data_2241446 _cell_angle_alpha 90.000 _cell_angle_beta 106.725 _cell_angle_gamma 90.000 _cell_length_a 13.1128 _cell_length_b 20.8621 _cell_length_c 17.6284 _exptl_crystal_F_000 2174.00 _reflns_d_resolution_high 0.7691 _cod_data_source_file sj5492Isup2.hkl _cod_data_source_block I _shelx_title ' MNSPD01_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 451.05 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1804.82 1634.32 49.23 o 6 0 0 3658.14 3678.18 110.65 o 8 0 0 241.08 440.40 61.23 o 10 0 0 843.12 924.73 95.48 o 12 0 0 2682.03 2488.19 172.99 o 14 0 0 16.51 -5.70 56.62 o 16 0 0 13.04 16.77 54.55 o 1 1 0 4.81 -3.94 11.64 o 2 1 0 57.29 41.80 10.06 o 3 1 0 5217.21 5070.80 94.84 o 4 1 0 283.65 257.16 19.04 o 5 1 0 7604.54 7591.70 113.60 o 6 1 0 231.07 255.68 17.83 o 7 1 0 7227.01 7264.40 117.16 o 8 1 0 11.06 9.76 15.69 o 9 1 0 3015.90 3068.85 101.88 o 10 1 0 140.81 113.81 32.91 o 11 1 0 482.41 418.45 65.50 o 12 1 0 0.05 10.94 31.79 o 13 1 0 8.12 1.36 43.24 o 14 1 0 4.79 13.05 33.67 o 15 1 0 13.42 36.63 39.30 o 16 1 0 32.02 51.36 47.72 o 1 2 0 1056.72 843.41 23.16 o 2 2 0 8975.13 8736.34 145.56 o 3 2 0 439.10 398.81 37.54 o 4 2 0 9980.32 9358.46 148.37 o 5 2 0 0.52 12.92 8.30 o 6 2 0 4974.72 4741.14 95.59 o 7 2 0 170.21 135.82 16.19 o 8 2 0 3412.75 3532.17 85.61 o 9 2 0 45.10 -0.66 23.72 o 10 2 0 1016.40 903.84 65.72 o 11 2 0 57.38 79.73 34.13 o 12 2 0 1427.49 1306.76 81.02 o 13 2 0 18.80 27.24 33.29 o 14 2 0 94.35 57.02 38.54 o 15 2 0 2.49 -11.18 44.65 o 16 2 0 480.44 723.30 91.88 o 1 3 0 23061.44 21670.23 333.34 o 2 3 0 944.78 1065.36 34.24 o 3 3 0 10127.35 9312.22 130.83 o 4 3 0 1258.13 1140.76 29.21 o 5 3 0 3667.58 3586.14 64.91 o 6 3 0 168.29 163.91 15.01 o 7 3 0 1906.50 1864.42 60.18 o 8 3 0 70.28 59.57 18.76 o 9 3 0 194.21 235.33 56.95 o 10 3 0 157.76 188.05 34.75 o 11 3 0 652.08 653.65 57.84 o 12 3 0 67.35 103.30 36.21 o 13 3 0 260.72 357.14 50.13 o 14 3 0 27.42 -18.82 39.81 o 15 3 0 263.96 184.34 62.23 o 16 3 0 3.69 -24.75 52.50 o 0 4 0 13850.24 14036.35 448.00 o 1 4 0 35.45 69.44 13.29 o 2 4 0 20864.01 19272.69 273.81 o 3 4 0 338.30 338.91 19.77 o 4 4 0 11538.97 10635.21 152.70 o 5 4 0 182.89 162.40 14.69 o 6 4 0 64.39 61.50 11.84 o 7 4 0 1151.61 1194.56 42.62 o 8 4 0 438.85 425.74 33.05 o 9 4 0 379.34 404.22 41.60 o 10 4 0 194.79 192.16 34.48 o 11 4 0 104.51 96.90 32.68 o 12 4 0 811.09 855.23 65.25 o 13 4 0 312.17 402.30 60.81 o 14 4 0 14.33 -36.77 52.47 o 15 4 0 31.47 114.20 51.63 o 16 4 0 3.00 31.16 56.50 o 1 5 0 19476.70 18365.30 293.72 o 2 5 0 134.09 170.10 17.42 o 3 5 0 3163.97 2991.59 59.56 o 4 5 0 13.87 19.91 11.20 o 5 5 0 186.49 282.72 19.91 o 6 5 0 128.85 132.76 17.59 o 7 5 0 1768.66 1733.38 65.03 o 8 5 0 375.13 323.60 30.87 o 9 5 0 906.43 994.41 60.27 o 10 5 0 146.27 134.95 34.90 o 11 5 0 22.65 14.46 27.91 o 12 5 0 336.80 399.78 87.46 o 13 5 0 74.40 55.30 41.95 o 14 5 0 554.69 499.63 83.55 o 15 5 0 15.83 25.57 48.19 o 16 5 0 50.93 13.60 55.02 o 0 6 0 177501.42 178383.73 3744.19 o 1 6 0 312.29 266.10 24.40 o 2 6 0 1293.85 1316.36 39.36 o 3 6 0 1146.88 1020.33 38.66 o 4 6 0 2290.78 2129.88 50.35 o 5 6 0 8472.88 7990.14 116.74 o 6 6 0 230.83 184.42 17.92 o 7 6 0 950.06 999.65 46.61 o 8 6 0 3878.70 3618.31 85.22 o 9 6 0 9.27 32.19 21.53 o 10 6 0 2067.89 2119.83 120.69 o 11 6 0 12.62 80.31 34.92 o 12 6 0 2435.90 2354.71 126.18 o 13 6 0 26.72 -19.83 34.88 o 14 6 0 1140.07 1317.11 106.48 o 15 6 0 3.38 59.12 50.79 o 1 7 0 6758.99 7583.10 126.32 o 2 7 0 2053.67 1761.52 54.50 o 3 7 0 379.02 422.40 27.82 o 4 7 0 240.42 251.39 23.86 o 5 7 0 4.80 9.97 13.45 o 6 7 0 1674.67 1814.66 47.94 o 7 7 0 2882.22 2975.12 72.60 o 8 7 0 2.90 -5.33 18.55 o 9 7 0 572.95 663.16 52.07 o 10 7 0 287.80 272.48 47.09 o 11 7 0 796.44 701.51 73.86 o 12 7 0 217.25 214.72 50.45 o 13 7 0 102.86 45.57 44.47 o 14 7 0 0.06 41.24 44.47 o 15 7 0 253.01 265.70 65.99 o 0 8 0 22962.74 20447.05 476.81 o 1 8 0 135.75 167.78 18.71 o 2 8 0 5613.12 5138.72 98.24 o 3 8 0 417.56 497.84 36.54 o 4 8 0 11716.78 11478.46 189.83 o 5 8 0 968.37 889.25 45.14 o 6 8 0 5740.55 5913.86 98.42 o 7 8 0 41.02 15.57 31.28 o 8 8 0 47.61 32.05 24.46 o 9 8 0 331.56 301.76 39.92 o 10 8 0 764.29 1001.64 77.12 o 11 8 0 187.84 168.61 45.79 o 12 8 0 777.66 733.07 76.87 o 13 8 0 0.34 -35.72 38.95 o 14 8 0 59.60 144.83 51.97 o 15 8 0 39.71 10.60 49.77 o 1 9 0 2.37 4.83 13.16 o 2 9 0 8.15 23.05 18.47 o 3 9 0 1921.41 1996.44 84.09 o 4 9 0 51.00 67.87 18.22 o 5 9 0 268.83 394.41 32.83 o 6 9 0 14.16 7.23 22.69 o 7 9 0 45.96 62.58 24.45 o 8 9 0 186.70 150.88 30.29 o 9 9 0 2450.35 2556.10 118.85 o 10 9 0 205.97 167.60 52.86 o 11 9 0 121.46 85.45 40.39 o 12 9 0 49.41 67.74 44.08 o 13 9 0 41.98 140.58 48.66 o 14 9 0 12.90 9.21 49.62 o 15 9 0 92.95 86.29 56.59 o 0 10 0 673.54 318.41 31.46 o 1 10 0 1867.63 1756.78 52.84 o 2 10 0 82.66 250.58 28.38 o 3 10 0 13.32 40.96 17.97 o 4 10 0 3301.14 3179.34 79.76 o 5 10 0 152.86 152.38 24.06 o 6 10 0 1891.40 1797.97 78.06 o 7 10 0 1373.62 1500.51 80.84 o 8 10 0 514.40 526.93 53.97 o 9 10 0 1147.88 1162.65 95.30 o 10 10 0 1368.60 1380.42 98.46 o 11 10 0 1107.82 944.67 120.23 o 12 10 0 775.79 800.24 105.40 o 13 10 0 30.74 -7.74 43.57 o 14 10 0 333.06 314.32 64.53 o 15 10 0 0.07 -12.75 50.09 o 1 11 0 9859.10 10180.86 174.24 o 2 11 0 178.49 202.09 30.27 o 3 11 0 147.13 125.89 23.99 o 4 11 0 3.51 18.41 18.27 o 5 11 0 4.79 37.35 20.53 o 6 11 0 15.42 33.28 21.94 o 7 11 0 75.06 104.76 33.07 o 8 11 0 244.46 215.38 42.60 o 9 11 0 3941.67 4150.01 132.78 o 10 11 0 90.44 122.34 39.97 o 11 11 0 24.77 61.16 75.37 o 12 11 0 32.60 65.49 50.04 o 13 11 0 62.15 43.66 45.77 o 14 11 0 4.28 0.16 45.70 o 0 12 0 45237.45 46703.93 847.41 o 1 12 0 1429.29 1540.92 58.58 o 2 12 0 12819.75 12774.01 236.17 o 3 12 0 2477.23 2460.67 72.08 o 4 12 0 166.96 120.56 24.72 o 5 12 0 2298.04 2135.88 77.59 o 6 12 0 325.88 327.35 36.39 o 7 12 0 14.39 20.93 29.24 o 8 12 0 98.15 36.46 34.42 o 9 12 0 1595.65 1693.48 97.02 o 10 12 0 177.35 79.96 38.43 o 11 12 0 10.85 44.29 48.28 o 12 12 0 748.74 985.44 130.25 o 13 12 0 36.85 -1.64 49.69 o 14 12 0 108.90 66.56 57.62 o 1 13 0 1075.33 1095.34 53.10 o 2 13 0 44.87 5.55 24.59 o 3 13 0 756.99 993.23 54.31 o 4 13 0 562.98 559.76 43.20 o 5 13 0 74.68 71.57 25.98 o 6 13 0 41.08 29.29 34.17 o 7 13 0 2755.60 2724.75 104.80 o 8 13 0 323.25 382.16 50.68 o 9 13 0 1350.73 1584.84 96.01 o 10 13 0 8.03 5.33 37.02 o 11 13 0 121.44 111.29 53.51 o 12 13 0 268.10 312.17 71.55 o 13 13 0 1.33 73.52 54.79 o 14 13 0 53.23 27.67 61.36 o 0 14 0 6110.33 5609.20 198.62 o 1 14 0 1077.74 1160.52 57.39 o 2 14 0 3168.34 3190.22 86.66 o 3 14 0 149.65 159.65 34.73 o 4 14 0 1023.56 1203.58 88.86 o 5 14 0 147.81 120.89 35.83 o 6 14 0 435.99 320.81 39.68 o 7 14 0 11.79 -23.42 31.09 o 8 14 0 872.56 839.13 90.82 o 9 14 0 67.77 62.01 39.89 o 10 14 0 86.69 66.17 69.65 o 11 14 0 473.32 575.21 135.84 o 12 14 0 562.03 790.77 96.45 o 13 14 0 44.29 45.54 59.60 o 1 15 0 474.44 532.93 41.87 o 2 15 0 814.71 912.11 56.95 o 3 15 0 21.48 -4.66 23.18 o 4 15 0 406.38 505.77 45.69 o 5 15 0 762.64 720.21 52.61 o 6 15 0 326.48 245.59 37.23 o 7 15 0 0.19 -26.28 39.63 o 8 15 0 1291.89 1340.84 89.71 o 9 15 0 351.32 364.44 61.36 o 10 15 0 0.11 -33.36 39.22 o 11 15 0 10.50 19.95 49.86 o 12 15 0 15.34 29.64 51.97 o 13 15 0 12.48 54.89 60.51 o 0 16 0 11117.71 10371.44 316.73 o 1 16 0 543.40 445.63 51.58 o 2 16 0 354.96 339.59 46.05 o 3 16 0 70.77 58.30 26.81 o 4 16 0 1426.84 1298.97 114.96 o 5 16 0 338.08 391.50 42.81 o 6 16 0 1539.13 1560.74 89.76 o 7 16 0 74.84 69.77 35.88 o 8 16 0 543.80 605.14 66.46 o 9 16 0 390.62 492.15 61.33 o 10 16 0 103.72 56.46 44.02 o 11 16 0 427.26 413.04 75.69 o 12 16 0 59.26 90.40 58.24 o 13 16 0 62.36 -19.73 59.52 o 1 17 0 14.82 75.22 36.40 o 2 17 0 509.44 604.94 58.43 o 3 17 0 597.01 547.64 47.82 o 4 17 0 447.40 396.01 42.15 o 5 17 0 999.08 915.31 92.53 o 6 17 0 216.01 187.95 42.32 o 7 17 0 139.89 138.90 40.14 o 8 17 0 128.59 78.42 42.05 o 9 17 0 44.65 24.54 41.63 o 10 17 0 0.32 -18.34 40.35 o 11 17 0 1.64 0.26 50.18 o 12 17 0 119.21 318.58 160.69 o 0 18 0 2961.31 2974.96 197.20 o 1 18 0 100.03 39.81 47.70 o 2 18 0 1076.36 1184.14 87.75 o 3 18 0 99.64 180.85 42.52 o 4 18 0 170.14 108.53 52.42 o 5 18 0 4346.97 4451.68 122.56 o 6 18 0 111.54 91.86 38.61 o 7 18 0 996.12 946.00 78.88 o 8 18 0 64.16 26.31 39.24 o 9 18 0 20.66 77.56 40.84 o 10 18 0 361.93 342.77 58.93 o 11 18 0 195.36 377.96 119.97 o 12 18 0 165.80 125.19 62.45 o 1 19 0 23.12 54.95 40.08 o 2 19 0 810.99 727.09 67.88 o 3 19 0 445.50 411.05 54.41 o 4 19 0 18.42 1.26 34.53 o 5 19 0 1036.69 1101.62 70.57 o 6 19 0 320.86 186.05 46.15 o 7 19 0 9.62 85.65 41.65 o 8 19 0 20.23 66.31 41.11 o 9 19 0 53.33 101.55 45.87 o 10 19 0 117.12 210.20 54.90 o 11 19 0 73.68 91.83 58.56 o 0 20 0 744.55 620.73 91.44 o 1 20 0 554.26 577.71 63.97 o 2 20 0 248.93 258.99 51.14 o 3 20 0 94.61 33.07 37.72 o 4 20 0 486.17 708.44 68.11 o 5 20 0 234.92 162.63 51.76 o 6 20 0 111.25 109.42 53.46 o 7 20 0 154.10 263.18 64.24 o 8 20 0 300.36 252.21 54.09 o 9 20 0 68.21 65.85 43.29 o 10 20 0 1.96 -4.43 44.28 o 11 20 0 96.40 188.89 66.09 o 1 21 0 138.41 131.34 45.44 o 2 21 0 7.49 11.02 40.00 o 3 21 0 0.00 33.12 41.80 o 4 21 0 31.55 6.02 39.66 o 5 21 0 33.94 -0.19 35.73 o 6 21 0 2.93 -0.33 50.92 o 7 21 0 8.22 -10.23 49.48 o 8 21 0 83.46 139.48 51.16 o 9 21 0 11.52 27.06 69.89 o 10 21 0 88.59 167.90 56.11 o 0 22 0 884.89 1086.65 121.76 o 1 22 0 34.28 117.49 47.38 o 2 22 0 2.76 93.74 46.71 o 3 22 0 193.32 270.81 53.34 o 4 22 0 112.51 69.72 42.58 o 5 22 0 76.68 9.05 70.50 o 6 22 0 33.27 -10.18 52.61 o 7 22 0 112.22 87.54 56.79 o 8 22 0 262.49 219.69 65.48 o 9 22 0 15.31 -23.83 59.82 o 1 23 0 14.51 50.14 45.88 o 2 23 0 151.65 215.80 61.98 o 3 23 0 116.69 129.00 87.36 o 4 23 0 0.22 13.34 44.27 o 5 23 0 0.16 110.19 58.98 o 6 23 0 79.21 40.95 53.63 o 7 23 0 53.04 9.39 71.51 o 8 23 0 165.61 15.15 105.93 o 0 24 0 274.08 341.95 127.83 o 1 24 0 195.40 204.38 82.78 o 2 24 0 326.26 247.01 111.35 o 3 24 0 35.03 154.38 71.65 o 4 24 0 225.88 217.76 110.85 o 5 24 0 195.96 415.67 144.86 o 6 24 0 96.99 126.24 125.26 o 7 24 0 74.61 -29.86 110.84 o 1 25 0 41.28 22.10 87.29 o 2 25 0 0.23 125.88 73.69 o 3 25 0 79.77 18.57 148.43 o 4 25 0 17.66 48.68 71.57 o 5 25 0 2.00 -83.92 105.20 o 6 25 0 70.29 -17.56 114.56 o 0 26 0 78.87 -11.59 89.54 o 1 26 0 95.64 72.16 78.47 o 2 26 0 29.99 183.42 85.51 o 3 26 0 49.52 103.68 72.99 o 4 26 0 79.29 108.30 126.03 o 1 27 0 7.73 53.72 82.67 o -15 0 1 21.72 72.75 67.19 o -13 0 1 150.74 235.66 73.91 o -11 0 1 548.34 495.30 148.74 o -9 0 1 205.44 192.91 46.24 o -7 0 1 459.58 648.96 35.54 o -5 0 1 548.76 515.92 48.33 o -3 0 1 44572.21 42614.00 920.96 o 1 0 1 16324.86 15672.38 491.23 o 3 0 1 12454.74 12094.38 229.92 o 5 0 1 782.06 728.80 39.56 o 7 0 1 9143.37 9976.90 217.63 o 9 0 1 3068.89 3240.04 149.41 o 11 0 1 4238.66 4305.80 381.71 o 13 0 1 746.64 773.60 106.43 o 15 0 1 149.24 249.84 69.35 o -16 1 1 96.18 92.07 58.11 o -15 1 1 2.26 0.43 42.69 o -14 1 1 315.17 277.19 60.50 o -13 1 1 0.02 11.47 33.03 o -12 1 1 32.63 -0.83 30.67 o -11 1 1 85.54 37.27 31.62 o -10 1 1 8.29 9.64 26.01 o -9 1 1 23.53 9.56 23.05 o -8 1 1 313.70 303.98 30.10 o -7 1 1 111.17 98.66 17.76 o -6 1 1 26859.16 27382.87 396.34 o -5 1 1 3.31 -7.21 10.10 o -4 1 1 298.28 327.60 20.29 o -3 1 1 228.28 224.85 18.81 o -2 1 1 141.44 85.40 15.67 o -1 1 1 592.07 483.01 32.32 o 1 1 1 80.87 74.80 8.10 o 2 1 1 35638.90 33983.66 595.00 o 3 1 1 3228.50 2975.27 61.88 o 4 1 1 2972.02 3202.96 57.98 o 5 1 1 3.23 15.03 9.93 o 6 1 1 1076.77 996.57 42.38 o 7 1 1 34.38 32.41 18.13 o 8 1 1 21.23 11.76 16.51 o 9 1 1 0.67 40.36 25.84 o 10 1 1 18.21 -27.62 27.62 o 11 1 1 430.46 410.15 81.72 o 12 1 1 72.32 48.62 32.24 o 13 1 1 232.96 219.01 51.39 o 14 1 1 0.34 9.10 34.57 o 15 1 1 13.99 115.27 58.85 o 16 1 1 9.11 -2.50 47.59 o -16 2 1 42.03 3.26 52.92 o -15 2 1 155.91 229.13 85.33 o -14 2 1 131.63 148.45 41.82 o -13 2 1 4.49 8.74 32.88 o -12 2 1 2.84 22.20 33.93 o -11 2 1 695.10 948.78 74.06 o -10 2 1 2.66 48.66 27.80 o -9 2 1 2.24 17.76 23.16 o -8 2 1 78.00 86.15 19.12 o -7 2 1 6061.06 6729.45 137.73 o -6 2 1 130.07 157.69 30.56 o -5 2 1 381.47 484.52 27.27 o -4 2 1 786.57 832.04 36.52 o -3 2 1 635.25 611.49 29.20 o -2 2 1 473.33 463.04 25.26 o -1 2 1 23771.78 22817.48 488.90 o 0 2 1 287.19 274.29 26.18 o 1 2 1 9960.45 10428.13 166.32 o 2 2 1 359.95 290.61 14.91 o 3 2 1 6015.82 5512.88 84.64 o 4 2 1 628.44 609.10 23.23 o 5 2 1 1833.28 1885.81 50.46 o 6 2 1 128.00 119.00 15.54 o 7 2 1 166.85 249.32 25.99 o 8 2 1 105.35 79.51 21.31 o 9 2 1 803.03 804.44 60.46 o 10 2 1 140.56 125.38 30.07 o 11 2 1 2402.45 2642.98 114.65 o 12 2 1 196.12 122.19 37.28 o 13 2 1 208.57 270.89 46.70 o 14 2 1 18.15 26.73 36.97 o 15 2 1 11.18 89.43 47.32 o 16 2 1 156.67 154.38 52.95 o -16 3 1 38.89 51.82 51.12 o -15 3 1 0.16 -0.80 44.86 o -14 3 1 5.65 12.55 44.04 o -13 3 1 77.73 54.40 34.67 o -12 3 1 699.74 715.93 59.26 o -11 3 1 21.51 49.06 29.19 o -10 3 1 1694.80 1654.96 89.33 o -9 3 1 31.73 1.43 22.67 o -8 3 1 11825.01 12385.26 210.64 o -7 3 1 431.72 391.37 34.98 o -6 3 1 102.78 75.63 17.34 o -5 3 1 1007.29 1038.96 39.00 o -4 3 1 6606.56 6322.69 108.06 o -3 3 1 1736.28 1798.46 37.38 o -2 3 1 22726.49 21722.18 300.97 o -1 3 1 2118.63 2079.04 44.11 o 0 3 1 4817.89 4986.17 86.91 o 1 3 1 106.32 38.30 14.21 o 2 3 1 9572.94 9318.92 129.20 o 3 3 1 1.40 5.04 8.93 o 4 3 1 3747.20 3696.49 69.06 o 5 3 1 2516.21 2483.03 51.61 o 6 3 1 2855.54 2805.29 56.44 o 7 3 1 370.94 375.06 23.88 o 8 3 1 2.52 6.91 16.91 o 9 3 1 158.96 139.31 29.92 o 10 3 1 2844.21 2794.29 97.33 o 11 3 1 6.73 5.96 27.64 o 12 3 1 0.81 12.97 30.55 o 13 3 1 47.41 -19.09 32.05 o 14 3 1 89.06 132.30 50.10 o 15 3 1 21.27 -15.46 44.90 o -16 4 1 0.29 17.11 53.09 o -15 4 1 198.02 125.98 58.88 o -14 4 1 81.04 44.73 45.06 o -13 4 1 133.15 126.72 47.29 o -12 4 1 49.65 -2.55 29.61 o -11 4 1 78.87 6.81 26.11 o -10 4 1 2.93 7.37 23.56 o 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