#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:48:23 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181916 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/15/2241588.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241588 _cell_angle_alpha 90.000 _cell_angle_beta 117.545 _cell_angle_gamma 90.000 _cell_length_a 24.9602 _cell_length_b 5.1055 _cell_length_c 12.4664 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.7294 _cod_data_source_file zl2658Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelxt_b.res in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 201.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 128.49 116.09 9.16 o 4 0 0 3374.47 3483.99 35.91 o 6 0 0 3044.26 3848.64 31.31 o 8 0 0 22607.97 23642.38 257.45 o 10 0 0 11391.68 12808.04 129.07 o 12 0 0 2152.64 3042.13 31.51 o 14 0 0 849.86 978.00 20.19 o 16 0 0 2618.73 2812.70 28.26 o 18 0 0 323.44 292.42 13.65 o 20 0 0 4400.45 4266.17 31.29 o 22 0 0 403.68 419.50 19.31 o 24 0 0 89.83 82.67 18.68 o 26 0 0 2283.39 2155.11 30.03 o 28 0 0 393.73 384.22 26.48 o 30 0 0 626.37 615.09 30.07 o 1 1 0 315.14 414.91 19.50 o 3 1 0 817.90 1025.48 23.78 o 5 1 0 5537.40 5902.29 44.00 o 7 1 0 2836.29 3280.63 54.02 o 9 1 0 3083.03 3299.03 22.79 o 11 1 0 2215.60 2345.14 28.77 o 13 1 0 2749.61 3331.26 18.50 o 15 1 0 110.09 127.32 15.11 o 17 1 0 2133.07 2247.11 54.20 o 19 1 0 1380.32 1372.97 39.54 o 21 1 0 928.74 983.41 18.62 o 23 1 0 1.55 8.89 11.35 o 25 1 0 55.87 45.73 14.91 o 27 1 0 911.39 883.04 17.84 o 29 1 0 497.18 487.56 45.33 o 0 2 0 9701.54 8943.44 82.07 o 2 2 0 430.74 455.75 12.91 o 4 2 0 6828.33 7332.03 260.94 o 6 2 0 874.61 1027.29 27.41 o 8 2 0 1532.96 1822.03 35.59 o 10 2 0 3356.01 3535.40 20.55 o 12 2 0 382.99 367.14 9.74 o 14 2 0 566.83 596.38 11.70 o 16 2 0 5662.57 5669.60 99.16 o 18 2 0 4.32 10.51 8.87 o 20 2 0 285.04 303.81 13.75 o 22 2 0 0.13 3.37 13.54 o 24 2 0 0.36 0.27 14.88 o 26 2 0 478.67 456.27 17.87 o 28 2 0 13.69 10.85 19.38 o 1 3 0 299.55 327.19 14.27 o 3 3 0 1018.17 984.05 40.37 o 5 3 0 181.29 186.53 12.98 o 7 3 0 0.14 14.63 15.68 o 9 3 0 983.61 1203.49 50.98 o 11 3 0 408.34 430.26 14.08 o 13 3 0 2.53 -0.68 8.59 o 15 3 0 476.04 491.36 16.24 o 17 3 0 989.46 1023.73 28.30 o 19 3 0 40.87 54.31 10.65 o 21 3 0 677.22 685.17 26.39 o 23 3 0 39.71 35.01 13.73 o 25 3 0 192.65 192.22 17.47 o 27 3 0 16.89 3.37 19.41 o 0 4 0 578.90 558.91 23.45 o 2 4 0 811.92 776.44 49.82 o 4 4 0 495.22 495.63 28.70 o 6 4 0 57.60 63.82 10.33 o 8 4 0 1276.44 1305.19 82.83 o 10 4 0 0.45 2.22 10.07 o 12 4 0 180.51 181.40 11.00 o 14 4 0 1.82 2.05 10.36 o 16 4 0 29.44 42.39 10.20 o 18 4 0 309.56 346.03 12.59 o 20 4 0 80.39 84.85 16.27 o 22 4 0 1204.12 1175.22 37.28 o 24 4 0 21.78 5.34 19.71 o 1 5 0 1845.61 1900.95 26.06 o 3 5 0 480.10 486.85 18.65 o 5 5 0 144.01 164.15 12.87 o 7 5 0 1189.79 1261.26 77.96 o 9 5 0 1437.43 1526.12 89.34 o 11 5 0 167.30 179.92 13.94 o 13 5 0 98.05 95.80 11.76 o 15 5 0 9.84 12.05 11.61 o 17 5 0 730.62 799.73 38.11 o 19 5 0 1366.58 1443.00 81.11 o 21 5 0 59.39 33.33 21.56 o 0 6 0 1332.48 1515.94 52.85 o 2 6 0 49.51 54.22 15.10 o 4 6 0 22.04 29.34 16.33 o 6 6 0 760.54 776.63 59.79 o 8 6 0 1162.68 1166.00 65.63 o 10 6 0 864.95 865.15 62.79 o 12 6 0 293.76 310.87 26.67 o 14 6 0 4.57 6.04 19.73 o -29 1 1 0.04 7.48 18.05 o -27 1 1 286.89 287.34 16.20 o -25 1 1 83.98 90.44 14.82 o -23 1 1 21.05 26.94 12.69 o -21 1 1 1034.87 1089.04 18.13 o -19 1 1 442.31 426.94 10.76 o -17 1 1 4464.94 4818.17 85.41 o -15 1 1 782.07 795.12 10.58 o -13 1 1 205.12 246.84 8.74 o -11 1 1 139.21 107.91 6.97 o -9 1 1 5213.20 5593.35 58.64 o -7 1 1 2830.95 3121.47 95.43 o -5 1 1 1731.78 1885.00 75.49 o -3 1 1 55.52 48.46 6.92 o -1 1 1 44.61 47.38 7.92 o 1 1 1 3419.52 3666.37 345.65 o 3 1 1 439.86 597.59 19.11 o 5 1 1 2762.94 3026.70 50.49 o 7 1 1 105.30 88.70 8.97 o 9 1 1 1394.37 1545.47 68.90 o 11 1 1 771.19 878.63 13.42 o 13 1 1 709.16 744.79 13.44 o 15 1 1 108.99 129.08 10.61 o 17 1 1 157.09 163.52 11.78 o 19 1 1 130.67 153.45 12.53 o 21 1 1 1108.10 1148.41 41.89 o 23 1 1 172.33 159.00 12.35 o 25 1 1 51.88 44.95 13.45 o 27 1 1 19.09 9.77 13.33 o -28 2 1 670.23 618.74 35.12 o -26 2 1 2162.44 2088.60 67.33 o -24 2 1 86.83 75.85 14.45 o -22 2 1 46.63 38.04 10.06 o -20 2 1 1839.23 1846.33 28.89 o -18 2 1 2085.70 2081.36 83.13 o -16 2 1 33.32 36.67 8.58 o -14 2 1 1111.04 1208.86 23.28 o -12 2 1 652.27 710.43 19.31 o -10 2 1 4968.17 5228.06 116.14 o -8 2 1 600.35 528.39 10.61 o -6 2 1 2726.38 3138.27 133.34 o -4 2 1 9245.62 9560.86 541.43 o -2 2 1 325.15 337.31 13.44 o 0 2 1 11373.79 10079.20 344.22 o 2 2 1 5316.14 4968.47 208.37 o 4 2 1 4475.71 4569.03 176.63 o 6 2 1 7.61 8.49 8.74 o 8 2 1 2029.84 2108.33 60.10 o 10 2 1 2195.40 2229.34 19.29 o 12 2 1 3794.66 4059.82 20.54 o 14 2 1 667.62 702.50 13.41 o 16 2 1 1702.27 1860.21 58.90 o 18 2 1 27.21 21.37 12.02 o 20 2 1 1072.39 1113.70 59.81 o 22 2 1 1367.93 1396.68 59.16 o 24 2 1 31.97 39.88 17.94 o 26 2 1 8.01 7.48 14.82 o 28 2 1 110.60 83.11 26.37 o -27 3 1 700.09 694.88 63.69 o -25 3 1 1196.13 1148.70 19.54 o -23 3 1 0.18 -1.07 11.31 o -21 3 1 7.46 6.29 10.84 o -19 3 1 789.02 804.20 24.84 o -17 3 1 1828.23 1870.00 53.98 o -15 3 1 2657.55 2779.47 118.67 o -13 3 1 70.53 76.83 9.23 o -11 3 1 518.37 530.82 23.08 o -9 3 1 2957.21 2883.74 97.44 o -7 3 1 4805.75 4990.60 209.24 o -5 3 1 3085.36 3155.32 99.96 o -3 3 1 727.53 737.81 17.68 o -1 3 1 3994.66 3687.12 33.38 o 1 3 1 3691.15 3364.11 129.05 o 3 3 1 18.24 10.75 9.26 o 5 3 1 5631.90 5386.29 282.79 o 7 3 1 509.35 514.62 24.41 o 9 3 1 3982.16 4406.27 289.57 o 11 3 1 38.30 37.12 7.54 o 13 3 1 2866.55 3103.16 115.28 o 15 3 1 2353.89 2501.37 125.24 o 17 3 1 2319.84 2436.77 20.95 o 19 3 1 633.09 611.17 20.14 o 21 3 1 1157.93 1201.08 18.40 o 23 3 1 558.87 583.40 17.37 o 25 3 1 11.01 8.08 18.99 o -24 4 1 17.64 10.77 17.85 o -22 4 1 388.81 382.55 14.23 o -20 4 1 232.64 209.84 12.60 o -18 4 1 1654.89 1752.24 45.26 o -16 4 1 407.11 432.20 15.93 o -14 4 1 676.89 725.40 28.92 o -12 4 1 37.26 26.17 9.79 o -10 4 1 2962.91 3255.33 134.36 o -8 4 1 520.21 529.54 21.64 o -6 4 1 850.13 795.08 37.44 o -4 4 1 66.15 69.54 9.18 o -2 4 1 0.57 -0.06 10.69 o 0 4 1 1297.92 1281.42 25.17 o 2 4 1 1525.50 1455.67 101.25 o 4 4 1 1242.24 1191.74 129.18 o 6 4 1 56.58 55.78 11.12 o 8 4 1 381.44 377.98 21.79 o 10 4 1 1121.18 1195.90 51.95 o 12 4 1 1259.77 1349.64 46.05 o 14 4 1 531.04 584.62 28.48 o 16 4 1 380.69 392.62 19.70 o 18 4 1 18.06 11.57 15.64 o 20 4 1 891.88 899.34 20.43 o 22 4 1 1071.37 1081.02 22.07 o -21 5 1 3.92 8.53 21.00 o -19 5 1 742.58 856.32 33.01 o -17 5 1 35.50 35.26 13.76 o -15 5 1 0.07 0.66 13.40 o -13 5 1 96.54 87.06 11.31 o -11 5 1 20.78 14.82 10.56 o -9 5 1 103.98 117.49 10.81 o -7 5 1 317.05 313.48 19.43 o -5 5 1 36.03 42.56 11.58 o -3 5 1 8.95 12.27 12.30 o -1 5 1 143.99 157.43 14.31 o 1 5 1 2461.98 2610.88 112.48 o 3 5 1 69.33 76.78 18.79 o 5 5 1 24.20 25.22 19.49 o 7 5 1 0.63 -2.81 19.42 o 9 5 1 269.08 280.10 34.84 o 11 5 1 308.83 309.99 19.44 o 13 5 1 18.29 20.33 13.80 o 15 5 1 3.99 6.59 13.99 o 17 5 1 24.76 19.48 15.70 o 19 5 1 144.08 153.59 20.31 o -16 6 1 0.68 1.69 15.90 o -14 6 1 5.25 1.36 17.02 o -12 6 1 77.33 79.85 16.53 o -10 6 1 10.38 14.42 16.16 o -8 6 1 11.52 13.27 16.17 o -6 6 1 263.59 287.60 16.95 o -4 6 1 472.70 495.43 18.42 o -2 6 1 16.85 20.40 18.05 o 0 6 1 11.06 18.23 25.41 o 2 6 1 157.06 150.76 26.82 o 4 6 1 75.85 82.89 17.70 o 6 6 1 78.79 77.64 17.37 o 8 6 1 62.34 60.93 17.42 o 10 6 1 24.00 15.68 18.09 o 12 6 1 92.94 101.29 19.91 o 14 6 1 452.48 489.88 54.78 o -30 0 2 25.43 16.76 19.12 o -28 0 2 194.78 194.70 23.34 o -26 0 2 1480.65 1507.25 22.45 o -24 0 2 1328.99 1369.84 24.52 o -22 0 2 346.99 371.07 16.48 o -20 0 2 3.95 7.89 10.70 o -18 0 2 3245.15 3687.92 35.12 o -16 0 2 1757.10 1796.63 16.88 o -14 0 2 3925.40 4023.12 30.31 o -12 0 2 132.04 107.80 7.34 o -10 0 2 3562.83 3770.24 40.20 o -8 0 2 1685.34 2103.54 21.22 o -6 0 2 2501.21 3060.67 32.33 o -4 0 2 45.43 43.86 11.60 o -2 0 2 18.88 22.90 6.74 o 0 0 2 26007.76 17879.26 663.38 o 8 0 2 3997.34 5341.45 42.83 o 10 0 2 1140.71 1226.15 22.08 o 12 0 2 15107.05 17833.44 67.13 o 14 0 2 1683.64 1594.98 21.27 o 16 0 2 111.90 173.06 15.90 o 18 0 2 512.57 463.70 18.31 o 20 0 2 23.90 0.48 12.80 o 22 0 2 2290.94 2410.54 28.37 o 24 0 2 458.56 426.35 23.49 o 26 0 2 184.40 142.18 23.67 o 28 0 2 59.52 58.44 25.93 o -31 1 2 354.02 332.76 16.78 o -29 1 2 18.80 17.86 13.72 o -27 1 2 439.73 428.82 16.02 o -25 1 2 1802.00 1840.77 17.25 o -23 1 2 0.64 5.65 8.62 o -21 1 2 3879.63 4181.64 54.62 o -19 1 2 1201.86 1220.65 30.06 o -17 1 2 742.40 714.96 11.21 o -15 1 2 4344.94 4461.24 51.17 o -13 1 2 5364.57 5857.38 71.94 o -11 1 2 525.35 606.33 11.06 o -9 1 2 8453.13 9008.64 122.98 o -7 1 2 55.43 37.47 4.44 o -3 1 2 462.50 477.05 15.43 o -1 1 2 4948.76 4378.65 117.08 o 1 1 2 4873.45 4735.23 49.34 o 3 1 2 10488.58 11083.83 94.72 o 5 1 2 12922.99 14252.49 88.32 o 7 1 2 2664.57 3623.26 40.35 o 9 1 2 36.45 42.31 13.46 o 11 1 2 3955.30 4280.45 37.17 o 13 1 2 762.57 740.38 17.64 o 15 1 2 2581.63 2722.45 40.17 o 17 1 2 17.88 13.78 11.60 o 19 1 2 81.07 81.09 10.74 o 21 1 2 3600.89 3663.34 30.07 o 23 1 2 291.59 325.44 15.99 o 25 1 2 69.94 75.05 16.65 o 27 1 2 0.00 0.42 18.55 o -30 2 2 158.60 144.05 20.58 o -28 2 2 123.04 122.91 18.06 o -26 2 2 212.49 208.49 11.44 o -24 2 2 269.63 271.39 11.74 o -22 2 2 47.10 59.49 10.69 o -20 2 2 473.84 464.47 10.07 o -18 2 2 1228.81 1322.31 28.74 o -16 2 2 161.42 161.36 7.35 o -14 2 2 398.36 352.22 8.62 o -12 2 2 70.35 85.09 8.18 o -10 2 2 679.56 780.39 11.64 o -8 2 2 145.78 189.49 7.82 o -6 2 2 94.59 57.43 7.19 o -4 2 2 3459.91 3652.14 182.22 o -2 2 2 106.62 87.21 7.34 o 0 2 2 35.12 29.85 8.54 o 2 2 2 3048.36 2754.07 195.31 o 4 2 2 334.15 448.21 25.37 o 6 2 2 605.87 649.64 24.86 o 8 2 2 2.81 18.79 13.28 o 10 2 2 40.96 37.95 13.83 o 12 2 2 0.47 2.16 9.86 o 14 2 2 74.82 86.30 11.13 o 16 2 2 2648.64 2931.20 49.25 o 18 2 2 19.09 21.47 10.79 o 20 2 2 0.08 16.46 12.93 o 22 2 2 714.67 735.87 17.69 o 24 2 2 309.52 373.38 17.45 o 26 2 2 196.99 146.17 64.43 o -27 3 2 135.37 123.17 17.46 o -25 3 2 274.93 271.85 12.06 o -23 3 2 133.18 128.99 11.68 o -21 3 2 259.33 257.77 10.98 o -19 3 2 142.36 133.84 10.89 o -17 3 2 0.42 4.15 8.81 o -15 3 2 299.64 299.49 14.86 o -13 3 2 120.92 108.39 8.48 o -11 3 2 59.60 78.33 8.28 o -9 3 2 1318.95 1433.20 29.77 o -7 3 2 372.44 390.67 10.40 o -5 3 2 114.09 112.09 8.46 o -3 3 2 1002.10 1007.21 39.76 o -1 3 2 3065.53 3006.64 127.14 o 1 3 2 493.63 435.82 18.01 o 3 3 2 0.97 -2.77 13.94 o 5 3 2 886.51 850.21 33.84 o 7 3 2 42.93 43.27 17.09 o 9 3 2 9.35 6.62 16.94 o 11 3 2 2082.92 2206.04 33.55 o 13 3 2 43.76 40.90 11.96 o 15 3 2 0.33 3.67 12.48 o 17 3 2 1101.58 1221.35 21.10 o 19 3 2 20.00 21.46 15.06 o 21 3 2 104.29 105.27 16.03 o 23 3 2 122.42 133.69 17.72 o 25 3 2 0.04 0.58 19.32 o -26 4 2 1.32 4.57 15.27 o -24 4 2 999.50 1062.80 40.70 o -22 4 2 1241.08 1286.14 30.94 o -20 4 2 209.77 246.24 12.98 o -18 4 2 273.98 267.77 12.05 o -16 4 2 85.19 99.04 10.69 o -14 4 2 1110.75 1239.49 52.96 o -12 4 2 418.20 367.90 17.39 o -10 4 2 400.05 424.81 15.21 o -8 4 2 217.33 198.90 14.00 o -6 4 2 304.17 296.66 10.04 o -4 4 2 988.46 973.94 54.18 o -2 4 2 1200.86 1211.62 41.16 o 0 4 2 726.36 696.91 21.30 o 2 4 2 1007.87 917.75 22.12 o 4 4 2 1911.67 1765.01 26.52 o 6 4 2 319.80 289.38 17.01 o 8 4 2 5.33 1.98 13.10 o 10 4 2 1474.91 1354.80 77.41 o 12 4 2 997.99 1100.59 59.86 o 14 4 2 276.68 303.63 21.60 o 16 4 2 155.69 152.77 14.85 o 18 4 2 67.64 57.39 17.65 o 20 4 2 613.79 640.73 19.91 o 22 4 2 5.13 10.24 20.07 o -21 5 2 145.40 141.92 17.00 o -19 5 2 2.31 3.17 14.79 o -17 5 2 785.42 823.94 22.37 o -15 5 2 337.59 354.17 15.02 o -13 5 2 1322.40 1366.62 42.71 o -11 5 2 269.99 255.00 13.95 o -9 5 2 96.48 89.60 11.40 o -7 5 2 659.50 696.51 37.08 o -5 5 2 1166.01 1259.77 63.49 o -3 5 2 93.70 97.44 14.38 o -1 5 2 866.82 863.05 26.08 o 1 5 2 514.53 518.78 23.12 o 3 5 2 1297.88 1197.45 26.78 o 5 5 2 1225.69 1192.53 26.08 o 7 5 2 69.83 61.62 18.83 o 9 5 2 22.19 11.02 21.08 o 11 5 2 171.44 188.97 14.83 o 13 5 2 1933.85 1948.86 145.86 o 15 5 2 8.14 7.26 14.79 o 17 5 2 105.03 111.59 22.05 o 19 5 2 57.91 34.87 23.78 o -16 6 2 523.70 539.58 21.49 o -14 6 2 687.74 732.54 19.24 o -12 6 2 269.76 283.52 17.96 o -10 6 2 1.05 4.59 16.48 o -8 6 2 590.16 642.94 22.69 o -6 6 2 2102.68 2249.54 43.95 o -4 6 2 420.88 464.89 29.63 o -2 6 2 31.97 29.33 23.56 o 0 6 2 159.03 167.22 23.78 o 2 6 2 1864.60 1849.64 34.43 o 4 6 2 887.96 838.93 28.48 o 6 6 2 21.94 16.57 24.19 o 8 6 2 57.07 62.75 18.76 o 10 6 2 149.88 151.50 19.58 o 12 6 2 604.29 625.20 84.90 o -31 1 3 476.77 410.04 19.74 o -29 1 3 2.52 -4.26 13.89 o -27 1 3 24.98 31.50 10.35 o -25 1 3 918.88 907.84 31.95 o -23 1 3 590.15 563.26 12.97 o -21 1 3 536.88 518.74 15.54 o -19 1 3 93.58 95.03 7.03 o -17 1 3 891.82 981.94 13.02 o -15 1 3 1326.99 1449.69 22.78 o -13 1 3 1131.94 1097.04 18.70 o -11 1 3 264.40 275.75 7.18 o -9 1 3 9229.77 10164.06 138.90 o -7 1 3 504.32 561.56 10.43 o -5 1 3 40736.39 35339.22 406.74 o -3 1 3 1178.49 1080.01 15.43 o -1 1 3 1063.60 1020.73 13.92 o 1 1 3 153.99 118.60 9.96 o 5 1 3 638.70 731.52 21.64 o 7 1 3 74.48 154.72 14.28 o 9 1 3 104.45 116.14 15.02 o 11 1 3 46.30 42.50 14.42 o 13 1 3 39.07 31.96 9.21 o 15 1 3 1153.62 1150.58 46.51 o 17 1 3 845.50 904.22 41.33 o 19 1 3 141.79 149.64 13.82 o 21 1 3 118.21 114.53 12.31 o 23 1 3 294.91 279.45 22.51 o 25 1 3 390.80 355.06 16.10 o -30 2 3 240.49 220.87 14.82 o -28 2 3 8.73 14.57 13.33 o -26 2 3 43.56 57.64 10.33 o -24 2 3 1021.50 1005.00 13.35 o -22 2 3 3023.01 3077.74 47.96 o -20 2 3 1732.40 1791.69 72.10 o -18 2 3 620.80 666.70 15.99 o -16 2 3 1728.79 1645.18 37.30 o -14 2 3 3929.83 3967.11 94.90 o -12 2 3 3051.09 3258.20 82.48 o -10 2 3 237.50 314.36 8.84 o -8 2 3 3479.93 3853.10 108.10 o -6 2 3 92.01 69.04 6.37 o -4 2 3 2723.42 2442.88 70.86 o -2 2 3 388.31 333.16 11.84 o 0 2 3 5466.62 5424.00 43.87 o 2 2 3 634.36 533.60 34.66 o 4 2 3 8128.26 7735.96 977.60 o 6 2 3 2111.41 2293.44 38.17 o 8 2 3 2253.40 2549.43 36.21 o 10 2 3 139.23 171.03 17.24 o 12 2 3 4979.48 5401.59 43.61 o 14 2 3 1329.12 1476.04 21.43 o 16 2 3 615.00 642.25 14.98 o 18 2 3 59.29 63.60 11.53 o 20 2 3 74.61 79.99 14.67 o 22 2 3 501.71 497.83 15.12 o 24 2 3 492.44 520.99 16.89 o -29 3 3 21.56 12.94 14.32 o -27 3 3 92.72 93.85 12.54 o -25 3 3 191.81 177.56 12.45 o -23 3 3 1593.41 1627.40 38.62 o -21 3 3 491.98 520.05 12.97 o 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