#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:48:23 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181916 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/15/2241595.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241595 _cell_angle_alpha 66.026 _cell_angle_beta 76.030 _cell_angle_gamma 78.744 _cell_length_a 9.3980 _cell_length_b 14.8760 _cell_length_c 17.9810 _exptl_crystal_F_000 1124.00 _reflns_d_resolution_high 0.7072 _cod_data_source_file wm5272Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S121 in P-1 (block yellow)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 219.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 807.33 672.80 27.27 o 2 0 0 16425.78 14107.01 475.02 o 3 0 0 6378.56 6130.03 90.80 o 4 0 0 19206.47 18963.58 246.90 o 5 0 0 13817.87 13473.00 229.04 o 6 0 0 3632.93 3938.99 69.92 o 7 0 0 1643.32 1682.53 72.68 o 8 0 0 3456.87 3527.36 58.45 o 9 0 0 202.69 163.04 14.63 o 10 0 0 1576.09 1562.31 27.75 o 11 0 0 163.38 141.08 9.22 o 12 0 0 2.74 6.40 10.46 o -12 1 0 225.60 251.83 24.22 o -11 1 0 1526.24 1557.19 65.93 o -10 1 0 242.25 263.92 13.05 o -9 1 0 765.20 792.58 16.23 o -8 1 0 833.50 871.93 22.57 o -7 1 0 0.83 4.50 6.42 o -6 1 0 2013.84 2063.56 36.80 o -5 1 0 2513.51 2407.90 49.61 o -4 1 0 1875.63 1752.61 49.25 o -3 1 0 24.63 67.06 3.50 o -2 1 0 2067.57 2028.37 68.58 o -1 1 0 10311.21 8877.27 293.91 o 1 1 0 31.27 30.85 1.78 o 2 1 0 11670.26 9481.25 152.08 o 3 1 0 11135.31 10834.72 198.74 o 4 1 0 3406.68 3479.94 82.94 o 5 1 0 4928.50 5191.55 181.58 o 6 1 0 67.99 95.73 7.02 o 7 1 0 8075.75 8407.01 289.54 o 8 1 0 4.30 10.56 7.10 o 9 1 0 179.58 165.34 9.66 o 10 1 0 718.15 719.13 16.51 o 11 1 0 752.38 716.73 21.50 o 12 1 0 922.23 940.06 39.39 o -12 2 0 742.67 734.50 18.95 o -11 2 0 176.51 119.68 12.97 o -10 2 0 1730.65 1861.56 38.89 o -9 2 0 3326.96 3080.49 78.30 o -8 2 0 1566.43 1608.32 50.71 o -7 2 0 17.36 21.09 12.71 o -6 2 0 13155.79 13958.41 602.51 o -5 2 0 2.71 4.92 3.76 o -4 2 0 19355.62 18602.55 597.55 o -3 2 0 172.90 147.01 7.15 o -1 2 0 3985.89 3143.39 62.13 o 0 2 0 1284.22 753.18 22.11 o 1 2 0 1039.21 800.77 22.43 o 2 2 0 34.65 18.33 1.47 o 3 2 0 643.95 571.27 18.01 o 4 2 0 3553.62 3706.42 54.96 o 5 2 0 13152.58 12741.12 317.87 o 6 2 0 3939.29 4185.34 74.37 o 7 2 0 1664.14 1683.54 38.20 o 8 2 0 18.41 9.41 5.92 o 9 2 0 2.78 -0.79 5.56 o 10 2 0 124.49 111.29 7.44 o 11 2 0 105.71 95.92 10.57 o 12 2 0 278.74 291.94 18.27 o -12 3 0 636.72 684.20 30.45 o -11 3 0 84.12 80.26 10.47 o -10 3 0 1740.85 1717.01 55.21 o -9 3 0 545.24 536.78 42.96 o -8 3 0 268.37 269.95 16.81 o -7 3 0 729.35 642.76 14.50 o -6 3 0 1201.12 1327.08 22.52 o -5 3 0 189.88 148.66 5.86 o -4 3 0 4021.12 3927.36 72.55 o -3 3 0 2.63 9.53 6.62 o -2 3 0 1193.27 1146.41 18.01 o -1 3 0 1039.03 847.07 16.77 o 0 3 0 391.06 268.87 7.74 o 2 3 0 11823.79 10286.51 231.71 o 3 3 0 96.65 105.01 5.69 o 4 3 0 1067.83 1246.07 38.92 o 5 3 0 1.60 12.99 4.13 o 6 3 0 402.89 445.07 18.01 o 7 3 0 3070.14 3198.43 83.94 o 8 3 0 5427.20 5375.91 93.20 o 9 3 0 174.18 135.18 15.49 o 10 3 0 415.62 451.00 15.75 o 11 3 0 76.31 71.23 8.49 o 12 3 0 285.99 263.06 32.30 o -12 4 0 120.43 129.77 24.76 o -11 4 0 69.62 62.62 11.22 o -10 4 0 380.28 372.26 15.63 o -9 4 0 2830.15 2985.87 121.47 o -8 4 0 8886.66 8997.04 844.20 o -7 4 0 238.85 174.49 11.25 o -6 4 0 1693.71 1774.83 34.29 o -5 4 0 256.37 211.96 10.86 o -4 4 0 1762.52 1461.58 26.42 o -3 4 0 3793.19 3918.47 103.99 o -2 4 0 2583.03 2782.64 96.58 o -1 4 0 225.85 176.38 6.55 o 0 4 0 23238.05 20585.53 463.16 o 1 4 0 412.95 353.75 14.83 o 2 4 0 8470.99 7847.34 165.03 o 3 4 0 247.35 237.11 12.58 o 4 4 0 4166.22 3330.08 181.58 o 5 4 0 1181.90 1065.82 43.95 o 6 4 0 1935.61 1994.22 73.74 o 7 4 0 2338.34 2689.03 68.25 o 8 4 0 549.19 582.92 17.48 o 9 4 0 843.97 892.13 23.42 o 10 4 0 5130.90 5369.58 104.78 o 11 4 0 430.80 436.41 25.22 o 12 4 0 464.74 503.61 32.83 o -12 5 0 716.71 782.43 84.14 o -11 5 0 33.38 34.91 11.50 o -10 5 0 834.30 795.04 54.61 o -9 5 0 101.09 98.84 10.46 o -8 5 0 19.94 15.89 10.46 o -7 5 0 1962.55 1962.02 61.89 o -6 5 0 671.55 777.93 15.90 o -5 5 0 334.43 312.82 7.36 o -4 5 0 189.29 192.90 9.73 o -3 5 0 151.91 147.62 12.84 o -2 5 0 497.32 457.93 16.22 o -1 5 0 9197.63 8144.13 218.71 o 0 5 0 3330.93 3084.06 55.47 o 1 5 0 79.27 77.22 3.59 o 3 5 0 649.03 725.90 24.36 o 4 5 0 11865.93 11494.23 288.28 o 5 5 0 235.90 250.46 7.68 o 6 5 0 11544.11 11840.21 226.28 o 7 5 0 2914.77 3102.68 63.63 o 8 5 0 251.26 268.76 19.33 o 9 5 0 1205.57 1212.97 48.72 o 10 5 0 60.46 59.59 10.29 o 11 5 0 273.47 223.29 16.11 o 12 5 0 669.32 710.70 32.44 o -11 6 0 78.91 66.14 10.61 o -10 6 0 3307.05 3318.72 101.35 o -9 6 0 809.87 781.72 30.65 o -8 6 0 1145.32 1225.60 65.86 o -7 6 0 241.99 264.14 10.92 o -6 6 0 3090.59 2970.74 78.38 o -5 6 0 7371.39 7848.96 150.63 o -4 6 0 13782.71 13207.96 238.44 o -3 6 0 1341.58 1193.68 18.19 o -2 6 0 18451.51 18014.95 851.68 o -1 6 0 1024.16 1006.27 24.56 o 0 6 0 33770.82 31781.58 717.83 o 1 6 0 5354.95 5189.95 115.84 o 2 6 0 800.39 635.75 20.39 o 3 6 0 2631.54 2623.22 94.06 o 4 6 0 598.54 482.75 31.44 o 5 6 0 3018.98 2759.75 97.04 o 6 6 0 2584.94 2520.27 153.91 o 7 6 0 21.23 22.77 14.17 o 8 6 0 2067.70 2181.02 63.81 o 9 6 0 1245.55 1242.10 38.26 o 10 6 0 62.27 97.57 17.87 o 11 6 0 1.51 21.36 13.34 o 12 6 0 113.65 87.79 29.39 o -11 7 0 353.92 326.45 26.81 o -10 7 0 843.51 748.81 26.35 o -9 7 0 470.81 422.33 18.09 o -8 7 0 246.02 245.37 14.43 o -7 7 0 24.11 34.09 5.48 o -6 7 0 1.11 2.48 5.38 o -5 7 0 4229.60 4149.84 74.10 o -4 7 0 279.53 272.23 10.86 o -3 7 0 368.84 351.03 13.64 o -2 7 0 2534.47 2666.48 41.99 o -1 7 0 504.89 499.43 10.22 o 0 7 0 13170.38 13987.38 869.42 o 1 7 0 1911.91 1948.52 37.18 o 2 7 0 4010.86 4055.81 96.04 o 3 7 0 3515.04 3534.07 86.05 o 4 7 0 209.55 204.41 7.81 o 5 7 0 149.15 116.28 5.35 o 6 7 0 3970.45 4038.98 90.03 o 7 7 0 92.52 90.03 14.17 o 8 7 0 789.16 771.73 43.56 o 9 7 0 585.86 656.17 32.30 o 10 7 0 13.09 15.56 8.94 o 11 7 0 815.58 782.30 51.77 o 12 7 0 452.81 404.00 17.99 o -11 8 0 23.75 13.41 10.19 o -10 8 0 11.72 21.49 14.52 o -9 8 0 44.64 35.69 20.12 o -8 8 0 3303.79 3481.20 75.76 o -7 8 0 179.69 194.71 15.49 o -6 8 0 958.63 1009.50 29.32 o -5 8 0 4545.69 4423.53 110.29 o -4 8 0 139.57 152.14 5.50 o -3 8 0 1089.56 1186.61 34.82 o -2 8 0 2369.06 2391.38 157.48 o -1 8 0 0.21 0.53 3.63 o 0 8 0 4625.24 4363.31 125.90 o 1 8 0 641.71 609.75 41.64 o 2 8 0 3519.99 3171.14 82.28 o 3 8 0 15.87 17.92 5.23 o 4 8 0 1282.31 1389.71 55.07 o 5 8 0 2883.14 2889.37 67.39 o 6 8 0 590.51 547.43 44.62 o 7 8 0 625.57 603.60 17.28 o 8 8 0 20.86 1.89 9.82 o 9 8 0 554.74 612.44 37.33 o 10 8 0 1574.64 1709.05 73.35 o 11 8 0 27.84 17.28 15.82 o 12 8 0 1660.32 1711.69 54.94 o -10 9 0 92.63 83.74 9.64 o -9 9 0 23.25 21.47 8.36 o -8 9 0 160.87 171.03 18.07 o -7 9 0 86.43 87.91 11.19 o -6 9 0 332.92 287.17 16.62 o -5 9 0 1229.33 1273.33 74.40 o -4 9 0 592.08 561.45 14.20 o -3 9 0 6365.06 6684.73 135.97 o -2 9 0 1450.26 1554.73 127.89 o -1 9 0 798.21 829.96 25.68 o 0 9 0 1656.20 1613.15 134.18 o 1 9 0 252.64 258.20 19.73 o 2 9 0 6503.61 6458.62 295.83 o 3 9 0 2600.00 2821.82 50.31 o 5 9 0 1555.19 1731.82 69.77 o 6 9 0 336.91 349.42 27.34 o 7 9 0 1385.46 1434.20 39.98 o 8 9 0 509.68 601.99 28.46 o 9 9 0 29.87 32.04 10.72 o 10 9 0 282.10 302.59 21.16 o 11 9 0 477.51 485.32 34.69 o -10 10 0 836.64 808.29 44.62 o -9 10 0 447.67 500.97 24.47 o -8 10 0 749.30 729.42 28.40 o -7 10 0 24.78 19.94 10.56 o -6 10 0 217.34 238.34 9.36 o -5 10 0 2259.82 2259.88 41.13 o -4 10 0 350.99 364.13 16.59 o -3 10 0 49.40 46.57 5.29 o -2 10 0 2415.33 2483.15 98.96 o -1 10 0 207.24 203.44 10.06 o 0 10 0 11397.17 11840.95 204.15 o 1 10 0 1184.31 1297.59 30.70 o 2 10 0 420.15 419.02 14.83 o 3 10 0 437.22 417.17 16.28 o 4 10 0 2450.46 2535.70 80.23 o 5 10 0 1927.25 2015.94 53.22 o 6 10 0 5288.46 5263.08 114.36 o 7 10 0 32.04 16.28 13.64 o 8 10 0 3874.20 4214.82 106.05 o 9 10 0 64.53 74.54 15.75 o 10 10 0 3409.70 3471.87 250.82 o 11 10 0 62.84 48.71 15.36 o -9 11 0 16.00 19.37 11.89 o -8 11 0 199.68 200.09 21.32 o -7 11 0 286.91 285.84 21.45 o -6 11 0 636.70 663.53 17.80 o -5 11 0 12.25 15.88 5.16 o -4 11 0 90.10 88.33 13.24 o -3 11 0 594.25 578.50 21.41 o -2 11 0 22.83 34.44 5.89 o -1 11 0 520.90 539.93 12.93 o 0 11 0 627.01 654.06 13.42 o 1 11 0 46.16 55.61 6.95 o 2 11 0 7167.27 6710.68 229.70 o 3 11 0 314.83 310.15 11.65 o 4 11 0 631.23 633.71 17.66 o 6 11 0 179.83 145.74 13.50 o 7 11 0 3416.03 3388.64 101.54 o 8 11 0 0.16 -10.03 12.56 o 9 11 0 524.93 461.65 23.17 o 10 11 0 76.66 54.95 14.39 o 11 11 0 4.57 8.95 19.57 o -9 12 0 1131.80 1113.20 43.03 o -8 12 0 367.93 369.76 14.91 o -7 12 0 428.33 422.13 16.75 o -6 12 0 2624.32 2849.65 238.57 o -5 12 0 34.59 35.58 8.43 o -4 12 0 1742.04 1850.08 40.73 o -3 12 0 122.55 129.88 8.71 o -2 12 0 4501.49 4703.17 89.65 o -1 12 0 738.64 732.24 17.50 o 0 12 0 179.59 168.48 8.96 o 1 12 0 909.00 882.39 22.37 o 2 12 0 791.91 868.08 27.63 o 3 12 0 28.96 32.09 5.17 o 4 12 0 3043.54 3038.79 74.93 o 5 12 0 952.46 883.19 30.45 o 6 12 0 1485.35 1573.04 88.64 o 7 12 0 0.57 32.70 17.74 o 8 12 0 956.87 1073.43 55.60 o 9 12 0 36.68 10.59 22.11 o 10 12 0 6.37 11.46 17.60 o -8 13 0 67.74 76.52 15.49 o -7 13 0 69.96 70.14 7.66 o -6 13 0 33.77 20.08 8.16 o -5 13 0 1.09 3.85 8.97 o -4 13 0 189.03 181.21 11.46 o -3 13 0 184.35 209.30 13.07 o -2 13 0 85.11 93.30 8.05 o -1 13 0 57.00 55.78 7.19 o 0 13 0 381.92 410.09 14.37 o 1 13 0 49.91 58.08 6.88 o 2 13 0 3179.98 3175.69 65.05 o 3 13 0 351.45 363.42 13.11 o 4 13 0 42.33 58.29 7.94 o 5 13 0 14.75 16.12 7.35 o 6 13 0 1193.29 1263.94 49.38 o 7 13 0 617.44 599.05 24.10 o 8 13 0 16.10 29.39 17.21 o 10 13 0 124.10 113.86 18.53 o -7 14 0 0.92 5.89 15.37 o -6 14 0 2.17 -1.24 10.04 o -5 14 0 31.07 32.02 9.19 o -4 14 0 23.44 25.68 12.05 o -3 14 0 2.25 11.22 8.60 o -2 14 0 211.18 172.64 18.67 o -1 14 0 5.14 5.12 8.74 o 0 14 0 779.59 804.94 26.35 o 1 14 0 3618.50 3668.97 80.10 o 3 14 0 386.34 345.02 14.59 o 4 14 0 3.87 24.52 16.95 o 5 14 0 644.20 600.04 23.20 o 6 14 0 1162.48 1124.40 66.73 o 7 14 0 2.01 -5.06 11.63 o 8 14 0 44.79 37.86 13.50 o 9 14 0 1400.15 1282.15 95.39 o -6 15 0 8.60 -3.02 14.24 o -5 15 0 422.54 408.94 18.68 o -4 15 0 144.45 131.66 14.96 o -3 15 0 502.12 522.53 31.84 o -2 15 0 109.71 121.70 10.37 o -1 15 0 315.29 299.19 13.37 o 0 15 0 1118.87 1095.74 29.50 o 1 15 0 25.19 29.67 6.87 o 2 15 0 621.61 594.39 18.12 o 3 15 0 1963.19 1956.54 48.71 o 4 15 0 1476.31 1476.37 49.71 o 5 15 0 1.08 -9.93 12.58 o 6 15 0 219.87 197.65 12.59 o 7 15 0 142.41 119.81 13.90 o -5 16 0 171.46 159.10 13.01 o -4 16 0 188.11 175.37 14.01 o -3 16 0 674.26 610.72 20.65 o -2 16 0 780.97 804.98 23.34 o -1 16 0 624.92 707.24 22.51 o 0 16 0 1071.34 1156.18 60.77 o 1 16 0 400.25 371.62 28.20 o 2 16 0 78.81 83.47 15.63 o 3 16 0 145.09 154.69 16.94 o 4 16 0 1311.22 1334.91 43.95 o 5 16 0 1.11 -0.93 14.96 o 6 16 0 747.65 704.37 37.53 o 7 16 0 463.63 545.45 39.06 o 8 16 0 1568.51 1715.53 65.93 o -4 17 0 1120.58 1143.86 29.26 o -3 17 0 905.77 911.53 26.18 o -2 17 0 35.49 25.82 10.99 o -1 17 0 49.34 48.99 10.01 o 0 17 0 712.99 668.04 22.73 o 1 17 0 1.05 -0.79 18.27 o 2 17 0 38.10 29.93 11.71 o 3 17 0 142.11 115.84 18.66 o 4 17 0 56.61 39.06 26.61 o 5 17 0 231.14 209.05 18.40 o 6 17 0 39.86 66.46 32.44 o 7 17 0 2.62 21.78 30.25 o -3 18 0 56.11 51.40 13.55 o -2 18 0 415.58 441.97 27.71 o -1 18 0 219.88 196.43 21.65 o 0 18 0 289.59 264.25 31.38 o 1 18 0 362.73 339.27 14.66 o 2 18 0 1049.65 1112.30 28.02 o 3 18 0 25.27 37.18 17.24 o 4 18 0 273.17 302.91 42.03 o 5 18 0 72.79 60.07 21.98 o 0 19 0 1524.70 1398.45 59.18 o 1 19 0 118.40 106.39 21.58 o 2 19 0 221.29 223.87 25.82 o 3 19 0 205.57 213.02 28.33 o -5 -18 1 97.34 61.43 32.70 o -4 -18 1 826.45 768.55 38.61 o -3 -18 1 143.81 135.17 29.66 o -2 -18 1 240.44 239.23 33.89 o -1 -18 1 668.90 669.47 30.35 o 0 -18 1 40.81 25.95 20.26 o 1 -18 1 3.67 7.93 10.30 o 2 -18 1 356.17 328.60 32.70 o -5 -17 1 1286.73 1294.64 36.24 o -4 -17 1 56.78 39.24 12.99 o -3 -17 1 140.85 146.29 30.58 o -2 -17 1 1746.07 1705.47 79.30 o -1 -17 1 1276.09 1115.67 44.09 o 1 -17 1 387.18 380.56 20.68 o 2 -17 1 0.92 -1.76 11.61 o 3 -17 1 855.13 822.82 52.03 o 4 -17 1 204.10 200.14 13.90 o -6 -16 1 16.21 21.05 15.89 o -5 -16 1 397.52 365.48 19.14 o -4 -16 1 308.98 305.96 28.73 o -3 -16 1 29.79 50.18 21.18 o -2 -16 1 440.09 466.04 20.47 o -1 -16 1 227.24 232.96 21.12 o 0 -16 1 280.04 293.64 20.79 o 1 -16 1 2.61 3.59 11.61 o 2 -16 1 217.87 223.14 10.87 o 3 -16 1 166.47 147.75 16.42 o 4 -16 1 33.17 39.31 17.32 o 5 -16 1 653.84 645.99 21.74 o -8 -15 1 41.95 23.96 18.80 o -6 -15 1 1.32 -7.91 10.52 o -5 -15 1 222.30 221.62 18.27 o -4 -15 1 40.71 37.73 13.90 o -3 -15 1 299.11 288.17 21.18 o -2 -15 1 204.68 174.68 21.71 o -1 -15 1 485.94 485.76 13.58 o 0 -15 1 3.45 8.60 9.45 o 1 -15 1 402.71 379.18 14.83 o 2 -15 1 18.42 20.01 7.34 o 3 -15 1 211.78 226.03 10.44 o 4 -15 1 14.43 15.02 11.05 o 5 -15 1 38.70 38.27 36.47 o 6 -15 1 24.38 44.17 14.69 o -9 -14 1 5.67 14.17 23.83 o -7 -14 1 0.01 5.43 16.95 o -6 -14 1 4.56 12.33 11.98 o -5 -14 1 40.90 43.56 16.81 o -4 -14 1 21.16 29.41 10.06 o -3 -14 1 814.20 823.08 25.77 o -2 -14 1 1000.68 967.22 57.39 o -1 -14 1 1770.58 1814.20 97.71 o 0 -14 1 804.14 808.25 25.95 o 1 -14 1 663.37 697.70 19.67 o 2 -14 1 510.67 494.97 16.27 o 3 -14 1 1686.34 1644.47 50.23 o 4 -14 1 177.01 178.32 12.91 o 5 -14 1 2.07 3.13 16.68 o 6 -14 1 477.55 444.27 15.42 o 7 -14 1 63.70 56.53 15.49 o -10 -13 1 64.91 90.29 22.90 o -9 -13 1 196.45 289.14 34.55 o -8 -13 1 216.25 167.87 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