#------------------------------------------------------------------------------ #$Date: 2016-04-06 19:49:14 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181917 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/16/2241603.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2241603 _cell_angle_alpha 90.000 _cell_angle_beta 115.188 _cell_angle_gamma 90.000 _cell_length_a 10.1879 _cell_length_b 10.0912 _cell_length_c 11.9055 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.7695 _cod_data_source_file wm5276Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' diop511_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10609.93 10509.78 294.63 o 4 0 0 2723.48 2849.85 49.14 o 6 0 0 9.16 8.72 1.02 o 8 0 0 165.21 162.90 4.46 o 10 0 0 569.78 544.59 17.44 o 1 1 0 1028.11 920.35 26.28 o 3 1 0 2847.22 2809.77 40.89 o 5 1 0 6.41 11.87 0.82 o 7 1 0 842.85 876.61 13.32 o 9 1 0 251.80 237.41 4.89 o 11 1 0 26.06 22.67 1.82 o 0 2 0 2395.26 2454.16 101.15 o 2 2 0 3898.71 3900.19 106.01 o 4 2 0 633.46 689.14 9.07 o 6 2 0 344.62 323.12 4.66 o 8 2 0 994.29 943.25 23.10 o 10 2 0 71.70 65.79 3.16 o 1 3 0 7450.30 7629.73 156.24 o 3 3 0 266.72 324.70 5.85 o 5 3 0 298.62 275.75 4.21 o 7 3 0 72.61 88.47 2.58 o 9 3 0 49.65 38.63 2.41 o 11 3 0 50.14 54.38 2.63 o 0 4 0 5875.20 6232.02 169.22 o 2 4 0 1274.75 1258.39 21.91 o 4 4 0 308.42 332.08 4.49 o 6 4 0 732.95 699.28 10.83 o 8 4 0 294.39 273.29 5.04 o 10 4 0 49.46 55.11 2.32 o 1 5 0 1121.22 1167.22 17.30 o 3 5 0 2182.18 2177.10 32.83 o 5 5 0 82.81 78.36 2.03 o 7 5 0 1067.24 960.48 14.82 o 9 5 0 0.90 2.06 1.25 o 11 5 0 47.13 55.77 8.48 o 0 6 0 1937.09 1940.26 43.58 o 2 6 0 593.22 601.31 8.58 o 4 6 0 244.35 250.08 3.66 o 6 6 0 10.77 14.77 1.11 o 8 6 0 78.70 71.96 2.35 o 10 6 0 92.56 112.13 4.36 o 1 7 0 524.76 482.14 8.16 o 3 7 0 257.73 244.70 3.98 o 5 7 0 1450.71 1439.29 19.11 o 7 7 0 51.14 47.16 1.99 o 9 7 0 223.87 212.00 4.40 o 0 8 0 11.99 11.51 1.45 o 2 8 0 165.17 180.93 3.40 o 4 8 0 405.01 379.67 6.29 o 6 8 0 98.09 80.34 2.84 o 8 8 0 43.18 50.38 2.62 o 1 9 0 0.16 1.47 1.17 o 3 9 0 24.25 23.22 1.58 o 5 9 0 0.85 -1.23 1.23 o 7 9 0 9.60 10.92 1.80 o 0 10 0 285.54 272.03 8.92 o 2 10 0 146.92 146.60 9.42 o 4 10 0 164.53 164.22 4.22 o 6 10 0 16.03 16.73 1.91 o 1 11 0 43.05 47.13 2.14 o 3 11 0 5.99 6.22 1.53 o 5 11 0 268.41 244.22 8.68 o 0 12 0 640.76 615.54 15.02 o 2 12 0 0.61 0.30 1.29 o 4 12 0 54.41 53.05 2.99 o 1 13 0 0.29 2.24 1.43 o -11 1 1 3.50 4.39 1.92 o -9 1 1 558.12 544.99 9.52 o -7 1 1 30.31 29.42 1.20 o -5 1 1 351.10 396.59 5.40 o -3 1 1 1164.30 1183.03 25.85 o -1 1 1 250.91 226.62 15.66 o 1 1 1 5045.03 5177.25 104.13 o 3 1 1 4902.37 4853.82 76.16 o 5 1 1 4120.03 4177.99 51.77 o 7 1 1 130.38 128.63 2.61 o 9 1 1 7.31 5.15 1.28 o 11 1 1 117.36 123.24 4.61 o -12 2 1 20.10 17.65 2.04 o -10 2 1 3.12 1.03 1.61 o -8 2 1 1399.24 1320.94 19.87 o -6 2 1 700.51 719.58 10.19 o -4 2 1 1946.02 2009.02 31.76 o -2 2 1 25707.22 27425.65 756.94 o 0 2 1 5995.48 6037.88 173.04 o 2 2 1 0.16 20.33 2.16 o 4 2 1 605.25 578.98 6.94 o 6 2 1 7.76 34.21 1.43 o 8 2 1 353.26 328.05 5.78 o 10 2 1 38.18 44.73 1.97 o -11 3 1 468.24 448.58 10.45 o -9 3 1 35.48 28.18 1.78 o -7 3 1 2.09 0.57 0.83 o -5 3 1 382.58 411.34 6.43 o -3 3 1 129.31 133.00 2.68 o -1 3 1 6196.90 5772.39 221.99 o 1 3 1 15062.05 15356.02 376.91 o 3 3 1 37.42 38.71 1.58 o 5 3 1 253.16 258.05 3.83 o 7 3 1 17.39 20.40 1.47 o 9 3 1 3.72 4.66 1.35 o 11 3 1 8.71 12.21 2.27 o -10 4 1 9.59 18.14 1.86 o -8 4 1 439.29 419.49 7.07 o -6 4 1 61.47 83.85 2.16 o -4 4 1 2438.60 2628.31 38.46 o -2 4 1 369.51 348.51 6.37 o 0 4 1 1136.45 1172.22 14.41 o 2 4 1 1579.19 1624.30 19.91 o 4 4 1 1804.99 1839.70 23.91 o 6 4 1 276.72 286.41 4.65 o 8 4 1 25.94 34.06 1.73 o 10 4 1 10.45 12.58 1.48 o -11 5 1 9.11 9.84 2.11 o -9 5 1 24.22 25.04 1.55 o -7 5 1 587.87 549.27 8.86 o -5 5 1 44.12 50.52 1.36 o -3 5 1 7608.05 8032.40 138.02 o -1 5 1 736.89 702.73 10.52 o 1 5 1 106.43 129.43 2.14 o 3 5 1 298.58 315.51 3.74 o 5 5 1 243.50 220.53 3.51 o 7 5 1 102.63 90.37 2.37 o 9 5 1 133.04 134.24 3.13 o -10 6 1 2.35 3.53 1.58 o -8 6 1 33.82 23.55 1.68 o -6 6 1 2.89 8.65 1.62 o -4 6 1 782.18 789.44 11.24 o -2 6 1 2068.01 2044.04 25.11 o 0 6 1 380.05 384.81 9.33 o 2 6 1 48.37 57.55 1.27 o 4 6 1 55.63 53.54 1.39 o 6 6 1 10.74 9.34 1.02 o 8 6 1 38.13 42.10 2.04 o 10 6 1 30.99 36.47 2.29 o -9 7 1 168.92 163.44 4.63 o -7 7 1 7.40 6.70 1.10 o -5 7 1 73.52 72.51 2.05 o -3 7 1 911.35 926.98 13.12 o -1 7 1 38.85 36.47 1.45 o 1 7 1 13.73 23.91 1.07 o 3 7 1 37.37 33.93 1.16 o 5 7 1 1260.12 1230.29 17.49 o 7 7 1 75.60 65.30 2.51 o 9 7 1 4.06 4.49 1.83 o -8 8 1 296.05 281.83 6.36 o -6 8 1 0.01 0.23 1.09 o -4 8 1 1365.98 1343.58 21.86 o -2 8 1 112.26 108.01 2.78 o 0 8 1 1.98 4.61 1.04 o 2 8 1 143.87 153.14 3.16 o 4 8 1 40.55 41.28 1.74 o 6 8 1 388.56 373.51 6.91 o 8 8 1 7.86 14.07 2.01 o -9 9 1 267.32 287.31 10.81 o -7 9 1 292.89 273.96 8.98 o -5 9 1 105.54 104.59 2.81 o -3 9 1 99.42 90.31 2.62 o -1 9 1 82.61 77.26 2.70 o 1 9 1 483.51 446.44 9.46 o 3 9 1 346.19 332.31 6.11 o 5 9 1 61.29 61.46 2.80 o 7 9 1 14.26 16.47 1.99 o -8 10 1 2.32 4.90 5.54 o -6 10 1 252.49 253.77 6.39 o -4 10 1 36.76 38.28 2.08 o -2 10 1 159.59 152.31 6.63 o 0 10 1 27.28 25.78 1.69 o 2 10 1 35.59 30.26 2.08 o 4 10 1 682.59 664.60 12.76 o 6 10 1 18.45 19.34 2.04 o -5 11 1 26.50 27.49 2.72 o -3 11 1 158.04 156.57 4.65 o -1 11 1 12.68 12.63 1.35 o 1 11 1 319.05 315.73 5.98 o 3 11 1 48.62 50.42 2.92 o 5 11 1 6.21 9.23 5.44 o -4 12 1 1.44 0.00 1.57 o -2 12 1 3.82 3.99 1.49 o 0 12 1 0.00 1.13 1.27 o 2 12 1 97.85 103.24 3.74 o 4 12 1 3.86 3.91 1.60 o -1 13 1 0.03 0.42 1.61 o 1 13 1 4.25 6.88 2.52 o -12 0 2 40.39 36.46 4.08 o -10 0 2 1318.10 1216.46 28.59 o -8 0 2 31.55 45.10 2.52 o -6 0 2 2163.82 2254.25 43.51 o -4 0 2 1335.57 1294.65 25.19 o -2 0 2 1062.62 1134.08 43.79 o 0 0 2 2318.10 2375.82 66.15 o 2 0 2 16343.93 16746.80 465.54 o 4 0 2 1054.41 1041.71 29.78 o 6 0 2 43.71 53.43 3.40 o 8 0 2 0.05 -0.18 1.37 o 10 0 2 50.15 42.87 3.24 o -11 1 2 12.27 9.76 2.07 o -9 1 2 114.03 104.99 3.02 o -7 1 2 1486.91 1501.44 20.86 o -5 1 2 0.18 2.81 0.51 o -3 1 2 1312.10 1472.73 28.48 o -1 1 2 6017.11 5887.54 134.57 o 1 1 2 6423.98 5883.81 225.87 o 3 1 2 1543.23 1574.79 24.91 o 5 1 2 2144.13 2206.10 28.59 o 7 1 2 140.61 137.37 2.85 o 9 1 2 170.89 184.87 3.58 o 11 1 2 0.45 2.02 1.86 o -12 2 2 0.33 3.76 1.70 o -10 2 2 71.41 72.36 3.31 o -8 2 2 53.78 55.41 1.90 o -6 2 2 1491.60 1492.90 23.46 o -4 2 2 2280.78 2281.64 39.49 o -2 2 2 5376.89 5103.17 189.02 o 0 2 2 9.43 10.52 0.45 o 2 2 2 158.19 134.65 2.39 o 4 2 2 96.05 91.28 1.59 o 6 2 2 228.54 215.73 4.26 o 8 2 2 49.84 51.66 1.84 o 10 2 2 43.22 48.19 2.26 o -11 3 2 244.95 242.35 5.43 o -9 3 2 144.18 119.19 2.99 o -7 3 2 9.47 10.90 0.91 o -5 3 2 148.99 149.09 2.76 o -3 3 2 188.12 157.46 3.15 o -1 3 2 3899.21 3689.32 63.45 o 1 3 2 983.78 886.86 14.14 o 3 3 2 561.68 617.99 8.83 o 5 3 2 96.08 94.12 2.15 o 7 3 2 358.50 342.66 6.49 o 9 3 2 235.80 244.39 4.59 o -12 4 2 80.13 96.86 3.92 o -10 4 2 204.74 189.30 4.16 o -8 4 2 8.50 14.00 1.24 o -6 4 2 0.47 0.54 0.69 o -4 4 2 3.59 2.00 0.55 o -2 4 2 799.16 750.48 13.19 o 0 4 2 329.56 386.54 6.99 o 2 4 2 198.04 194.71 2.39 o 4 4 2 106.86 134.77 2.07 o 6 4 2 130.36 139.61 3.20 o 8 4 2 41.54 56.81 2.22 o 10 4 2 26.92 31.12 1.94 o -11 5 2 0.92 6.89 1.83 o -9 5 2 66.72 83.44 2.60 o -7 5 2 582.80 559.78 9.01 o -5 5 2 28.03 26.00 1.17 o -3 5 2 1621.60 1640.31 27.31 o -1 5 2 165.70 146.35 2.35 o 1 5 2 617.73 615.56 8.21 o 3 5 2 904.52 838.61 9.28 o 5 5 2 670.51 663.90 8.69 o 7 5 2 4.27 2.52 1.13 o 9 5 2 0.02 1.91 1.54 o -10 6 2 247.85 240.98 4.56 o -8 6 2 44.53 65.31 2.29 o -6 6 2 41.11 48.35 1.71 o -4 6 2 0.79 1.21 0.65 o -2 6 2 2015.79 2178.13 31.97 o 0 6 2 388.23 399.72 6.30 o 2 6 2 3208.56 3277.13 38.27 o 4 6 2 96.66 90.73 1.88 o 6 6 2 154.38 156.29 3.15 o 8 6 2 306.98 310.79 5.66 o -9 7 2 89.41 100.53 3.02 o -7 7 2 513.42 533.13 9.29 o -5 7 2 94.87 95.37 2.59 o -3 7 2 725.80 694.58 11.56 o -1 7 2 110.28 106.15 2.96 o 1 7 2 74.78 82.57 2.02 o 3 7 2 47.14 55.12 1.57 o 5 7 2 83.83 73.14 2.24 o 7 7 2 186.33 203.68 4.17 o 9 7 2 53.81 55.49 3.09 o -10 8 2 19.92 22.99 2.74 o -8 8 2 24.63 22.69 1.72 o -6 8 2 795.03 775.39 12.10 o -4 8 2 1738.84 1689.49 28.84 o -2 8 2 27.08 33.37 1.83 o 0 8 2 300.83 317.79 5.90 o 2 8 2 14.74 14.15 1.07 o 4 8 2 0.04 0.94 1.00 o 6 8 2 1.60 1.06 1.29 o 8 8 2 27.78 30.53 2.14 o -9 9 2 1.17 2.36 3.46 o -7 9 2 3.75 4.39 1.48 o -5 9 2 171.99 173.39 3.95 o -3 9 2 638.73 610.22 11.46 o -1 9 2 488.74 462.00 8.75 o 1 9 2 463.00 460.41 8.07 o 3 9 2 29.65 33.91 1.92 o 5 9 2 39.31 42.56 2.56 o 7 9 2 126.71 134.96 4.63 o -8 10 2 36.10 30.16 2.80 o -6 10 2 513.60 497.87 10.91 o -4 10 2 92.55 84.85 2.80 o -2 10 2 82.95 89.17 4.28 o 0 10 2 3.03 3.35 1.36 o 2 10 2 88.17 86.76 3.00 o 4 10 2 372.83 366.57 7.61 o 6 10 2 46.67 48.93 3.63 o -7 11 2 28.83 39.91 5.27 o -5 11 2 223.67 202.62 7.83 o -3 11 2 0.94 1.17 1.25 o -1 11 2 179.18 172.92 3.95 o 1 11 2 28.37 31.92 1.71 o 3 11 2 102.16 102.51 3.96 o 5 11 2 69.48 58.81 3.40 o -4 12 2 172.42 177.46 5.52 o -2 12 2 131.50 144.13 3.83 o 0 12 2 150.86 151.48 3.69 o 2 12 2 374.74 378.15 7.92 o -1 13 2 98.76 103.22 9.51 o -11 1 3 221.06 196.36 5.05 o -9 1 3 76.50 72.55 2.70 o -7 1 3 632.09 604.07 7.45 o -5 1 3 288.22 268.91 4.61 o -3 1 3 643.10 571.03 11.26 o -1 1 3 11036.45 11274.70 311.78 o 1 1 3 4239.85 4601.10 102.08 o 3 1 3 2809.79 3063.55 37.08 o 5 1 3 1969.94 1959.05 22.17 o 7 1 3 1259.40 1247.96 15.18 o 9 1 3 25.97 25.62 1.56 o -12 2 3 95.36 86.77 3.75 o -10 2 3 89.86 84.08 3.41 o -8 2 3 58.23 73.03 1.91 o -6 2 3 1663.77 1724.93 26.59 o -4 2 3 13.43 19.53 1.17 o -2 2 3 937.90 1075.89 20.93 o 0 2 3 532.08 415.06 5.90 o 2 2 3 49.14 51.91 1.08 o 4 2 3 111.54 176.27 2.40 o 6 2 3 13.64 23.66 1.30 o 8 2 3 161.96 156.06 3.01 o 10 2 3 215.38 222.37 6.17 o -11 3 3 141.64 148.19 5.88 o -9 3 3 1312.16 1262.29 20.70 o -7 3 3 1374.30 1273.34 16.76 o -5 3 3 916.11 930.91 17.74 o -3 3 3 1700.47 1963.34 43.90 o -1 3 3 354.36 367.63 6.92 o 1 3 3 76.24 95.31 1.48 o 3 3 3 2402.02 2456.21 27.50 o 5 3 3 299.07 293.96 4.72 o 7 3 3 15.30 30.44 2.08 o 9 3 3 53.29 55.63 2.38 o -12 4 3 12.85 14.29 2.49 o -10 4 3 102.20 113.72 3.69 o -8 4 3 53.25 56.82 2.25 o -6 4 3 129.71 144.50 2.85 o -4 4 3 1041.49 1172.11 17.41 o -2 4 3 0.96 1.70 0.65 o 0 4 3 34.47 47.13 1.13 o 2 4 3 873.89 872.37 9.23 o 4 4 3 793.09 811.69 9.92 o 6 4 3 883.55 869.16 12.77 o 8 4 3 98.02 73.27 2.53 o 10 4 3 1.94 2.06 1.75 o -11 5 3 24.78 30.31 2.39 o -9 5 3 3.95 13.44 1.43 o -7 5 3 12.17 11.63 1.08 o -5 5 3 773.01 830.15 13.65 o -3 5 3 1793.67 1641.75 24.51 o -1 5 3 619.07 603.85 7.81 o 1 5 3 63.83 52.93 1.14 o 3 5 3 304.37 310.39 3.77 o 5 5 3 143.82 135.42 2.64 o 7 5 3 10.59 7.98 1.29 o 9 5 3 102.22 103.84 3.79 o -10 6 3 116.01 112.52 3.56 o -8 6 3 304.07 289.67 5.33 o -6 6 3 816.05 748.40 13.10 o -4 6 3 597.96 581.69 7.97 o -2 6 3 309.69 307.35 4.39 o 0 6 3 587.28 633.32 8.07 o 2 6 3 50.60 57.33 1.36 o 4 6 3 52.99 57.88 1.63 o 6 6 3 18.62 15.07 1.49 o 8 6 3 136.51 122.16 3.43 o -9 7 3 2.64 4.96 1.58 o -7 7 3 27.41 28.52 2.13 o -5 7 3 1337.86 1340.12 23.90 o -3 7 3 474.02 464.73 6.53 o -1 7 3 235.13 216.69 3.83 o 1 7 3 387.59 359.18 4.69 o 3 7 3 51.15 52.35 1.79 o 5 7 3 80.68 81.09 2.42 o 7 7 3 53.54 59.94 3.25 o -10 8 3 155.62 159.43 6.66 o -8 8 3 51.17 47.00 2.27 o -6 8 3 189.69 177.25 4.32 o -4 8 3 156.68 153.81 3.77 o -2 8 3 364.94 360.54 8.96 o 0 8 3 83.38 89.72 2.81 o 2 8 3 80.66 74.58 2.18 o 4 8 3 126.06 123.45 2.83 o 6 8 3 81.99 81.79 2.83 o 8 8 3 0.02 -0.89 2.04 o -9 9 3 206.50 226.94 10.05 o -7 9 3 60.26 72.61 2.69 o -5 9 3 40.61 42.10 2.60 o -3 9 3 159.00 154.34 4.26 o -1 9 3 28.65 27.21 1.86 o 1 9 3 104.13 96.87 2.73 o 3 9 3 87.84 84.51 2.89 o 5 9 3 12.61 17.13 1.84 o 7 9 3 7.91 6.82 2.77 o -8 10 3 29.24 32.33 3.51 o -6 10 3 886.05 906.50 15.17 o -4 10 3 258.81 278.46 8.51 o -2 10 3 162.91 152.06 3.58 o 0 10 3 37.38 37.85 1.74 o 2 10 3 178.17 171.63 4.09 o 4 10 3 4.83 4.73 2.40 o 6 10 3 6.34 6.64 4.24 o -7 11 3 41.91 52.94 5.54 o -5 11 3 206.53 189.63 5.12 o -3 11 3 6.64 6.08 1.40 o -1 11 3 131.53 123.33 3.17 o 1 11 3 18.26 22.68 1.98 o 3 11 3 2.23 6.13 1.67 o -4 12 3 9.78 11.12 2.00 o -2 12 3 37.18 36.07 2.19 o 0 12 3 3.95 4.43 1.52 o 2 12 3 218.48 216.19 6.16 o -12 0 4 6.66 7.66 3.74 o -10 0 4 439.57 435.24 11.29 o -8 0 4 304.37 337.75 6.73 o -6 0 4 2.83 7.15 0.94 o -2 0 4 1800.19 1655.52 69.57 o 0 0 4 1104.90 1129.02 22.39 o 2 0 4 75.15 105.25 2.45 o 4 0 4 2090.24 2148.58 37.53 o 6 0 4 3208.11 3334.64 53.05 o 8 0 4 1146.92 1135.75 20.71 o 10 0 4 138.99 131.62 6.53 o -11 1 4 13.69 16.46 1.91 o -9 1 4 115.44 104.99 2.68 o -7 1 4 12.56 9.26 0.82 o -5 1 4 2239.86 2296.81 27.13 o -3 1 4 826.66 884.11 17.25 o -1 1 4 26.37 22.86 0.75 o 1 1 4 957.44 965.90 15.41 o 3 1 4 1227.79 1229.56 12.92 o 5 1 4 109.33 113.89 1.97 o 7 1 4 51.80 62.27 1.76 o 9 1 4 8.06 9.24 1.75 o -12 2 4 184.63 174.63 5.17 o -10 2 4 55.85 49.60 2.46 o -8 2 4 34.03 40.78 1.41 o -6 2 4 151.66 130.29 2.23 o -4 2 4 3679.59 3718.98 50.64 o -2 2 4 4822.54 5143.74 102.19 o 0 2 4 30.78 29.32 0.79 o 2 2 4 34.68 37.88 0.84 o 4 2 4 371.03 346.92 4.56 o 6 2 4 131.81 127.44 2.26 o 8 2 4 0.13 5.78 1.30 o -11 3 4 6.96 9.58 1.86 o -9 3 4 132.42 139.85 3.12 o -7 3 4 81.20 90.18 1.70 o -5 3 4 3.43 4.28 0.54 o -3 3 4 110.66 131.08 3.43 o -1 3 4 1.99 -0.02 0.34 o 1 3 4 1872.16 1971.60 23.64 o 3 3 4 236.06 191.33 2.52 o 5 3 4 21.08 19.61 1.00 o 7 3 4 340.87 351.81 5.79 o 9 3 4 111.29 126.69 3.40 o -12 4 4 40.91 43.04 4.06 o -10 4 4 6.44 10.54 1.69 o -8 4 4 5.00 3.65 0.97 o -6 4 4 142.73 127.73 2.60 o -4 4 4 155.39 145.01 2.22 o -2 4 4 398.55 386.26 5.02 o 0 4 4 320.57 342.50 3.98 o 2 4 4 339.83 357.61 4.06 o 4 4 4 44.88 31.32 1.24 o 6 4 4 163.53 158.03 3.77 o 8 4 4 704.85 720.25 14.52 o -11 5 4 2.90 4.17 1.80 o -9 5 4 111.11 127.02 3.33 o -7 5 4 140.93 120.23 2.91 o -5 5 4 749.74 767.18 12.67 o -3 5 4 62.22 65.66 1.50 o -1 5 4 48.98 46.10 1.09 o 1 5 4 814.15 775.03 9.57 o 3 5 4 224.21 221.26 3.02 o 5 5 4 327.96 326.63 6.35 o 7 5 4 19.06 30.15 1.90 o 9 5 4 88.17 86.88 4.32 o -10 6 4 220.37 250.21 5.70 o -8 6 4 26.07 29.65 1.57 o -6 6 4 91.91 84.00 2.58 o -4 6 4 227.31 212.99 3.60 o -2 6 4 379.30 387.85 5.50 o 0 6 4 81.48 76.15 1.64 o 2 6 4 148.96 144.22 2.34 o 4 6 4 415.00 399.87 5.85 o 6 6 4 13.70 11.06 1.50 o 8 6 4 57.10 65.27 3.80 o -11 7 4 15.18 18.61 2.28 o -9 7 4 456.86 475.78 9.59 o -7 7 4 163.89 163.70 3.70 o -5 7 4 694.20 678.95 10.71 o -3 7 4 223.97 207.21 3.40 o -1 7 4 436.81 386.70 6.80 o 1 7 4 988.71 949.69 13.57 o 3 7 4 242.49 237.91 3.93 o 5 7 4 10.02 11.88 1.41 o 7 7 4 86.55 100.17 3.49 o -10 8 4 151.81 171.80 7.62 o -8 8 4 211.95 238.33 5.11 o -6 8 4 593.59 569.58 13.95 o -4 8 4 453.10 470.02 9.29 o -2 8 4 467.06 431.41 7.51 o 0 8 4 140.33 135.51 2.79 o 2 8 4 112.79 115.25 2.67 o 4 8 4 104.80 104.36 2.96 o 6 8 4 16.22 12.08 1.89 o -9 9 4 63.05 70.02 3.93 o -7 9 4 361.25 341.66 6.48 o -5 9 4 47.00 42.65 2.60 o -3 9 4 50.50 48.56 2.88 o -1 9 4 0.21 1.55 1.18 o 1 9 4 51.28 60.06 2.32 o 3 9 4 222.72 235.21 5.35 o 5 9 4 1.29 1.10 1.71 o -8 10 4 0.55 2.29 1.98 o -6 10 4 38.89 35.99 2.03 o -4 10 4 676.44 690.28 14.43 o -2 10 4 298.86 293.86 5.79 o 0 10 4 14.05 13.88 1.55 o 2 10 4 22.60 24.34 2.08 o 4 10 4 0.68 0.18 1.84 o -7 11 4 0.24 1.37 2.33 o -5 11 4 13.42 11.93 1.44 o -3 11 4 6.25 6.06 1.29 o -1 11 4 145.91 143.18 4.02 o 1 11 4 7.01 9.42 1.57 o 3 11 4 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