data_2241428 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.6408 _cell_length_b 12.9891 _cell_length_c 16.8190 _exptl_crystal_F_000 1424.00 _reflns_d_resolution_high 0.8281 _cod_data_source_file pk25691sup2.hkl _cod_data_source_block 1 _shelx_title ' b12k_61 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 360.32 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 129830.71 136786.58 3530.59 o 4 0 0 7072.73 6565.30 262.55 o 6 0 0 643.50 206.03 260.24 o 8 0 0 11679.30 11126.16 502.54 o 10 0 0 7104.19 6746.52 405.92 o 12 0 0 8991.33 8122.25 593.02 o 14 0 0 8755.44 9226.64 689.42 o 16 0 0 2757.90 2733.17 606.27 o 2 1 0 27241.69 27687.97 576.74 o 4 1 0 11047.00 11988.61 266.16 o 6 1 0 125.00 152.54 70.23 o 8 1 0 2687.44 2549.07 131.12 o 10 1 0 6855.87 6791.07 352.34 o 12 1 0 4086.98 4407.97 319.42 o 14 1 0 498.12 258.13 222.41 o 16 1 0 609.31 402.64 265.50 o 0 2 0 3077.40 2887.40 107.92 o 2 2 0 18370.17 18588.88 431.42 o 4 2 0 314.91 306.20 70.77 o 6 2 0 5110.09 5027.90 217.97 o 8 2 0 9181.07 8644.65 294.93 o 10 2 0 157.20 116.45 100.83 o 12 2 0 1559.80 1247.06 222.47 o 14 2 0 16.31 -49.08 209.29 o 16 2 0 1623.36 1448.57 304.65 o 2 3 0 66131.34 64486.20 1592.15 o 4 3 0 29699.43 29589.02 777.67 o 6 3 0 1482.51 1137.22 142.86 o 8 3 0 36.97 6.52 120.64 o 10 3 0 612.71 502.34 132.09 o 12 3 0 1045.49 1189.72 184.01 o 14 3 0 5745.12 5998.37 404.45 o 16 3 0 10650.58 11921.42 605.31 o 0 4 0 8966.13 8652.19 346.45 o 2 4 0 745.66 794.10 114.18 o 4 4 0 17668.65 17572.97 503.90 o 6 4 0 7113.83 6721.22 293.94 o 8 4 0 2197.11 2100.36 237.02 o 10 4 0 112.82 -99.56 124.35 o 12 4 0 236.40 174.73 159.38 o 14 4 0 51.43 297.67 214.90 o 16 4 0 84.38 105.22 316.82 o 2 5 0 10551.61 9947.49 312.55 o 4 5 0 44.91 -111.35 111.35 o 6 5 0 9.67 28.37 101.38 o 8 5 0 4545.48 4487.83 248.22 o 10 5 0 6249.51 7148.86 310.04 o 12 5 0 1229.72 1615.25 274.47 o 14 5 0 26.42 -213.40 271.37 o 16 5 0 1040.28 1253.81 619.82 o 0 6 0 52072.75 51050.77 1996.68 o 2 6 0 40847.25 38553.24 951.92 o 4 6 0 4429.02 3518.98 314.34 o 6 6 0 614.63 843.31 174.69 o 8 6 0 2289.37 2099.35 197.04 o 10 6 0 2138.76 2222.69 338.57 o 12 6 0 2223.00 1928.82 290.08 o 14 6 0 4617.29 5306.59 427.13 o 16 6 0 685.79 348.00 296.11 o 2 7 0 4294.57 4090.29 160.49 o 4 7 0 344.51 472.65 187.75 o 6 7 0 7972.81 7725.10 350.24 o 8 7 0 5961.23 5835.15 306.00 o 10 7 0 141.36 -35.17 244.26 o 12 7 0 985.07 1083.20 272.88 o 14 7 0 877.10 606.96 267.81 o 0 8 0 40132.09 41191.87 1420.51 o 2 8 0 19893.16 19560.38 473.62 o 4 8 0 1283.06 1092.28 227.88 o 6 8 0 4169.92 4664.80 323.17 o 8 8 0 1600.20 1972.80 296.65 o 10 8 0 1032.30 1119.69 217.81 o 12 8 0 470.58 862.16 348.50 o 14 8 0 498.39 81.84 398.02 o 2 9 0 1277.56 1388.35 128.86 o 4 9 0 9328.62 8594.43 363.23 o 6 9 0 6697.59 6626.63 629.23 o 8 9 0 511.72 725.63 226.38 o 10 9 0 536.41 592.94 335.44 o 12 9 0 1348.81 799.07 395.60 o 14 9 0 3322.22 3428.78 557.85 o 0 10 0 455.44 721.15 178.72 o 2 10 0 201.64 387.98 178.46 o 4 10 0 3720.51 3862.04 254.22 o 6 10 0 5161.99 4867.56 420.15 o 8 10 0 155.57 -162.73 278.39 o 10 10 0 149.43 96.85 225.72 o 12 10 0 464.76 22.11 695.37 o 2 11 0 3799.88 3881.63 247.61 o 4 11 0 860.85 1177.80 154.33 o 6 11 0 15.63 -93.88 199.11 o 8 11 0 22.10 240.62 201.47 o 10 11 0 6.79 -32.98 221.30 o 12 11 0 37.22 -68.97 278.71 o 0 12 0 4334.11 4196.44 385.33 o 2 12 0 11190.96 12140.80 475.75 o 4 12 0 8544.54 8226.80 424.80 o 6 12 0 1652.64 1428.78 202.89 o 8 12 0 43.91 -159.21 198.94 o 10 12 0 1081.60 1196.06 324.97 o 2 13 0 124.37 115.37 190.22 o 4 13 0 6.89 264.12 151.19 o 6 13 0 515.11 561.85 155.63 o 8 13 0 9.30 21.28 203.74 o 0 14 0 4381.15 4594.01 442.85 o 2 14 0 2349.94 2648.75 301.12 o 4 14 0 1371.75 1166.52 208.35 o 6 14 0 50.34 -137.09 166.69 o 2 15 0 61.17 -120.00 226.57 o 4 15 0 218.72 1.28 211.41 o 1 1 1 57799.68 61638.10 877.09 o 2 1 1 1436.21 1655.19 53.29 o 3 1 1 10508.71 10189.72 167.35 o 4 1 1 14.23 47.70 44.65 o 5 1 1 739.76 574.13 51.95 o 6 1 1 61.90 -21.33 50.27 o 7 1 1 7173.05 7045.89 147.76 o 8 1 1 2713.92 2545.55 90.59 o 9 1 1 3473.98 3328.38 126.06 o 10 1 1 11049.97 11245.11 261.38 o 11 1 1 3021.91 3050.31 162.77 o 12 1 1 2111.12 2087.68 179.46 o 13 1 1 3659.56 3714.19 235.39 o 14 1 1 11.09 -149.69 149.69 o 15 1 1 2087.10 2848.62 297.35 o 16 1 1 60.73 214.69 184.20 o 17 1 1 157.31 94.54 200.18 o 0 2 1 11269.28 11248.03 233.32 o 1 2 1 2460.78 2513.55 67.73 o 2 2 1 807.26 986.86 53.05 o 3 2 1 19272.78 19253.89 321.46 o 4 2 1 567.37 742.95 79.77 o 5 2 1 14618.53 14074.58 245.19 o 6 2 1 3421.70 3264.01 104.35 o 7 2 1 8341.26 8183.70 159.54 o 8 2 1 7254.70 7230.87 163.09 o 9 2 1 3732.74 3687.57 117.88 o 10 2 1 61.07 23.49 74.95 o 11 2 1 5924.87 5949.82 179.25 o 12 2 1 20.91 24.92 128.77 o 13 2 1 293.72 177.58 163.90 o 14 2 1 27.80 -145.92 145.92 o 15 2 1 2485.00 2655.69 229.54 o 16 2 1 497.46 561.63 187.01 o 17 2 1 3617.66 4056.38 300.91 o 1 3 1 11171.55 11468.50 224.62 o 2 3 1 16034.67 16770.06 344.67 o 3 3 1 728.89 667.01 65.18 o 4 3 1 2858.95 2957.38 101.60 o 5 3 1 120.11 131.34 62.24 o 6 3 1 1567.94 1715.14 108.69 o 7 3 1 41.26 19.43 71.71 o 8 3 1 92.99 159.94 71.41 o 9 3 1 2585.43 2718.66 104.07 o 10 3 1 67.05 -26.62 75.61 o 11 3 1 126.78 194.73 103.35 o 12 3 1 206.46 213.41 123.11 o 13 3 1 81.96 74.69 146.13 o 14 3 1 41.65 290.40 169.08 o 15 3 1 431.06 271.36 165.44 o 16 3 1 28.07 -24.85 178.70 o 17 3 1 56.27 128.44 202.09 o 0 4 1 26300.85 25288.30 539.09 o 1 4 1 16761.05 16782.61 270.35 o 2 4 1 2863.59 2860.57 111.23 o 3 4 1 40942.10 40779.12 765.82 o 4 4 1 2002.59 2170.04 103.16 o 5 4 1 6402.89 6233.14 177.12 o 6 4 1 11458.22 11526.83 271.79 o 7 4 1 2641.47 2897.48 171.88 o 8 4 1 24527.79 23463.00 473.38 o 9 4 1 177.72 136.71 82.57 o 10 4 1 3062.08 3113.36 128.60 o 11 4 1 127.57 188.68 112.24 o 12 4 1 539.30 479.53 135.15 o 13 4 1 3803.50 3740.93 234.79 o 14 4 1 144.92 -124.87 168.41 o 15 4 1 5236.16 6046.00 333.16 o 16 4 1 180.04 56.52 191.50 o 17 4 1 5326.67 6460.56 399.99 o 1 5 1 28104.76 27554.39 415.51 o 2 5 1 132.48 148.74 57.74 o 3 5 1 27300.25 26470.75 548.71 o 4 5 1 2903.96 2507.92 122.04 o 5 5 1 5869.21 5431.38 191.38 o 6 5 1 1706.03 1427.00 108.78 o 7 5 1 5315.05 5336.93 205.22 o 8 5 1 1172.37 1229.81 124.97 o 9 5 1 6028.16 6344.40 255.69 o 10 5 1 76.56 29.59 96.15 o 11 5 1 528.32 673.27 137.17 o 12 5 1 2909.24 3075.00 172.42 o 13 5 1 668.15 631.76 176.69 o 14 5 1 1481.45 1522.78 212.61 o 15 5 1 767.24 687.90 216.54 o 16 5 1 535.84 492.79 215.83 o 0 6 1 4.61 -67.83 67.83 o 1 6 1 560.97 660.60 67.41 o 2 6 1 126.35 71.53 85.22 o 3 6 1 1223.80 1349.20 99.76 o 4 6 1 7100.99 7485.32 223.15 o 5 6 1 21.13 -6.38 73.56 o 6 6 1 25.23 62.97 81.95 o 7 6 1 1296.71 1457.03 130.63 o 8 6 1 88.04 -48.31 89.17 o 9 6 1 2599.15 2419.47 166.44 o 10 6 1 404.22 655.66 197.50 o 11 6 1 288.19 349.90 136.54 o 12 6 1 71.16 -145.42 145.42 o 13 6 1 382.69 258.71 169.94 o 14 6 1 3.74 -70.91 165.07 o 15 6 1 358.99 499.54 228.92 o 16 6 1 315.65 664.76 255.37 o 1 7 1 51417.59 49342.54 804.41 o 2 7 1 287.48 363.07 57.09 o 3 7 1 11147.90 10389.12 255.25 o 4 7 1 230.17 158.76 83.02 o 5 7 1 1711.99 1779.62 153.74 o 6 7 1 3.30 -96.07 96.07 o 7 7 1 44.55 -85.16 85.16 o 8 7 1 1967.06 2238.76 147.74 o 9 7 1 881.34 1069.57 130.42 o 10 7 1 6893.31 7616.06 366.61 o 11 7 1 5463.37 4802.37 294.32 o 12 7 1 528.01 681.29 160.92 o 13 7 1 5672.35 6006.64 308.30 o 14 7 1 7.29 42.01 201.51 o 15 7 1 1948.78 2197.58 244.30 o 0 8 1 2010.14 2291.56 261.76 o 1 8 1 71.30 26.90 58.75 o 2 8 1 4858.66 4668.11 127.23 o 3 8 1 9.68 -75.73 75.73 o 4 8 1 1836.92 1756.70 156.75 o 5 8 1 731.85 835.69 157.80 o 6 8 1 704.33 639.07 114.55 o 7 8 1 1825.41 2213.60 165.28 o 8 8 1 7.37 -33.90 98.38 o 9 8 1 3351.32 3285.92 186.05 o 10 8 1 818.35 912.89 227.38 o 11 8 1 1749.22 2335.16 267.97 o 12 8 1 2031.94 1776.96 319.69 o 13 8 1 1668.80 1709.86 245.30 o 14 8 1 277.48 40.96 255.04 o 15 8 1 646.99 944.66 295.21 o 1 9 1 30.01 -26.53 63.39 o 2 9 1 3099.22 3152.02 118.56 o 3 9 1 732.06 659.47 78.08 o 4 9 1 356.00 334.16 87.32 o 5 9 1 8.92 -42.06 80.96 o 6 9 1 1135.28 1346.65 171.91 o 7 9 1 1718.48 1669.21 175.40 o 8 9 1 170.64 55.54 121.53 o 9 9 1 281.60 474.01 142.74 o 10 9 1 579.66 602.19 162.43 o 11 9 1 200.47 473.43 189.07 o 12 9 1 14.92 26.65 220.53 o 13 9 1 105.46 32.27 314.45 o 14 9 1 100.48 -199.32 207.27 o 0 10 1 296.16 564.47 124.90 o 1 10 1 935.96 977.24 98.26 o 2 10 1 16.31 51.44 75.59 o 3 10 1 8078.86 8106.07 231.22 o 4 10 1 2681.75 2896.09 144.22 o 5 10 1 10739.08 10918.20 377.01 o 6 10 1 4453.69 4363.82 210.24 o 7 10 1 1016.94 812.81 165.59 o 8 10 1 1219.45 1352.11 190.47 o 9 10 1 15.65 -144.52 144.52 o 10 10 1 231.35 247.36 190.52 o 11 10 1 49.65 12.41 158.77 o 12 10 1 218.86 -177.66 292.14 o 13 10 1 1041.26 1005.84 699.58 o 1 11 1 742.59 772.68 106.65 o 2 11 1 203.96 285.21 107.92 o 3 11 1 1999.03 2155.84 154.21 o 4 11 1 839.50 717.59 98.11 o 5 11 1 7612.15 7429.50 230.63 o 6 11 1 903.00 729.02 160.37 o 7 11 1 2896.76 3439.19 226.61 o 8 11 1 42.62 -119.44 119.44 o 9 11 1 330.29 396.48 237.27 o 10 11 1 249.01 414.37 185.31 o 11 11 1 34.53 39.79 173.33 o 12 11 1 119.41 -137.15 243.81 o 0 12 1 377.28 311.92 134.28 o 1 12 1 490.60 277.33 102.18 o 2 12 1 331.04 261.53 120.02 o 3 12 1 121.47 105.79 99.64 o 4 12 1 37.53 -91.97 91.97 o 5 12 1 77.29 108.94 97.25 o 6 12 1 25.72 78.62 116.08 o 7 12 1 183.80 334.59 134.47 o 8 12 1 389.85 -41.97 144.70 o 9 12 1 191.57 133.21 171.63 o 10 12 1 179.38 59.91 179.45 o 11 12 1 83.01 -74.87 236.07 o 1 13 1 6956.74 7046.92 256.22 o 2 13 1 375.27 189.70 126.12 o 3 13 1 5421.00 5801.42 264.15 o 4 13 1 470.44 481.58 115.18 o 5 13 1 225.19 392.85 125.95 o 6 13 1 386.18 475.28 117.25 o 7 13 1 93.00 79.72 134.46 o 8 13 1 1221.53 899.91 171.52 o 9 13 1 121.13 -30.51 199.70 o 0 14 1 149.92 27.97 170.81 o 1 14 1 57.03 -144.48 144.48 o 2 14 1 1254.05 1567.58 196.77 o 3 14 1 506.36 366.03 122.47 o 4 14 1 755.36 636.68 147.63 o 5 14 1 35.79 50.31 105.26 o 6 14 1 3.12 -27.35 123.27 o 7 14 1 1079.55 968.19 141.29 o 1 15 1 403.28 71.31 121.30 o 2 15 1 55.94 -20.15 123.85 o 3 15 1 162.30 181.91 163.84 o 4 15 1 119.63 -83.86 112.75 o 5 15 1 68.01 119.13 126.92 o 0 0 2 43693.46 45664.07 1329.76 o 1 0 2 5124.47 5273.66 117.69 o 2 0 2 27510.64 28120.66 495.16 o 3 0 2 4005.52 4773.50 124.16 o 4 0 2 5033.56 4801.95 123.78 o 5 0 2 17781.60 18951.53 391.94 o 6 0 2 442.55 374.39 100.89 o 7 0 2 1860.71 1950.30 162.02 o 8 0 2 2139.59 1998.14 170.10 o 9 0 2 29257.05 28650.43 807.87 o 10 0 2 1520.07 1509.02 186.61 o 11 0 2 29718.88 27365.16 975.30 o 12 0 2 6065.24 6345.30 411.51 o 13 0 2 1842.33 1846.59 265.55 o 14 0 2 2516.09 2846.68 318.59 o 15 0 2 228.66 9.61 231.34 o 16 0 2 37.14 -62.70 374.07 o 17 0 2 219.26 413.25 321.71 o 1 1 2 64172.66 66686.80 850.65 o 2 1 2 2197.16 2370.69 63.00 o 3 1 2 4173.99 4404.42 97.74 o 4 1 2 24.59 -52.00 52.00 o 5 1 2 455.64 318.21 45.93 o 6 1 2 767.14 854.98 63.80 o 7 1 2 1055.14 1081.34 72.22 o 8 1 2 25.35 99.07 54.87 o 9 1 2 4840.81 4663.77 141.57 o 10 1 2 35.34 -84.59 84.59 o 11 1 2 4058.44 3895.65 250.06 o 12 1 2 86.24 352.96 150.79 o 13 1 2 1634.91 1443.82 187.36 o 14 1 2 604.13 592.16 163.64 o 15 1 2 238.65 329.30 177.23 o 16 1 2 111.91 -169.24 169.24 o 17 1 2 27.59 18.64 202.75 o 0 2 2 1257.73 1370.00 52.79 o 1 2 2 7159.38 7256.15 124.39 o 2 2 2 5738.48 5888.82 116.23 o 3 2 2 1198.59 1314.66 63.13 o 4 2 2 29652.12 30016.25 475.59 o 5 2 2 165.74 195.80 56.02 o 6 2 2 1619.94 1994.82 95.91 o 7 2 2 458.38 215.38 65.62 o 8 2 2 74.69 7.76 58.66 o 9 2 2 1256.28 1190.87 83.25 o 10 2 2 913.72 881.14 88.70 o 11 2 2 2423.40 2446.12 129.80 o 12 2 2 1819.85 1803.08 182.68 o 13 2 2 876.29 587.98 213.65 o 14 2 2 396.84 121.44 168.90 o 15 2 2 981.15 955.67 192.37 o 16 2 2 3.18 -178.26 178.26 o 17 2 2 2182.16 2361.07 254.77 o 1 3 2 15224.73 14739.37 238.63 o 2 3 2 14061.00 14781.63 264.82 o 3 3 2 10266.03 9911.86 230.89 o 4 3 2 24503.19 24999.71 478.21 o 5 3 2 27293.01 25932.75 466.66 o 6 3 2 2592.04 2359.83 109.12 o 7 3 2 56128.38 54224.24 929.65 o 8 3 2 2599.34 2772.91 117.00 o 9 3 2 14320.01 14360.92 256.15 o 10 3 2 12.33 12.15 82.37 o 11 3 2 478.46 421.15 111.21 o 12 3 2 375.68 238.62 126.02 o 13 3 2 2298.77 2046.40 169.62 o 14 3 2 3674.45 3623.01 251.47 o 15 3 2 4.93 -177.80 177.80 o 16 3 2 4889.37 4829.69 349.92 o 17 3 2 447.30 343.54 213.24 o 0 4 2 7702.18 7326.12 193.33 o 1 4 2 24.52 -26.84 39.41 o 2 4 2 643.93 679.99 55.86 o 3 4 2 8868.13 9597.62 229.52 o 4 4 2 11571.56 12075.46 255.63 o 5 4 2 3914.60 3665.71 147.43 o 6 4 2 798.98 832.17 90.19 o 7 4 2 1500.55 1399.55 98.37 o 8 4 2 79.15 -45.38 76.28 o 9 4 2 1191.17 1191.89 105.18 o 10 4 2 893.62 846.73 105.00 o 11 4 2 58.01 130.12 108.20 o 12 4 2 2.00 81.25 132.89 o 13 4 2 1123.73 991.54 178.98 o 14 4 2 1.05 -32.95 181.31 o 15 4 2 3138.06 3342.38 280.26 o 16 4 2 0.20 -125.09 200.90 o 17 4 2 408.98 -665.81 665.81 o 1 5 2 23199.76 22141.62 343.67 o 2 5 2 15.42 -44.14 44.14 o 3 5 2 667.36 494.00 65.79 o 4 5 2 1484.97 1522.64 147.68 o 5 5 2 86.94 -65.41 65.41 o 6 5 2 11209.64 11387.91 292.19 o 7 5 2 3807.64 4044.23 157.13 o 8 5 2 89.92 -14.11 89.75 o 9 5 2 3144.89 3432.22 159.37 o 10 5 2 102.83 75.31 114.93 o 11 5 2 141.82 13.53 117.98 o 12 5 2 60.75 -77.92 103.79 o 13 5 2 51.58 144.90 143.80 o 14 5 2 866.70 895.28 197.20 o 15 5 2 235.86 273.78 263.08 o 16 5 2 553.36 767.87 205.79 o 0 6 2 13076.41 12955.67 359.99 o 1 6 2 704.46 874.54 109.24 o 2 6 2 21597.01 20866.55 346.17 o 3 6 2 6749.38 6987.06 188.60 o 4 6 2 4997.09 4674.90 170.15 o 5 6 2 1018.13 890.73 97.85 o 6 6 2 1223.17 1433.49 116.25 o 7 6 2 3705.09 3725.55 167.08 o 8 6 2 464.98 588.13 102.70 o 9 6 2 16517.73 16349.06 417.49 o 10 6 2 1795.41 2291.80 178.16 o 11 6 2 11457.12 11656.15 367.60 o 12 6 2 3837.73 4149.96 210.55 o 13 6 2 3020.10 3391.62 228.88 o 14 6 2 1291.42 995.81 255.08 o 15 6 2 180.73 502.20 222.14 o 16 6 2 342.96 239.63 232.06 o 1 7 2 276.04 168.54 65.34 o 2 7 2 902.07 802.85 67.50 o 3 7 2 3396.49 3032.63 125.44 o 4 7 2 33.49 75.42 65.66 o 5 7 2 823.41 842.62 97.97 o 6 7 2 19.61 20.02 85.82 o 7 7 2 511.24 579.03 117.17 o 8 7 2 1328.50 1367.03 139.18 o 9 7 2 261.32 154.85 115.21 o 10 7 2 2518.99 2251.33 197.11 o 11 7 2 476.42 344.60 174.14 o 12 7 2 109.24 -20.21 169.49 o 13 7 2 1355.11 1297.23 176.30 o 14 7 2 8.43 -19.32 178.70 o 15 7 2 0.05 111.28 198.52 o 0 8 2 3104.24 3121.39 164.41 o 1 8 2 1089.12 1100.65 90.49 o 2 8 2 3279.54 3096.01 110.55 o 3 8 2 648.95 780.82 72.15 o 4 8 2 747.88 650.31 89.98 o 5 8 2 62.18 -60.30 72.99 o 6 8 2 8.17 33.15 167.52 o 7 8 2 332.63 138.61 115.85 o 8 8 2 17.88 76.79 104.08 o 9 8 2 3024.83 3197.72 204.98 o 10 8 2 3.00 19.38 137.26 o 11 8 2 1853.73 2293.09 229.86 o 12 8 2 1081.88 1246.60 229.90 o 13 8 2 619.94 469.94 191.97 o 14 8 2 744.56 548.57 183.90 o 15 8 2 429.72 191.44 197.46 o 1 9 2 3001.12 2948.25 125.07 o 2 9 2 2190.20 2302.65 119.96 o 3 9 2 7923.52 8091.52 197.69 o 4 9 2 1642.49 1715.28 97.14 o 5 9 2 13783.75 14247.04 346.08 o 6 9 2 2158.63 2237.98 160.80 o 7 9 2 7511.32 7747.12 339.13 o 8 9 2 40.67 72.28 135.00 o 9 9 2 2884.70 2647.25 210.78 o 10 9 2 88.81 -67.71 173.26 o 11 9 2 1007.74 1394.86 226.54 o 12 9 2 391.09 144.40 261.28 o 13 9 2 3.34 80.18 234.22 o 14 9 2 392.51 746.71 237.77 o 0 10 2 20.57 133.28 150.03 o 1 10 2 235.32 144.95 78.19 o 2 10 2 282.11 37.24 82.21 o 3 10 2 6.27 -69.81 69.81 o 4 10 2 19.63 114.97 83.07 o 5 10 2 3055.15 2953.22 152.02 o 6 10 2 398.60 319.01 129.60 o 7 10 2 1018.70 1312.69 159.11 o 8 10 2 1210.85 1304.62 170.65 o 9 10 2 3.11 -117.30 117.30 o 10 10 2 2.39 -141.04 149.05 o 11 10 2 64.23 -28.42 181.50 o 12 10 2 79.91 -71.62 190.61 o 13 10 2 592.51 -38.27 426.48 o 1 11 2 2038.63 2099.41 140.24 o 2 11 2 403.87 169.89 90.88 o 3 11 2 2140.32 1935.59 174.86 o 4 11 2 2075.59 2000.56 137.43 o 5 11 2 2099.90 2119.47 123.23 o 6 11 2 466.63 495.40 116.26 o 7 11 2 3292.18 3780.45 287.79 o 8 11 2 56.92 116.22 154.57 o 9 11 2 1580.81 1688.67 227.00 o 10 11 2 49.72 -182.84 191.09 o 11 11 2 138.02 211.03 179.56 o 12 11 2 187.76 101.70 228.49 o 0 12 2 6460.39 6841.57 340.07 o 1 12 2 5.09 18.33 124.53 o 2 12 2 3043.05 3282.80 172.00 o 3 12 2 52.47 17.07 114.39 o 4 12 2 1041.30 856.19 157.66 o 5 12 2 1186.29 1375.27 126.01 o 6 12 2 337.28 358.46 118.79 o 7 12 2 1208.78 1446.82 155.11 o 8 12 2 415.95 434.08 151.55 o 9 12 2 556.73 461.04 151.75 o 10 12 2 152.03 388.90 249.08 o 11 12 2 612.01 729.90 215.40 o 1 13 2 106.91 3.25 99.84 o 2 13 2 44.22 -2.18 101.91 o 3 13 2 900.52 810.47 123.41 o 4 13 2 78.04 82.72 96.12 o 5 13 2 391.79 105.62 115.05 o 6 13 2 135.71 113.29 106.33 o 7 13 2 17.60 103.86 112.49 o 8 13 2 136.00 215.21 142.08 o 9 13 2 39.00 30.84 159.19 o 0 14 2 2731.21 3164.62 271.54 o 1 14 2 349.19 355.37 132.82 o 2 14 2 924.57 741.49 141.26 o 3 14 2 569.83 637.89 124.87 o 4 14 2 6.62 -119.77 119.77 o 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