#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:44:30 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181914 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/13/2241351.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241351 _cell_angle_alpha 87.377 _cell_angle_beta 86.955 _cell_angle_gamma 72.339 _cell_length_a 12.1000 _cell_length_b 12.5686 _cell_length_c 29.1490 _exptl_crystal_F_000 2028.00 _reflns_d_resolution_high 0.7710 _cod_data_source_file fk2092Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 14186n in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 417.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5311.66 5523.01 84.05 o 2 0 0 17189.05 16157.64 252.19 o 3 0 0 1168.56 1291.88 45.85 o 4 0 0 54.86 108.08 15.85 o 5 0 0 2755.47 2565.29 59.23 o 6 0 0 1051.38 995.13 41.42 o 7 0 0 334.17 456.93 46.42 o 8 0 0 4508.95 3953.60 93.76 o 9 0 0 15328.64 14237.61 293.51 o 10 0 0 784.10 818.85 71.35 o 11 0 0 2292.19 2330.00 116.60 o 12 0 0 1808.33 2192.70 122.21 o 13 0 0 1428.48 1592.27 112.37 o 14 0 0 8.85 55.71 91.58 o -14 1 0 781.23 720.38 131.03 o -13 1 0 10.98 12.23 76.64 o -12 1 0 21.20 37.78 61.33 o -11 1 0 1319.27 1239.96 91.07 o -10 1 0 746.09 875.46 74.75 o -9 1 0 1044.84 1165.30 77.79 o -8 1 0 11947.71 11431.66 201.28 o -7 1 0 154.80 158.35 27.81 o -6 1 0 6693.64 6150.03 117.02 o -5 1 0 692.88 487.12 33.76 o -4 1 0 13445.29 13615.58 196.45 o -3 1 0 5759.05 5515.44 106.95 o -2 1 0 12386.53 12856.69 266.77 o -1 1 0 59095.01 62881.06 1304.98 o 0 1 0 1294.61 1578.27 27.27 o 1 1 0 33154.10 33236.90 493.93 o 2 1 0 2613.22 2068.11 35.91 o 3 1 0 424.77 282.75 15.31 o 4 1 0 929.84 882.12 35.82 o 5 1 0 11861.42 11738.19 185.80 o 6 1 0 8341.70 7971.97 147.17 o 7 1 0 4868.35 4693.28 97.51 o 8 1 0 80.21 107.35 26.63 o 9 1 0 307.80 376.05 40.50 o 10 1 0 5633.18 5177.18 151.03 o 11 1 0 859.45 1123.23 94.34 o 12 1 0 1901.09 2181.45 114.41 o 13 1 0 1356.50 1448.53 153.31 o 14 1 0 1280.70 1619.25 132.23 o 15 1 0 26.41 55.24 137.68 o -14 2 0 1027.15 1168.46 148.61 o -13 2 0 1223.50 1636.77 135.14 o -12 2 0 877.83 888.05 110.59 o -11 2 0 347.35 385.29 103.65 o -10 2 0 1357.58 1408.15 91.84 o -9 2 0 567.11 613.92 63.38 o -8 2 0 10786.93 10442.90 191.35 o -7 2 0 208.75 237.67 40.98 o -6 2 0 1490.20 1515.87 51.64 o -5 2 0 17188.85 17047.63 266.41 o -4 2 0 32482.81 31748.52 463.37 o -3 2 0 727.83 604.41 33.39 o -2 2 0 2231.73 2560.86 70.68 o -1 2 0 713.68 1338.98 31.54 o 0 2 0 621.46 1049.53 23.01 o 1 2 0 2394.24 2164.22 37.11 o 2 2 0 32511.93 32788.21 509.95 o 3 2 0 98.17 150.71 10.99 o 4 2 0 534.88 546.22 22.28 o 5 2 0 2456.68 2458.33 73.55 o 6 2 0 5607.63 6183.60 106.65 o 7 2 0 2060.87 1725.24 57.66 o 8 2 0 27561.51 25703.55 393.82 o 9 2 0 9294.54 8813.07 178.43 o 10 2 0 646.10 995.71 122.65 o 11 2 0 36.11 97.37 50.79 o 12 2 0 935.25 988.83 86.48 o 13 2 0 461.19 397.30 86.57 o 14 2 0 2252.33 2322.50 202.24 o 15 2 0 822.58 1059.18 122.85 o -13 3 0 180.40 228.10 111.63 o -12 3 0 6995.47 6711.06 233.25 o -11 3 0 518.34 549.08 86.26 o -10 3 0 6015.15 6154.16 180.34 o -9 3 0 969.70 1069.51 81.31 o -8 3 0 1574.76 1770.48 82.14 o -7 3 0 157.00 200.29 29.21 o -6 3 0 3465.21 3510.77 86.62 o -5 3 0 11121.14 11094.29 187.51 o -4 3 0 77.99 38.76 19.33 o -3 3 0 13005.97 13031.98 205.10 o -2 3 0 4319.25 4856.76 88.27 o -1 3 0 148.75 85.12 11.99 o 0 3 0 7191.73 8962.15 130.22 o 1 3 0 9864.93 9921.09 187.89 o 2 3 0 12511.00 12389.79 208.16 o 3 3 0 5749.47 6461.58 99.71 o 4 3 0 306.78 280.57 15.65 o 5 3 0 3418.02 3570.74 63.27 o 6 3 0 5593.54 5676.83 98.97 o 7 3 0 15871.93 15394.84 229.26 o 8 3 0 35693.49 33761.10 470.86 o 9 3 0 2273.01 2083.18 78.19 o 10 3 0 929.27 970.25 80.35 o 11 3 0 413.84 500.97 63.96 o 12 3 0 6143.55 5816.05 200.08 o 13 3 0 218.50 105.54 66.86 o 14 3 0 377.38 325.35 80.63 o 15 3 0 596.94 805.91 105.98 o -13 4 0 3370.60 2958.22 267.09 o -12 4 0 1324.69 1260.50 161.21 o -11 4 0 225.55 179.99 83.82 o -10 4 0 1270.78 906.92 95.89 o -9 4 0 2960.16 3345.41 207.91 o -8 4 0 1401.80 1524.31 116.30 o -7 4 0 1220.48 1182.77 74.22 o -6 4 0 301.85 331.16 36.70 o -5 4 0 19605.60 19825.31 338.01 o -4 4 0 11078.85 11480.59 192.92 o -3 4 0 13974.45 14860.98 235.14 o -2 4 0 13219.85 14514.74 226.07 o -1 4 0 2623.13 3209.58 62.93 o 0 4 0 60.56 56.15 12.39 o 1 4 0 1661.85 1501.89 35.84 o 2 4 0 7526.55 7679.30 115.74 o 3 4 0 18080.82 18313.72 357.16 o 4 4 0 81075.08 78891.51 1114.87 o 5 4 0 6481.44 6592.18 88.93 o 6 4 0 4463.75 4258.20 80.32 o 7 4 0 2920.34 2778.31 71.43 o 8 4 0 254.20 230.89 29.24 o 9 4 0 1.05 3.23 27.08 o 10 4 0 2633.48 2590.38 128.82 o 11 4 0 531.24 1020.92 194.82 o 12 4 0 212.78 333.91 68.75 o 13 4 0 1753.30 1962.95 120.64 o 14 4 0 84.19 130.41 74.27 o 15 4 0 2762.14 2477.54 151.04 o -12 5 0 2593.16 2812.46 262.63 o -11 5 0 216.60 320.47 127.57 o -10 5 0 13.96 10.35 67.75 o -9 5 0 2555.19 2388.04 136.29 o -8 5 0 4052.43 3879.04 159.85 o -7 5 0 1632.42 1808.47 99.68 o -6 5 0 7620.29 7082.59 146.02 o -5 5 0 12289.68 11868.66 206.94 o -4 5 0 1095.88 1109.06 51.95 o -3 5 0 3216.11 3550.61 82.27 o -2 5 0 10640.76 11101.21 184.34 o -1 5 0 2050.54 2078.23 47.70 o 0 5 0 48.32 76.82 15.58 o 1 5 0 625.51 777.75 41.97 o 2 5 0 811.08 993.69 32.99 o 3 5 0 38291.23 38061.74 545.12 o 4 5 0 59409.88 60030.96 850.75 o 5 5 0 3909.44 3450.37 75.91 o 6 5 0 6128.85 5417.60 94.03 o 7 5 0 13.82 40.22 22.20 o 8 5 0 2476.27 2449.89 94.08 o 9 5 0 432.06 389.31 49.21 o 10 5 0 1929.89 1765.20 103.91 o 11 5 0 1276.89 1355.91 103.47 o 12 5 0 5.64 70.63 66.68 o 13 5 0 319.58 116.27 80.30 o 14 5 0 906.92 1052.36 144.38 o 15 5 0 196.54 223.50 87.00 o -12 6 0 184.25 521.03 154.11 o -11 6 0 52.28 51.38 127.08 o -10 6 0 1034.35 1161.62 133.15 o -9 6 0 230.81 276.28 89.28 o -8 6 0 701.99 559.96 74.90 o -7 6 0 265.40 286.74 50.39 o -6 6 0 262.89 341.06 42.41 o -5 6 0 0.56 -4.99 28.92 o -4 6 0 6347.85 6400.73 130.61 o -3 6 0 7816.21 8833.14 161.56 o -2 6 0 23851.88 25612.82 390.11 o -1 6 0 2393.19 2949.71 74.91 o 0 6 0 16861.83 18152.14 287.92 o 1 6 0 21.34 79.30 17.43 o 2 6 0 34301.31 35518.00 482.66 o 3 6 0 1826.34 1761.36 48.09 o 4 6 0 2430.46 2268.93 52.61 o 5 6 0 10984.68 10607.67 178.90 o 6 6 0 13740.54 13190.89 217.80 o 7 6 0 3740.47 3224.44 83.71 o 8 6 0 426.66 479.10 58.79 o 9 6 0 18.82 15.40 34.87 o 10 6 0 5834.49 5733.98 224.38 o 11 6 0 2793.32 3138.23 133.70 o 12 6 0 43.41 77.41 62.18 o 13 6 0 1271.13 1281.92 104.16 o 14 6 0 132.37 299.85 80.80 o 15 6 0 1594.01 1534.28 128.46 o -11 7 0 1141.10 1172.48 191.74 o -10 7 0 723.65 900.00 191.42 o -9 7 0 960.68 859.92 119.61 o -8 7 0 1422.41 1350.80 132.04 o -7 7 0 430.16 433.24 92.34 o -6 7 0 5787.60 5629.43 165.96 o -5 7 0 1418.61 1445.22 77.91 o -4 7 0 790.85 898.47 53.37 o -3 7 0 497.87 586.05 47.98 o -2 7 0 33.15 49.79 23.32 o -1 7 0 32499.42 37483.43 555.47 o 0 7 0 2978.91 2999.01 71.75 o 1 7 0 8266.59 9147.30 149.18 o 2 7 0 1241.25 1073.94 44.37 o 3 7 0 31420.48 30953.93 428.99 o 4 7 0 3821.72 3374.49 71.45 o 5 7 0 9567.30 9558.11 168.81 o 6 7 0 5596.08 5332.37 122.78 o 7 7 0 656.82 593.87 52.93 o 8 7 0 7.48 -10.72 36.27 o 9 7 0 373.95 333.51 52.58 o 10 7 0 1041.43 1223.14 82.69 o 11 7 0 888.46 792.37 69.90 o 12 7 0 14676.87 13836.81 314.56 o 13 7 0 981.31 1042.75 95.81 o 14 7 0 875.14 979.05 145.43 o 15 7 0 98.58 160.60 81.52 o -10 8 0 17.00 42.30 222.92 o -9 8 0 1048.98 893.08 123.99 o -8 8 0 3883.10 3973.18 259.17 o -7 8 0 1300.04 1096.02 140.89 o -6 8 0 5738.44 5805.28 215.42 o -5 8 0 1128.65 1127.46 85.85 o -4 8 0 3717.51 4030.95 168.25 o -3 8 0 1287.42 1477.11 113.43 o -2 8 0 5575.17 5951.12 158.75 o -1 8 0 7.84 15.89 32.83 o 0 8 0 223.78 388.23 42.98 o 1 8 0 2064.76 2314.95 97.57 o 2 8 0 724.25 589.45 35.82 o 3 8 0 2573.60 2216.81 67.09 o 4 8 0 50.19 85.03 24.14 o 5 8 0 184.58 209.88 24.07 o 6 8 0 7405.93 6895.21 166.70 o 7 8 0 2881.35 2684.50 108.28 o 8 8 0 6016.92 5714.44 186.12 o 9 8 0 554.68 460.55 59.46 o 10 8 0 1771.69 1843.71 104.49 o 11 8 0 4566.21 4305.55 158.31 o 12 8 0 4455.66 4065.49 280.38 o 13 8 0 168.72 266.89 87.65 o 14 8 0 1749.13 1820.29 145.19 o 15 8 0 116.92 214.71 103.83 o -9 9 0 694.06 486.17 246.58 o -8 9 0 8.02 67.42 94.43 o -7 9 0 576.44 298.80 126.06 o -6 9 0 1046.70 824.72 97.94 o -5 9 0 12651.94 12588.99 292.12 o -4 9 0 203.55 361.83 87.70 o -3 9 0 8.69 15.11 53.78 o -2 9 0 5889.91 6644.03 179.11 o -1 9 0 13291.63 14235.79 302.14 o 0 9 0 96.19 99.42 42.98 o 1 9 0 229.67 240.67 65.10 o 2 9 0 254.94 261.94 33.30 o 3 9 0 191.37 144.30 32.68 o 4 9 0 2488.90 2492.64 122.45 o 5 9 0 178.69 152.05 42.42 o 6 9 0 553.91 498.31 55.98 o 7 9 0 4120.17 4210.40 154.29 o 8 9 0 25234.56 23838.94 460.11 o 9 9 0 24.86 179.51 53.40 o 10 9 0 8825.89 9040.12 228.35 o 11 9 0 47.48 85.29 62.92 o 12 9 0 306.15 435.67 85.07 o 13 9 0 951.29 966.33 112.20 o 14 9 0 783.78 969.72 118.11 o 15 9 0 13.04 115.12 98.38 o -8 10 0 896.89 1092.21 139.67 o -7 10 0 75.18 128.96 100.27 o -6 10 0 10.25 -78.51 81.64 o -5 10 0 1065.69 1107.19 97.92 o -4 10 0 476.71 497.83 75.28 o -3 10 0 2123.75 2002.63 112.50 o -2 10 0 4566.53 4834.10 200.33 o -1 10 0 3448.78 4026.30 149.52 o 0 10 0 8301.35 8778.22 215.42 o 1 10 0 929.07 945.77 72.77 o 2 10 0 12137.93 12422.24 246.35 o 3 10 0 356.40 321.11 51.08 o 4 10 0 4590.98 4717.66 119.61 o 5 10 0 1953.31 1950.05 94.56 o 6 10 0 7426.90 7155.55 188.48 o 7 10 0 8088.80 8143.76 203.01 o 8 10 0 324.66 451.58 60.37 o 9 10 0 4108.07 4055.45 153.08 o 10 10 0 586.48 548.32 76.03 o 11 10 0 4737.15 4234.50 166.10 o 12 10 0 1453.87 1871.82 203.60 o 13 10 0 6.73 -2.38 83.62 o 14 10 0 1171.58 1265.95 135.87 o -7 11 0 483.32 473.13 122.23 o -6 11 0 985.34 830.60 127.73 o -5 11 0 2272.53 2357.90 233.88 o -4 11 0 1781.63 2010.21 125.67 o -3 11 0 11.33 0.52 63.52 o -2 11 0 3035.29 3601.86 174.44 o -1 11 0 30.93 82.67 61.79 o 0 11 0 4327.02 4374.05 215.61 o 1 11 0 91.87 128.00 55.24 o 2 11 0 1950.54 2039.16 101.77 o 3 11 0 14927.79 14988.74 290.56 o 4 11 0 1217.46 1081.70 94.73 o 5 11 0 53.04 121.79 59.51 o 6 11 0 1562.33 1754.28 116.47 o 7 11 0 4926.38 4879.37 162.15 o 8 11 0 2138.95 2133.36 112.22 o 9 11 0 32.76 51.19 58.20 o 10 11 0 94.93 60.49 67.94 o 11 11 0 795.86 770.22 90.09 o 12 11 0 12.37 116.69 70.12 o 13 11 0 8.26 40.66 83.71 o 14 11 0 1835.55 2035.97 162.75 o -6 12 0 1337.96 1296.11 158.34 o -5 12 0 129.93 119.05 108.15 o -4 12 0 3163.88 3450.16 168.37 o -3 12 0 801.51 833.74 94.57 o -2 12 0 7998.63 8114.34 232.02 o -1 12 0 1253.63 1493.32 110.03 o 0 12 0 521.06 489.08 74.59 o 1 12 0 15.00 25.29 56.33 o 2 12 0 4788.02 5185.68 323.08 o 3 12 0 353.37 433.37 71.19 o 4 12 0 301.32 300.93 73.71 o 5 12 0 500.83 610.60 86.55 o 6 12 0 114.13 -25.25 61.82 o 7 12 0 4754.24 4644.07 192.30 o 8 12 0 112.59 57.67 71.45 o 9 12 0 205.11 224.36 79.53 o 10 12 0 1196.25 1258.07 103.69 o 11 12 0 91.79 29.67 70.93 o 12 12 0 373.82 376.54 87.38 o 13 12 0 207.19 224.29 92.00 o -5 13 0 2045.19 2360.12 362.90 o -4 13 0 7.35 44.15 93.23 o -3 13 0 3155.21 3634.05 176.77 o -2 13 0 2766.68 2647.26 154.69 o -1 13 0 5483.24 5366.33 204.68 o 0 13 0 2689.76 2766.17 151.11 o 1 13 0 4904.16 5162.73 188.62 o 2 13 0 107.80 90.23 78.16 o 3 13 0 881.71 1116.51 122.21 o 4 13 0 822.11 821.48 91.70 o 5 13 0 579.91 478.90 87.11 o 6 13 0 2196.38 2163.58 143.00 o 7 13 0 995.78 876.32 104.23 o 8 13 0 347.84 322.50 86.74 o 9 13 0 14.45 173.68 85.46 o 10 13 0 1835.25 2050.02 151.12 o 11 13 0 141.32 177.53 91.89 o 12 13 0 3134.96 3397.32 295.53 o -3 14 0 215.14 9.90 111.40 o -2 14 0 845.77 741.12 103.90 o -1 14 0 631.20 814.55 151.02 o 0 14 0 36.43 68.88 85.38 o 1 14 0 4.57 14.91 97.61 o 2 14 0 3978.01 4082.32 205.01 o 3 14 0 1671.50 1670.94 139.71 o 4 14 0 2555.24 2456.18 141.93 o 5 14 0 440.10 353.28 107.04 o 6 14 0 2290.59 1911.92 146.01 o 7 14 0 592.38 464.36 99.74 o 8 14 0 144.82 50.93 79.22 o 9 14 0 72.38 121.50 86.34 o 10 14 0 185.38 321.42 98.18 o 11 14 0 382.82 409.17 107.06 o -1 15 0 1.68 2.92 82.35 o 0 15 0 589.59 430.52 106.66 o 1 15 0 585.95 348.93 172.77 o 2 15 0 340.23 483.90 108.14 o 3 15 0 1403.38 1825.71 156.31 o 4 15 0 1375.22 1360.98 136.80 o 5 15 0 644.23 598.48 97.95 o 6 15 0 4176.60 4007.31 189.39 o 7 15 0 55.92 -16.17 86.46 o 8 15 0 1774.44 1766.15 161.15 o 9 15 0 1310.64 1077.18 129.07 o 10 15 0 536.59 439.52 109.30 o 2 16 0 2626.99 2409.00 378.40 o 3 16 0 1166.34 1572.00 216.40 o 4 16 0 172.21 114.18 104.50 o 5 16 0 15.88 51.88 98.01 o 6 16 0 88.54 96.02 84.73 o 7 16 0 980.45 814.21 109.61 o -7 -16 1 2088.75 2130.32 151.67 o -6 -16 1 32.91 -31.28 88.74 o -5 -16 1 1977.55 2053.01 166.43 o -4 -16 1 12.28 -91.40 91.40 o -3 -16 1 567.05 464.07 113.79 o -10 -15 1 7.95 -31.15 99.86 o -9 -15 1 0.90 243.31 94.13 o -8 -15 1 286.80 177.32 111.13 o -7 -15 1 1251.19 1196.34 155.74 o -6 -15 1 1382.71 1325.47 120.34 o -5 -15 1 4013.11 3837.78 185.83 o -4 -15 1 136.72 83.73 87.95 o -3 -15 1 725.55 959.13 208.20 o -2 -15 1 194.64 118.37 92.10 o -1 -15 1 1297.13 936.14 128.62 o 0 -15 1 0.47 2.62 92.20 o 1 -15 1 799.93 818.84 110.93 o -11 -14 1 1101.97 1304.14 136.56 o -10 -14 1 535.83 687.12 110.72 o -9 -14 1 1463.49 1739.78 170.07 o -8 -14 1 1133.25 1245.19 216.03 o -7 -14 1 1333.80 1321.71 126.64 o -6 -14 1 646.10 742.40 119.78 o -5 -14 1 4398.63 4746.08 197.19 o -4 -14 1 118.83 99.17 69.73 o -3 -14 1 1266.34 1316.69 200.02 o -2 -14 1 3.85 134.55 83.62 o -1 -14 1 965.31 1148.43 176.83 o 0 -14 1 806.80 1244.60 113.32 o 1 -14 1 872.92 672.03 97.99 o 2 -14 1 1.46 -72.05 72.05 o 3 -14 1 1324.97 1527.38 130.16 o -12 -13 1 241.76 219.71 94.96 o -11 -13 1 134.80 179.29 93.86 o -10 -13 1 4639.23 4770.84 222.12 o -9 -13 1 2262.65 2063.24 148.86 o -8 -13 1 0.28 2.82 91.66 o -7 -13 1 11.79 154.26 77.54 o -6 -13 1 3.87 -67.37 67.37 o -5 -13 1 1125.65 1188.13 114.47 o -4 -13 1 3523.36 3493.98 159.56 o -3 -13 1 1111.19 1189.21 116.35 o -2 -13 1 1418.18 1541.37 188.46 o -1 -13 1 13.52 12.06 61.21 o 0 -13 1 81.60 -41.24 83.54 o 1 -13 1 416.75 474.70 88.01 o 2 -13 1 598.47 753.26 98.25 o 3 -13 1 487.68 534.83 95.05 o 4 -13 1 20.68 91.77 89.56 o 5 -13 1 221.86 237.46 115.34 o -13 -12 1 501.04 467.56 103.14 o -12 -12 1 112.90 46.00 73.03 o -11 -12 1 20.52 122.34 69.66 o -10 -12 1 1621.85 1823.17 116.60 o -9 -12 1 104.09 84.45 71.19 o -8 -12 1 2671.32 2420.79 147.31 o -7 -12 1 5217.05 4981.96 264.16 o -6 -12 1 689.27 574.95 86.59 o -5 -12 1 45.34 -30.67 65.43 o -4 -12 1 617.43 610.01 90.38 o -3 -12 1 9920.00 9794.72 248.03 o -2 -12 1 182.01 198.28 60.68 o -1 -12 1 16.18 41.57 87.70 o 0 -12 1 832.09 819.40 93.55 o 1 -12 1 1162.93 1469.01 148.03 o 2 -12 1 20.23 79.63 65.65 o 3 -12 1 404.93 561.00 86.35 o 4 -12 1 570.17 599.28 156.78 o 5 -12 1 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