#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:46:23 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181915 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/14/2241435.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241435 _cell_angle_alpha 73.110 _cell_angle_beta 75.530 _cell_angle_gamma 89.010 _cell_length_a 9.8506 _cell_length_b 11.0603 _cell_length_c 17.8574 _exptl_crystal_F_000 892.00 _reflns_d_resolution_high 0.7486 _cod_data_source_file pk2570Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Quest15mz239_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 193.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 389.90 371.40 16.11 o 3 0 0 18761.33 19399.09 352.64 o 4 0 0 8895.31 9098.99 176.84 o 5 0 0 89.04 97.56 13.18 o 6 0 0 580.11 638.27 25.38 o 7 0 0 8632.23 8706.93 160.19 o 8 0 0 1276.51 1357.58 37.14 o 9 0 0 420.81 426.17 23.91 o 10 0 0 124.05 143.13 19.15 o 11 0 0 304.20 253.29 19.43 o 12 0 0 14.23 45.55 73.26 o -12 1 0 171.06 197.58 27.26 o -11 1 0 147.01 89.75 19.05 o -10 1 0 128.82 142.03 22.06 o -9 1 0 711.29 792.41 35.38 o -8 1 0 3970.57 3776.25 84.00 o -7 1 0 404.39 327.64 20.70 o -6 1 0 71.36 71.06 10.93 o -5 1 0 1725.70 1547.21 36.49 o -4 1 0 173.94 178.41 13.61 o -3 1 0 954.03 911.87 24.81 o -2 1 0 462.98 402.18 15.20 o -1 1 0 2098.98 2086.47 36.52 o 1 1 0 27.67 -2.91 2.91 o 2 1 0 6155.14 6310.28 213.47 o 3 1 0 19759.54 21323.65 692.20 o 4 1 0 1264.99 1360.07 50.84 o 5 1 0 5152.45 5140.29 146.87 o 6 1 0 1580.97 1733.75 47.98 o 7 1 0 4429.44 4661.70 90.88 o 8 1 0 178.03 154.83 14.10 o 9 1 0 1503.29 1403.87 56.33 o 10 1 0 344.20 339.42 22.32 o 11 1 0 52.44 27.41 46.33 o 12 1 0 262.81 237.11 59.55 o -12 2 0 12.53 6.58 22.12 o -11 2 0 53.95 45.07 21.47 o -10 2 0 187.99 225.73 25.97 o -9 2 0 19.63 11.36 12.21 o -8 2 0 77.31 61.11 12.66 o -7 2 0 133.14 101.15 14.01 o -6 2 0 8.66 9.74 8.48 o -5 2 0 2003.21 1667.95 37.66 o -4 2 0 231.79 171.16 15.67 o -3 2 0 11425.50 11214.35 188.28 o -2 2 0 287.25 286.30 15.95 o -1 2 0 2671.52 2779.37 47.75 o 0 2 0 8312.17 9054.70 157.72 o 1 2 0 9683.86 10311.84 199.88 o 2 2 0 9493.70 11117.78 233.64 o 3 2 0 1080.80 925.66 22.00 o 4 2 0 6380.74 5966.91 96.00 o 5 2 0 2076.03 1813.55 42.39 o 6 2 0 18152.07 18751.69 351.60 o 7 2 0 1508.22 1550.05 41.25 o 8 2 0 1.82 -2.71 21.33 o 9 2 0 2365.92 2386.61 109.55 o 10 2 0 276.73 280.09 56.60 o 11 2 0 2.39 40.58 70.81 o 12 2 0 19.33 176.91 213.40 o -12 3 0 532.49 679.63 46.55 o -11 3 0 1843.55 1991.93 61.94 o -10 3 0 2036.39 2067.41 63.44 o -9 3 0 1.73 17.12 15.19 o -8 3 0 1910.05 1800.43 51.36 o -7 3 0 599.44 588.65 24.79 o -6 3 0 32.77 29.70 9.18 o -5 3 0 282.75 176.30 19.66 o -4 3 0 564.91 494.59 22.77 o -3 3 0 3365.97 3520.15 72.23 o -2 3 0 7523.69 8272.87 131.03 o -1 3 0 81.98 118.23 13.07 o 0 3 0 10.06 -6.60 6.82 o 1 3 0 5488.08 5329.09 97.94 o 2 3 0 45.08 89.50 12.31 o 3 3 0 81.17 77.42 10.33 o 4 3 0 3582.95 3508.69 65.19 o 5 3 0 840.26 747.31 23.95 o 6 3 0 1670.63 1640.11 72.95 o 7 3 0 42.15 26.75 22.48 o 8 3 0 223.54 161.00 38.85 o 9 3 0 57.36 51.78 33.61 o 10 3 0 80.64 61.91 37.92 o 11 3 0 529.15 517.37 81.91 o 12 3 0 7.91 16.22 61.72 o -12 4 0 16.38 64.11 36.12 o -11 4 0 96.20 163.72 30.05 o -10 4 0 6.35 23.58 16.72 o -9 4 0 1068.94 962.16 42.64 o -8 4 0 351.13 272.73 27.32 o -7 4 0 909.76 874.21 35.65 o -6 4 0 3708.53 3229.37 71.51 o -5 4 0 170.85 190.72 16.06 o -4 4 0 281.55 280.41 18.94 o -3 4 0 6.09 20.73 9.88 o -2 4 0 4823.24 4807.12 83.24 o -1 4 0 167.89 165.60 15.14 o 0 4 0 621.23 761.40 25.15 o 1 4 0 642.47 649.33 23.35 o 2 4 0 1428.02 1474.41 36.31 o 3 4 0 6374.91 6314.21 112.70 o 4 4 0 23.24 23.93 8.22 o 5 4 0 5.10 19.56 5.75 o 6 4 0 3545.10 3291.93 111.76 o 7 4 0 1000.16 936.55 60.30 o 8 4 0 544.63 530.26 56.26 o 9 4 0 287.50 275.55 56.30 o 10 4 0 1085.03 1067.56 84.59 o 11 4 0 267.94 313.51 73.67 o -12 5 0 234.96 615.03 78.06 o -11 5 0 893.05 1104.00 49.89 o -10 5 0 79.80 97.00 25.72 o -9 5 0 151.88 160.47 22.58 o -8 5 0 2798.52 2712.40 74.89 o -7 5 0 1125.99 1029.63 47.21 o -6 5 0 156.43 159.16 21.17 o -5 5 0 1757.56 1615.04 44.21 o -4 5 0 2786.47 2764.80 61.91 o -3 5 0 198.90 215.05 19.35 o -2 5 0 5558.86 5161.69 91.33 o -1 5 0 72.30 29.26 10.85 o 0 5 0 0.20 -4.91 9.90 o 1 5 0 4064.87 3760.81 77.86 o 2 5 0 720.66 642.74 23.64 o 3 5 0 2321.30 2288.78 52.01 o 4 5 0 201.94 215.87 18.00 o 5 5 0 921.85 773.12 24.41 o 6 5 0 792.12 815.11 29.41 o 7 5 0 79.91 106.92 30.82 o 8 5 0 124.08 132.99 38.94 o 9 5 0 256.62 344.96 62.54 o 10 5 0 0.50 -1.36 63.56 o 11 5 0 371.87 427.25 85.68 o -11 6 0 462.02 534.88 60.95 o -10 6 0 682.96 763.92 42.40 o -9 6 0 1580.19 1622.28 55.31 o -8 6 0 57.77 65.68 18.48 o -7 6 0 1163.27 1152.80 47.09 o -6 6 0 233.06 252.20 27.88 o -5 6 0 3097.82 2922.49 67.97 o -4 6 0 1991.97 1860.92 50.35 o -3 6 0 18.27 24.78 12.11 o -2 6 0 5.84 10.63 10.81 o -1 6 0 893.09 799.78 30.55 o 0 6 0 5525.46 5412.87 102.33 o 1 6 0 8.42 18.34 10.43 o 2 6 0 47.33 108.98 14.77 o 3 6 0 604.16 616.40 27.09 o 4 6 0 1769.33 1780.40 50.51 o 5 6 0 296.42 238.31 20.26 o 6 6 0 1176.27 1180.78 32.28 o 7 6 0 1903.87 1968.72 90.29 o 8 6 0 122.81 96.26 34.32 o 9 6 0 294.70 313.81 57.38 o 10 6 0 892.44 874.84 89.24 o 11 6 0 0.22 16.43 49.53 o -11 7 0 138.88 647.75 67.34 o -10 7 0 367.30 474.11 40.61 o -9 7 0 80.39 133.54 24.13 o -8 7 0 757.33 682.80 38.91 o -7 7 0 79.71 76.31 17.05 o -6 7 0 895.38 873.92 47.30 o -5 7 0 4596.65 4343.33 93.30 o -4 7 0 5.22 9.71 12.27 o -3 7 0 1159.75 1116.86 40.16 o -2 7 0 8747.73 8383.75 151.78 o -1 7 0 2635.53 2693.22 68.74 o 0 7 0 589.71 600.78 29.74 o 1 7 0 1036.17 1059.62 37.32 o 2 7 0 7456.97 7294.93 134.07 o 3 7 0 172.11 181.02 19.83 o 4 7 0 2980.60 2938.01 63.10 o 5 7 0 1416.17 1465.67 53.37 o 6 7 0 497.42 437.15 22.96 o 7 7 0 361.65 338.89 39.71 o 8 7 0 216.78 169.80 45.59 o 9 7 0 738.25 892.82 78.49 o 10 7 0 0.01 16.73 42.55 o -10 8 0 1165.71 1221.93 53.15 o -9 8 0 64.46 177.99 42.59 o -8 8 0 57.91 125.99 33.18 o -7 8 0 64.85 67.66 17.40 o -6 8 0 489.97 501.55 35.64 o -5 8 0 905.02 752.29 41.60 o -4 8 0 672.98 567.21 33.31 o -3 8 0 3889.22 3659.00 83.88 o -2 8 0 367.26 328.25 27.79 o -1 8 0 591.62 614.36 35.29 o 0 8 0 1923.46 1854.45 53.38 o 1 8 0 3549.89 3523.89 76.14 o 2 8 0 2074.17 2114.15 54.13 o 3 8 0 5.56 6.40 12.34 o 4 8 0 1793.16 1938.76 52.36 o 5 8 0 1263.72 1311.28 43.52 o 6 8 0 1798.77 1677.76 53.63 o 7 8 0 548.21 510.74 30.18 o 8 8 0 459.23 555.10 81.52 o 9 8 0 127.03 120.48 42.95 o 10 8 0 130.06 75.82 99.72 o -10 9 0 160.97 293.29 86.21 o -9 9 0 51.53 62.88 34.98 o -8 9 0 65.26 100.53 25.49 o -7 9 0 240.75 213.89 28.90 o -6 9 0 238.97 230.06 32.91 o -5 9 0 1207.66 1004.11 47.56 o -4 9 0 44.61 38.31 17.26 o -3 9 0 50.51 56.41 19.53 o -2 9 0 68.96 34.02 18.01 o -1 9 0 201.95 132.49 22.97 o 0 9 0 71.37 69.36 19.35 o 1 9 0 96.28 70.20 17.09 o 2 9 0 1108.50 950.30 38.83 o 3 9 0 927.90 934.47 37.83 o 4 9 0 3530.17 3423.12 77.70 o 5 9 0 318.75 336.51 28.08 o 6 9 0 106.08 141.85 37.70 o 7 9 0 10.83 6.82 14.37 o 8 9 0 1625.77 1783.18 111.46 o 9 9 0 3.31 23.00 86.42 o -9 10 0 70.08 176.29 72.57 o -8 10 0 255.87 298.35 37.34 o -7 10 0 13.93 71.14 22.14 o -6 10 0 200.12 206.48 32.40 o -5 10 0 1564.41 1396.29 59.50 o -4 10 0 892.81 797.76 43.31 o -3 10 0 439.19 319.21 34.21 o -2 10 0 4.03 -17.46 17.46 o -1 10 0 32.55 12.19 18.99 o 0 10 0 486.14 434.22 35.70 o 1 10 0 540.77 400.40 34.39 o 2 10 0 291.71 270.19 27.37 o 3 10 0 1152.66 1180.72 44.29 o 4 10 0 2915.95 2870.31 79.29 o 5 10 0 67.19 46.96 17.73 o 6 10 0 151.75 169.64 29.33 o 7 10 0 53.96 13.90 15.72 o -8 11 0 1255.82 1395.62 156.00 o -7 11 0 917.45 957.31 52.37 o -6 11 0 17.19 109.92 35.82 o -5 11 0 14.05 15.81 20.52 o -4 11 0 3473.31 3018.72 92.53 o -3 11 0 0.31 5.57 16.90 o -2 11 0 48.47 -2.92 19.10 o -1 11 0 114.42 62.73 21.01 o 0 11 0 15.27 -12.41 22.68 o 1 11 0 210.81 190.19 25.95 o 2 11 0 123.62 210.73 27.02 o 3 11 0 558.26 562.10 40.57 o 4 11 0 25.82 22.49 19.37 o 5 11 0 60.67 54.03 21.07 o 6 11 0 2.01 -10.77 34.29 o 7 11 0 17.97 -13.61 29.62 o -7 12 0 135.51 590.31 88.40 o -6 12 0 49.10 329.85 61.51 o -5 12 0 468.01 591.33 45.77 o -4 12 0 723.80 733.83 48.90 o -3 12 0 43.55 219.15 50.54 o -2 12 0 821.42 783.04 46.29 o -1 12 0 528.32 502.91 47.75 o 0 12 0 386.67 428.34 39.89 o 1 12 0 3675.85 3549.57 94.11 o 2 12 0 10.88 8.07 19.57 o 3 12 0 777.56 760.79 47.54 o 4 12 0 157.36 137.54 31.22 o 5 12 0 106.43 90.89 28.68 o 6 12 0 311.47 217.21 52.67 o -5 13 0 241.78 590.69 70.01 o -4 13 0 500.61 817.08 74.36 o -3 13 0 55.84 384.01 65.01 o -2 13 0 653.97 803.02 67.73 o -1 13 0 214.48 255.00 42.75 o 0 13 0 106.84 172.14 33.63 o 1 13 0 210.20 234.34 39.15 o 2 13 0 2233.48 2036.52 74.91 o 3 13 0 22.12 5.68 29.34 o 4 13 0 48.62 38.40 38.88 o -2 14 0 67.89 274.74 94.27 o -1 14 0 16.45 133.25 63.02 o 0 14 0 22.81 50.64 56.16 o -3 -13 1 69.70 70.67 54.95 o -2 -13 1 1918.14 1995.90 76.69 o -1 -13 1 25.82 34.44 29.14 o 0 -13 1 243.44 301.15 54.07 o 1 -13 1 235.48 446.64 74.68 o 2 -13 1 930.84 1042.02 56.43 o 3 -13 1 200.53 419.17 57.53 o 4 -13 1 337.07 722.29 66.45 o 5 -13 1 936.36 1243.28 96.30 o -5 -12 1 68.12 58.56 34.91 o -4 -12 1 689.56 813.51 74.10 o -3 -12 1 526.99 391.03 43.52 o -2 -12 1 0.73 17.39 22.18 o -1 -12 1 2773.91 2731.74 80.81 o 0 -12 1 345.01 419.73 44.61 o 1 -12 1 1678.60 1596.93 64.24 o 2 -12 1 495.71 556.81 42.61 o 3 -12 1 463.75 543.59 41.95 o 4 -12 1 814.86 839.33 48.29 o 5 -12 1 831.22 983.68 54.94 o 6 -12 1 429.96 587.84 49.32 o 7 -12 1 88.81 420.74 58.19 o -7 -11 1 183.30 109.85 50.45 o -6 -11 1 80.41 71.34 26.83 o -5 -11 1 6.57 -4.62 26.45 o -4 -11 1 160.54 116.19 25.24 o -3 -11 1 31.69 13.61 19.74 o -2 -11 1 99.55 168.68 32.01 o -1 -11 1 276.01 216.29 29.35 o 0 -11 1 1.62 -7.53 18.56 o 1 -11 1 531.21 461.11 41.00 o 2 -11 1 18.24 7.66 21.21 o 3 -11 1 25.25 61.32 35.60 o 4 -11 1 2170.58 1824.21 66.21 o 5 -11 1 130.25 200.61 34.68 o 6 -11 1 413.60 537.74 40.11 o 7 -11 1 473.57 511.10 42.55 o 8 -11 1 2036.60 1963.25 136.80 o -8 -10 1 161.99 75.72 43.59 o -7 -10 1 170.43 152.43 29.77 o -6 -10 1 98.80 68.72 21.93 o -5 -10 1 768.96 727.15 42.28 o -4 -10 1 4332.97 4365.14 131.04 o -3 -10 1 360.13 363.08 34.34 o -2 -10 1 477.36 433.97 36.11 o -1 -10 1 1040.63 1020.10 46.13 o 0 -10 1 3079.95 2849.12 82.59 o 1 -10 1 493.95 463.00 37.09 o 2 -10 1 65.28 43.44 19.13 o 3 -10 1 2366.11 2121.91 75.49 o 4 -10 1 1250.60 1118.97 48.55 o 5 -10 1 198.82 133.52 25.01 o 6 -10 1 542.65 536.02 37.84 o 7 -10 1 1060.10 1027.28 64.84 o 8 -10 1 37.35 149.12 39.25 o 9 -10 1 41.64 171.11 45.55 o -7 -9 1 394.76 316.73 30.51 o -6 -9 1 33.91 38.88 16.77 o -5 -9 1 37.83 63.46 29.74 o -4 -9 1 825.20 713.88 36.85 o -3 -9 1 308.64 232.57 29.03 o -2 -9 1 245.08 202.04 28.94 o -1 -9 1 585.39 563.95 34.24 o 0 -9 1 68.97 54.12 18.20 o 1 -9 1 186.54 148.71 24.15 o 2 -9 1 436.34 329.61 32.56 o 3 -9 1 551.11 395.81 33.25 o 4 -9 1 155.11 170.92 28.55 o 5 -9 1 2426.78 2137.88 72.94 o 6 -9 1 451.81 347.72 33.61 o 7 -9 1 107.35 114.46 33.01 o 8 -9 1 624.26 559.31 44.59 o 9 -9 1 61.37 132.84 56.91 o 10 -9 1 432.28 517.95 73.47 o -9 -8 1 51.39 86.51 99.72 o -8 -8 1 158.89 311.69 89.24 o -7 -8 1 712.70 712.11 31.66 o -6 -8 1 1933.05 1836.55 59.85 o -5 -8 1 0.90 -4.91 12.89 o -4 -8 1 1447.41 1437.13 47.76 o -3 -8 1 516.42 492.73 30.13 o -2 -8 1 1147.99 1190.05 42.03 o -1 -8 1 641.94 598.49 32.13 o 0 -8 1 7056.13 6944.34 141.37 o 1 -8 1 1931.77 1911.96 58.83 o 2 -8 1 3666.23 3438.87 80.05 o 3 -8 1 2642.47 2396.91 64.74 o 4 -8 1 0.42 -1.62 15.22 o 5 -8 1 129.06 104.59 25.96 o 6 -8 1 295.51 279.60 30.42 o 7 -8 1 179.24 166.32 28.66 o 8 -8 1 1.51 19.10 19.35 o 9 -8 1 1308.57 1337.57 57.52 o 10 -8 1 395.47 423.49 42.95 o -10 -7 1 139.96 102.00 81.91 o -9 -7 1 444.65 450.80 82.68 o -8 -7 1 35.78 48.29 29.30 o -7 -7 1 2077.83 1924.66 60.34 o -6 -7 1 50.81 38.74 11.76 o -5 -7 1 2543.04 2515.93 83.04 o -4 -7 1 449.35 439.88 24.84 o -3 -7 1 299.80 271.43 22.90 o -2 -7 1 1078.60 1082.25 37.15 o -1 -7 1 1701.47 1544.14 45.52 o 0 -7 1 231.27 254.75 24.87 o 1 -7 1 1834.90 1803.82 50.31 o 2 -7 1 8961.27 8366.96 152.13 o 3 -7 1 1724.67 1570.22 48.20 o 4 -7 1 83.81 69.25 16.52 o 5 -7 1 347.19 323.60 30.33 o 6 -7 1 1846.16 1706.74 59.35 o 7 -7 1 726.40 695.04 38.00 o 8 -7 1 248.39 309.39 29.02 o 9 -7 1 183.30 188.28 27.05 o 10 -7 1 74.33 233.11 41.80 o 11 -7 1 39.11 35.52 49.05 o -10 -6 1 300.40 325.24 64.65 o -9 -6 1 103.43 127.29 40.85 o -8 -6 1 578.26 448.08 70.14 o -7 -6 1 1552.46 1526.41 47.31 o -6 -6 1 1506.56 1369.07 35.66 o -5 -6 1 336.60 319.51 25.92 o -4 -6 1 2138.77 2080.36 56.85 o -3 -6 1 436.64 298.95 20.36 o -2 -6 1 662.62 776.04 29.60 o -1 -6 1 21.88 16.97 10.81 o 0 -6 1 9963.63 9673.85 177.44 o 1 -6 1 5.82 -4.93 10.33 o 2 -6 1 993.59 848.99 32.89 o 3 -6 1 494.06 483.51 27.66 o 4 -6 1 844.74 812.25 33.97 o 5 -6 1 1166.59 950.37 36.89 o 6 -6 1 4226.57 4012.83 87.66 o 7 -6 1 3684.36 3258.42 82.73 o 8 -6 1 15.37 8.05 15.39 o 9 -6 1 3549.73 3428.33 85.26 o 10 -6 1 45.11 161.28 45.56 o 11 -6 1 229.98 410.27 64.73 o -11 -5 1 22.71 -0.79 53.71 o -10 -5 1 1.57 -9.43 46.63 o -9 -5 1 391.39 440.30 61.61 o -8 -5 1 1663.37 1562.97 98.41 o -7 -5 1 509.44 483.84 28.41 o -6 -5 1 858.69 825.45 24.40 o -5 -5 1 6.06 4.10 7.55 o -4 -5 1 274.67 214.50 21.72 o -3 -5 1 6092.68 6216.57 154.66 o -2 -5 1 406.63 352.42 19.26 o -1 -5 1 3516.26 3608.99 76.03 o 0 -5 1 93.39 87.00 14.01 o 1 -5 1 7122.61 6383.89 113.92 o 2 -5 1 3267.45 3227.28 67.63 o 3 -5 1 3416.54 3239.57 68.80 o 4 -5 1 5776.34 5341.36 96.49 o 5 -5 1 588.52 636.03 29.04 o 6 -5 1 1661.58 1514.85 42.27 o 7 -5 1 436.73 374.07 34.78 o 8 -5 1 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