data_2241389 _cell_angle_alpha 90.000 _cell_angle_beta 93.759 _cell_angle_gamma 90.000 _cell_length_a 9.6650 _cell_length_b 33.8756 _cell_length_c 11.1543 _exptl_crystal_F_000 1432.00 _reflns_d_resolution_high 0.7565 _cod_data_source_file rz5179Isup2.hkl _cod_data_source_block I _shelx_title ' GUA4EEBPH4 (MONOKLINIC, P21/C)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 196.94 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7838.53 7567.52 73.50 o 2 0 0 9662.15 9840.46 157.05 o 3 0 0 36479.16 33987.51 744.36 o 4 0 0 2837.50 3070.10 52.69 o 5 0 0 1967.06 2200.85 60.49 o 6 0 0 10.66 -9.75 13.67 o 7 0 0 158.66 183.42 20.49 o 8 0 0 97.24 81.95 21.47 o 9 0 0 2385.30 2322.80 67.30 o 10 0 0 744.26 659.47 40.98 o 11 0 0 166.82 186.32 36.08 o 12 0 0 305.23 406.79 67.30 o 1 1 0 664.45 636.37 26.67 o 2 1 0 590.83 672.19 61.47 o 3 1 0 1713.89 1766.37 90.24 o 4 1 0 518.24 538.30 21.94 o 5 1 0 4006.09 4189.43 180.48 o 6 1 0 1.49 4.88 9.67 o 7 1 0 2433.87 2213.75 43.08 o 8 1 0 66.22 45.82 18.02 o 9 1 0 500.80 610.44 48.28 o 10 1 0 47.86 30.83 22.72 o 11 1 0 110.65 161.22 25.16 o 12 1 0 1.19 -23.64 23.64 o 0 2 0 84.56 76.06 10.95 o 1 2 0 7063.90 6844.58 27.72 o 2 2 0 2432.12 2388.35 114.64 o 3 2 0 4049.88 3920.41 158.52 o 4 2 0 242.91 247.86 20.49 o 5 2 0 38.03 50.50 5.86 o 6 2 0 1480.14 1559.19 88.28 o 7 2 0 1172.93 1206.40 29.27 o 8 2 0 1323.40 1297.84 32.07 o 9 2 0 21.80 32.59 29.75 o 10 2 0 27.36 31.25 18.04 o 11 2 0 90.04 98.93 29.21 o 12 2 0 42.51 68.46 25.45 o 1 3 0 70.05 77.35 12.47 o 3 3 0 1075.08 1056.61 81.46 o 4 3 0 34.49 34.24 4.38 o 5 3 0 113.08 91.59 5.57 o 6 3 0 446.69 482.77 23.92 o 7 3 0 799.01 759.06 25.37 o 8 3 0 4802.55 4636.22 151.70 o 9 3 0 42.89 46.11 19.86 o 10 3 0 665.94 725.26 29.64 o 11 3 0 5.62 33.38 21.08 o 12 3 0 9.37 75.08 32.30 o 0 4 0 26375.64 25458.14 53.70 o 1 4 0 1230.46 1205.89 16.90 o 2 4 0 6.98 22.44 6.35 o 3 4 0 321.85 350.55 11.69 o 4 4 0 134.89 143.29 6.33 o 5 4 0 41.62 27.55 6.33 o 6 4 0 103.48 105.21 6.35 o 7 4 0 243.04 212.23 15.18 o 8 4 0 0.05 -12.31 15.13 o 9 4 0 30.02 56.69 21.46 o 10 4 0 102.82 139.96 21.03 o 11 4 0 22.29 12.55 24.48 o 12 4 0 184.49 179.79 47.30 o 1 5 0 1625.91 1414.61 17.92 o 2 5 0 14262.69 13204.12 546.31 o 3 5 0 11159.30 11653.55 190.55 o 4 5 0 4065.59 4305.92 124.87 o 5 5 0 3952.16 4302.98 61.17 o 6 5 0 1101.45 1036.06 24.42 o 7 5 0 292.51 346.29 17.20 o 8 5 0 999.40 998.51 28.28 o 9 5 0 1970.34 2025.82 46.16 o 10 5 0 517.20 438.58 30.12 o 11 5 0 43.22 47.87 37.57 o 12 5 0 179.83 244.84 89.26 o 0 6 0 2011.42 2043.80 60.49 o 1 6 0 255.76 277.64 16.57 o 2 6 0 8402.44 7451.46 120.36 o 3 6 0 10424.39 10323.09 258.52 o 4 6 0 3997.15 4324.84 60.56 o 5 6 0 1542.82 1609.34 25.08 o 6 6 0 137.64 140.18 8.41 o 7 6 0 2357.44 2583.58 100.97 o 8 6 0 0.83 3.19 11.25 o 9 6 0 242.44 221.65 19.68 o 10 6 0 0.00 6.33 20.00 o 11 6 0 78.10 46.84 32.20 o 12 6 0 55.95 64.17 40.98 o 1 7 0 24.85 26.07 3.46 o 2 7 0 991.12 918.76 15.61 o 3 7 0 513.72 444.87 38.04 o 4 7 0 1955.19 2302.20 90.73 o 5 7 0 994.01 1078.55 53.65 o 6 7 0 45.96 37.38 8.12 o 7 7 0 246.45 283.25 27.80 o 8 7 0 1253.65 1352.40 60.49 o 9 7 0 394.38 370.67 22.94 o 10 7 0 67.97 53.60 18.20 o 11 7 0 155.47 158.13 28.33 o 12 7 0 473.56 514.10 38.27 o 1 8 0 10004.46 9394.25 234.62 o 2 8 0 12608.33 12275.28 661.43 o 3 8 0 7689.88 7406.91 117.91 o 4 8 0 772.25 802.29 28.28 o 5 8 0 2660.01 2731.72 176.09 o 6 8 0 811.29 946.92 44.87 o 7 8 0 63.53 81.12 13.44 o 8 8 0 4079.13 4067.50 76.16 o 9 8 0 425.96 446.41 23.11 o 10 8 0 2.40 27.54 20.27 o 11 8 0 62.45 75.18 23.43 o 12 8 0 145.24 134.02 27.18 o 1 9 0 10721.00 9751.44 349.24 o 2 9 0 4.75 -3.46 3.46 o 3 9 0 829.48 824.66 17.58 o 4 9 0 827.08 759.51 42.93 o 5 9 0 1386.31 1442.01 22.44 o 6 9 0 7.53 10.11 7.81 o 7 9 0 33.52 50.68 15.50 o 8 9 0 406.34 387.80 34.14 o 9 9 0 1146.24 1054.59 38.06 o 10 9 0 203.47 154.02 25.98 o 11 9 0 3.33 10.24 24.15 o 12 9 0 377.42 370.21 30.14 o 1 10 0 11938.06 10776.77 274.13 o 2 10 0 2178.67 2016.11 110.73 o 3 10 0 6341.29 6272.81 102.23 o 4 10 0 4799.60 4991.91 85.17 o 5 10 0 1485.86 1655.13 32.72 o 6 10 0 679.14 687.86 28.28 o 7 10 0 474.47 449.22 36.08 o 8 10 0 2844.34 2840.02 85.85 o 9 10 0 608.89 573.51 25.16 o 10 10 0 703.42 704.31 37.57 o 11 10 0 18.79 -0.21 31.20 o 12 10 0 109.75 93.38 34.20 o 1 11 0 355.86 299.70 9.27 o 2 11 0 3764.59 3194.52 54.14 o 3 11 0 2027.34 2039.36 32.28 o 4 11 0 4299.20 3959.45 67.93 o 5 11 0 3438.34 3266.37 57.60 o 6 11 0 9.45 2.55 7.53 o 7 11 0 1935.28 1931.32 68.28 o 8 11 0 0.17 7.31 27.80 o 9 11 0 9.14 21.79 15.67 o 10 11 0 338.60 358.46 25.16 o 11 11 0 2.55 -0.49 42.45 o 12 11 0 348.88 331.87 41.94 o 1 12 0 5524.48 5260.75 97.06 o 2 12 0 49.78 45.94 5.51 o 3 12 0 2640.09 2623.85 40.55 o 4 12 0 14.83 9.27 7.31 o 5 12 0 0.17 -1.06 8.61 o 6 12 0 66.05 66.84 15.12 o 7 12 0 124.59 150.85 19.51 o 8 12 0 1008.66 876.16 27.80 o 9 12 0 872.25 850.10 55.61 o 10 12 0 501.87 474.03 25.54 o 11 12 0 34.73 23.91 28.33 o 12 12 0 224.71 241.03 52.18 o 1 13 0 2170.18 2055.69 102.42 o 2 13 0 3375.79 3602.75 63.06 o 3 13 0 7130.55 7356.93 227.29 o 4 13 0 0.89 1.50 7.50 o 5 13 0 146.67 127.31 10.98 o 6 13 0 1435.42 1385.56 27.39 o 7 13 0 2061.86 2043.56 43.45 o 8 13 0 336.87 376.14 28.57 o 9 13 0 6.41 16.10 26.83 o 10 13 0 33.11 39.62 21.25 o 11 13 0 61.30 79.94 31.56 o 12 13 0 0.10 10.06 30.01 o 1 14 0 194.76 182.64 7.50 o 2 14 0 600.54 580.74 43.41 o 3 14 0 527.00 619.16 38.53 o 4 14 0 91.32 105.82 8.61 o 5 14 0 395.49 386.92 15.18 o 6 14 0 1096.45 1067.17 34.63 o 7 14 0 340.19 384.42 18.58 o 8 14 0 82.23 65.34 19.23 o 9 14 0 16.47 22.08 20.74 o 10 14 0 309.26 295.41 32.67 o 11 14 0 4.49 -17.06 25.80 o 12 14 0 47.79 71.03 29.96 o 1 15 0 1217.94 1107.40 23.73 o 2 15 0 629.08 541.03 16.06 o 3 15 0 785.73 835.27 18.26 o 4 15 0 6.91 4.79 7.91 o 5 15 0 901.94 870.45 65.85 o 6 15 0 1502.06 1572.25 59.02 o 7 15 0 1111.96 1195.89 85.36 o 8 15 0 1700.27 1627.60 40.00 o 9 15 0 461.98 464.59 28.29 o 10 15 0 72.78 65.74 22.35 o 11 15 0 3.60 18.53 25.51 o 12 15 0 19.23 42.81 30.01 o 1 16 0 2738.91 2784.87 169.74 o 2 16 0 782.85 785.73 17.90 o 3 16 0 5213.98 5743.00 341.45 o 4 16 0 140.13 140.84 13.67 o 5 16 0 46.38 48.97 17.06 o 6 16 0 1479.63 1471.84 59.02 o 7 16 0 42.63 50.68 14.44 o 8 16 0 75.01 66.56 13.44 o 9 16 0 90.38 115.55 39.02 o 10 16 0 32.70 55.01 24.39 o 11 16 0 11.28 24.91 26.38 o 1 17 0 0.00 1.47 5.51 o 2 17 0 791.02 716.39 24.88 o 3 17 0 166.91 145.16 6.77 o 4 17 0 1630.03 1638.26 33.40 o 5 17 0 808.90 681.93 19.31 o 6 17 0 0.00 -9.74 9.74 o 7 17 0 32.80 5.70 16.18 o 8 17 0 1.12 9.93 15.83 o 9 17 0 5.41 4.35 19.16 o 10 17 0 92.81 61.48 20.36 o 11 17 0 25.85 25.44 52.20 o 1 18 0 2262.00 2271.66 41.69 o 2 18 0 4906.60 5221.24 267.78 o 3 18 0 1092.51 1201.97 53.65 o 4 18 0 368.58 415.61 24.88 o 5 18 0 1753.69 1654.59 69.28 o 6 18 0 98.48 89.40 13.65 o 7 18 0 8.50 7.20 14.63 o 8 18 0 198.14 194.88 21.77 o 9 18 0 20.93 18.75 17.10 o 10 18 0 16.07 13.03 18.48 o 11 18 0 393.33 374.68 26.82 o 1 19 0 932.89 900.88 42.93 o 2 19 0 13.06 15.39 6.84 o 3 19 0 6.30 0.99 5.23 o 4 19 0 713.08 694.54 18.58 o 5 19 0 1234.15 1275.12 29.17 o 6 19 0 2216.18 2136.11 44.09 o 7 19 0 13.84 4.16 14.29 o 8 19 0 459.53 405.73 32.67 o 9 19 0 21.03 34.97 39.02 o 10 19 0 0.04 -16.24 23.33 o 11 19 0 47.53 58.06 29.57 o 1 20 0 187.05 180.33 36.10 o 2 20 0 54.24 58.82 8.78 o 3 20 0 1839.63 2007.31 122.91 o 4 20 0 297.33 307.49 13.74 o 5 20 0 189.03 182.15 13.33 o 6 20 0 103.92 95.80 14.03 o 7 20 0 15.48 1.55 20.49 o 8 20 0 271.82 219.23 23.41 o 9 20 0 166.12 170.62 22.04 o 10 20 0 130.36 100.24 25.00 o 11 20 0 7.90 5.01 27.78 o 1 21 0 332.90 320.96 14.65 o 2 21 0 17.77 16.10 8.28 o 3 21 0 269.77 239.69 12.05 o 4 21 0 267.24 240.22 27.32 o 5 21 0 101.55 103.30 13.67 o 6 21 0 288.53 251.37 19.23 o 7 21 0 108.21 119.11 16.80 o 8 21 0 2.12 8.96 29.26 o 9 21 0 17.01 19.09 20.96 o 10 21 0 251.74 316.23 50.24 o 11 21 0 278.92 260.47 39.02 o 1 22 0 1685.35 1971.59 81.95 o 2 22 0 515.16 488.22 20.98 o 3 22 0 1.59 3.26 11.21 o 4 22 0 461.61 422.43 24.89 o 5 22 0 406.91 353.31 34.63 o 6 22 0 151.30 114.12 14.82 o 7 22 0 34.32 39.08 15.42 o 8 22 0 388.84 344.87 20.00 o 9 22 0 250.16 219.40 22.08 o 10 22 0 237.00 264.85 36.10 o 11 22 0 20.61 21.21 28.18 o 1 23 0 235.34 189.60 13.05 o 2 23 0 26.35 30.88 8.72 o 3 23 0 29.76 21.94 9.67 o 4 23 0 58.58 73.08 20.98 o 5 23 0 854.90 773.55 23.18 o 6 23 0 21.11 11.11 13.33 o 7 23 0 1242.91 1228.26 29.57 o 8 23 0 202.41 195.56 27.80 o 9 23 0 60.36 52.07 19.57 o 10 23 0 142.62 152.94 24.02 o 1 24 0 42.09 24.40 12.69 o 2 24 0 494.94 458.09 24.88 o 3 24 0 985.53 1017.88 46.81 o 4 24 0 771.44 801.91 25.97 o 5 24 0 65.26 46.78 11.00 o 6 24 0 435.37 408.48 29.75 o 7 24 0 79.12 66.83 14.96 o 8 24 0 39.45 39.04 22.48 o 9 24 0 0.61 22.19 22.64 o 10 24 0 272.23 340.34 30.41 o 2 25 0 19.58 20.74 8.61 o 3 25 0 509.96 525.01 22.43 o 4 25 0 35.26 37.58 11.66 o 5 25 0 193.08 126.05 22.92 o 6 25 0 9.06 7.56 12.74 o 7 25 0 127.43 113.72 17.90 o 8 25 0 1.70 -6.85 21.70 o 9 25 0 249.01 262.81 25.98 o 10 25 0 33.44 53.01 56.10 o 1 26 0 763.12 770.46 62.44 o 2 26 0 43.23 23.16 8.20 o 3 26 0 137.28 130.60 13.18 o 4 26 0 2484.67 2339.59 48.27 o 5 26 0 33.82 53.50 18.04 o 6 26 0 65.14 48.43 15.13 o 7 26 0 0.21 -7.43 13.42 o 8 26 0 333.83 306.77 22.08 o 9 26 0 2.50 9.79 28.50 o 10 26 0 5.58 6.12 26.79 o 1 27 0 87.52 97.55 20.49 o 2 27 0 2071.53 2145.76 74.63 o 3 27 0 9.26 10.71 10.38 o 4 27 0 0.35 6.79 12.35 o 5 27 0 154.08 162.18 15.13 o 6 27 0 294.27 342.57 19.96 o 7 27 0 445.38 442.17 23.05 o 8 27 0 5.38 -30.24 30.24 o 9 27 0 110.87 148.89 20.96 o 10 27 0 51.11 14.92 28.05 o 2 28 0 45.04 53.37 13.28 o 3 28 0 276.21 316.55 15.18 o 4 28 0 799.73 817.49 24.48 o 5 28 0 48.44 44.69 14.14 o 6 28 0 18.87 23.15 14.53 o 7 28 0 3.37 0.98 16.57 o 8 28 0 34.50 43.01 18.59 o 9 28 0 7.94 -11.37 24.84 o 1 29 0 648.95 558.01 35.10 o 2 29 0 356.86 355.15 32.20 o 3 29 0 53.51 41.57 12.74 o 4 29 0 327.08 347.30 17.90 o 5 29 0 88.87 73.88 20.00 o 6 29 0 278.85 241.51 19.96 o 7 29 0 112.83 115.66 19.57 o 8 29 0 14.68 8.15 19.96 o 9 29 0 125.73 109.09 26.10 o 1 30 0 54.40 43.91 18.53 o 2 30 0 554.63 626.24 22.89 o 3 30 0 4.55 -7.64 12.74 o 4 30 0 54.97 20.91 13.44 o 5 30 0 7.66 15.46 13.33 o 6 30 0 249.53 284.41 28.79 o 7 30 0 80.89 83.09 33.65 o 8 30 0 95.03 100.56 24.02 o 9 30 0 129.84 121.96 45.36 o 1 31 0 653.36 731.67 46.81 o 2 31 0 315.90 287.54 19.02 o 3 31 0 4.69 -4.48 14.60 o 4 31 0 45.27 3.53 12.88 o 5 31 0 965.27 1074.86 103.91 o 6 31 0 16.70 54.65 16.56 o 7 31 0 1.89 3.89 23.43 o 8 31 0 88.61 86.55 21.79 o 9 31 0 48.02 16.00 31.69 o 0 32 0 648.89 660.88 29.31 o 1 32 0 130.57 124.89 25.35 o 2 32 0 9.34 -3.92 23.43 o 3 32 0 153.88 137.94 15.12 o 4 32 0 60.96 55.33 18.04 o 5 32 0 68.39 103.21 19.51 o 6 32 0 46.76 44.90 28.77 o 7 32 0 82.68 77.41 20.83 o 8 32 0 20.64 17.89 51.22 o 1 33 0 25.01 31.12 14.17 o 2 33 0 282.36 265.28 34.63 o 3 33 0 4.46 12.59 12.88 o 4 33 0 582.76 596.88 22.35 o 5 33 0 178.70 234.82 18.58 o 6 33 0 40.14 42.92 19.16 o 7 33 0 118.25 107.61 26.83 o 8 33 0 375.67 413.43 35.13 o 1 34 0 66.97 47.26 13.76 o 2 34 0 270.18 253.77 37.57 o 3 34 0 16.14 13.25 15.50 o 4 34 0 105.08 103.76 17.90 o 5 34 0 106.58 86.67 18.88 o 6 34 0 41.19 20.89 20.27 o 7 34 0 93.76 113.54 27.81 o 8 34 0 256.67 350.69 30.34 o 1 35 0 45.49 42.40 13.71 o 2 35 0 387.58 406.79 44.89 o 3 35 0 397.16 416.97 24.61 o 4 35 0 46.47 23.23 20.98 o 5 35 0 39.26 8.35 14.99 o 6 35 0 33.91 25.77 18.74 o 7 35 0 368.34 356.97 27.93 o 0 36 0 14.91 44.77 21.47 o 1 36 0 95.80 49.68 15.61 o 2 36 0 318.39 329.74 24.40 o 3 36 0 119.33 113.36 18.76 o 4 36 0 79.34 59.51 22.45 o 5 36 0 83.75 104.40 32.18 o 6 36 0 55.45 35.01 24.47 o 7 36 0 92.26 173.58 29.53 o 1 37 0 141.13 145.62 26.83 o 2 37 0 39.06 8.78 19.51 o 3 37 0 219.00 212.76 55.61 o 4 37 0 67.19 74.88 21.94 o 5 37 0 1.46 0.54 23.41 o 6 37 0 77.36 59.69 29.26 o 7 37 0 227.50 206.08 65.85 o 0 38 0 52.56 33.51 23.33 o 1 38 0 9.13 7.48 19.02 o 2 38 0 111.69 83.91 34.16 o 3 38 0 60.51 15.23 17.43 o 4 38 0 64.83 93.46 23.19 o 5 38 0 4.18 33.41 20.67 o 6 38 0 18.12 70.11 23.61 o 1 39 0 136.75 151.34 31.69 o 2 39 0 15.55 7.91 20.83 o 3 39 0 19.28 18.88 27.24 o 4 39 0 1.70 -14.43 20.13 o 5 39 0 0.26 11.73 17.13 o 6 39 0 49.79 92.50 25.12 o 0 40 0 37.74 46.78 32.67 o 1 40 0 82.06 75.86 17.31 o 2 40 0 31.03 17.65 19.02 o 3 40 0 1.00 -4.25 15.66 o 4 40 0 13.79 3.60 24.81 o 5 40 0 10.00 11.47 23.33 o 1 41 0 81.51 88.51 20.55 o 2 41 0 60.53 80.49 37.55 o 3 41 0 83.75 95.99 24.47 o 4 41 0 56.78 77.49 17.58 o 5 41 0 445.15 490.37 64.87 o 0 42 0 554.69 644.47 43.40 o 1 42 0 399.27 347.01 23.19 o 2 42 0 86.48 94.53 21.25 o 3 42 0 31.36 20.60 23.83 o 4 42 0 75.98 65.49 26.34 o 1 43 0 0.50 19.62 21.44 o 2 43 0 7.28 -0.92 25.56 o 3 43 0 33.69 34.41 21.03 o 0 44 0 6.02 15.42 30.41 o 1 44 0 7.81 42.67 20.34 o 2 44 0 4.92 25.98 19.16 o -12 1 1 14.50 47.79 27.59 o -11 1 1 333.08 348.27 42.93 o -10 1 1 528.99 479.97 32.69 o -9 1 1 6.09 4.70 19.32 o -8 1 1 38.53 59.45 18.04 o -7 1 1 485.84 492.06 49.75 o -6 1 1 273.42 317.94 36.59 o -5 1 1 2482.95 2409.28 63.41 o -4 1 1 612.14 576.03 16.10 o -3 1 1 1723.16 1747.74 36.95 o -2 1 1 15248.98 14928.23 195.46 o -1 1 1 11006.67 11015.62 67.95 o 0 1 1 2128.90 2485.59 18.62 o 1 1 1 3050.48 3014.81 21.72 o 2 1 1 45.59 58.04 3.06 o 3 1 1 560.10 563.18 12.67 o 4 1 1 406.09 509.27 16.10 o 5 1 1 413.19 393.25 10.00 o 6 1 1 56.09 37.68 7.73 o 7 1 1 476.45 517.37 19.27 o 8 1 1 208.50 148.97 21.96 o 9 1 1 656.80 676.48 25.85 o 10 1 1 52.62 25.83 16.21 o 11 1 1 418.20 467.02 28.62 o 12 1 1 67.61 37.85 30.24 o -12 2 1 296.71 279.99 30.01 o -11 2 1 196.88 247.20 77.08 o -10 2 1 117.96 118.48 22.45 o -9 2 1 1731.86 1739.31 41.73 o -8 2 1 962.60 877.64 36.10 o -7 2 1 144.79 184.83 14.49 o -6 2 1 24.79 26.34 10.36 o -5 2 1 13.78 2.23 7.50 o -4 2 1 744.42 714.63 29.75 o -3 2 1 30.88 52.57 4.15 o -2 2 1 709.31 691.56 38.53 o -1 2 1 5002.54 4978.98 43.50 o 0 2 1 2005.50 1874.84 28.47 o 1 2 1 12296.38 12118.75 87.96 o 2 2 1 4160.56 4200.11 47.93 o 3 2 1 2580.78 2712.87 44.87 o 4 2 1 106.06 112.20 5.51 o 5 2 1 208.44 272.82 15.61 o 6 2 1 26.37 28.53 8.66 o 7 2 1 25.61 17.08 12.41 o 8 2 1 242.42 242.80 16.12 o 9 2 1 105.81 67.95 16.17 o 10 2 1 31.35 17.82 18.95 o 11 2 1 557.41 585.82 88.77 o 12 2 1 98.46 61.27 32.47 o -12 3 1 13.42 42.08 28.26 o -11 3 1 8.31 23.90 47.32 o -10 3 1 180.30 208.79 25.86 o -9 3 1 1575.10 1545.69 66.83 o -8 3 1 432.16 459.88 19.65 o -7 3 1 134.59 149.42 13.74 o -6 3 1 515.52 518.70 17.92 o -5 3 1 551.15 580.85 44.39 o -4 3 1 462.17 487.32 20.98 o -3 3 1 80.01 91.37 7.80 o -2 3 1 668.03 601.84 11.22 o -1 3 1 11113.16 11048.76 274.45 o 0 3 1 11.56 9.41 0.69 o 1 3 1 49.83 38.54 1.38 o 2 3 1 13386.83 13530.36 227.29 o 3 3 1 164.21 167.88 17.55 o 4 3 1 7975.80 8083.72 299.00 o 5 3 1 1382.24 1415.76 22.74 o 6 3 1 73.49 83.40 9.84 o 7 3 1 0.00 -14.35 20.98 o 8 3 1 33.34 63.31 38.53 o 9 3 1 87.40 52.69 16.56 o 10 3 1 21.67 9.28 19.31 o 11 3 1 67.11 40.98 24.15 o 12 3 1 1.12 5.56 31.00 o -12 4 1 11.82 23.70 34.14 o -11 4 1 35.10 25.23 24.11 o -10 4 1 54.01 37.57 34.63 o -9 4 1 929.36 917.92 33.70 o -8 4 1 565.51 564.45 22.04 o -7 4 1 19.27 8.38 20.00 o -6 4 1 7.78 3.31 8.12 o -5 4 1 4460.82 4765.63 122.91 o -4 4 1 609.52 620.68 17.06 o -3 4 1 3229.41 3520.27 124.87 o -2 4 1 391.82 424.38 7.59 o -1 4 1 26829.84 22166.49 682.41 o 0 4 1 2845.77 2633.11 27.78 o 1 4 1 2727.89 2524.88 44.39 o 2 4 1 11387.92 11218.33 128.64 o 3 4 1 993.21 1047.04 21.56 o 4 4 1 24.59 22.45 5.38 o 5 4 1 475.65 484.67 13.80 o 6 4 1 1199.73 1363.83 39.51 o 7 4 1 746.19 725.70 28.79 o 8 4 1 394.19 400.58 23.28 o 9 4 1 88.55 32.16 17.08 o 10 4 1 669.02 556.31 31.16 o 11 4 1 228.96 211.47 26.83 o 12 4 1 15.52 17.60 31.94 o -12 5 1 7.72 15.21 31.86 o -11 5 1 186.62 187.33 42.93 o -10 5 1 58.49 59.61 20.34 o -9 5 1 557.57 675.29 46.33 o -8 5 1 689.04 604.59 26.82 o -7 5 1 3975.18 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2992.20 89.75 o -3 10 2 1268.53 1232.44 20.74 o -2 10 2 3384.13 3252.76 53.18 o -1 10 2 7253.12 6729.63 292.19 o 0 10 2 57.39 28.28 7.80 o 1 10 2 0.03 1.47 3.46 o 2 10 2 571.20 524.41 11.71 o 3 10 2 1.17 6.24 3.25 o 4 10 2 5.70 3.78 6.35 o 5 10 2 86.47 71.11 12.69 o 6 10 2 182.95 184.40 7.19 o 7 10 2 0.19 -14.52 15.61 o 8 10 2 274.42 255.41 18.58 o 9 10 2 64.15 81.89 17.55 o 10 10 2 73.64 38.10 21.35 o 11 10 2 36.48 8.84 34.09 o 12 10 2 54.81 39.48 42.01 o -12 11 2 449.73 488.03 34.71 o -11 11 2 1.48 35.78 28.97 o -10 11 2 353.38 320.31 34.63 o -9 11 2 154.67 101.46 22.90 o -8 11 2 1362.37 1303.96 103.40 o -7 11 2 1106.69 1022.24 28.77 o -6 11 2 20.76 10.28 11.25 o -5 11 2 979.73 937.70 32.18 o -4 11 2 1080.80 1137.42 23.43 o -3 11 2 3157.52 3105.12 50.36 o -2 11 2 3.15 5.10 4.43 o -1 11 2 6789.55 6599.71 155.11 o 0 11 2 2310.20 2024.28 69.26 o 1 11 2 11.90 5.08 3.25 o 2 11 2 1804.76 1740.56 72.67 o 3 11 2 24.81 27.89 3.41 o 4 11 2 401.76 449.23 13.54 o 5 11 2 75.65 90.73 8.89 o 6 11 2 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6.89 11.20 o -5 19 2 78.12 71.36 11.66 o -4 19 2 494.66 514.41 13.14 o -3 19 2 344.83 326.98 10.47 o -2 19 2 239.49 210.72 8.12 o -1 19 2 6.99 2.71 6.52 o 0 19 2 3311.09 3161.80 111.22 o 1 19 2 2.85 -4.90 7.80 o 2 19 2 1.50 -2.27 7.94 o 3 19 2 300.23 323.33 12.05 o 4 19 2 0.66 6.64 8.61 o 5 19 2 1313.29 1375.61 31.24 o 6 19 2 2022.06 1939.03 48.77 o 7 19 2 19.02 18.53 20.98 o 8 19 2 82.51 59.15 17.20 o 9 19 2 2.35 18.15 23.19 o 10 19 2 26.19 28.72 23.19 o 11 19 2 19.81 7.30 40.49 o -11 20 2 296.90 309.29 70.22 o -10 20 2 36.32 25.18 29.75 o -9 20 2 1.72 17.01 24.13 o -8 20 2 1599.36 1563.77 61.45 o -7 20 2 12.36 7.80 13.44 o -6 20 2 1066.73 1012.24 44.39 o -5 20 2 11.53 1.64 10.98 o -4 20 2 125.74 121.06 10.68 o -3 20 2 2.54 5.20 20.00 o -2 20 2 95.67 92.40 8.29 o -1 20 2 409.03 399.36 22.94 o 0 20 2 241.21 286.80 22.45 o 1 20 2 274.26 289.74 21.47 o 2 20 2 109.17 98.59 11.22 o 3 20 2 780.80 788.56 26.33 o 4 20 2 345.80 328.29 13.10 o 5 20 2 874.96 786.11 19.68 o 6 20 2 120.03 129.00 12.63 o 7 20 2 3.82 14.81 12.81 o 8 20 2 93.72 52.05 13.33 o 9 20 2 24.25 11.76 20.27 o 10 20 2 37.35 45.53 27.79 o 11 20 2 81.40 41.51 39.73 o -11 21 2 245.85 274.32 76.57 o -10 21 2 1330.03 1370.49 96.59 o -9 21 2 114.46 141.20 28.77 o -8 21 2 374.51 393.55 23.11 o -7 21 2 54.51 38.12 22.92 o -6 21 2 847.09 840.77 25.12 o -5 21 2 214.98 246.53 17.58 o -4 21 2 451.38 452.88 23.43 o -3 21 2 95.28 107.15 8.12 o -2 21 2 0.34 2.32 5.89 o -1 21 2 1103.74 956.06 40.00 o 1 21 2 5.16 0.91 6.79 o 2 21 2 61.79 47.63 9.84 o 3 21 2 322.20 266.56 18.55 o 4 21 2 213.85 219.65 12.74 o 5 21 2 32.34 38.24 9.74 o 6 21 2 501.81 484.25 17.34 o 7 21 2 2050.42 2044.45 46.20 o 8 21 2 2.95 -11.58 16.64 o 9 21 2 12.21 -5.53 32.20 o 10 21 2 0.76 -11.16 62.44 o -11 22 2 15.34 17.04 28.95 o -10 22 2 1074.96 1080.76 52.20 o -9 22 2 154.12 94.40 20.96 o -8 22 2 264.34 195.27 21.25 o -7 22 2 166.26 134.29 23.90 o -6 22 2 242.22 214.66 17.08 o -5 22 2 170.62 162.03 14.13 o -4 22 2 301.68 286.63 16.59 o -3 22 2 15.25 24.96 14.16 o -2 22 2 4877.10 4928.32 104.38 o -1 22 2 189.37 230.23 23.43 o 1 22 2 22.46 13.67 13.67 o 2 22 2 297.93 263.14 19.02 o 3 22 2 729.61 672.49 20.74 o 4 22 2 1.91 1.13 10.00 o 5 22 2 1514.27 1381.73 32.72 o 6 22 2 13.36 7.41 11.66 o 7 22 2 481.31 465.59 21.35 o 8 22 2 103.94 90.15 19.57 o 9 22 2 452.30 435.04 34.14 o 10 22 2 172.87 232.96 33.28 o -10 23 2 442.72 403.24 37.50 o -9 23 2 69.30 48.65 22.64 o -8 23 2 1186.26 1189.29 34.71 o -7 23 2 855.78 822.32 35.61 o -6 23 2 26.46 45.22 17.08 o -5 23 2 266.97 270.04 15.83 o -4 23 2 272.62 259.18 14.44 o -3 23 2 942.99 920.63 20.36 o -2 23 2 347.47 393.52 12.41 o -1 23 2 1018.50 942.46 29.64 o 0 23 2 2772.40 2819.38 109.26 o 2 23 2 1409.27 1373.73 32.12 o 3 23 2 20.38 17.04 13.16 o 4 23 2 1169.61 1001.81 24.81 o 5 23 2 757.06 759.40 22.42 o 6 23 2 987.89 938.56 23.67 o 7 23 2 161.25 130.99 15.13 o 8 23 2 27.87 40.70 15.69 o 9 23 2 23.81 34.35 32.69 o 10 23 2 88.04 125.77 38.86 o -10 24 2 144.41 145.31 27.49 o -9 24 2 538.63 440.72 61.94 o -8 24 2 56.23 56.92 22.71 o -7 24 2 17.28 19.88 28.30 o -6 24 2 59.46 78.78 12.20 o -5 24 2 1471.77 1412.64 33.08 o -4 24 2 327.91 320.33 23.41 o -3 24 2 219.22 218.86 14.14 o -2 24 2 46.39 36.54 6.77 o -1 24 2 52.63 53.67 14.65 o 1 24 2 497.51 457.62 20.00 o 2 24 2 699.08 705.08 18.62 o 3 24 2 46.97 49.21 10.00 o 4 24 2 562.29 570.50 17.58 o 5 24 2 48.48 61.69 20.98 o 6 24 2 126.02 97.28 16.10 o 7 24 2 425.88 408.85 21.35 o 8 24 2 110.53 81.56 20.27 o 9 24 2 108.32 121.38 28.79 o 10 24 2 38.79 97.39 43.90 o -10 25 2 17.40 28.41 26.79 o -9 25 2 59.11 81.30 30.24 o -8 25 2 13.44 -15.27 19.43 o -7 25 2 251.88 219.30 18.74 o -6 25 2 236.14 182.09 22.92 o -5 25 2 121.06 112.91 14.63 o -4 25 2 63.76 65.64 11.36 o -3 25 2 162.45 167.81 11.72 o -2 25 2 154.63 155.45 9.56 o -1 25 2 170.99 166.81 17.55 o 1 25 2 1364.70 1324.82 53.67 o 2 25 2 23.68 22.86 10.47 o 3 25 2 19.64 32.80 9.67 o 4 25 2 337.15 353.92 16.59 o 5 25 2 62.59 33.81 11.92 o 6 25 2 47.19 34.27 12.88 o 7 25 2 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