 26.67 o 4 2 1 324.19 404.85 40.99 o 5 2 1 1.25 10.98 28.33 o 1 3 1 1569.02 1728.42 33.47 o 2 3 1 471.18 513.67 22.54 o 3 3 1 306.56 275.89 29.60 o 4 3 1 130.94 155.28 30.78 o 5 3 1 2.28 57.69 56.89 o 1 4 1 4075.19 4416.18 73.20 o 2 4 1 764.67 740.33 25.24 o 3 4 1 401.02 406.39 32.56 o 4 4 1 258.85 275.83 35.61 o 1 5 1 901.47 981.28 39.09 o 2 5 1 395.28 460.64 29.00 o 3 5 1 97.65 115.98 26.95 o 4 5 1 25.94 -24.62 29.60 o 1 6 1 1653.15 1762.72 44.45 o 2 6 1 443.81 447.16 23.73 o 3 6 1 179.89 239.17 31.11 o 4 6 1 191.33 225.36 39.96 o 1 7 1 942.77 897.99 31.21 o 2 7 1 222.37 227.98 20.66 o 3 7 1 104.30 124.70 31.35 o 4 7 1 68.99 100.19 44.11 o 1 8 1 986.91 914.79 32.17 o 2 8 1 435.40 496.60 31.45 o 3 8 1 20.72 106.00 32.05 o 4 8 1 71.77 111.87 43.87 o 1 9 1 333.60 349.47 22.02 o 2 9 1 66.91 89.27 21.48 o 3 9 1 89.18 85.30 31.40 o 4 9 1 36.13 -22.70 48.65 o 1 10 1 145.02 194.15 29.37 o 2 10 1 59.42 99.74 23.11 o 3 10 1 28.29 57.71 30.72 o 1 11 1 3.26 23.97 26.54 o 2 11 1 9.21 30.03 29.69 o 3 11 1 1.82 47.84 32.06 o 1 12 1 116.78 121.03 31.02 o 2 12 1 63.70 58.28 33.97 o 3 12 1 2.63 54.77 40.05 o 1 13 1 14.56 -7.20 29.89 o 2 13 1 2.70 20.75 42.27 o 1 14 1 10.64 20.68 31.02 o 0 -14 2 75.64 -18.21 45.77 o 1 -14 2 13.34 30.10 43.29 o 2 -14 2 1.51 -59.03 59.03 o 0 -13 2 70.85 141.92 40.04 o 1 -13 2 93.95 62.94 33.85 o 2 -13 2 72.32 43.89 32.67 o 0 -12 2 43.50 25.85 26.80 o 1 -12 2 51.49 48.50 24.27 o 2 -12 2 6.97 16.18 24.68 o 3 -12 2 9.27 47.37 49.16 o 0 -11 2 339.38 378.52 33.17 o 1 -11 2 56.58 82.66 20.23 o 2 -11 2 15.59 50.89 20.45 o 3 -11 2 68.57 71.09 24.49 o 0 -10 2 9.18 82.14 36.26 o 1 -10 2 347.72 361.28 21.53 o 2 -10 2 101.55 109.44 23.47 o 3 -10 2 11.50 37.34 27.08 o 0 -9 2 1924.07 1851.53 59.82 o 1 -9 2 422.40 450.15 29.80 o 2 -9 2 7.41 12.16 13.77 o 3 -9 2 134.38 164.17 36.35 o 4 -9 2 42.31 55.32 36.13 o 0 -8 2 194.32 198.56 21.03 o 1 -8 2 95.26 152.01 17.01 o 2 -8 2 672.88 617.02 26.35 o 3 -8 2 97.79 100.26 18.63 o 4 -8 2 22.97 18.09 17.96 o 0 -7 2 4042.85 3856.98 82.79 o 1 -7 2 362.22 375.19 17.43 o 2 -7 2 380.58 389.56 18.77 o 3 -7 2 168.26 154.27 18.23 o 4 -7 2 46.99 84.88 25.44 o 0 -6 2 3118.81 3218.12 71.71 o 1 -6 2 28.72 94.34 16.17 o 2 -6 2 323.05 331.28 17.43 o 3 -6 2 206.21 218.37 20.86 o 4 -6 2 69.55 103.92 22.18 o 1 -5 2 460.74 540.39 18.22 o 2 -5 2 3505.75 3480.98 61.38 o 3 -5 2 90.51 103.21 15.96 o 4 -5 2 9.78 65.04 21.30 o 0 -4 2 6851.25 7080.72 130.22 o 1 -4 2 137.30 194.04 12.56 o 2 -4 2 489.22 535.35 15.84 o 3 -4 2 739.86 681.57 28.08 o 4 -4 2 137.98 102.83 22.95 o 0 -3 2 11264.17 12035.09 638.17 o 1 -3 2 1488.68 1410.41 23.98 o 2 -3 2 3152.63 3186.29 72.11 o 3 -3 2 295.69 272.86 16.56 o 4 -3 2 1.68 3.64 12.04 o 5 -3 2 153.44 25.60 18.76 o 0 -2 2 2832.36 2760.93 137.23 o 1 -2 2 869.47 894.55 17.47 o 2 -2 2 2958.11 2877.10 44.06 o 3 -2 2 620.37 634.50 22.88 o 4 -2 2 76.43 75.06 19.42 o 5 -2 2 19.88 77.01 48.49 o 0 -1 2 5479.22 5912.83 105.48 o 1 -1 2 10330.54 11624.91 140.70 o 2 -1 2 625.67 623.69 15.75 o 3 -1 2 1290.53 1289.49 32.03 o 4 -1 2 73.04 98.74 23.28 o 5 -1 2 107.79 86.31 32.97 o 1 0 2 4441.02 5049.48 78.95 o 2 0 2 2073.39 2243.66 49.77 o 3 0 2 38.76 30.34 14.11 o 4 0 2 0.12 35.80 21.08 o 5 0 2 14.01 52.71 29.65 o 0 1 2 5189.93 5703.37 160.30 o 1 1 2 9902.96 11414.35 307.22 o 2 1 2 771.56 726.32 24.14 o 3 1 2 1351.56 1344.94 47.70 o 4 1 2 77.69 52.63 24.09 o 5 1 2 100.91 70.09 28.06 o 0 2 2 2183.10 2499.99 352.44 o 1 2 2 961.64 969.71 23.48 o 2 2 2 2868.62 2844.09 62.13 o 3 2 2 591.78 601.94 36.49 o 4 2 2 71.78 102.31 32.59 o 5 2 2 21.18 58.49 27.71 o 0 3 2 11633.14 12947.35 361.45 o 1 3 2 1411.71 1409.34 28.82 o 2 3 2 3052.05 3254.08 89.85 o 3 3 2 393.60 419.85 38.43 o 4 3 2 3.64 30.23 24.93 o 5 3 2 142.35 237.35 74.12 o 0 4 2 6709.11 6821.18 191.93 o 1 4 2 101.03 196.30 24.39 o 2 4 2 600.01 661.62 23.40 o 3 4 2 752.89 712.12 40.90 o 4 4 2 139.07 149.08 33.40 o 0 5 2 922.18 892.74 44.31 o 1 5 2 412.27 571.37 27.92 o 2 5 2 3505.57 3551.90 65.96 o 3 5 2 86.82 156.47 27.16 o 4 5 2 6.00 -2.74 30.16 o 0 6 2 3184.81 3162.85 74.47 o 1 6 2 45.24 159.70 15.88 o 2 6 2 262.34 277.08 20.48 o 3 6 2 226.40 250.15 33.30 o 4 6 2 74.03 110.12 33.84 o 0 7 2 3656.16 3425.62 84.19 o 1 7 2 342.95 343.80 20.40 o 2 7 2 474.66 493.24 24.78 o 3 7 2 129.97 162.51 30.69 o 4 7 2 46.25 130.76 42.78 o 0 8 2 162.40 169.31 22.74 o 1 8 2 85.80 134.06 18.05 o 2 8 2 681.01 716.04 31.82 o 3 8 2 120.36 120.69 30.30 o 4 8 2 26.42 57.63 41.35 o 0 9 2 1974.43 1858.95 88.46 o 1 9 2 469.51 478.02 29.99 o 2 9 2 1.30 25.35 20.34 o 3 9 2 127.85 169.63 32.75 o 4 9 2 44.36 74.85 45.17 o 0 10 2 13.30 172.12 90.47 o 1 10 2 349.97 318.83 32.94 o 2 10 2 117.53 114.96 25.24 o 3 10 2 17.26 63.25 30.40 o 0 11 2 345.75 346.82 52.93 o 1 11 2 48.78 60.72 27.35 o 2 11 2 10.22 8.82 30.14 o 3 11 2 74.78 105.48 30.83 o 0 12 2 30.99 52.33 41.53 o 1 12 2 56.54 74.79 28.80 o 2 12 2 5.32 25.62 34.10 o 3 12 2 6.27 46.64 39.86 o 0 13 2 87.62 125.20 50.51 o 1 13 2 93.30 84.69 31.36 o 2 13 2 67.35 73.59 41.94 o 0 14 2 72.63 78.78 52.97 o 1 14 2 13.24 7.46 27.93 o 1 -14 3 1.37 68.46 34.79 o 1 -13 3 24.93 24.10 31.05 o 2 -13 3 4.18 26.83 33.34 o 1 -12 3 0.86 4.53 26.05 o 2 -12 3 6.46 32.59 25.69 o 3 -12 3 3.62 19.66 46.63 o 1 -11 3 489.94 471.86 28.51 o 2 -11 3 53.90 81.96 23.18 o 3 -11 3 34.92 4.62 22.23 o 1 -10 3 14.71 41.81 17.49 o 2 -10 3 50.65 58.42 19.10 o 3 -10 3 10.51 4.23 17.74 o 1 -9 3 892.14 934.18 29.52 o 2 -9 3 315.14 317.96 25.11 o 3 -9 3 12.12 2.69 19.20 o 4 -9 3 31.60 31.38 31.53 o 1 -8 3 22.97 28.45 11.21 o 2 -8 3 191.99 179.43 17.48 o 3 -8 3 32.96 38.41 16.29 o 4 -8 3 3.71 22.53 21.44 o 1 -7 3 1615.99 1732.07 39.19 o 2 -7 3 201.66 162.98 14.58 o 3 -7 3 172.97 167.96 18.57 o 4 -7 3 89.02 94.40 23.74 o 1 -6 3 11.99 31.74 9.69 o 2 -6 3 67.74 80.61 12.26 o 3 -6 3 3.49 10.39 13.55 o 4 -6 3 18.20 24.19 34.79 o 1 -5 3 9142.58 9820.02 120.85 o 2 -5 3 2050.29 2021.64 44.12 o 3 -5 3 43.90 66.15 17.01 o 4 -5 3 110.28 110.58 22.23 o 1 -4 3 20.03 46.97 6.13 o 2 -4 3 56.78 81.88 7.73 o 3 -4 3 8.81 47.00 14.16 o 4 -4 3 24.16 41.22 17.02 o 1 -3 3 5086.60 5249.29 110.90 o 2 -3 3 945.97 988.86 44.57 o 3 -3 3 332.65 329.65 16.44 o 4 -3 3 465.55 418.31 30.20 o 5 -3 3 16.27 63.61 40.33 o 1 -2 3 214.20 204.89 8.56 o 2 -2 3 155.52 171.99 10.06 o 3 -2 3 5.54 17.00 11.75 o 4 -2 3 17.07 22.89 17.62 o 5 -2 3 3.08 46.39 59.79 o 1 -1 3 44764.45 52290.89 617.69 o 2 -1 3 4216.88 3894.69 59.17 o 3 -1 3 283.18 301.52 19.12 o 4 -1 3 567.16 498.16 33.24 o 5 -1 3 21.37 66.64 34.44 o 1 0 3 1092.45 1116.49 21.63 o 2 0 3 306.13 248.20 14.06 o 3 0 3 97.81 103.77 15.93 o 4 0 3 1.13 -19.52 21.78 o 5 0 3 8.64 0.18 26.75 o 1 1 3 44984.38 52445.76 784.42 o 2 1 3 4625.45 4241.21 80.37 o 3 1 3 260.71 280.26 22.11 o 4 1 3 570.65 527.74 39.22 o 5 1 3 20.29 23.08 23.20 o 1 2 3 191.24 193.29 13.30 o 2 2 3 145.18 165.92 20.32 o 3 2 3 6.83 11.82 21.47 o 4 2 3 14.93 17.49 30.91 o 5 2 3 2.84 14.16 24.29 o 1 3 3 4978.35 5319.21 90.27 o 2 3 3 951.83 1108.85 61.57 o 3 3 3 401.90 505.18 40.58 o 4 3 3 484.13 498.93 45.38 o 5 3 3 15.08 34.53 52.00 o 1 4 3 23.21 32.03 10.07 o 2 4 3 60.00 122.09 14.29 o 3 4 3 8.30 67.33 26.16 o 4 4 3 22.85 79.47 30.70 o 1 5 3 9501.51 9770.55 150.11 o 2 5 3 2050.93 2044.49 44.65 o 3 5 3 39.88 111.74 41.24 o 4 5 3 123.49 121.97 33.22 o 1 6 3 13.16 55.84 14.21 o 2 6 3 65.31 84.92 16.84 o 3 6 3 2.79 73.69 26.05 o 4 6 3 18.84 29.81 37.57 o 1 7 3 1827.13 1879.48 44.53 o 2 7 3 250.90 257.10 20.77 o 3 7 3 148.17 181.07 31.25 o 4 7 3 99.90 160.38 45.45 o 1 8 3 27.01 46.29 16.76 o 2 8 3 187.05 221.04 22.64 o 3 8 3 32.30 50.57 30.67 o 4 8 3 4.17 65.21 51.68 o 1 9 3 814.19 826.37 38.01 o 2 9 3 258.79 297.04 28.87 o 3 9 3 7.35 15.92 29.48 o 4 9 3 30.96 31.65 42.98 o 1 10 3 15.37 55.80 24.47 o 2 10 3 48.66 63.91 24.91 o 3 10 3 10.22 46.36 29.26 o 1 11 3 490.17 485.59 45.20 o 2 11 3 58.37 76.65 35.11 o 3 11 3 29.56 63.68 33.72 o 1 12 3 0.65 27.66 20.93 o 2 12 3 6.07 62.05 34.96 o 3 12 3 3.81 51.05 41.69 o 1 13 3 21.27 31.55 21.38 o 2 13 3 5.08 37.11 34.77 o 1 14 3 1.57 9.12 22.07 o 0 -14 4 4.00 -19.72 35.99 o 1 -14 4 16.55 24.79 32.42 o 0 -13 4 355.50 272.68 46.69 o 1 -13 4 30.53 7.78 27.45 o 2 -13 4 16.52 -2.61 32.37 o 0 -12 4 34.55 25.18 26.88 o 1 -12 4 6.71 32.37 28.14 o 2 -12 4 10.02 4.24 15.48 o 3 -12 4 4.52 22.74 40.70 o 0 -11 4 271.82 243.33 33.35 o 1 -11 4 109.42 124.00 21.33 o 2 -11 4 258.66 220.24 27.70 o 3 -11 4 72.51 48.99 24.69 o 0 -10 4 128.67 142.28 24.67 o 1 -10 4 23.04 47.11 18.08 o 2 -10 4 10.04 31.96 18.08 o 3 -10 4 41.56 15.98 18.75 o 0 -9 4 162.90 159.69 22.86 o 1 -9 4 775.50 836.01 30.04 o 2 -9 4 1001.53 963.69 39.19 o 3 -9 4 62.84 34.13 18.02 o 4 -9 4 9.58 74.48 18.10 o 0 -8 4 1204.55 1074.56 60.71 o 1 -8 4 107.39 138.33 12.81 o 2 -8 4 114.79 144.15 17.07 o 3 -8 4 219.02 227.26 27.62 o 4 -8 4 4.40 30.68 19.79 o 0 -7 4 3098.37 3131.13 177.80 o 1 -7 4 1248.18 1183.36 26.02 o 2 -7 4 380.48 379.45 19.18 o 3 -7 4 528.25 429.90 33.92 o 4 -7 4 15.98 -5.15 23.83 o 0 -6 4 625.21 651.08 36.50 o 1 -6 4 643.31 654.77 18.39 o 2 -6 4 286.76 284.01 16.10 o 3 -6 4 62.18 51.13 16.32 o 4 -6 4 8.42 24.94 21.21 o 0 -5 4 5428.50 4932.76 213.38 o 1 -5 4 1192.93 1236.96 29.15 o 2 -5 4 559.38 528.30 21.13 o 3 -5 4 1743.61 1750.21 52.72 o 4 -5 4 47.05 23.75 18.60 o 0 -4 4 1208.60 1222.49 99.02 o 1 -4 4 631.80 638.51 15.97 o 2 -4 4 483.25 485.43 17.69 o 3 -4 4 45.13 55.87 11.18 o 4 -4 4 24.66 43.61 17.48 o 0 -3 4 26796.04 30250.91 511.43 o 1 -3 4 3465.86 3579.84 57.07 o 2 -3 4 288.60 280.11 11.06 o 3 -3 4 1385.25 1340.66 31.34 o 4 -3 4 106.25 104.41 20.51 o 0 -2 4 3689.98 4116.06 69.03 o 1 -2 4 829.48 899.23 18.51 o 2 -2 4 937.41 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