data_2241514 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.2634 _cell_length_b 7.7451 _cell_length_c 20.4103 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.7702 _cod_data_source_file nk2233Isup2.hkl _cod_data_source_block I _shelx_title ' MonoBrCz' _shelx_refln_list_code 4 _shelx_f_calc_maximum 250.96 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, z' 'x, -y+1/2, z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, -z' '-x, y-1/2, -z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 109.48 249.73 37.89 o 6 0 0 1386.04 1052.31 37.90 o 8 0 0 683.85 707.25 90.48 o 10 0 0 8787.48 9399.44 330.35 o 12 0 0 5078.34 5664.32 275.33 o 14 0 0 2893.90 3383.08 2980.75 o 2 1 0 29216.12 29549.78 219.50 o 4 1 0 29453.57 30234.60 233.41 o 6 1 0 17618.74 18729.01 156.09 o 8 1 0 5266.22 5636.10 133.77 o 10 1 0 2982.02 2929.04 72.15 o 12 1 0 6.17 47.36 14.45 o 14 1 0 442.00 569.97 84.76 o 16 1 0 93.24 75.39 17.35 o 0 2 0 7298.09 7881.88 124.91 o 2 2 0 51.40 81.20 11.80 o 4 2 0 1492.70 1873.17 50.74 o 6 2 0 1700.06 1684.29 48.99 o 8 2 0 330.93 268.39 46.81 o 10 2 0 324.91 367.99 77.20 o 12 2 0 49.25 67.46 42.79 o 14 2 0 487.14 600.77 84.97 o 16 2 0 14.75 50.93 48.78 o 2 3 0 137.60 29.45 27.40 o 4 3 0 15721.45 15559.82 322.71 o 6 3 0 19395.52 22776.76 666.05 o 8 3 0 2204.40 2490.33 74.18 o 10 3 0 432.74 356.63 52.29 o 12 3 0 554.86 465.86 72.67 o 14 3 0 52.10 -3.56 40.14 o 16 3 0 240.06 309.66 104.68 o 18 3 0 45.16 63.02 43.00 o 0 4 0 6838.83 6734.51 216.97 o 2 4 0 19580.67 20245.46 437.78 o 4 4 0 4422.86 4452.43 108.07 o 6 4 0 84.69 56.75 14.38 o 8 4 0 1891.65 1790.86 53.67 o 10 4 0 1087.65 1045.59 117.79 o 12 4 0 967.40 1106.56 153.90 o 14 4 0 493.06 546.75 124.57 o 16 4 0 329.39 285.17 125.43 o 18 4 0 2.13 61.60 49.64 o 2 5 0 69.96 57.10 15.87 o 4 5 0 2460.98 2477.66 151.83 o 6 5 0 464.13 459.36 51.13 o 8 5 0 302.71 260.41 37.42 o 10 5 0 651.84 745.43 93.42 o 12 5 0 9.34 -3.98 45.12 o 14 5 0 67.59 64.66 36.11 o 16 5 0 26.23 35.93 36.35 o 0 6 0 1042.44 1436.87 261.95 o 2 6 0 214.06 224.44 68.38 o 4 6 0 264.32 262.25 42.46 o 6 6 0 22.80 12.24 22.64 o 8 6 0 5.11 8.03 23.45 o 10 6 0 90.81 87.80 40.98 o 12 6 0 13.27 -7.56 51.50 o 14 6 0 28.34 -3.90 49.75 o 2 7 0 104.59 85.11 24.54 o 4 7 0 1598.75 1593.09 247.18 o 6 7 0 155.23 229.00 80.73 o 8 7 0 583.07 754.04 148.93 o 12 7 0 0.40 38.02 61.37 o 14 7 0 0.01 -57.26 57.26 o 0 8 0 28.63 45.87 52.00 o 2 8 0 623.87 555.31 51.27 o 4 8 0 26.97 102.16 50.36 o 6 8 0 13.34 15.37 23.64 o 8 8 0 0.88 65.37 90.36 o 10 8 0 181.77 135.69 88.56 o 12 8 0 37.25 -2.33 61.03 o 2 9 0 0.12 48.51 40.53 o 4 9 0 6.19 62.64 34.61 o 6 9 0 0.45 111.98 78.19 o 8 9 0 49.61 -51.42 52.44 o 0 10 0 3.37 67.46 56.68 o 2 10 0 111.28 57.01 44.03 o 1 1 1 13757.56 13696.93 83.81 o 2 1 1 502.43 908.37 15.73 o 3 1 1 844.01 625.98 11.75 o 4 1 1 1153.45 1034.50 15.28 o 5 1 1 9890.62 9884.72 66.95 o 6 1 1 152.87 118.50 10.11 o 7 1 1 17287.58 18914.93 224.45 o 8 1 1 1141.96 1226.85 30.85 o 9 1 1 5330.38 5395.32 45.70 o 10 1 1 187.80 165.62 21.21 o 11 1 1 306.76 173.07 20.73 o 12 1 1 3.23 15.16 8.29 o 13 1 1 24.45 32.61 14.94 o 14 1 1 139.01 124.88 12.99 o 15 1 1 181.38 230.95 73.06 o 16 1 1 52.87 25.57 18.94 o 17 1 1 31.63 144.06 52.99 o 0 2 1 597.69 451.63 64.45 o 1 2 1 34848.78 35332.43 234.72 o 2 2 1 1582.21 1743.49 27.18 o 3 2 1 14676.55 13641.17 98.74 o 4 2 1 275.91 205.02 19.92 o 5 2 1 4845.99 4163.82 44.44 o 6 2 1 632.88 560.01 22.77 o 7 2 1 225.88 338.21 22.79 o 8 2 1 134.20 127.08 26.29 o 9 2 1 1292.23 1176.41 44.80 o 10 2 1 37.34 56.72 17.60 o 11 2 1 4243.61 4434.08 132.56 o 12 2 1 2.79 2.44 11.98 o 13 2 1 2420.42 2691.26 227.38 o 14 2 1 149.32 109.03 18.18 o 15 2 1 449.40 486.12 48.27 o 16 2 1 156.80 178.80 32.15 o 17 2 1 60.09 31.34 33.75 o 1 3 1 845.85 762.29 31.52 o 2 3 1 14.73 4.88 9.03 o 3 3 1 3329.83 3040.62 45.77 o 4 3 1 33.67 51.25 9.49 o 5 3 1 5719.55 5605.49 108.61 o 6 3 1 98.45 67.20 17.73 o 7 3 1 2909.02 3036.01 38.69 o 8 3 1 220.87 217.40 31.60 o 9 3 1 828.39 844.48 56.82 o 10 3 1 11.63 10.97 10.80 o 11 3 1 394.23 477.40 50.50 o 12 3 1 147.37 179.82 23.87 o 13 3 1 6.86 89.86 29.41 o 14 3 1 45.18 -5.18 28.18 o 15 3 1 65.65 18.11 33.13 o 16 3 1 5.58 -6.79 26.31 o 17 3 1 159.72 192.97 75.55 o 18 3 1 0.36 -17.35 41.95 o 0 4 1 1499.60 1657.30 55.80 o 1 4 1 554.13 593.13 54.57 o 2 4 1 229.97 304.81 26.68 o 3 4 1 15.10 46.64 10.86 o 4 4 1 341.10 532.19 43.42 o 5 4 1 789.56 696.27 60.37 o 6 4 1 0.62 3.27 21.56 o 7 4 1 376.90 350.57 46.99 o 8 4 1 75.86 43.19 15.28 o 9 4 1 226.25 237.09 49.80 o 10 4 1 188.00 224.60 28.04 o 11 4 1 6.27 5.22 25.04 o 12 4 1 101.92 119.93 31.69 o 13 4 1 30.50 80.33 92.84 o 14 4 1 20.52 70.93 20.05 o 15 4 1 39.01 31.39 28.00 o 16 4 1 0.04 75.89 33.47 o 17 4 1 0.26 -29.45 29.45 o 18 4 1 23.76 32.18 31.12 o 1 5 1 235.99 334.24 40.65 o 2 5 1 718.11 612.61 57.03 o 3 5 1 1368.82 1103.23 90.78 o 4 5 1 383.70 340.12 43.42 o 5 5 1 3052.88 2991.36 54.93 o 6 5 1 58.25 101.11 24.44 o 7 5 1 2797.96 3225.93 97.26 o 8 5 1 1.81 35.06 21.36 o 9 5 1 1010.45 1328.97 113.71 o 10 5 1 197.20 232.49 28.55 o 11 5 1 152.58 167.54 38.68 o 12 5 1 21.29 23.68 49.33 o 13 5 1 50.39 37.35 54.82 o 14 5 1 12.70 41.05 25.05 o 15 5 1 19.46 72.94 37.80 o 16 5 1 6.28 30.89 33.26 o 17 5 1 45.21 38.40 55.03 o 0 6 1 375.61 417.59 51.98 o 1 6 1 1936.00 1714.78 99.68 o 2 6 1 34.55 42.66 18.03 o 3 6 1 2414.20 2464.15 76.82 o 4 6 1 512.28 472.76 49.83 o 5 6 1 5.90 34.11 17.40 o 6 6 1 139.33 178.81 22.56 o 7 6 1 15.36 38.08 17.60 o 8 6 1 5.90 -19.69 33.30 o 9 6 1 225.04 145.27 42.05 o 10 6 1 60.98 31.76 34.36 o 11 6 1 519.00 554.58 92.65 o 12 6 1 27.64 64.30 26.74 o 13 6 1 123.53 196.97 71.84 o 14 6 1 4.32 19.84 23.54 o 15 6 1 52.12 40.65 26.98 o 1 7 1 90.62 112.00 16.03 o 2 7 1 14.89 38.10 20.04 o 3 7 1 729.34 743.63 74.94 o 4 7 1 5.71 6.08 14.74 o 5 7 1 41.61 54.33 26.04 o 6 7 1 335.04 308.61 36.37 o 7 7 1 156.55 58.46 40.68 o 8 7 1 12.79 94.27 44.25 o 9 7 1 54.39 47.25 31.16 o 10 7 1 19.03 66.98 40.63 o 11 7 1 0.06 -20.99 38.06 o 12 7 1 1.60 -7.00 33.77 o 13 7 1 14.43 37.63 44.50 o 14 7 1 10.24 -18.92 39.02 o 0 8 1 3.12 -4.75 29.42 o 1 8 1 35.40 80.75 28.01 o 2 8 1 2.82 17.43 16.59 o 3 8 1 53.92 34.75 18.52 o 4 8 1 1.30 23.55 20.84 o 5 8 1 19.37 37.19 18.81 o 6 8 1 3.61 26.73 23.44 o 7 8 1 17.83 47.30 25.57 o 8 8 1 13.88 45.22 50.93 o 9 8 1 0.81 39.70 27.04 o 10 8 1 1.66 24.29 47.92 o 11 8 1 22.00 -54.93 54.93 o 1 9 1 0.57 28.02 26.26 o 2 9 1 60.62 32.12 30.46 o 3 9 1 71.16 50.55 26.73 o 4 9 1 45.23 35.57 18.52 o 5 9 1 70.78 121.82 83.61 o 6 9 1 0.17 19.33 36.86 o 7 9 1 29.93 28.64 95.39 o 8 9 1 8.68 -21.44 30.43 o 0 10 1 35.84 52.74 40.02 o 1 10 1 14.08 37.26 24.45 o 2 0 2 13341.42 12346.53 96.37 o 3 0 2 22180.60 21324.07 222.84 o 4 0 2 18955.33 18630.13 178.86 o 5 0 2 4724.37 3429.17 48.80 o 6 0 2 242.50 195.50 22.17 o 7 0 2 4.03 8.63 8.57 o 8 0 2 15.14 21.25 24.61 o 9 0 2 4070.99 3871.57 100.91 o 10 0 2 4518.91 5070.49 172.26 o 11 0 2 287.45 168.63 25.79 o 12 0 2 1288.21 1284.27 104.05 o 13 0 2 791.10 851.84 69.02 o 14 0 2 658.14 557.32 45.54 o 15 0 2 354.51 296.37 72.57 o 16 0 2 1139.04 1015.94 1124.96 o 1 1 2 11257.82 13185.51 80.68 o 2 1 2 119.27 146.62 8.04 o 3 1 2 3599.21 2966.40 48.49 o 4 1 2 4449.32 4727.66 62.65 o 5 1 2 3174.59 3103.47 26.07 o 6 1 2 6539.21 6311.86 56.30 o 7 1 2 6491.28 7074.59 111.74 o 8 1 2 2226.67 1880.20 37.02 o 9 1 2 200.11 146.79 15.88 o 10 1 2 1277.67 1131.20 47.93 o 11 1 2 88.21 46.98 11.99 o 12 1 2 321.43 317.11 23.43 o 13 1 2 37.42 16.64 6.10 o 14 1 2 3.90 -9.01 13.96 o 15 1 2 19.00 2.27 17.50 o 16 1 2 19.69 11.02 31.22 o 17 1 2 58.43 55.37 30.07 o 0 2 2 1521.40 1691.79 33.14 o 1 2 2 4233.83 5092.76 49.13 o 2 2 2 10632.07 11405.30 77.56 o 3 2 2 3311.28 3744.15 34.99 o 4 2 2 207.79 261.12 17.98 o 5 2 2 2.08 12.60 7.51 o 6 2 2 5.67 13.35 7.78 o 7 2 2 849.72 981.65 48.89 o 8 2 2 42.89 60.90 22.40 o 9 2 2 0.93 9.14 7.66 o 10 2 2 197.35 228.88 38.66 o 11 2 2 277.33 237.56 58.80 o 12 2 2 240.23 213.06 20.00 o 13 2 2 33.74 30.19 14.56 o 14 2 2 98.81 80.35 19.78 o 15 2 2 78.07 40.92 26.87 o 16 2 2 40.44 50.17 22.73 o 17 2 2 3.12 12.64 24.62 o 18 2 2 0.06 -42.05 42.05 o 1 3 2 2191.53 1764.22 39.61 o 2 3 2 5018.79 5153.60 58.17 o 3 3 2 1844.31 1261.77 29.80 o 4 3 2 7099.60 7187.83 114.25 o 5 3 2 229.97 202.17 18.05 o 6 3 2 4751.49 4752.07 91.33 o 7 3 2 3315.93 4000.59 74.25 o 8 3 2 3055.97 2892.41 75.20 o 9 3 2 1968.10 2092.59 70.88 o 10 3 2 1565.03 1588.95 104.81 o 11 3 2 149.41 123.22 41.78 o 12 3 2 148.60 207.51 44.42 o 13 3 2 204.32 130.63 20.21 o 14 3 2 15.81 24.25 22.48 o 15 3 2 0.10 -20.89 28.76 o 16 3 2 91.79 39.95 36.06 o 17 3 2 6.20 40.55 28.32 o 18 3 2 30.86 59.33 39.12 o 0 4 2 10825.14 10311.81 222.52 o 1 4 2 2838.17 2720.84 56.32 o 2 4 2 8219.94 8121.44 128.44 o 3 4 2 2638.91 2308.33 53.72 o 4 4 2 1357.14 1254.44 52.44 o 5 4 2 703.36 623.28 50.04 o 6 4 2 478.82 618.39 60.61 o 7 4 2 7.32 19.03 18.00 o 8 4 2 1190.95 1171.52 106.99 o 9 4 2 475.73 423.39 36.76 o 10 4 2 527.35 534.88 51.51 o 11 4 2 493.11 508.19 54.64 o 12 4 2 733.46 752.93 66.27 o 13 4 2 173.91 297.41 72.70 o 14 4 2 578.71 743.37 104.45 o 15 4 2 46.57 58.04 52.00 o 16 4 2 83.92 63.38 67.70 o 17 4 2 16.77 21.94 64.44 o 18 4 2 0.82 -22.20 31.89 o 1 5 2 700.20 827.47 74.89 o 2 5 2 5.14 21.78 12.25 o 3 5 2 166.69 187.36 28.68 o 4 5 2 1023.01 935.16 80.73 o 5 5 2 805.54 799.32 73.42 o 6 5 2 1566.38 1779.04 66.99 o 7 5 2 18.44 53.31 15.39 o 8 5 2 156.22 183.43 16.67 o 9 5 2 479.00 601.31 44.10 o 10 5 2 76.09 47.69 62.44 o 11 5 2 3.20 -0.90 29.48 o 12 5 2 34.67 1.20 29.01 o 13 5 2 2.38 23.96 28.83 o 14 5 2 6.50 62.37 27.31 o 15 5 2 18.58 37.47 29.34 o 16 5 2 4.45 66.67 30.23 o 17 5 2 0.97 -6.32 34.50 o 0 6 2 81.08 111.97 42.04 o 1 6 2 124.46 81.90 20.07 o 2 6 2 303.27 323.26 46.30 o 3 6 2 614.50 540.37 50.88 o 4 6 2 194.23 246.03 31.26 o 5 6 2 223.96 228.96 20.93 o 6 6 2 74.83 45.63 21.54 o 7 6 2 135.88 84.94 22.66 o 8 6 2 129.08 98.68 19.21 o 9 6 2 0.39 71.48 33.83 o 10 6 2 0.31 4.77 63.36 o 11 6 2 0.06 56.75 21.79 o 12 6 2 37.40 23.05 30.36 o 13 6 2 13.08 78.10 44.96 o 14 6 2 46.21 31.81 30.89 o 15 6 2 6.84 -5.49 48.19 o 1 7 2 145.40 150.87 19.95 o 2 7 2 236.42 224.86 38.48 o 3 7 2 41.59 52.66 19.07 o 4 7 2 336.91 332.34 33.45 o 5 7 2 213.57 242.34 22.35 o 6 7 2 354.50 346.71 38.34 o 7 7 2 35.64 62.72 28.27 o 8 7 2 352.78 416.00 60.98 o 9 7 2 114.20 151.35 43.10 o 10 7 2 80.04 145.95 59.55 o 11 7 2 57.74 56.85 44.02 o 12 7 2 29.77 84.76 57.10 o 13 7 2 2.18 16.90 40.99 o 14 7 2 6.14 -10.69 22.99 o 0 8 2 1059.35 1023.96 198.76 o 1 8 2 291.88 264.26 36.95 o 2 8 2 61.58 92.84 18.24 o 3 8 2 2.79 -27.40 27.40 o 4 8 2 26.96 5.75 14.29 o 5 8 2 20.62 65.18 32.22 o 6 8 2 26.85 10.82 24.71 o 7 8 2 22.02 81.29 26.46 o 8 8 2 29.85 58.36 61.21 o 9 8 2 10.83 10.56 55.27 o 10 8 2 83.22 16.83 60.75 o 11 8 2 31.36 -42.18 42.18 o 1 9 2 0.16 -4.43 29.88 o 2 9 2 0.07 14.34 26.58 o 3 9 2 4.17 53.01 29.65 o 4 9 2 103.54 39.38 22.17 o 5 9 2 45.67 26.16 18.92 o 6 9 2 1.33 -12.10 56.77 o 7 9 2 17.39 -2.40 34.10 o 8 9 2 1.20 18.87 36.09 o 0 10 2 22.63 12.48 17.88 o 1 10 2 1.81 30.12 26.12 o 1 1 3 789.83 892.10 19.08 o 2 1 3 62978.97 65954.95 215.32 o 3 1 3 34831.91 39695.84 287.06 o 4 1 3 2281.35 1749.02 42.93 o 5 1 3 3582.82 3487.86 58.52 o 6 1 3 4724.11 4785.76 45.34 o 7 1 3 3638.53 2930.17 53.46 o 8 1 3 6023.36 6636.99 110.06 o 9 1 3 3620.29 3440.73 46.21 o 10 1 3 326.40 282.78 27.75 o 11 1 3 408.33 417.99 28.98 o 12 1 3 474.07 420.27 36.38 o 13 1 3 125.20 108.04 28.81 o 14 1 3 132.19 121.61 13.22 o 15 1 3 1.19 11.84 12.62 o 16 1 3 105.59 18.61 24.99 o 17 1 3 201.70 170.02 52.23 o 0 2 3 21108.35 21977.04 175.46 o 1 2 3 9569.00 8262.73 58.57 o 2 2 3 40173.10 41592.70 247.03 o 3 2 3 41923.34 45913.57 176.43 o 4 2 3 2695.23 2057.34 28.85 o 5 2 3 650.28 749.40 68.47 o 6 2 3 55.02 123.92 10.67 o 7 2 3 1126.94 1289.16 41.40 o 8 2 3 1419.68 1532.54 47.49 o 9 2 3 2225.80 2601.38 69.02 o 10 2 3 1625.39 1629.53 56.25 o 11 2 3 1652.64 1828.16 99.86 o 12 2 3 1394.99 1419.75 90.75 o 13 2 3 620.99 652.08 49.13 o 14 2 3 653.06 749.38 83.19 o 15 2 3 285.45 206.22 25.44 o 16 2 3 110.35 78.59 22.72 o 17 2 3 138.71 131.42 65.42 o 18 2 3 5.17 -2.85 20.46 o 1 3 3 1277.54 1182.19 34.46 o 2 3 3 43.43 22.58 7.89 o 3 3 3 32.92 21.17 6.02 o 4 3 3 9310.53 9929.18 155.59 o 5 3 3 3009.09 2852.33 57.82 o 6 3 3 2685.11 2517.74 94.71 o 7 3 3 5305.80 5637.69 62.62 o 8 3 3 1725.66 1673.46 54.91 o 9 3 3 218.28 211.91 23.03 o 10 3 3 211.01 174.76 34.52 o 11 3 3 102.56 62.34 31.27 o 12 3 3 35.27 25.40 15.60 o 13 3 3 87.75 66.53 77.60 o 14 3 3 8.75 54.60 19.91 o 15 3 3 62.05 16.88 16.38 o 16 3 3 77.37 30.20 34.58 o 17 3 3 11.63 13.89 47.84 o 18 3 3 34.99 -35.51 46.14 o 0 4 3 195.62 294.13 40.56 o 1 4 3 416.90 319.94 28.32 o 2 4 3 8.85 -8.19 12.02 o 3 4 3 1668.58 1852.56 51.37 o 4 4 3 664.01 548.61 48.49 o 5 4 3 44.47 14.76 10.31 o 6 4 3 1.41 42.38 15.16 o 7 4 3 63.61 84.22 28.31 o 8 4 3 96.69 77.74 27.67 o 9 4 3 2.57 -4.07 15.35 o 10 4 3 270.86 286.63 27.61 o 11 4 3 73.45 73.80 22.89 o 12 4 3 1.86 -1.66 46.31 o 13 4 3 16.22 23.66 29.37 o 14 4 3 9.16 12.65 23.42 o 15 4 3 8.60 9.01 19.11 o 16 4 3 68.55 67.39 71.28 o 17 4 3 11.42 -1.68 44.16 o 18 4 3 2.67 -46.90 47.68 o 1 5 3 696.89 735.99 73.89 o 2 5 3 196.86 157.61 26.84 o 3 5 3 1932.37 2265.30 65.43 o 4 5 3 1017.29 925.62 82.22 o 5 5 3 1733.09 1735.30 55.58 o 6 5 3 2365.77 2679.64 74.14 o 7 5 3 1729.25 1609.68 172.39 o 8 5 3 239.79 360.20 37.69 o 9 5 3 302.16 338.76 34.03 o 10 5 3 226.32 319.72 27.95 o 11 5 3 158.20 189.49 34.58 o 12 5 3 104.61 129.90 35.92 o 13 5 3 9.08 47.10 50.87 o 14 5 3 22.56 40.31 36.18 o 15 5 3 35.67 20.19 19.53 o 16 5 3 2.97 -25.66 54.58 o 17 5 3 12.96 33.81 42.29 o 0 6 3 1614.59 1563.67 118.62 o 1 6 3 2308.82 2479.41 76.50 o 2 6 3 580.26 569.50 48.34 o 3 6 3 250.22 323.17 28.79 o 4 6 3 835.08 939.34 75.25 o 5 6 3 261.40 367.72 29.73 o 6 6 3 34.03 19.13 17.42 o 7 6 3 190.43 113.64 24.20 o 8 6 3 9.98 -12.35 30.02 o 9 6 3 91.85 65.39 14.58 o 10 6 3 121.22 151.15 33.68 o 11 6 3 144.61 113.19 40.89 o 12 6 3 173.67 105.38 33.76 o 13 6 3 266.31 335.97 128.71 o 14 6 3 40.27 129.76 59.17 o 15 6 3 14.96 65.89 38.28 o 1 7 3 40.65 28.91 21.69 o 2 7 3 0.96 36.55 22.82 o 3 7 3 1.76 16.66 19.53 o 4 7 3 10.95 8.43 35.22 o 5 7 3 122.90 97.57 18.01 o 6 7 3 48.06 29.90 14.33 o 7 7 3 97.13 86.98 27.12 o 8 7 3 22.22 39.28 27.96 o 9 7 3 0.14 -9.76 57.39 o 10 7 3 80.07 67.79 32.72 o 11 7 3 1.40 -25.57 52.76 o 12 7 3 5.15 -29.57 39.16 o 13 7 3 0.59 -13.36 33.94 o 14 7 3 0.39 30.91 40.35 o 0 8 3 52.38 52.28 27.76 o 1 8 3 223.29 234.67 21.27 o 2 8 3 158.97 147.56 26.88 o 3 8 3 28.05 23.15 15.95 o 4 8 3 0.61 0.73 22.90 o 5 8 3 32.23 38.96 20.64 o 6 8 3 5.66 36.59 41.06 o 7 8 3 1.88 20.85 48.54 o 8 8 3 0.76 -26.62 41.74 o 9 8 3 8.79 -0.76 29.01 o 10 8 3 18.85 51.27 42.79 o 11 8 3 1.56 -41.64 41.64 o 1 9 3 156.83 131.88 32.41 o 2 9 3 5.87 -0.49 25.52 o 3 9 3 3.49 16.51 16.96 o 4 9 3 106.68 96.26 36.02 o 5 9 3 37.02 17.94 19.29 o 6 9 3 18.44 44.36 30.35 o 7 9 3 15.68 48.70 58.96 o 8 9 3 29.72 43.39 42.72 o 0 0 4 2666.37 1980.33 50.59 o 1 0 4 45999.11 44644.76 587.21 o 2 0 4 26078.26 26707.52 255.87 o 3 0 4 2837.54 2392.36 55.26 o 4 0 4 10420.87 11864.69 128.80 o 5 0 4 6887.10 7068.01 90.74 o 6 0 4 197.36 199.59 26.12 o 7 0 4 953.53 931.69 51.75 o 8 0 4 5979.86 7496.82 164.49 o 9 0 4 2967.75 3504.28 57.33 o 10 0 4 1940.49 2093.64 89.42 o 11 0 4 3367.96 3793.56 90.82 o 12 0 4 797.52 863.89 107.19 o 13 0 4 1744.54 1652.00 141.99 o 14 0 4 734.52 617.10 72.28 o 15 0 4 410.89 409.55 65.75 o 16 0 4 6.19 10.12 25.33 o 1 1 4 13.09 13.81 6.84 o 2 1 4 395.82 340.06 30.57 o 3 1 4 15603.98 16599.77 173.72 o 4 1 4 19108.44 21802.11 151.59 o 5 1 4 2937.16 2631.62 29.31 o 6 1 4 3936.21 3674.31 41.06 o 7 1 4 5060.00 4780.19 79.57 o 8 1 4 1645.21 1363.50 31.55 o 9 1 4 2355.07 2336.90 55.63 o 10 1 4 80.29 45.69 13.27 o 11 1 4 1158.06 1034.28 86.34 o 12 1 4 0.11 22.70 18.46 o 13 1 4 12.93 26.69 12.78 o 14 1 4 189.25 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38.35 o 2 1 21 248.88 188.55 32.93 o 3 1 21 4.87 75.16 20.11 o 4 1 21 7.45 38.87 33.49 o 5 1 21 386.79 424.47 63.52 o 6 1 21 270.34 217.37 35.90 o 7 1 21 5.71 27.42 29.46 o 8 1 21 80.72 116.24 37.07 o 9 1 21 47.97 42.90 43.94 o 10 1 21 0.90 25.35 32.67 o 11 1 21 14.65 54.73 49.93 o 0 2 21 206.27 228.61 34.59 o 1 2 21 468.35 526.76 55.83 o 2 2 21 173.64 94.96 17.70 o 3 2 21 31.18 87.49 18.14 o 4 2 21 114.22 56.75 20.67 o 5 2 21 51.51 21.70 24.55 o 6 2 21 0.23 22.26 48.31 o 7 2 21 0.13 19.13 23.03 o 8 2 21 76.61 94.00 41.07 o 9 2 21 7.83 11.40 29.99 o 10 2 21 56.64 78.79 50.98 o 11 2 21 34.46 61.71 43.42 o 1 3 21 42.14 4.84 18.00 o 2 3 21 10.20 8.38 38.72 o 3 3 21 104.83 100.96 26.27 o 4 3 21 28.63 -14.07 24.56 o 5 3 21 27.17 55.65 35.04 o 6 3 21 28.12 90.23 38.34 o 7 3 21 33.01 4.86 42.12 o 8 3 21 11.50 105.82 43.24 o 9 3 21 43.19 25.24 33.61 o 10 3 21 9.78 12.30 25.68 o 0 4 21 2.45 33.52 37.74 o 1 4 21 3.52 104.05 33.85 o 2 4 21 24.99 31.18 33.84 o 3 4 21 0.73 -3.79 28.69 o 4 4 21 13.76 34.54 62.15 o 5 4 21 1.57 21.97 28.96 o 6 4 21 8.35 -31.44 34.30 o 7 4 21 0.33 30.70 36.85 o 8 4 21 9.67 30.27 41.77 o 9 4 21 2.33 49.37 30.30 o 1 5 21 0.78 20.90 21.01 o 2 5 21 5.57 -35.95 38.92 o 3 5 21 10.46 74.21 31.70 o 4 5 21 70.85 88.45 38.00 o 5 5 21 4.15 87.85 34.02 o 6 5 21 21.59 31.39 39.92 o 7 5 21 27.45 0.93 40.19 o 0 6 21 1.91 37.19 65.37 o 1 6 21 16.24 12.71 29.95 o 2 6 21 51.87 47.07 31.55 o 0 0 22 119.89 251.41 60.76 o 1 0 22 302.51 187.36 32.63 o 2 0 22 136.00 185.55 43.95 o 3 0 22 2.06 53.36 32.19 o 4 0 22 256.52 429.58 86.97 o 5 0 22 50.33 43.92 26.95 o 6 0 22 17.49 -0.08 42.24 o 7 0 22 142.67 75.76 43.30 o 8 0 22 88.65 48.73 60.37 o 9 0 22 22.42 47.50 45.30 o 10 0 22 71.45 -22.85 61.37 o 11 0 22 31.81 49.41 68.28 o 1 1 22 65.36 67.71 20.32 o 2 1 22 56.92 47.02 18.15 o 3 1 22 27.69 52.94 22.84 o 4 1 22 26.83 61.94 41.92 o 5 1 22 116.83 100.42 21.73 o 6 1 22 24.65 31.00 33.00 o 7 1 22 8.46 56.58 44.46 o 8 1 22 74.93 38.59 34.51 o 9 1 22 0.14 -44.85 44.85 o 10 1 22 30.68 63.40 43.73 o 0 2 22 139.17 58.05 38.77 o 1 2 22 0.65 47.98 21.49 o 2 2 22 5.71 -4.93 37.25 o 3 2 22 0.47 72.29 33.20 o 4 2 22 31.29 74.26 40.22 o 5 2 22 9.61 46.74 27.94 o 6 2 22 0.08 50.25 27.78 o 7 2 22 1.11 37.23 27.20 o 8 2 22 0.20 90.54 42.22 o 9 2 22 6.53 19.64 37.62 o 10 2 22 3.79 14.31 48.03 o 1 3 22 69.23 90.52 30.24 o 2 3 22 0.75 12.43 35.28 o 3 3 22 35.58 7.43 29.43 o 4 3 22 2.21 4.62 46.56 o 5 3 22 18.21 -18.43 36.65 o 6 3 22 69.30 45.63 27.27 o 7 3 22 36.94 38.24 33.29 o 8 3 22 24.08 18.61 71.56 o 9 3 22 7.32 14.45 27.18 o 0 4 22 46.12 24.95 83.83 o 1 4 22 71.97 5.96 31.28 o 2 4 22 84.21 104.24 36.64 o 3 4 22 7.26 108.55 41.57 o 4 4 22 7.61 15.87 32.11 o 5 4 22 10.49 38.44 49.84 o 6 4 22 23.73 59.81 38.71 o 7 4 22 0.18 11.57 63.76 o 1 5 22 31.13 61.11 27.12 o 2 5 22 7.35 63.84 34.59 o 3 5 22 19.32 40.63 35.80 o 4 5 22 9.16 14.10 66.99 o 5 5 22 6.45 42.54 35.39 o 1 1 23 0.21 14.64 21.15 o 2 1 23 7.64 70.83 30.77 o 3 1 23 47.30 65.96 26.06 o 4 1 23 2.88 23.49 28.44 o 5 1 23 76.49 78.38 34.87 o 6 1 23 14.78 44.25 26.39 o 7 1 23 31.86 28.28 27.06 o 8 1 23 1.50 1.94 45.40 o 9 1 23 15.00 59.60 49.34 o 0 2 23 59.33 80.85 42.28 o 1 2 23 120.07 159.55 40.86 o 2 2 23 1.02 7.88 25.16 o 3 2 23 104.46 97.74 30.27 o 4 2 23 4.71 18.11 28.49 o 5 2 23 9.95 24.52 43.04 o 6 2 23 15.49 74.70 47.57 o 7 2 23 3.71 -38.79 46.74 o 8 2 23 0.89 -32.08 32.08 o 9 2 23 13.96 30.47 23.16 o 1 3 23 3.44 -26.05 26.05 o 2 3 23 18.37 20.10 25.67 o 3 3 23 3.11 49.90 34.05 o 4 3 23 1.87 30.69 39.61 o 5 3 23 42.74 69.23 32.64 o 6 3 23 0.24 26.82 39.41 o 7 3 23 11.93 44.58 37.49 o 0 4 23 22.74 -42.52 42.52 o 1 4 23 13.34 44.07 20.18 o 2 4 23 0.60 51.10 31.88 o 3 4 23 1.20 52.62 56.88 o 4 4 23 6.08 4.06 36.20 o 5 4 23 0.95 20.24 36.23 o 0 0 24 114.84 106.38 50.72 o 1 0 24 10.38 -25.38 34.37 o 2 0 24 156.97 123.82 55.89 o 3 0 24 39.78 56.30 42.61 o 4 0 24 52.12 67.89 39.52 o 5 0 24 6.60 9.54 20.60 o 6 0 24 28.04 30.23 35.41 o 7 0 24 9.12 -16.20 63.20 o 8 0 24 54.26 100.23 87.61 o 1 1 24 0.11 22.88 27.75 o 2 1 24 5.39 1.56 45.36 o 3 1 24 5.78 18.51 24.77 o 4 1 24 53.68 40.11 21.06 o 5 1 24 6.61 39.45 41.17 o 6 1 24 24.43 72.02 37.70 o 7 1 24 17.86 5.90 48.72 o 8 1 24 94.56 51.55 67.70 o 0 2 24 7.86 19.44 83.06 o 1 2 24 8.50 37.01 31.14 o 2 2 24 2.39 8.59 26.62 o 3 2 24 2.97 -22.97 22.97 o 4 2 24 0.49 1.25 26.57 o 5 2 24 3.09 34.73 59.56 o 6 2 24 16.54 63.43 29.73 o 7 2 24 0.96 7.43 22.93 o 1 3 24 21.23 5.47 33.76 o 2 3 24 18.34 40.94 23.92 o 3 3 24 0.77 -14.83 35.89 o 4 3 24 34.45 9.44 28.69 o 5 3 24 27.58 13.68 23.65 o 0 4 24 31.64 9.35 24.30 o 1 4 24 1.71 17.84 23.94 o 2 4 24 81.96 6.25 116.73 o 1 1 25 0.08 -12.09 23.00 o 2 1 25 4.87 -26.99 26.99 o 3 1 25 27.35 9.83 26.12 o 4 1 25 2.12 28.91 24.13 o 5 1 25 13.08 21.16 31.56 o 6 1 25 0.72 23.26 30.21 o 0 2 25 24.24 111.40 49.81 o 1 2 25 99.05 164.59 49.83 o 2 2 25 7.33 35.72 27.92 o 3 2 25 17.77 36.06 32.75 o 4 2 25 1.17 29.60 32.58 o 5 2 25 6.14 -7.02 36.92 o 1 3 25 0.03 -0.77 33.63 o 2 3 25 3.13 21.76 35.56 o 0 0 26 35.03 7.62 26.14 o 1 0 26 14.54 28.65 38.05 o 2 0 26 49.53 51.71 36.95 o 3 0 26 4.78 15.89 36.75 o 1 1 26 4.12 31.53 29.74 o 2 1 26 7.10 82.45 30.86 o 3 1 26 0.49 21.95 27.30 o