data_2241378 _cell_angle_alpha 90.000 _cell_angle_beta 102.205 _cell_angle_gamma 90.000 _cell_length_a 18.0213 _cell_length_b 19.4619 _cell_length_c 13.8664 _exptl_crystal_F_000 2712.00 _reflns_d_resolution_high 0.7489 _cod_data_source_file pj2026Isup2.hkl _cod_data_source_block I _shelx_title ' I in space group C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 544.45 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6160.89 9387.08 145.07 o 4 0 0 254267.42 248235.20 3654.53 o 6 0 0 3624.11 3111.30 75.44 o 8 0 0 4090.30 3571.79 85.70 o 10 0 0 22180.75 21739.91 356.55 o 12 0 0 4723.28 4644.58 217.90 o 14 0 0 15835.70 14508.14 306.48 o 16 0 0 5548.21 4637.58 253.13 o 18 0 0 1.10 -38.64 54.42 o 20 0 0 3338.76 3287.72 149.33 o 3 1 0 60996.58 68305.50 565.13 o 5 1 0 1527.56 1863.55 31.54 o 7 1 0 44131.33 42776.89 396.37 o 9 1 0 3061.40 3898.20 85.02 o 11 1 0 939.59 914.68 38.00 o 13 1 0 284.36 411.13 46.96 o 15 1 0 1583.69 1800.42 67.42 o 17 1 0 773.12 1029.39 64.17 o 19 1 0 2287.24 2612.09 225.21 o 0 2 0 1482.96 1256.01 102.54 o 2 2 0 10496.26 9683.46 81.27 o 4 2 0 18.87 20.10 10.89 o 6 2 0 13976.52 13843.59 122.54 o 8 2 0 19095.50 20650.25 219.51 o 10 2 0 4206.16 4638.07 69.98 o 12 2 0 19.26 11.47 19.34 o 14 2 0 1562.78 1870.57 67.25 o 16 2 0 811.56 1155.48 104.99 o 18 2 0 61.04 51.36 45.62 o 20 2 0 207.81 174.17 56.18 o 1 3 0 18539.73 20607.66 208.17 o 3 3 0 17732.08 20289.28 187.65 o 5 3 0 7893.32 7917.95 81.33 o 7 3 0 12933.69 11524.63 117.48 o 9 3 0 1655.69 1950.27 46.04 o 11 3 0 13675.84 12806.84 165.51 o 13 3 0 10649.82 10041.87 172.51 o 15 3 0 235.66 173.92 57.41 o 17 3 0 2280.67 2259.98 114.00 o 19 3 0 3114.77 2975.40 173.03 o 21 3 0 262.05 135.97 48.52 o 0 4 0 7335.92 8871.67 173.91 o 2 4 0 20266.79 19673.35 228.71 o 4 4 0 370.84 427.97 18.19 o 6 4 0 2431.68 2072.46 36.42 o 8 4 0 133.92 241.98 21.50 o 10 4 0 304.49 205.11 22.14 o 12 4 0 2163.24 2509.09 62.38 o 14 4 0 877.94 859.59 51.55 o 16 4 0 790.97 1079.17 74.92 o 18 4 0 304.94 214.83 50.71 o 20 4 0 2300.24 2394.85 118.48 o 22 4 0 1074.58 1489.97 217.89 o 1 5 0 264.65 343.96 15.52 o 3 5 0 4702.51 5181.27 68.87 o 5 5 0 24.61 52.52 12.58 o 7 5 0 22634.06 22937.92 219.99 o 9 5 0 2922.10 2654.99 54.80 o 11 5 0 3997.63 4051.31 78.88 o 13 5 0 279.55 168.86 33.10 o 15 5 0 2869.49 2556.37 135.05 o 17 5 0 2726.13 3447.94 121.11 o 19 5 0 8.13 -44.44 44.44 o 21 5 0 14.10 -21.97 61.52 o 23 5 0 215.95 471.02 163.42 o 0 6 0 39950.98 40988.17 572.87 o 2 6 0 21741.68 21306.66 223.97 o 4 6 0 22480.15 23606.65 223.54 o 6 6 0 31696.30 29929.43 298.03 o 8 6 0 543.73 365.04 23.13 o 10 6 0 9036.71 7531.79 120.64 o 12 6 0 3332.53 3210.12 75.54 o 14 6 0 7358.36 7352.70 161.71 o 16 6 0 809.03 765.92 66.39 o 18 6 0 738.34 653.74 67.95 o 20 6 0 1458.80 1574.27 108.23 o 22 6 0 21.66 128.17 121.76 o 1 7 0 2900.54 2705.41 48.34 o 3 7 0 124.13 210.40 17.26 o 5 7 0 571.80 457.46 22.94 o 7 7 0 35490.84 38234.64 410.96 o 9 7 0 33523.41 35249.88 418.87 o 11 7 0 453.52 722.88 38.02 o 13 7 0 21106.33 23227.42 326.18 o 15 7 0 3257.09 2815.92 93.27 o 17 7 0 1424.00 1492.10 125.87 o 19 7 0 1075.44 1184.53 87.80 o 21 7 0 422.96 514.74 89.95 o 0 8 0 9509.79 9526.74 159.38 o 2 8 0 6070.59 5841.35 79.55 o 4 8 0 1277.48 1916.43 57.81 o 6 8 0 6325.36 7005.72 90.58 o 8 8 0 10616.04 10059.62 145.10 o 10 8 0 1180.55 711.86 39.34 o 12 8 0 2915.93 2812.55 87.33 o 14 8 0 5487.75 5276.06 126.46 o 16 8 0 322.75 293.63 48.31 o 18 8 0 344.58 468.12 66.06 o 20 8 0 487.50 393.08 82.37 o 22 8 0 41.60 -48.06 128.17 o 1 9 0 5.18 9.68 12.86 o 3 9 0 624.15 551.32 38.48 o 5 9 0 6252.26 7022.17 110.54 o 7 9 0 1925.86 1175.59 39.17 o 9 9 0 2727.04 3078.38 108.71 o 11 9 0 5227.97 4756.58 96.36 o 13 9 0 5294.06 4905.37 135.97 o 15 9 0 1470.85 1466.04 76.80 o 17 9 0 278.83 317.40 57.09 o 19 9 0 878.55 687.94 76.49 o 21 9 0 115.53 129.75 76.47 o 0 10 0 27310.48 25971.56 388.33 o 2 10 0 4892.43 5677.49 82.49 o 4 10 0 15540.58 16267.40 189.11 o 6 10 0 5905.57 6050.39 100.37 o 8 10 0 8.19 12.45 22.51 o 10 10 0 11238.70 11960.79 175.29 o 12 10 0 255.10 240.78 35.20 o 14 10 0 21.02 -37.24 37.24 o 16 10 0 6589.39 6659.15 231.71 o 18 10 0 135.11 133.74 62.13 o 20 10 0 1234.08 1254.72 197.06 o 1 11 0 11754.37 11683.88 141.92 o 3 11 0 23244.86 21517.53 240.79 o 5 11 0 693.49 918.07 39.79 o 7 11 0 7979.55 6834.52 137.79 o 9 11 0 10153.38 10584.16 159.66 o 11 11 0 15.98 48.23 29.13 o 13 11 0 5646.61 5680.91 139.67 o 15 11 0 1.47 -5.36 47.17 o 17 11 0 1465.43 1401.90 83.06 o 19 11 0 260.89 197.20 62.48 o 21 11 0 315.22 435.78 115.35 o 0 12 0 3940.19 3676.49 93.70 o 2 12 0 615.11 490.38 28.37 o 4 12 0 408.91 601.77 34.35 o 6 12 0 176.01 253.64 28.50 o 8 12 0 436.27 263.36 33.07 o 10 12 0 2238.75 2174.88 65.81 o 12 12 0 0.02 -10.33 30.34 o 14 12 0 54.61 118.05 49.95 o 16 12 0 216.05 206.52 51.31 o 18 12 0 34.67 -37.20 46.82 o 20 12 0 0.27 -32.04 83.31 o 1 13 0 35344.26 36288.13 420.55 o 3 13 0 15004.41 16134.47 213.63 o 5 13 0 1601.60 1847.91 57.10 o 7 13 0 1428.91 1888.84 53.36 o 9 13 0 6533.36 7005.85 157.51 o 11 13 0 793.37 899.40 50.62 o 13 13 0 3335.54 3370.88 128.10 o 15 13 0 1.82 36.88 45.80 o 17 13 0 871.40 939.13 75.64 o 19 13 0 575.01 502.37 90.08 o 0 14 0 7862.83 6309.59 188.16 o 2 14 0 1870.72 2033.21 59.17 o 4 14 0 15305.64 13737.84 191.55 o 6 14 0 13257.90 13573.90 192.27 o 8 14 0 13205.95 12436.90 165.91 o 10 14 0 3914.73 3678.39 77.27 o 12 14 0 321.98 154.34 45.95 o 14 14 0 3077.66 3063.02 108.02 o 16 14 0 2862.04 3319.44 135.38 o 18 14 0 74.24 -12.71 66.18 o 1 15 0 5084.50 5948.86 122.53 o 3 15 0 5.86 27.16 24.94 o 5 15 0 11.25 -10.12 25.48 o 7 15 0 2699.06 2750.45 65.76 o 9 15 0 1202.17 1354.42 50.91 o 11 15 0 330.77 398.79 53.58 o 13 15 0 6.05 -23.93 43.18 o 15 15 0 138.77 154.81 60.72 o 17 15 0 213.83 66.11 71.54 o 19 15 0 436.71 560.74 131.37 o 0 16 0 2128.72 2033.84 106.96 o 2 16 0 7282.05 6741.37 118.92 o 4 16 0 5457.44 5706.01 113.18 o 6 16 0 1328.16 1071.61 51.32 o 8 16 0 721.83 920.04 44.36 o 10 16 0 2056.84 2396.21 138.59 o 12 16 0 771.90 819.68 81.38 o 14 16 0 440.64 527.80 72.42 o 16 16 0 216.72 115.58 66.39 o 18 16 0 334.06 219.97 83.47 o 1 17 0 533.69 545.29 48.62 o 3 17 0 18143.78 18459.61 251.26 o 5 17 0 142.62 48.91 29.49 o 7 17 0 4204.87 4531.64 88.95 o 9 17 0 3015.07 3075.23 101.88 o 11 17 0 331.62 220.47 67.82 o 13 17 0 2835.33 2564.30 184.06 o 15 17 0 42.94 30.68 61.26 o 17 17 0 968.50 1127.12 317.22 o 0 18 0 234.94 260.72 59.84 o 2 18 0 33.47 81.58 30.72 o 4 18 0 61.47 121.63 31.36 o 6 18 0 30.67 35.13 30.51 o 8 18 0 249.46 163.97 55.53 o 10 18 0 1121.74 1503.80 100.10 o 12 18 0 254.71 143.67 60.15 o 14 18 0 883.87 800.12 88.98 o 16 18 0 393.06 304.88 91.57 o 1 19 0 549.28 359.89 39.65 o 3 19 0 432.34 386.14 41.34 o 5 19 0 369.38 282.66 59.74 o 7 19 0 710.54 786.68 79.26 o 9 19 0 118.08 56.49 55.25 o 11 19 0 185.01 263.69 66.90 o 13 19 0 62.44 32.33 61.77 o 15 19 0 6.19 62.99 78.43 o 0 20 0 1414.27 1320.42 105.33 o 2 20 0 102.92 47.63 39.17 o 4 20 0 200.93 271.81 59.88 o 6 20 0 638.07 558.79 72.47 o 8 20 0 770.24 544.43 77.02 o 10 20 0 2680.62 2864.23 142.82 o 12 20 0 362.43 592.58 83.68 o 14 20 0 216.14 96.48 80.07 o 1 21 0 1150.30 904.75 81.38 o 3 21 0 4174.78 4533.03 150.13 o 5 21 0 849.30 944.84 86.68 o 7 21 0 2482.99 2578.60 131.32 o 9 21 0 775.06 505.82 78.60 o 11 21 0 455.51 416.19 77.79 o 13 21 0 1965.36 1892.25 148.29 o 0 22 0 2885.05 3386.88 243.52 o 2 22 0 140.73 206.16 62.12 o 4 22 0 11.13 48.12 59.26 o 6 22 0 214.73 299.16 69.05 o 8 22 0 345.27 624.05 85.84 o 10 22 0 510.03 787.28 90.81 o 12 22 0 453.57 468.01 153.80 o 1 23 0 1498.06 1223.91 243.52 o 3 23 0 2326.61 1929.59 150.56 o 5 23 0 98.81 36.82 64.01 o 7 23 0 9.43 -27.74 62.73 o 9 23 0 272.13 256.24 75.12 o 0 24 0 2658.94 2822.93 256.34 o 2 24 0 370.61 480.15 101.88 o 4 24 0 1036.84 1051.78 126.88 o 6 24 0 575.87 446.96 103.07 o 8 24 0 5.89 -5.85 70.25 o 1 25 0 553.26 550.19 109.73 o 3 25 0 409.14 445.32 103.05 o 5 25 0 7.23 -53.24 82.12 o -23 1 1 73.81 73.70 121.76 o -21 1 1 1853.62 1517.27 152.82 o -19 1 1 91.91 91.85 58.53 o -17 1 1 901.11 1157.94 57.27 o -15 1 1 1429.96 1434.07 82.21 o -13 1 1 1360.27 1320.01 55.49 o -11 1 1 2364.99 1778.61 57.04 o -9 1 1 9258.36 8902.40 112.19 o -7 1 1 9405.50 9568.43 98.44 o -5 1 1 3687.70 3788.24 40.37 o -3 1 1 32706.27 34348.25 322.79 o 1 1 1 27203.52 30535.59 322.69 o 3 1 1 34702.99 37415.69 331.36 o 5 1 1 45035.10 45791.39 487.40 o 7 1 1 15612.69 16504.50 173.21 o 9 1 1 30653.24 30450.20 345.11 o 11 1 1 11312.25 11444.65 163.05 o 13 1 1 633.67 716.86 39.26 o 15 1 1 4499.56 4813.18 133.32 o 17 1 1 1127.89 1043.79 64.52 o 19 1 1 763.30 821.40 71.22 o 21 1 1 1952.84 1691.84 102.90 o -22 2 1 1974.98 2085.96 256.34 o -20 2 1 421.99 325.05 63.62 o -18 2 1 3136.09 2912.11 131.19 o -16 2 1 231.22 233.00 43.44 o -14 2 1 9182.30 9918.71 167.74 o -12 2 1 24365.92 23751.44 253.67 o -10 2 1 10791.66 10774.08 127.59 o -8 2 1 12190.16 11339.83 139.10 o -6 2 1 10952.26 10804.92 100.62 o -4 2 1 17731.50 17671.96 161.25 o -2 2 1 177083.28 179797.75 1712.48 o 0 2 1 114.77 146.66 11.36 o 2 2 1 42793.86 42103.85 389.80 o 4 2 1 40334.04 39989.99 332.01 o 6 2 1 1689.09 1969.17 33.31 o 8 2 1 17845.77 17985.86 190.88 o 10 2 1 53.80 129.93 20.30 o 12 2 1 8941.51 8363.58 209.45 o 14 2 1 4007.53 3653.72 92.33 o 16 2 1 21.33 -4.69 26.03 o 18 2 1 7416.26 7965.63 225.23 o 20 2 1 196.94 195.09 68.41 o -23 3 1 33.73 128.17 128.17 o -21 3 1 12.80 108.94 118.56 o -19 3 1 1526.57 1528.87 82.04 o -17 3 1 62.50 10.17 36.43 o -15 3 1 7664.24 7615.60 134.20 o -13 3 1 590.90 623.22 39.57 o -11 3 1 2306.21 1946.40 81.89 o -9 3 1 87.57 95.38 19.58 o -7 3 1 2051.48 1640.77 33.41 o -5 3 1 9429.55 9118.15 90.35 o -3 3 1 38299.95 41161.46 343.76 o -1 3 1 72427.16 77836.88 834.39 o 1 3 1 12501.40 12544.52 130.77 o 3 3 1 29110.87 30285.34 290.20 o 5 3 1 1887.38 1867.71 30.59 o 7 3 1 113.95 55.53 12.63 o 9 3 1 9800.21 10413.02 122.18 o 11 3 1 5756.46 5901.15 86.45 o 13 3 1 1081.30 989.26 43.82 o 15 3 1 1617.67 1263.35 66.14 o 17 3 1 127.82 119.66 49.75 o 19 3 1 212.22 200.47 56.79 o 21 3 1 492.67 300.87 80.22 o -22 4 1 684.20 64.08 70.49 o -20 4 1 70.87 117.16 108.94 o -18 4 1 6211.71 6885.18 201.87 o -16 4 1 3180.66 3076.47 108.93 o -14 4 1 7154.70 7004.01 136.60 o -12 4 1 6518.83 6161.26 166.50 o -10 4 1 654.69 504.56 34.11 o -8 4 1 3052.86 3339.77 51.91 o -6 4 1 22866.85 23331.29 199.58 o -4 4 1 2283.79 1846.70 29.88 o -2 4 1 33256.49 33472.98 342.89 o 0 4 1 45676.05 49709.82 481.80 o 2 4 1 68721.95 71356.81 715.18 o 4 4 1 41125.00 42585.59 406.07 o 6 4 1 2928.85 2689.64 41.70 o 8 4 1 45540.39 44413.05 403.44 o 10 4 1 1747.39 2321.86 53.28 o 12 4 1 5554.40 5885.72 106.17 o 14 4 1 70.40 38.94 27.25 o 16 4 1 62.99 26.85 52.58 o 18 4 1 962.62 825.33 78.98 o 20 4 1 314.72 309.66 62.99 o -21 5 1 1741.14 1896.91 233.91 o -19 5 1 1949.37 2236.45 110.24 o -17 5 1 225.23 251.01 51.15 o -15 5 1 10984.99 11060.58 175.51 o -13 5 1 17.80 86.40 26.84 o -11 5 1 13354.85 13284.35 183.84 o -9 5 1 203.57 147.63 21.53 o -7 5 1 11144.23 10663.74 109.04 o -5 5 1 1426.59 981.40 56.36 o -3 5 1 9061.57 8956.78 99.49 o -1 5 1 6677.67 6245.36 100.64 o 1 5 1 37915.96 38861.68 396.35 o 3 5 1 190.33 270.18 16.87 o 5 5 1 14026.64 14602.70 146.53 o 7 5 1 12242.97 12946.18 142.07 o 9 5 1 2373.23 2215.70 58.76 o 11 5 1 11863.68 12050.07 155.81 o 13 5 1 2597.91 2410.01 69.02 o 15 5 1 1642.02 1614.45 64.04 o 17 5 1 980.45 1253.83 84.73 o 19 5 1 927.09 901.34 80.92 o 21 5 1 2068.83 2871.00 214.68 o -22 6 1 728.31 736.97 179.44 o -20 6 1 122.06 128.78 65.49 o -18 6 1 95.94 90.72 49.61 o -16 6 1 1270.21 1430.20 81.57 o -14 6 1 5411.55 5071.42 111.45 o -12 6 1 1018.45 1070.18 47.27 o -10 6 1 186.74 185.65 22.90 o -8 6 1 2366.40 2203.10 47.66 o -6 6 1 1140.30 1230.04 42.26 o -4 6 1 3341.24 3302.90 76.21 o -2 6 1 18526.46 18967.80 202.12 o 0 6 1 298.04 279.67 15.04 o 2 6 1 14833.69 14070.32 154.25 o 4 6 1 4502.94 4892.36 63.44 o 6 6 1 14956.66 16011.28 171.14 o 8 6 1 843.62 1206.89 41.18 o 10 6 1 475.54 623.41 31.85 o 12 6 1 3056.94 2838.88 70.40 o 14 6 1 7592.78 7375.69 130.38 o 16 6 1 706.74 745.65 59.49 o 18 6 1 2092.79 1608.92 97.62 o 20 6 1 107.68 61.61 56.17 o -21 7 1 95.53 108.94 115.35 o -19 7 1 3.93 -51.37 51.37 o -17 7 1 647.53 686.16 66.68 o -15 7 1 2730.84 2419.53 102.07 o -13 7 1 172.06 351.31 35.54 o -11 7 1 1.02 16.74 20.29 o -9 7 1 1293.42 1278.05 46.92 o -7 7 1 2041.65 2276.46 46.98 o -5 7 1 259.43 368.31 19.67 o -3 7 1 1357.17 1633.02 35.29 o -1 7 1 2335.94 2534.28 43.85 o 1 7 1 20319.17 20743.92 236.48 o 3 7 1 18372.41 19609.86 212.15 o 5 7 1 777.74 810.22 26.14 o 7 7 1 3142.33 3438.36 61.61 o 9 7 1 4561.71 4817.97 166.50 o 11 7 1 1129.34 1352.74 91.47 o 13 7 1 5287.52 5440.56 106.57 o 15 7 1 782.51 743.54 66.60 o 17 7 1 857.32 627.93 60.10 o 19 7 1 25.51 55.93 53.01 o 21 7 1 2.15 86.03 72.23 o -22 8 1 683.80 874.76 189.05 o -20 8 1 13.87 -9.73 61.04 o -18 8 1 4668.40 4841.69 147.95 o -16 8 1 1454.14 1430.02 84.05 o -14 8 1 7565.07 8138.22 178.98 o -12 8 1 3270.02 3055.63 77.77 o -10 8 1 24.81 89.83 28.85 o -8 8 1 4554.93 5888.14 148.48 o -6 8 1 11689.25 10740.88 126.14 o -4 8 1 6297.83 7423.93 111.74 o -2 8 1 9504.31 8922.66 132.47 o 0 8 1 17479.21 17630.41 190.38 o 2 8 1 18731.21 18033.77 212.80 o 4 8 1 16230.96 15841.99 179.76 o 6 8 1 45.30 88.38 16.27 o 8 8 1 24100.84 26603.04 299.53 o 10 8 1 342.07 463.24 37.08 o 12 8 1 4629.74 5035.98 101.74 o 14 8 1 201.11 196.70 42.55 o 16 8 1 61.19 67.57 43.81 o 18 8 1 1644.42 2116.37 113.16 o 20 8 1 598.46 849.48 114.88 o -21 9 1 1993.60 1993.03 240.32 o -19 9 1 2792.75 2806.91 151.73 o -17 9 1 7.20 -47.22 47.22 o -15 9 1 7119.27 7065.18 152.06 o -13 9 1 60.93 0.66 28.64 o -11 9 1 3021.24 2768.86 71.86 o -9 9 1 6859.63 7010.94 137.15 o -7 9 1 10453.63 10533.26 150.20 o -5 9 1 48220.30 49547.86 1038.91 o -3 9 1 29677.56 31461.03 311.69 o -1 9 1 41.84 71.56 15.26 o 1 9 1 6760.02 6038.24 118.22 o 3 9 1 1079.79 1457.59 36.46 o 5 9 1 69723.96 70934.14 785.45 o 7 9 1 928.01 671.80 29.90 o 9 9 1 19278.38 18693.85 249.32 o 11 9 1 3118.57 3439.97 116.77 o 13 9 1 1863.90 1925.31 97.12 o 15 9 1 2587.49 2557.70 97.92 o 17 9 1 2461.13 2330.66 157.25 o 19 9 1 152.63 100.18 56.02 o 21 9 1 1012.38 1291.48 123.93 o -20 10 1 15.48 -25.37 68.89 o -18 10 1 73.97 68.26 51.79 o -16 10 1 848.84 860.02 71.91 o -14 10 1 3699.17 4067.57 112.32 o -12 10 1 895.58 1029.52 70.59 o -10 10 1 152.49 77.64 27.00 o -8 10 1 9192.26 9013.31 138.07 o -6 10 1 5263.56 5249.12 92.84 o -4 10 1 2838.30 2759.23 56.86 o -2 10 1 7743.83 7005.36 104.68 o 0 10 1 576.39 458.48 24.52 o 2 10 1 960.92 1127.86 45.62 o 4 10 1 617.96 1086.78 47.80 o 6 10 1 910.44 811.99 35.31 o 8 10 1 22.46 2.72 21.38 o 10 10 1 398.15 345.92 42.25 o 12 10 1 129.05 61.99 37.65 o 14 10 1 1122.86 1159.02 71.00 o 16 10 1 92.63 99.21 46.26 o 18 10 1 12.19 5.67 45.52 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