#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:44:30 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181914 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/13/2241326.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241326 _cell_angle_alpha 90.000 _cell_angle_beta 112.577 _cell_angle_gamma 90.000 _cell_length_a 14.7890 _cell_length_b 17.5387 _cell_length_c 19.0163 _exptl_crystal_F_000 2048.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file zs2352Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 569.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12.42 3.52 7.04 o 2 0 0 14705.90 19780.93 348.65 o 3 0 0 37559.66 37552.02 656.58 o 4 0 0 30233.41 33920.38 596.24 o 5 0 0 17450.39 16258.00 295.31 o 6 0 0 5435.89 5756.86 120.10 o 7 0 0 3870.70 4224.37 97.17 o 8 0 0 15801.99 15145.61 365.76 o 9 0 0 622.19 405.39 41.64 o 10 0 0 3932.57 3719.57 144.26 o 11 0 0 3623.67 3751.47 154.03 o 12 0 0 556.39 458.68 88.10 o 13 0 0 1820.13 1791.63 267.44 o 14 0 0 1885.27 2130.41 163.63 o 15 0 0 681.64 904.81 123.75 o 16 0 0 2204.99 2408.12 169.15 o 2 1 0 7729.43 8367.21 107.39 o 3 1 0 181.55 509.66 28.95 o 4 1 0 2705.51 2689.78 47.55 o 5 1 0 35.40 103.36 19.67 o 6 1 0 9606.85 8922.07 148.14 o 7 1 0 921.65 758.84 26.53 o 8 1 0 660.92 834.29 31.74 o 9 1 0 575.43 468.13 35.41 o 10 1 0 338.76 248.88 58.67 o 11 1 0 692.24 834.34 62.67 o 12 1 0 47.96 -20.10 54.84 o 13 1 0 560.90 541.98 70.11 o 14 1 0 332.57 554.59 108.80 o 15 1 0 89.98 152.11 76.23 o 16 1 0 1.04 57.78 141.71 o 0 2 0 460.32 660.15 28.70 o 1 2 0 1152.64 1115.65 20.97 o 2 2 0 27989.91 30684.19 598.78 o 3 2 0 24793.64 25501.55 318.26 o 4 2 0 117101.33 127874.19 1575.37 o 5 2 0 29675.88 27514.01 346.83 o 6 2 0 13470.23 13166.69 174.66 o 7 2 0 4588.92 4223.99 70.42 o 8 2 0 3272.26 3182.73 60.15 o 9 2 0 33.96 79.21 23.34 o 10 2 0 134.70 153.72 33.03 o 11 2 0 6589.40 6928.78 152.54 o 12 2 0 198.78 173.99 57.80 o 13 2 0 2616.81 2801.81 104.39 o 14 2 0 566.31 565.36 92.95 o 15 2 0 116.26 -26.90 81.27 o 16 2 0 403.35 512.76 87.73 o 1 3 0 5845.66 5196.30 76.73 o 2 3 0 14543.16 14526.11 224.23 o 3 3 0 19679.60 25127.38 382.48 o 4 3 0 1207.31 1385.16 34.63 o 5 3 0 1032.21 1404.80 37.25 o 6 3 0 4207.73 4376.11 70.85 o 7 3 0 24379.06 25404.68 326.28 o 8 3 0 1037.73 925.31 36.46 o 9 3 0 6703.40 6744.52 105.13 o 10 3 0 2828.46 2839.49 80.97 o 11 3 0 1573.35 1843.51 115.21 o 12 3 0 6.49 14.40 55.32 o 13 3 0 550.31 574.22 70.14 o 14 3 0 999.27 1283.02 89.08 o 15 3 0 0.90 -73.26 73.26 o 16 3 0 326.29 319.52 86.75 o 0 4 0 6365.64 5975.71 114.37 o 1 4 0 371.46 485.34 23.61 o 2 4 0 20718.10 18912.69 291.93 o 3 4 0 5621.84 5792.27 89.51 o 4 4 0 18562.31 18841.35 263.83 o 5 4 0 3969.39 3622.93 66.31 o 6 4 0 576.70 565.89 27.21 o 7 4 0 1922.52 1857.76 44.39 o 8 4 0 27514.73 27741.01 358.04 o 9 4 0 590.98 666.01 48.26 o 10 4 0 61.86 135.02 36.76 o 11 4 0 33.70 66.35 48.86 o 12 4 0 679.41 688.86 191.24 o 13 4 0 34.03 159.66 66.25 o 14 4 0 151.23 179.00 73.47 o 15 4 0 114.75 177.78 79.23 o 16 4 0 216.96 294.81 86.25 o 1 5 0 9116.29 9864.94 141.85 o 2 5 0 5219.62 5073.26 79.98 o 3 5 0 7988.48 8890.83 216.60 o 4 5 0 3171.80 3421.84 63.05 o 5 5 0 139.34 156.78 22.61 o 6 5 0 87.37 66.47 35.58 o 7 5 0 7217.69 7729.13 125.52 o 8 5 0 3077.93 2782.16 63.04 o 9 5 0 1791.16 2126.31 60.61 o 10 5 0 789.88 1109.84 70.21 o 11 5 0 1957.68 1907.39 76.44 o 12 5 0 46.16 78.81 70.90 o 13 5 0 1.05 -75.57 75.57 o 14 5 0 1679.98 1474.54 193.28 o 15 5 0 19.59 137.08 93.41 o 16 5 0 2.06 173.83 105.53 o 0 6 0 162.61 179.93 26.65 o 1 6 0 3286.92 3331.82 57.67 o 2 6 0 3854.42 4455.01 156.60 o 3 6 0 317.25 376.85 24.51 o 4 6 0 997.13 1389.33 57.29 o 5 6 0 1055.17 909.20 33.25 o 6 6 0 43.24 24.61 23.36 o 7 6 0 445.04 367.63 30.80 o 8 6 0 1260.73 1221.60 44.08 o 9 6 0 304.47 172.31 45.21 o 10 6 0 47.74 65.00 47.24 o 11 6 0 721.97 859.26 60.99 o 12 6 0 146.60 146.13 72.51 o 13 6 0 60.61 -35.67 85.32 o 14 6 0 176.49 138.96 89.51 o 15 6 0 450.88 453.10 99.55 o 1 7 0 2292.05 2373.03 50.28 o 2 7 0 212.15 268.59 19.16 o 3 7 0 86.14 126.99 20.69 o 4 7 0 4.29 11.47 21.47 o 5 7 0 3.83 242.11 43.07 o 6 7 0 94.10 -17.23 23.77 o 7 7 0 3903.51 3804.01 77.64 o 8 7 0 2.54 -21.60 28.64 o 9 7 0 699.40 732.07 51.16 o 10 7 0 310.72 432.64 50.96 o 11 7 0 2487.22 2499.33 88.89 o 12 7 0 211.30 153.22 76.02 o 13 7 0 21.69 -5.26 109.08 o 14 7 0 183.86 185.38 114.20 o 15 7 0 919.21 798.56 108.50 o 0 8 0 9551.79 9732.31 188.00 o 1 8 0 3681.53 3541.81 59.98 o 2 8 0 3160.23 3713.21 67.60 o 3 8 0 6673.07 6462.24 105.56 o 4 8 0 1708.29 1594.78 43.86 o 5 8 0 1002.23 867.47 47.33 o 6 8 0 2330.52 2037.45 78.83 o 7 8 0 1591.54 1579.85 71.81 o 8 8 0 907.73 883.32 43.17 o 9 8 0 1607.30 1397.11 63.31 o 10 8 0 2137.03 2215.33 82.73 o 11 8 0 143.11 97.32 52.62 o 12 8 0 1029.33 1081.83 118.13 o 13 8 0 2081.74 2090.75 138.41 o 14 8 0 27.53 -3.95 87.98 o 15 8 0 1494.18 1581.52 159.19 o 1 9 0 995.12 1558.25 39.38 o 2 9 0 779.61 718.10 37.37 o 3 9 0 1938.95 1663.85 55.73 o 4 9 0 163.63 139.23 25.85 o 5 9 0 5816.02 5730.43 150.76 o 6 9 0 2375.93 2272.05 61.60 o 7 9 0 293.09 283.54 34.18 o 8 9 0 45.61 11.88 32.99 o 9 9 0 51.88 65.40 45.78 o 10 9 0 54.39 31.26 48.95 o 11 9 0 78.76 33.54 54.73 o 12 9 0 476.47 392.04 73.37 o 13 9 0 98.51 119.41 188.27 o 14 9 0 1155.86 1002.27 144.32 o 0 10 0 16240.21 14520.49 275.99 o 1 10 0 2464.86 2259.60 48.32 o 2 10 0 969.28 945.71 41.97 o 3 10 0 6908.09 6282.48 123.29 o 4 10 0 962.13 910.34 41.61 o 5 10 0 8226.70 7427.66 125.09 o 6 10 0 1128.18 1293.39 47.31 o 7 10 0 630.63 698.27 43.08 o 8 10 0 4145.80 3970.07 89.15 o 9 10 0 1274.64 1457.28 82.85 o 10 10 0 3002.34 3173.31 169.84 o 11 10 0 1362.82 1140.07 87.37 o 12 10 0 479.27 456.76 78.55 o 13 10 0 64.69 189.35 115.53 o 14 10 0 417.43 675.28 136.59 o 1 11 0 4061.65 4229.45 72.86 o 2 11 0 3225.54 2945.39 59.16 o 3 11 0 1212.61 1073.52 50.47 o 4 11 0 321.23 396.52 30.08 o 5 11 0 474.81 436.52 57.40 o 6 11 0 2362.63 2168.68 85.33 o 7 11 0 554.58 548.14 49.94 o 8 11 0 393.68 535.28 63.60 o 9 11 0 2409.18 2504.80 146.98 o 10 11 0 1908.23 2178.54 203.15 o 11 11 0 660.16 676.39 91.41 o 12 11 0 16.63 -45.22 87.80 o 13 11 0 335.00 98.27 118.18 o 14 11 0 222.91 219.58 209.38 o 0 12 0 3264.57 2873.86 97.32 o 1 12 0 92.96 104.22 24.15 o 2 12 0 882.19 1179.79 37.88 o 3 12 0 4915.63 4568.49 95.00 o 4 12 0 561.75 877.62 52.21 o 5 12 0 9196.71 8976.83 172.08 o 6 12 0 185.76 347.11 47.66 o 7 12 0 94.25 174.12 47.60 o 8 12 0 5699.58 5320.34 127.35 o 9 12 0 20.90 -0.65 62.59 o 10 12 0 5.07 97.58 68.68 o 11 12 0 1835.99 1754.44 103.96 o 12 12 0 17.68 26.53 76.00 o 13 12 0 1134.30 1401.20 146.75 o 1 13 0 1893.65 2100.98 64.03 o 2 13 0 2389.80 2333.61 67.33 o 3 13 0 928.89 865.71 47.56 o 4 13 0 2356.36 2592.69 81.87 o 5 13 0 2124.05 2138.47 76.44 o 6 13 0 528.04 508.23 52.40 o 7 13 0 1267.35 1161.90 64.38 o 8 13 0 1.54 54.45 65.52 o 9 13 0 334.94 352.87 73.38 o 10 13 0 398.62 477.22 99.03 o 11 13 0 621.87 726.67 133.12 o 12 13 0 167.63 203.09 83.63 o 13 13 0 6.83 12.32 124.42 o 0 14 0 1601.27 1514.17 103.81 o 1 14 0 2120.73 2069.24 76.36 o 2 14 0 4350.50 5576.20 111.05 o 3 14 0 4362.87 4093.41 96.47 o 4 14 0 7827.39 8011.58 146.29 o 5 14 0 1694.82 1741.01 72.49 o 6 14 0 164.40 207.05 51.67 o 7 14 0 1358.65 1356.95 80.76 o 8 14 0 2341.02 2604.03 92.33 o 9 14 0 503.75 359.88 107.33 o 10 14 0 6.18 98.68 77.16 o 11 14 0 514.16 609.04 91.47 o 12 14 0 402.86 414.47 94.29 o 1 15 0 2401.72 2428.51 86.92 o 2 15 0 1673.71 1620.75 84.82 o 3 15 0 136.27 108.72 44.13 o 4 15 0 76.14 59.23 45.51 o 5 15 0 5005.84 4745.98 122.55 o 6 15 0 6028.29 5539.78 136.64 o 7 15 0 784.11 785.68 68.40 o 8 15 0 2.38 -28.19 59.94 o 9 15 0 2425.96 2376.98 115.22 o 10 15 0 156.13 44.57 80.48 o 11 15 0 979.52 908.91 98.74 o 0 16 0 43.63 51.44 78.12 o 1 16 0 1173.30 1108.82 93.97 o 2 16 0 6785.12 6971.65 156.11 o 3 16 0 179.41 72.56 62.98 o 4 16 0 5954.54 5570.83 139.06 o 5 16 0 0.79 33.81 49.71 o 6 16 0 500.80 598.20 74.15 o 7 16 0 1694.06 1624.54 83.41 o 8 16 0 22.26 171.26 78.78 o 9 16 0 423.97 425.94 90.38 o 10 16 0 29.35 -53.40 83.72 o 1 17 0 444.60 426.99 62.99 o 2 17 0 837.28 774.51 70.32 o 3 17 0 42.10 12.71 59.89 o 4 17 0 618.20 648.49 68.74 o 5 17 0 1728.07 1972.86 158.47 o 6 17 0 3033.08 2788.74 222.45 o 7 17 0 29.69 -6.77 72.23 o 8 17 0 0.07 -24.95 95.31 o 9 17 0 137.23 133.61 87.57 o 0 18 0 0.64 27.32 89.48 o 1 18 0 5009.91 4853.65 138.05 o 2 18 0 94.77 173.93 64.74 o 3 18 0 73.09 -32.58 62.40 o 4 18 0 2691.69 2516.79 104.22 o 5 18 0 30.05 129.19 82.79 o 6 18 0 3579.35 3372.55 118.41 o 7 18 0 3547.81 3971.94 149.12 o 8 18 0 495.89 642.17 135.48 o 1 19 0 610.21 568.52 93.97 o 2 19 0 1494.63 1451.53 89.63 o 3 19 0 1040.87 943.82 132.57 o 4 19 0 102.62 50.56 70.29 o 5 19 0 954.49 1109.23 85.30 o 6 19 0 377.60 407.45 79.12 o 7 19 0 1098.09 1214.08 90.77 o 0 20 0 904.33 1047.99 207.62 o 1 20 0 369.34 474.50 78.53 o 2 20 0 350.69 563.74 79.40 o 3 20 0 91.63 193.65 76.97 o 4 20 0 678.56 927.14 89.63 o 5 20 0 774.45 886.28 96.36 o 1 21 0 52.95 90.85 76.10 o 2 21 0 7.11 -3.67 77.98 o -16 1 1 63.55 -9.72 77.18 o -15 1 1 35.81 69.06 73.11 o -14 1 1 366.44 421.23 72.25 o -13 1 1 36.22 76.84 61.78 o -12 1 1 791.10 851.19 67.45 o -11 1 1 433.16 408.08 55.59 o -10 1 1 49.99 120.43 25.64 o -9 1 1 96.98 101.52 26.23 o -8 1 1 268.93 227.05 26.23 o -7 1 1 7715.66 8383.82 119.38 o -6 1 1 47.14 48.21 17.25 o -5 1 1 4709.95 4866.11 77.90 o -4 1 1 23276.17 23472.76 294.76 o -3 1 1 5244.29 4875.23 125.32 o -2 1 1 339.77 314.56 10.87 o 1 1 1 71.79 90.08 9.36 o 2 1 1 259.13 164.09 11.71 o 3 1 1 160854.95 170217.14 2312.36 o 4 1 1 2623.13 2328.93 46.07 o 5 1 1 152.86 295.83 20.02 o 6 1 1 3474.60 3159.53 63.53 o 7 1 1 2259.86 2404.46 74.70 o 8 1 1 414.07 440.62 28.66 o 9 1 1 2.68 15.54 26.54 o 10 1 1 124.28 92.85 49.27 o 11 1 1 405.15 385.49 57.90 o 12 1 1 175.40 124.64 59.70 o 13 1 1 504.55 588.15 73.26 o 14 1 1 48.22 -26.70 68.45 o 15 1 1 352.67 326.26 81.77 o 16 1 1 174.92 38.74 83.64 o -16 2 1 243.98 250.81 81.46 o -15 2 1 15.39 -7.81 71.67 o -14 2 1 279.32 516.00 112.25 o -13 2 1 464.02 539.13 69.90 o -12 2 1 31.69 -15.69 52.01 o -11 2 1 1490.18 1673.69 59.61 o -10 2 1 2331.18 2323.68 56.26 o -9 2 1 1099.01 937.24 33.74 o -8 2 1 697.18 732.50 29.92 o -7 2 1 238.57 254.54 21.98 o -6 2 1 33.56 83.37 20.36 o -5 2 1 2018.12 1824.15 38.24 o -4 2 1 324246.34 346184.41 4260.23 o -3 2 1 15941.71 16481.18 208.66 o -2 2 1 4145.93 3346.21 52.36 o -1 2 1 999.32 865.76 21.94 o 0 2 1 293.53 408.64 11.88 o 1 2 1 57.38 219.66 11.06 o 2 2 1 102.06 201.72 23.54 o 3 2 1 54598.89 54061.09 666.10 o 4 2 1 11940.12 12933.46 167.95 o 5 2 1 1358.10 1387.48 38.39 o 6 2 1 5323.10 4957.71 87.33 o 7 2 1 1786.43 1759.61 63.68 o 8 2 1 1634.66 1895.31 59.33 o 9 2 1 1767.34 1612.88 52.36 o 10 2 1 3577.25 3269.46 85.54 o 11 2 1 3776.28 3969.49 113.46 o 12 2 1 239.77 155.31 77.20 o 13 2 1 1010.94 1009.26 79.47 o 14 2 1 250.26 218.56 71.21 o 15 2 1 10.03 30.72 78.22 o 16 2 1 434.09 289.45 86.97 o -16 3 1 71.60 57.32 78.52 o -15 3 1 275.49 212.75 75.53 o -14 3 1 1511.41 1924.82 97.69 o -13 3 1 493.64 334.55 66.97 o -12 3 1 35.92 -28.72 53.60 o -11 3 1 12.28 118.51 37.48 o -10 3 1 1674.52 1500.95 54.02 o -9 3 1 2341.89 2264.23 53.60 o -8 3 1 2220.75 2632.58 57.18 o -7 3 1 5864.61 5774.72 89.34 o -6 3 1 7742.15 7859.63 112.08 o -5 3 1 714.94 1258.31 57.48 o -4 3 1 7932.78 8042.28 119.92 o -3 3 1 961.27 1073.54 28.57 o -2 3 1 6059.64 6718.46 102.34 o -1 3 1 12054.03 11931.51 185.99 o 0 3 1 696.59 804.25 20.37 o 1 3 1 16115.21 20116.97 274.38 o 2 3 1 1149.01 1263.20 30.25 o 3 3 1 8307.62 10659.66 152.08 o 4 3 1 2321.15 2152.42 43.40 o 5 3 1 13402.46 15071.81 197.33 o 6 3 1 6935.93 6802.59 99.01 o 7 3 1 16638.61 17469.61 256.04 o 8 3 1 268.72 315.36 44.91 o 9 3 1 4653.30 4408.96 90.84 o 10 3 1 2736.52 2565.19 70.03 o 11 3 1 6.70 116.02 73.65 o 12 3 1 127.56 102.63 63.49 o 13 3 1 34.08 61.59 64.26 o 14 3 1 513.84 689.30 81.34 o 15 3 1 43.16 -21.82 77.22 o 16 3 1 29.09 -1.58 83.76 o -16 4 1 1646.92 1658.44 148.31 o -15 4 1 648.95 805.23 101.08 o -14 4 1 178.57 165.42 77.71 o -13 4 1 1506.79 1527.97 85.40 o -12 4 1 620.09 498.25 69.17 o -11 4 1 203.34 230.22 40.62 o -10 4 1 1541.38 1684.03 58.94 o -9 4 1 1287.31 1015.19 53.51 o -8 4 1 60831.65 60587.17 756.30 o -7 4 1 1430.17 1588.19 42.08 o -6 4 1 16904.79 16399.47 235.91 o -5 4 1 20951.46 19746.53 277.59 o -4 4 1 8657.25 8726.87 130.03 o -3 4 1 37570.83 36697.93 499.01 o -2 4 1 22859.22 23715.70 325.65 o -1 4 1 8.27 55.47 15.69 o 0 4 1 55548.57 65871.79 884.47 o 1 4 1 14395.27 13430.65 187.21 o 2 4 1 60.48 256.50 23.87 o 3 4 1 14085.71 14782.64 208.50 o 4 4 1 85.75 134.62 17.78 o 5 4 1 15512.68 13464.89 194.62 o 6 4 1 6117.32 5460.50 91.45 o 7 4 1 7548.85 8370.27 121.21 o 8 4 1 22222.58 21498.58 282.34 o 9 4 1 2287.44 1919.06 59.53 o 10 4 1 1860.29 1947.83 63.57 o 11 4 1 2911.71 3099.21 104.11 o 12 4 1 695.72 795.24 77.71 o 13 4 1 1063.74 898.29 79.09 o 14 4 1 606.16 498.05 80.40 o 15 4 1 7.77 8.61 76.49 o -16 5 1 194.49 219.89 100.35 o -15 5 1 84.80 -59.82 86.67 o -14 5 1 413.54 395.47 85.14 o -13 5 1 73.69 57.88 62.37 o -12 5 1 99.05 159.17 72.63 o -11 5 1 229.41 253.05 41.74 o -10 5 1 1457.05 1370.85 60.64 o -9 5 1 2243.69 2054.24 56.54 o -8 5 1 46.20 67.32 27.58 o -7 5 1 362.02 304.37 28.07 o -6 5 1 4987.81 4646.01 83.29 o -5 5 1 1937.57 2414.29 64.02 o -4 5 1 663.67 583.31 37.22 o -3 5 1 8420.93 9752.96 143.05 o -2 5 1 2283.40 2593.48 55.76 o -1 5 1 6002.99 6414.01 98.45 o 0 5 1 344.59 287.66 21.37 o 1 5 1 23042.11 22730.65 312.81 o 2 5 1 8313.98 7374.10 110.68 o 3 5 1 895.12 1051.68 31.55 o 4 5 1 1626.15 1335.91 38.10 o 5 5 1 99.96 84.66 22.15 o 6 5 1 2322.41 2246.27 58.65 o 7 5 1 10318.63 10204.64 157.55 o 8 5 1 5.41 18.70 28.61 o 9 5 1 2965.99 3041.66 86.15 o 10 5 1 916.67 789.79 51.94 o 11 5 1 7333.28 7157.08 189.26 o 12 5 1 50.99 -8.70 68.01 o 13 5 1 317.38 302.81 83.91 o 14 5 1 414.69 622.27 123.73 o 15 5 1 62.17 -26.19 95.98 o -16 6 1 95.25 234.60 103.35 o -15 6 1 914.33 721.76 102.14 o -14 6 1 1217.72 1267.48 231.56 o -13 6 1 4082.93 4586.25 158.37 o -12 6 1 1138.56 1172.37 75.33 o -11 6 1 3840.82 3750.60 105.84 o -10 6 1 4148.15 4120.79 104.32 o -9 6 1 278.86 267.67 33.01 o -8 6 1 2098.74 1886.30 53.63 o -7 6 1 3053.65 3011.95 66.32 o -6 6 1 29.52 15.95 23.36 o -5 6 1 22141.65 20927.64 296.26 o -4 6 1 1451.87 1753.87 44.21 o -3 6 1 10192.60 9715.41 143.91 o -2 6 1 22271.70 21088.38 329.35 o -1 6 1 273.44 286.14 14.86 o 0 6 1 33141.44 35205.88 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