data_2241607 _cell_angle_alpha 90 _cell_angle_beta 93.9050(10) _cell_angle_gamma 90 _cell_length_a 27.3226(5) _cell_length_b 7.3618(2) _cell_length_c 14.6742(4) _exptl_crystal_F_000 1408 _reflns_d_resolution_high ? _cod_data_source_file su5280Isup2.hkl _cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.21 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 4406.66 4239.04 84.09 o 10 0 0 17539.20 17861.40 531.59 o 14 0 0 154.65 123.70 4.87 o 16 0 0 2.50 5.34 2.10 < 18 0 0 3825.42 4130.80 75.09 o 20 0 0 113.52 96.57 4.39 o 22 0 0 77.49 95.61 4.96 o 24 0 0 812.63 806.57 16.91 o 26 0 0 182.00 155.55 6.87 o 28 0 0 0.00 5.15 4.10 < 30 0 0 115.62 123.47 7.44 o 32 0 0 10.60 7.73 6.01 < 34 0 0 105.00 76.14 15.74 o 7 1 0 4.28 1.81 0.86 < 9 1 0 4398.44 4283.83 62.03 o 11 1 0 451.53 438.27 7.07 o 13 1 0 5762.96 5488.07 79.30 o 15 1 0 801.85 899.41 13.19 o 17 1 0 562.41 523.54 8.79 o 19 1 0 0.10 -1.81 1.81 < 21 1 0 63.29 58.39 3.34 o 23 1 0 39.58 41.50 3.82 o 25 1 0 936.55 913.17 14.33 o 27 1 0 31.07 34.54 3.53 o 29 1 0 28.94 27.95 3.72 o 31 1 0 0.05 -1.91 4.48 < 33 1 0 2.81 7.16 5.44 < 35 1 0 3.83 -1.24 58.20 < 0 2 0 6548.76 6150.68 252.40 o 2 2 0 8681.06 7851.37 235.27 o 4 2 0 87.70 92.39 3.34 o 6 2 0 204.07 198.13 5.44 o 8 2 0 1850.71 1826.73 32.65 o 10 2 0 4112.43 4106.77 71.78 o 12 2 0 7133.29 7146.58 107.53 o 14 2 0 817.48 842.42 14.05 o 16 2 0 135.29 123.96 3.72 o 18 2 0 14.29 9.35 2.39 o 20 2 0 60.35 60.40 3.63 o 22 2 0 804.65 847.67 16.81 o 24 2 0 40.79 38.26 3.72 o 26 2 0 154.82 151.72 5.92 o 28 2 0 1003.28 1005.08 19.96 o 30 2 0 540.22 568.01 14.32 o 32 2 0 13.84 14.31 5.63 < 34 2 0 37.54 79.86 26.71 < 1 3 0 0.84 -2.10 2.10 < 3 3 0 7748.61 7949.31 201.48 o 5 3 0 208.54 203.06 7.35 o 7 3 0 322.45 295.84 7.54 o 9 3 0 102.19 101.35 4.49 o 11 3 0 38.23 47.13 3.43 o 13 3 0 8738.20 8867.29 133.17 o 15 3 0 627.17 610.58 10.89 o 17 3 0 26.38 24.23 2.86 o 19 3 0 4.98 -0.67 2.67 < 21 3 0 723.96 770.09 14.80 o 23 3 0 1739.47 1882.68 31.46 o 25 3 0 1324.42 1312.06 23.61 o 27 3 0 25.91 28.24 4.67 o 29 3 0 326.86 334.52 10.31 o 31 3 0 23.05 5.34 6.30 < 33 3 0 40.87 50.09 12.31 o 0 4 0 847.78 901.41 36.62 o 2 4 0 544.83 536.14 12.32 o 4 4 0 5559.28 5948.38 137.51 o 6 4 0 29.81 32.06 5.53 o 8 4 0 884.44 811.85 26.29 o 10 4 0 1971.32 2025.26 40.04 o 12 4 0 2793.92 2732.01 56.21 o 14 4 0 300.98 280.45 8.21 o 16 4 0 1077.61 1121.95 18.54 o 18 4 0 408.24 423.96 10.12 o 20 4 0 1.99 1.24 3.24 < 22 4 0 355.40 373.02 8.97 o 24 4 0 345.31 364.32 10.59 o 26 4 0 943.32 1007.36 24.83 o 28 4 0 32.90 26.33 6.11 o 30 4 0 199.30 209.93 16.32 o 32 4 0 18.41 10.30 21.47 < 1 5 0 0.29 15.17 4.58 o 3 5 0 1402.36 1534.01 30.90 o 5 5 0 0.02 0.38 3.34 < 7 5 0 1.51 6.58 3.72 < 9 5 0 145.38 129.97 7.54 o 11 5 0 34.14 32.92 6.11 o 13 5 0 0.48 8.78 5.44 < 15 5 0 478.17 517.27 18.62 o 17 5 0 493.83 527.67 17.57 o 19 5 0 0.00 1.91 4.10 < 21 5 0 131.52 125.96 7.63 o 23 5 0 74.14 81.01 6.87 o 25 5 0 230.26 233.71 11.74 o 27 5 0 24.90 17.08 7.92 < 29 5 0 109.22 110.78 13.93 o 0 6 0 1807.76 1858.38 57.41 o 2 6 0 2183.43 2366.33 45.67 o 4 6 0 1817.40 1821.38 36.26 o 6 6 0 60.07 69.37 6.49 o 8 6 0 68.42 60.59 6.30 o 10 6 0 1293.62 1240.22 30.40 o 12 6 0 590.95 622.46 15.56 o 14 6 0 87.91 105.53 8.01 o 16 6 0 1372.95 1415.64 34.69 o 18 6 0 82.23 86.44 7.35 o 20 6 0 316.03 318.29 10.88 o 22 6 0 46.21 31.01 6.77 o 24 6 0 21.79 18.13 8.11 < 26 6 0 172.52 163.55 10.88 o 28 6 0 71.03 80.34 17.84 o 1 7 0 2012.69 2004.62 44.39 o 3 7 0 0.00 6.58 7.16 < 5 7 0 459.04 452.97 14.51 o 7 7 0 119.26 89.41 8.68 o 9 7 0 895.23 909.78 26.27 o 11 7 0 171.69 174.15 9.35 o 13 7 0 638.02 600.37 17.19 o 15 7 0 54.24 38.16 6.39 o 17 7 0 490.93 406.56 14.70 o 19 7 0 155.57 135.88 9.45 o 21 7 0 3.87 11.73 7.06 < 23 7 0 40.20 21.37 9.54 < 25 7 0 4.21 16.79 15.07 < 0 8 0 64.42 96.75 13.83 o 2 8 0 18.36 8.49 7.16 < 4 8 0 74.13 52.19 8.40 o 6 8 0 230.54 174.73 13.93 o 8 8 0 0.07 -6.39 9.16 < 10 8 0 461.40 488.15 19.95 o 12 8 0 63.50 36.45 10.02 o 14 8 0 44.69 41.98 10.40 o 16 8 0 17.03 27.67 10.02 < 18 8 0 62.60 49.14 14.98 o 20 8 0 41.15 61.25 15.36 o 1 9 0 3.39 8.87 10.69 < 3 9 0 80.67 94.84 17.37 o 5 9 0 114.35 166.02 15.27 o 7 9 0 91.39 104.57 18.41 o 9 9 0 49.44 55.34 12.40 o 11 9 0 92.75 137.87 14.88 o 13 9 0 0.43 1.53 13.55 < -35 1 1 31.49 -24.42 24.42 < -33 1 1 100.47 62.31 15.65 o -31 1 1 33.87 27.10 4.67 o -29 1 1 51.68 59.73 3.82 o -27 1 1 486.07 486.01 9.45 o -25 1 1 102.56 117.08 3.91 o -23 1 1 88.97 89.98 3.34 o -21 1 1 8.80 20.13 2.19 o -19 1 1 292.87 290.19 5.54 o -17 1 1 81.17 95.99 2.86 o -15 1 1 95.14 102.68 2.77 o -13 1 1 2.27 4.29 1.53 < -11 1 1 8407.46 8665.12 117.44 o -7 1 1 4951.67 4485.42 75.02 o -5 1 1 8825.06 8282.67 148.12 o -3 1 1 546.70 485.77 9.87 o 7 1 1 6839.79 6403.48 106.14 o 9 1 1 858.29 818.70 11.87 o 11 1 1 9.73 11.16 1.53 o 13 1 1 831.77 828.67 11.57 o 15 1 1 292.43 299.11 5.92 o 17 1 1 4926.13 5209.47 71.23 o 19 1 1 113.43 96.47 3.72 o 21 1 1 6.71 11.45 2.29 o 23 1 1 20.41 14.98 2.96 o 25 1 1 3.14 -0.95 3.43 < 27 1 1 5.76 10.30 3.24 o 29 1 1 744.80 748.26 16.04 o 31 1 1 183.51 181.40 7.06 o 33 1 1 0.29 2.67 5.06 < -34 2 1 85.68 102.76 23.85 o -32 2 1 48.87 63.16 6.01 o -30 2 1 0.69 3.53 3.43 < -28 2 1 62.57 64.88 4.58 o -26 2 1 349.89 346.86 8.59 o -24 2 1 943.82 937.08 18.44 o -22 2 1 29.73 33.49 3.34 o -20 2 1 1077.97 1100.69 17.87 o -18 2 1 200.65 194.60 4.87 o -16 2 1 0.12 0.19 1.91 < -14 2 1 6.66 5.15 2.00 < -12 2 1 113.91 99.63 3.15 o -10 2 1 3920.29 4452.77 71.73 o -6 2 1 12925.20 12547.90 275.08 o -4 2 1 1710.55 1574.76 37.02 o -2 2 1 684.73 656.99 19.53 o 0 2 1 1266.13 1215.64 24.97 o 2 2 1 585.45 518.58 12.34 o 6 2 1 11035.40 9977.66 207.09 o 8 2 1 4017.28 3984.55 80.28 o 10 2 1 5.60 2.58 1.72 < 12 2 1 27.06 25.86 2.10 o 14 2 1 0.41 3.82 2.00 < 16 2 1 78.83 66.22 3.34 o 18 2 1 106.34 101.82 4.01 o 20 2 1 329.04 311.57 8.02 o 22 2 1 89.31 87.02 4.68 o 24 2 1 189.66 205.75 6.87 o 26 2 1 32.20 27.19 4.48 o 28 2 1 0.28 1.72 4.01 < 30 2 1 592.59 620.65 14.89 o 32 2 1 8.28 10.02 5.92 < 34 2 1 0.02 -23.18 23.18 < -33 3 1 216.70 279.69 42.18 o -31 3 1 255.96 300.51 16.60 o -29 3 1 38.26 40.26 5.82 o -27 3 1 114.29 101.14 6.77 o -25 3 1 240.87 273.90 7.83 o -23 3 1 2862.99 2879.42 45.69 o -21 3 1 11402.20 11904.90 187.67 o -19 3 1 2224.83 2326.32 37.63 o -17 3 1 488.77 495.87 8.98 o -15 3 1 8.74 6.01 2.10 < -13 3 1 127.00 115.85 4.39 o -11 3 1 8188.69 8359.58 169.34 o -9 3 1 17990.20 19253.20 486.21 o -7 3 1 2917.23 3247.51 68.40 o -5 3 1 9995.01 10179.40 216.66 o -3 3 1 1166.63 1160.18 22.89 o -1 3 1 3420.12 3598.62 98.35 o 1 3 1 0.32 0.38 3.43 < 3 3 1 10756.10 11577.30 214.65 o 5 3 1 7825.05 8003.04 146.05 o 7 3 1 3718.90 3787.32 83.78 o 9 3 1 949.73 985.96 22.57 o 11 3 1 18.15 24.52 3.15 o 13 3 1 5281.70 5333.25 75.35 o 15 3 1 2226.75 2306.44 34.21 o 17 3 1 155.98 152.12 5.44 o 19 3 1 1147.87 1239.70 19.59 o 21 3 1 2597.24 2828.61 45.78 o 23 3 1 10.40 25.95 4.29 o 25 3 1 1168.14 1234.86 22.36 o 27 3 1 246.03 268.26 8.68 o 29 3 1 884.61 937.34 20.34 o 31 3 1 60.54 58.87 7.73 o 33 3 1 52.08 67.45 9.25 o -32 4 1 171.04 133.68 26.34 o -30 4 1 0.71 3.15 6.87 < -28 4 1 26.94 22.80 6.49 o -26 4 1 13.40 12.88 5.92 < -24 4 1 891.33 888.26 25.88 o -22 4 1 1991.54 2076.29 44.00 o -20 4 1 139.64 145.43 6.68 o -18 4 1 468.84 464.19 11.46 o -16 4 1 73.46 72.42 4.48 o -14 4 1 458.03 495.17 15.18 o -12 4 1 80.23 63.17 5.25 o -10 4 1 930.56 1236.24 25.52 o -8 4 1 352.12 375.71 11.65 o -6 4 1 3401.85 3444.44 68.08 o -4 4 1 120.87 95.62 5.44 o -2 4 1 324.21 362.93 9.93 o 0 4 1 550.40 547.52 15.38 o 2 4 1 1953.32 1952.66 56.56 o 4 4 1 615.39 624.59 21.31 o 6 4 1 5350.31 5550.33 140.43 o 8 4 1 1875.98 1876.73 40.62 o 10 4 1 48.08 60.21 4.48 o 12 4 1 633.60 636.64 12.90 o 14 4 1 1.37 1.91 3.05 < 16 4 1 829.91 804.88 14.52 o 18 4 1 65.59 60.68 4.58 o 20 4 1 408.14 404.84 9.16 o 22 4 1 211.30 205.94 6.58 o 24 4 1 1186.45 1277.83 26.37 o 26 4 1 26.15 24.81 5.44 o 28 4 1 10.05 13.36 5.53 < 30 4 1 1.38 -1.72 6.68 < 32 4 1 104.62 120.51 13.17 o -29 5 1 8.50 11.16 7.63 < -27 5 1 0.06 10.59 8.11 < -25 5 1 18.96 7.63 5.34 < -23 5 1 71.38 55.82 5.82 o -21 5 1 571.86 581.15 14.99 o -19 5 1 49.12 63.16 5.92 o -17 5 1 225.22 222.27 9.26 o -15 5 1 170.40 175.49 8.40 o -13 5 1 860.11 875.48 21.97 o -11 5 1 28.92 21.18 4.96 o -9 5 1 1302.56 1311.10 25.15 o -7 5 1 321.55 381.75 10.31 o -5 5 1 49.92 40.74 4.58 o -3 5 1 157.47 163.76 6.58 o -1 5 1 365.00 342.56 10.60 o 1 5 1 1563.03 1450.89 30.34 o 3 5 1 3503.37 3299.09 74.15 o 5 5 1 194.27 217.03 10.40 o 7 5 1 1160.18 1218.61 42.16 o 9 5 1 14.47 18.80 5.92 o 11 5 1 103.50 87.69 8.40 o 13 5 1 1.88 4.96 4.10 < 15 5 1 288.20 278.61 8.97 o 17 5 1 27.01 21.56 4.87 o 19 5 1 137.44 123.57 6.20 o 21 5 1 67.66 66.88 5.92 o 23 5 1 133.27 127.29 7.82 o 25 5 1 82.47 85.49 7.44 o 27 5 1 53.30 51.62 8.11 o 29 5 1 58.74 71.08 11.35 o -28 6 1 8.26 19.75 11.16 < -26 6 1 189.21 203.44 9.92 o -24 6 1 5.88 10.59 5.82 < -22 6 1 2.63 0.10 5.53 < -20 6 1 431.77 408.16 11.36 o -18 6 1 86.45 56.87 6.58 o -16 6 1 372.92 345.05 12.12 o -14 6 1 561.30 506.89 13.84 o -12 6 1 428.22 381.66 10.88 o -10 6 1 207.39 226.85 8.49 o -8 6 1 261.32 202.53 8.78 o -6 6 1 177.48 159.85 8.30 o -4 6 1 1003.63 985.76 22.84 o -2 6 1 1479.06 1476.94 31.94 o 0 6 1 2618.14 2776.04 57.77 o 2 6 1 825.47 858.92 19.11 o 4 6 1 11236.90 11130.40 197.20 o 6 6 1 0.20 13.83 5.92 < 8 6 1 481.50 443.57 15.56 o 10 6 1 685.60 635.93 19.00 o 12 6 1 895.41 863.73 24.26 o 14 6 1 294.74 291.19 14.51 o 16 6 1 1261.39 1184.27 30.20 o 18 6 1 28.71 26.90 6.87 o 20 6 1 59.94 50.57 6.97 o 22 6 1 0.34 5.92 6.39 < 24 6 1 0.13 -6.87 6.87 < 26 6 1 20.84 12.31 10.59 < 28 6 1 32.16 45.03 21.28 < -25 7 1 85.46 116.12 14.03 o -23 7 1 0.01 -3.24 8.68 < -21 7 1 11.04 12.50 7.16 < -19 7 1 50.87 30.24 8.40 o -17 7 1 12.51 14.79 6.11 < -15 7 1 104.29 77.67 8.21 o -13 7 1 138.92 111.55 7.82 o -11 7 1 5.88 4.01 6.30 < -9 7 1 2019.79 2078.07 41.80 o -7 7 1 331.44 285.96 12.89 o -5 7 1 15.13 29.10 7.35 o -3 7 1 257.29 236.78 10.69 o -1 7 1 914.93 882.26 21.68 o 1 7 1 1430.73 1493.80 35.56 o 3 7 1 2012.16 2011.46 46.40 o 5 7 1 482.86 476.57 15.08 o 7 7 1 200.52 199.93 10.69 o 9 7 1 22.27 34.06 7.44 o 11 7 1 429.07 350.23 16.04 o 13 7 1 33.20 20.70 8.97 < 15 7 1 286.01 280.39 14.89 o 17 7 1 377.85 332.44 12.98 o 19 7 1 228.53 236.76 13.17 o 21 7 1 1.84 -8.59 8.59 < 23 7 1 6.42 14.69 12.12 < -20 8 1 16.79 10.78 14.22 < -18 8 1 8.48 21.66 10.02 < -16 8 1 57.61 59.35 11.74 o -14 8 1 56.72 51.14 9.73 o -12 8 1 22.95 40.36 9.64 o -10 8 1 43.47 11.54 8.78 < -8 8 1 29.47 32.82 7.92 o -6 8 1 29.22 19.56 11.07 < -4 8 1 20.12 0.19 8.49 < -2 8 1 33.41 6.20 7.54 < 0 8 1 126.47 112.40 9.16 o 2 8 1 123.37 106.77 8.49 o 4 8 1 10.34 12.02 7.92 < 6 8 1 212.12 147.05 14.79 o 8 8 1 6.84 -8.40 8.40 < 10 8 1 322.33 344.92 21.66 o 12 8 1 25.35 11.73 7.44 < 14 8 1 98.37 102.86 12.50 o 16 8 1 150.59 199.62 15.17 o 18 8 1 28.51 24.33 12.50 < 20 8 1 0.89 -8.59 15.17 < -13 9 1 1.01 2.96 13.17 < -11 9 1 0.61 11.35 11.26 < -9 9 1 19.55 33.11 10.97 o -7 9 1 318.60 359.89 19.18 o -5 9 1 31.97 9.92 15.65 < -3 9 1 97.14 142.45 16.22 o -1 9 1 18.38 10.49 11.35 < 1 9 1 39.43 29.96 14.02 < 3 9 1 98.22 112.88 18.22 o 5 9 1 165.13 233.11 18.03 o 7 9 1 63.57 62.78 13.64 o 9 9 1 232.00 341.44 22.14 o 11 9 1 1.00 1.24 11.16 < 13 9 1 196.18 278.26 19.66 o -34 0 2 3.53 8.40 13.55 < -32 0 2 745.24 665.72 31.03 o -30 0 2 1310.13 1254.89 26.66 o -28 0 2 37.11 31.20 3.05 o -26 0 2 92.01 60.40 3.53 o -24 0 2 27.22 22.90 2.86 o -22 0 2 682.60 696.75 16.14 o -20 0 2 1377.49 1550.18 31.18 o -18 0 2 2850.37 2758.40 60.07 o -14 0 2 41.90 34.35 2.29 o -12 0 2 220.71 197.43 4.87 o -10 0 2 6666.84 6716.79 196.46 o -8 0 2 10625.30 10658.70 407.71 o 2 0 2 9.65 2.67 2.00 < 4 0 2 2529.81 2129.88 68.34 o 6 0 2 5301.02 5168.51 108.79 o 8 0 2 18454.40 18086.00 383.66 o 10 0 2 20187.80 21256.70 813.58 o 12 0 2 5017.36 4691.21 93.73 o 14 0 2 487.38 495.96 13.56 o 16 0 2 0.02 0.38 2.67 < 18 0 2 1662.04 1756.03 33.02 o 20 0 2 9498.41 9956.02 185.85 o 22 0 2 224.41 195.08 6.68 o 24 0 2 628.20 683.62 17.19 o 26 0 2 186.60 210.61 8.02 o 28 0 2 14.67 22.23 5.34 o 30 0 2 182.71 186.27 10.69 o 32 0 2 34.65 47.61 10.40 o 34 0 2 589.96 560.37 21.57 o -35 1 2 9.88 -17.94 17.94 < -33 1 2 83.95 51.24 16.98 o -31 1 2 150.10 140.46 15.08 o -29 1 2 155.05 135.40 6.77 o -27 1 2 3.28 4.96 2.00 < -25 1 2 4.65 4.58 1.91 < -23 1 2 118.41 111.07 3.34 o -21 1 2 626.64 617.83 9.65 o -19 1 2 3245.10 3313.73 47.80 o -17 1 2 123.86 137.99 3.24 o -15 1 2 923.73 920.97 14.25 o -13 1 2 13.72 15.55 1.34 o -11 1 2 392.94 425.27 7.83 o -9 1 2 62.34 64.99 2.29 o -7 1 2 8744.74 8181.94 131.39 o -5 1 2 4127.78 4583.55 90.94 o -1 1 2 1781.43 1680.10 28.03 o 1 1 2 771.39 753.81 16.41 o 3 1 2 0.00 2.19 0.86 < 5 1 2 6634.60 6427.59 109.76 o 7 1 2 515.61 623.81 10.52 o 9 1 2 1685.83 1883.45 28.60 o 11 1 2 4357.16 4155.75 63.13 o 13 1 2 59.46 59.73 2.39 o 15 1 2 179.30 190.79 4.39 o 17 1 2 157.26 157.09 4.29 o 19 1 2 343.42 315.99 6.68 o 21 1 2 125.71 122.62 4.20 o 23 1 2 916.80 944.56 16.81 o 25 1 2 346.36 366.15 9.54 o 27 1 2 46.41 47.61 4.29 o 29 1 2 17.19 15.17 4.67 o 31 1 2 1.95 8.87 5.25 < 33 1 2 58.83 53.62 7.92 o -34 2 2 19.03 5.92 19.75 < -32 2 2 152.04 145.99 27.58 o -30 2 2 31.75 21.37 3.91 o -28 2 2 253.39 312.16 11.07 o -26 2 2 456.77 467.09 11.84 o -24 2 2 0.04 3.05 2.96 < -22 2 2 8.43 4.10 2.77 < -20 2 2 1013.89 1021.24 17.11 o -18 2 2 1040.97 1103.39 20.07 o -16 2 2 1722.72 1609.01 24.22 o -14 2 2 99.62 91.61 3.34 o -12 2 2 2.27 -0.67 2.00 < -10 2 2 1642.63 1644.38 30.30 o -8 2 2 2245.48 2249.51 35.28 o -6 2 2 7205.64 7399.56 125.17 o -4 2 2 15288.40 15288.10 365.74 o -2 2 2 4673.15 4225.60 77.27 o 0 2 2 1500.89 1441.44 31.61 o 2 2 2 766.67 791.35 18.48 o 4 2 2 157.62 146.16 4.77 o 6 2 2 1320.42 1200.23 22.24 o 8 2 2 14564.20 14651.10 265.62 o 10 2 2 2018.32 2176.94 32.43 o 12 2 2 1221.27 1202.29 17.99 o 14 2 2 892.20 854.45 13.38 o 16 2 2 0.50 0.86 2.77 < 18 2 2 44.97 35.30 3.43 o 20 2 2 1399.81 1431.22 22.76 o 22 2 2 24.59 29.96 4.10 o 24 2 2 594.61 623.03 12.70 o 26 2 2 10.80 22.90 4.77 o 28 2 2 28.41 19.27 4.87 o 30 2 2 115.44 99.23 7.25 o 32 2 2 57.03 75.95 9.45 o 34 2 2 45.66 37.69 12.78 < -33 3 2 61.83 58.87 20.13 < -31 3 2 0.00 7.06 6.49 < -29 3 2 281.26 246.51 9.83 o -27 3 2 16.03 19.08 4.10 o -25 3 2 87.90 94.84 6.39 o -23 3 2 0.66 0.48 3.53 < -21 3 2 3.65 10.40 5.15 < -19 3 2 5212.19 5238.99 90.25 o -17 3 2 96.19 81.01 4.10 o -15 3 2 491.01 481.30 11.46 o -13 3 2 7.73 7.25 2.39 o -11 3 2 1007.93 1036.83 20.85 o -9 3 2 4871.22 4971.50 83.56 o -7 3 2 3619.88 3824.43 69.97 o -5 3 2 166.29 135.64 4.10 o -3 3 2 21540.40 21670.50 545.87 o -1 3 2 536.99 513.03 13.19 o 1 3 2 213.81 226.17 6.30 o 3 3 2 534.26 534.11 11.85 o 5 3 2 57.30 70.04 3.53 o 7 3 2 12677.00 12801.70 290.66 o 9 3 2 145.05 125.03 4.39 o 11 3 2 3609.13 3826.24 68.59 o 13 3 2 1857.85 1886.96 29.40 o 15 3 2 171.94 177.99 4.77 o 17 3 2 27.56 21.75 2.86 o 19 3 2 455.31 461.23 10.02 o 21 3 2 166.48 150.49 6.58 o 23 3 2 2090.02 2171.77 34.83 o 25 3 2 99.20 96.75 6.68 o 27 3 2 0.13 0.48 4.96 < 29 3 2 117.96 124.42 8.11 o 31 3 2 18.20 12.02 9.35 < 33 3 2 73.77 60.40 12.50 o -32 4 2 140.09 348.75 100.38 o -30 4 2 0.03 13.45 10.11 < -28 4 2 222.94 239.33 9.73 o -26 4 2 151.12 164.32 7.25 o -24 4 2 202.02 183.70 7.06 o -22 4 2 284.78 273.05 8.69 o -20 4 2 5541.67 5678.16 92.70 o -18 4 2 89.20 88.93 5.34 o -16 4 2 16.08 18.70 3.53 o -14 4 2 256.28 250.45 7.83 o -12 4 2 337.56 318.76 8.31 o -10 4 2 538.97 574.97 11.65 o -8 4 2 1838.81 2110.14 36.11 o -6 4 2 0.27 7.06 3.24 < -4 4 2 170.10 195.56 7.16 o -2 4 2 1321.61 1640.80 36.94 o 0 4 2 102.68 86.27 6.58 o 2 4 2 55.88 48.95 5.06 o 4 4 2 68.26 59.92 3.91 o 6 4 2 764.92 997.55 23.41 o 8 4 2 11.83 11.35 3.34 o 10 4 2 99.47 107.07 5.34 o 12 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1707.21 1675.74 28.61 o -13 3 7 629.74 648.88 15.76 o -11 3 7 6239.03 6230.82 101.80 o -9 3 7 25.96 24.23 3.05 o -7 3 7 3905.69 3907.09 65.58 o -5 3 7 2864.55 2848.57 50.58 o -3 3 7 1308.29 1336.84 26.41 o -1 3 7 626.10 671.89 15.38 o 1 3 7 4174.92 4306.19 74.99 o 3 3 7 1240.89 1224.95 28.89 o 5 3 7 1212.96 1207.84 30.51 o 7 3 7 120.08 127.01 6.58 o 9 3 7 256.93 302.10 10.31 o 11 3 7 916.97 959.58 19.59 o 13 3 7 275.74 265.34 11.07 o 15 3 7 1731.86 1787.85 42.09 o 17 3 7 1685.70 1813.55 38.25 o 19 3 7 242.20 233.34 9.64 o 21 3 7 1.73 -5.72 5.72 < 23 3 7 51.75 59.82 8.21 o 25 3 7 8.77 11.64 8.11 < 27 3 7 1071.29 1091.19 28.37 o 29 3 7 1110.05 1152.03 44.89 o -28 4 7 139.43 156.77 27.39 o -26 4 7 507.49 557.10 15.75 o -24 4 7 58.56 66.21 4.20 o -22 4 7 2.20 4.96 3.34 < -20 4 7 7.01 10.78 3.15 o -18 4 7 285.11 295.77 8.49 o -16 4 7 1038.97 1057.51 21.02 o -14 4 7 925.77 960.44 19.59 o -12 4 7 105.81 77.29 7.06 o -10 4 7 18.82 19.08 5.34 o -8 4 7 1444.34 1375.54 34.14 o -6 4 7 34.28 43.22 4.10 o -4 4 7 1203.98 1128.44 22.95 o -2 4 7 214.12 211.98 7.73 o 0 4 7 0.15 -2.29 4.67 < 2 4 7 2001.41 2101.33 40.89 o 4 4 7 36.32 44.75 5.53 o 6 4 7 403.74 379.02 12.32 o 8 4 7 207.59 200.80 8.49 o 10 4 7 98.04 85.59 6.68 o 12 4 7 456.21 510.39 15.28 o 14 4 7 255.50 244.80 8.40 o 16 4 7 0.91 2.86 3.82 < 18 4 7 79.59 76.62 7.82 o 20 4 7 13.06 19.94 6.68 < 22 4 7 101.75 88.45 8.11 o 24 4 7 71.13 62.02 8.78 o 26 4 7 72.38 69.08 14.03 o 28 4 7 1.65 -0.38 10.78 < -27 5 7 0.30 -20.23 23.09 < -25 5 7 10.07 10.02 5.44 < -23 5 7 238.05 276.46 11.36 o -21 5 7 19.11 22.23 4.58 o -19 5 7 97.88 79.10 5.53 o -17 5 7 12.37 18.41 4.58 o -15 5 7 142.66 137.03 6.97 o -13 5 7 123.83 123.19 6.11 o -11 5 7 129.29 139.41 7.06 o -9 5 7 0.33 -3.72 3.72 < -7 5 7 327.58 291.22 9.16 o -5 5 7 2.82 3.91 4.96 < -3 5 7 2.99 5.63 5.72 < -1 5 7 209.21 216.93 9.64 o 1 5 7 12.34 19.84 6.11 o 3 5 7 356.70 362.64 12.22 o 5 5 7 233.53 212.83 9.83 o 7 5 7 494.87 533.51 15.18 o 9 5 7 339.94 401.95 13.94 o 11 5 7 10.07 7.16 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20.99 o 1 9 7 2.56 14.98 17.36 < 3 9 7 41.15 59.44 27.76 < -32 0 8 408.46 439.43 48.68 o -30 0 8 46.73 29.96 21.47 < -28 0 8 52.29 30.34 12.78 < -26 0 8 282.93 300.05 19.47 o -24 0 8 0.01 15.46 10.30 < -22 0 8 141.71 110.79 12.21 o -18 0 8 767.96 723.86 32.67 o -16 0 8 678.95 690.39 24.74 o -14 0 8 455.93 517.24 11.65 o -12 0 8 0.10 1.34 3.15 < -10 0 8 1827.68 2041.57 50.57 o -8 0 8 1052.17 1109.53 27.06 o -6 0 8 3923.86 3820.89 105.74 o -2 0 8 838.30 830.63 21.89 o 0 0 8 326.73 357.49 12.51 o 2 0 8 502.96 518.50 13.09 o 4 0 8 2554.82 2387.94 63.16 o 12 0 8 0.62 -1.34 2.29 < 14 0 8 111.94 127.68 5.15 o 16 0 8 466.35 454.84 13.65 o 18 0 8 1358.69 1372.77 28.20 o 20 0 8 1545.63 1691.02 37.10 o 22 0 8 1219.06 1284.55 28.28 o 24 0 8 77.63 84.73 7.16 o 26 0 8 39.56 57.53 10.40 o 28 0 8 0.56 -3.15 8.68 < 30 0 8 15.51 -3.34 12.59 < -31 1 8 18.65 4.96 13.93 < -29 1 8 126.79 171.56 18.42 o -27 1 8 91.69 77.48 11.93 o -25 1 8 0.17 5.25 8.11 < -23 1 8 114.11 112.79 10.31 o -21 1 8 156.55 124.63 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