data_2241619 _cell_angle_alpha 90.000 _cell_angle_beta 112.411 _cell_angle_gamma 90.000 _cell_length_a 15.6414 _cell_length_b 30.8358 _cell_length_c 14.7380 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7981 _cod_data_source_file pk25752sup2.hkl _cod_data_source_block 2 _shelx_title ' owen-12-11-14 in P21/c No14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 435.15 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 50238.59 43552.52 508.49 o 3 0 0 40241.52 42905.74 624.09 o 4 0 0 3378.83 2416.50 149.84 o 5 0 0 3502.37 3031.46 227.93 o 6 0 0 188.90 309.32 97.32 o 7 0 0 1598.92 1855.36 234.71 o 8 0 0 615.54 564.74 162.71 o 9 0 0 11.84 111.09 68.83 o 10 0 0 3402.25 3288.74 377.51 o 11 0 0 82.04 48.60 68.99 o 12 0 0 578.52 462.69 221.26 o 13 0 0 7098.82 10636.72 518.02 o 14 0 0 5822.57 7496.61 415.01 o 15 0 0 159.34 101.18 58.28 o 16 0 0 58.43 91.14 54.10 o 17 0 0 21.78 -22.71 40.20 o 1 1 0 104266.00 89869.58 1664.41 o 2 1 0 21469.68 26421.02 692.29 o 3 1 0 1528.77 1726.76 90.53 o 4 1 0 2854.70 2623.45 125.82 o 5 1 0 80.62 66.46 59.04 o 6 1 0 12.66 13.69 48.81 o 7 1 0 3075.83 4096.51 232.89 o 8 1 0 6391.54 7756.35 347.68 o 9 1 0 8.45 38.41 82.63 o 10 1 0 101.26 58.86 51.79 o 11 1 0 431.76 526.03 74.95 o 12 1 0 63.26 160.40 55.16 o 13 1 0 1669.87 2245.82 200.96 o 14 1 0 223.00 752.76 149.47 o 15 1 0 97.32 92.19 55.14 o 16 1 0 8.44 21.07 35.51 o 17 1 0 0.03 -54.07 27.03 o 18 1 0 16.42 9.35 25.40 o 1 2 0 19213.62 24411.88 1657.91 o 2 2 0 228.97 329.97 26.01 o 3 2 0 9651.03 10088.72 435.59 o 4 2 0 5635.58 5424.97 195.84 o 5 2 0 679.60 704.11 82.21 o 6 2 0 1840.07 1760.59 136.24 o 7 2 0 1.03 53.36 45.96 o 8 2 0 2862.34 2740.49 212.14 o 9 2 0 673.89 839.54 127.75 o 10 2 0 269.50 176.46 71.19 o 11 2 0 34.18 88.96 58.05 o 12 2 0 212.27 232.12 58.17 o 13 2 0 3493.95 4723.10 243.73 o 14 2 0 569.26 995.90 123.05 o 15 2 0 70.94 -61.31 44.58 o 16 2 0 24.25 38.59 35.04 o 17 2 0 59.92 -56.81 41.05 o 18 2 0 51.97 49.50 24.98 o 1 3 0 24501.17 26890.26 1752.73 o 2 3 0 21428.01 20183.85 733.68 o 3 3 0 520.80 273.28 124.42 o 4 3 0 1240.13 1264.25 135.74 o 5 3 0 2.35 19.60 38.60 o 6 3 0 588.74 777.88 93.30 o 7 3 0 731.33 566.12 83.99 o 8 3 0 8167.79 8746.21 508.75 o 9 3 0 1269.92 1302.33 195.93 o 10 3 0 64.68 -38.57 72.18 o 11 3 0 3122.82 3592.23 246.92 o 12 3 0 313.33 478.27 92.48 o 13 3 0 564.15 829.73 111.15 o 14 3 0 3816.20 4869.14 232.39 o 15 3 0 363.48 332.01 56.67 o 16 3 0 1.15 55.03 76.75 o 17 3 0 20.85 19.03 30.94 o 18 3 0 55.85 39.62 29.05 o 0 4 0 22915.17 30662.94 460.81 o 1 4 0 1366.09 1508.22 70.97 o 2 4 0 1887.55 1150.86 113.56 o 3 4 0 9142.36 10322.46 415.68 o 4 4 0 50.76 53.91 43.92 o 5 4 0 1194.85 1236.74 107.71 o 6 4 0 931.39 987.57 101.74 o 7 4 0 8530.30 9724.80 354.81 o 8 4 0 53.17 144.26 89.58 o 9 4 0 1179.99 1241.98 161.56 o 10 4 0 330.46 295.03 92.67 o 11 4 0 1002.46 1288.47 114.77 o 12 4 0 246.36 388.12 69.81 o 13 4 0 0.34 -6.10 48.94 o 14 4 0 17.37 27.18 61.32 o 15 4 0 84.76 -6.68 47.96 o 16 4 0 191.71 168.83 75.49 o 17 4 0 335.06 172.42 46.86 o 18 4 0 24.71 35.82 28.01 o 1 5 0 1555.42 1863.37 129.83 o 2 5 0 2883.16 2929.94 99.54 o 3 5 0 11933.54 12417.72 571.52 o 4 5 0 2801.26 2629.10 120.65 o 5 5 0 13463.21 13307.03 835.88 o 6 5 0 2.36 -29.36 49.00 o 7 5 0 2778.39 2396.03 176.02 o 8 5 0 1181.94 1273.01 141.64 o 9 5 0 7055.01 8298.09 403.65 o 10 5 0 204.30 254.19 76.95 o 11 5 0 1041.92 1145.51 97.31 o 12 5 0 718.40 1008.12 97.87 o 13 5 0 1241.28 1637.79 126.88 o 14 5 0 266.05 355.23 66.95 o 15 5 0 423.22 288.74 51.24 o 16 5 0 3.42 -47.52 41.86 o 17 5 0 66.29 63.37 53.22 o 0 6 0 6916.44 7797.99 293.34 o 1 6 0 5918.69 7704.27 236.30 o 2 6 0 91.93 105.98 38.22 o 3 6 0 13960.74 13832.68 536.89 o 4 6 0 3146.91 3336.03 150.32 o 5 6 0 16166.56 14636.86 309.99 o 6 6 0 19770.00 20200.02 488.90 o 7 6 0 1084.56 1138.98 123.89 o 8 6 0 13965.19 13883.25 476.09 o 9 6 0 914.06 947.59 144.44 o 10 6 0 60.28 49.14 65.60 o 11 6 0 702.45 729.89 82.08 o 12 6 0 46.80 67.97 48.11 o 13 6 0 147.32 296.14 65.10 o 14 6 0 363.11 332.32 67.85 o 15 6 0 29.86 -16.58 52.25 o 16 6 0 361.34 317.31 69.50 o 17 6 0 427.71 308.69 93.83 o 1 7 0 4315.04 4905.31 164.24 o 2 7 0 6678.55 7197.77 208.84 o 3 7 0 1079.14 974.20 76.72 o 4 7 0 1198.31 1267.82 93.47 o 5 7 0 4200.80 3651.32 258.59 o 6 7 0 887.86 1013.13 118.88 o 7 7 0 2884.17 2826.90 203.56 o 8 7 0 472.17 679.32 112.29 o 9 7 0 7037.11 8398.91 414.51 o 10 7 0 296.86 199.27 66.02 o 11 7 0 2971.87 3401.35 217.45 o 12 7 0 948.42 1403.20 127.96 o 13 7 0 547.77 729.78 91.90 o 14 7 0 465.20 465.92 76.44 o 15 7 0 1.59 -40.90 44.82 o 16 7 0 303.79 200.02 66.97 o 17 7 0 695.82 405.23 173.80 o 0 8 0 1118.99 1085.54 136.52 o 1 8 0 2502.06 2948.60 153.37 o 2 8 0 717.74 1083.41 88.82 o 3 8 0 2853.08 2287.57 185.64 o 4 8 0 481.15 557.24 65.90 o 5 8 0 7551.73 7510.74 293.70 o 6 8 0 10542.49 10790.14 860.15 o 7 8 0 1848.92 2136.91 174.77 o 8 8 0 2424.51 2279.63 202.75 o 9 8 0 1203.29 1306.07 233.33 o 10 8 0 1114.16 1090.20 104.14 o 11 8 0 927.26 810.74 103.43 o 12 8 0 1724.39 1882.92 314.09 o 13 8 0 319.25 419.69 99.69 o 14 8 0 44.92 46.27 65.44 o 15 8 0 11.50 -1.80 54.92 o 16 8 0 130.93 155.38 54.69 o 17 8 0 106.90 75.43 23.14 o 1 9 0 2855.28 2587.03 150.49 o 2 9 0 1453.79 1677.95 118.63 o 3 9 0 191.01 194.38 44.31 o 4 9 0 19571.15 18811.14 435.85 o 5 9 0 5150.98 4784.03 237.33 o 6 9 0 11869.68 11131.74 400.23 o 7 9 0 14136.62 14899.52 472.57 o 8 9 0 4360.20 4513.47 285.16 o 9 9 0 0.31 -5.72 75.63 o 10 9 0 51.34 13.48 44.17 o 11 9 0 297.11 284.88 66.81 o 12 9 0 944.02 1151.41 150.85 o 13 9 0 216.53 209.74 73.27 o 14 9 0 46.66 -17.24 92.03 o 15 9 0 197.97 150.24 51.67 o 16 9 0 235.11 165.84 46.49 o 17 9 0 380.57 188.37 81.94 o 0 10 0 32797.38 34523.88 801.76 o 1 10 0 272.15 302.46 59.02 o 2 10 0 7202.72 6577.25 238.14 o 3 10 0 1052.82 1221.56 92.69 o 4 10 0 5775.02 6320.74 209.60 o 5 10 0 1039.96 1261.94 176.64 o 6 10 0 4363.12 5261.83 227.71 o 7 10 0 796.10 784.82 119.89 o 8 10 0 0.14 44.14 59.66 o 9 10 0 10231.76 11464.52 621.04 o 10 10 0 1399.74 1374.07 115.83 o 11 10 0 122.65 150.42 53.14 o 12 10 0 1733.59 2139.64 183.54 o 13 10 0 1363.02 1366.06 147.47 o 14 10 0 278.23 231.85 77.45 o 15 10 0 218.14 170.81 62.86 o 16 10 0 13.09 -12.75 29.05 o 17 10 0 233.58 131.26 68.84 o 1 11 0 3290.14 3634.87 201.98 o 2 11 0 5103.29 6102.40 461.15 o 3 11 0 1561.72 1209.38 102.53 o 4 11 0 11592.25 11251.86 365.57 o 5 11 0 4684.63 4322.79 299.36 o 6 11 0 9598.35 8771.71 289.55 o 7 11 0 16191.91 17473.81 540.92 o 8 11 0 3202.40 3658.55 266.04 o 9 11 0 5.86 31.74 60.15 o 10 11 0 5230.85 5529.57 319.56 o 11 11 0 545.80 471.87 127.94 o 12 11 0 599.85 594.63 121.74 o 13 11 0 35.73 16.92 67.97 o 14 11 0 336.72 307.51 63.96 o 15 11 0 468.10 440.22 89.18 o 16 11 0 348.90 275.93 59.22 o 17 11 0 223.77 159.59 43.90 o 0 12 0 9.89 14.20 50.34 o 1 12 0 163.76 166.53 55.44 o 2 12 0 9557.50 9882.16 609.65 o 3 12 0 8323.61 9917.01 394.98 o 4 12 0 50540.37 55486.79 661.62 o 5 12 0 4908.43 6415.24 292.34 o 6 12 0 2506.41 2769.34 166.53 o 7 12 0 2581.07 2691.30 215.03 o 8 12 0 2035.77 2688.73 228.56 o 9 12 0 4598.38 5362.01 351.51 o 10 12 0 126.89 84.42 45.30 o 11 12 0 1121.74 1131.67 114.86 o 12 12 0 254.14 338.93 89.11 o 13 12 0 256.29 145.64 67.32 o 14 12 0 13.79 -109.53 59.95 o 15 12 0 239.54 265.70 54.93 o 16 12 0 239.94 198.67 34.21 o 17 12 0 253.75 214.75 47.42 o 1 13 0 977.35 1178.92 130.81 o 2 13 0 891.34 669.11 90.66 o 3 13 0 27037.50 29113.62 594.48 o 4 13 0 7224.45 8571.32 265.91 o 5 13 0 1796.07 2354.47 233.80 o 6 13 0 1763.98 1374.21 123.54 o 7 13 0 8431.25 8535.39 391.63 o 8 13 0 33.54 -30.23 79.28 o 9 13 0 1351.86 1456.35 117.98 o 10 13 0 696.24 559.78 113.67 o 11 13 0 1214.12 1111.71 109.54 o 12 13 0 2832.74 2899.50 468.27 o 13 13 0 42.12 86.64 163.31 o 14 13 0 135.05 114.14 62.06 o 15 13 0 4.01 63.89 63.08 o 16 13 0 486.02 327.50 82.05 o 0 14 0 11663.49 12495.99 564.95 o 1 14 0 3085.27 3336.87 214.62 o 2 14 0 9582.91 10004.92 403.53 o 3 14 0 3068.52 3315.68 166.79 o 4 14 0 4.18 103.05 43.57 o 5 14 0 433.62 537.66 76.27 o 6 14 0 611.11 681.28 87.54 o 7 14 0 1936.17 2010.34 156.96 o 8 14 0 5646.82 6184.39 477.86 o 9 14 0 50.80 105.87 52.88 o 10 14 0 30.38 -36.89 68.47 o 11 14 0 83.22 2.81 54.52 o 12 14 0 179.37 118.96 53.60 o 13 14 0 176.95 83.45 95.78 o 14 14 0 16.47 -1.89 38.94 o 15 14 0 104.55 92.49 36.26 o 16 14 0 175.60 144.42 37.05 o 1 15 0 9800.09 10207.19 389.47 o 2 15 0 23507.72 24535.24 1834.77 o 3 15 0 11167.96 12112.32 325.44 o 4 15 0 1235.15 1252.42 111.76 o 5 15 0 36.08 75.73 36.25 o 6 15 0 1168.45 1233.54 139.51 o 7 15 0 425.94 335.17 73.50 o 8 15 0 603.34 578.99 149.15 o 9 15 0 822.07 810.46 95.53 o 10 15 0 9.74 -28.14 76.91 o 11 15 0 503.53 422.62 69.44 o 12 15 0 46.83 -78.85 89.93 o 13 15 0 122.35 133.95 45.33 o 14 15 0 614.34 488.20 63.89 o 15 15 0 160.45 150.22 32.61 o 16 15 0 90.28 63.72 25.27 o 0 16 0 9.99 187.73 79.75 o 1 16 0 8066.86 8418.76 364.26 o 2 16 0 10123.35 10118.36 332.18 o 3 16 0 1.71 44.42 36.48 o 4 16 0 2584.88 2555.88 166.40 o 5 16 0 1115.68 1441.42 137.78 o 6 16 0 2259.76 1796.14 168.80 o 7 16 0 1486.23 1619.53 167.33 o 8 16 0 2559.62 2786.71 224.75 o 9 16 0 0.26 -3.31 51.33 o 10 16 0 2711.58 2694.97 170.15 o 11 16 0 206.33 116.86 63.70 o 12 16 0 1404.39 1278.52 131.22 o 13 16 0 13.84 35.31 38.39 o 14 16 0 46.44 -3.42 54.39 o 15 16 0 51.91 49.96 41.97 o 16 16 0 3.32 4.85 27.48 o 1 17 0 14697.18 14859.51 488.30 o 2 17 0 1482.56 1837.22 186.03 o 3 17 0 1643.86 2122.35 139.60 o 4 17 0 256.01 419.35 76.23 o 5 17 0 989.98 1042.01 111.15 o 6 17 0 3593.84 3458.04 211.25 o 7 17 0 1436.68 1520.09 164.45 o 8 17 0 16.13 -25.82 66.13 o 9 17 0 1642.20 1623.32 246.73 o 10 17 0 507.62 394.34 156.04 o 11 17 0 7.45 -35.33 71.18 o 12 17 0 367.85 374.12 65.64 o 13 17 0 1539.68 1456.27 107.40 o 14 17 0 37.75 -19.55 27.03 o 15 17 0 1.49 11.84 21.87 o 16 17 0 16.27 -0.20 23.14 o 0 18 0 3796.56 3788.15 380.17 o 1 18 0 10028.92 8850.33 391.20 o 2 18 0 6.91 31.26 44.27 o 3 18 0 0.15 49.73 56.81 o 4 18 0 2875.41 2947.45 570.64 o 5 18 0 113.55 69.48 143.95 o 6 18 0 250.42 273.65 85.27 o 7 18 0 87.53 161.66 53.25 o 8 18 0 203.61 253.19 65.03 o 9 18 0 225.15 222.87 73.65 o 10 18 0 218.76 233.00 81.76 o 11 18 0 68.61 64.15 55.60 o 12 18 0 2816.74 2868.86 151.14 o 13 18 0 1605.66 1601.99 94.27 o 14 18 0 38.37 62.46 37.38 o 15 18 0 35.35 -13.93 30.88 o 1 19 0 78.77 92.03 63.54 o 2 19 0 185.73 184.25 63.51 o 3 19 0 215.59 165.74 81.48 o 4 19 0 4060.47 3883.20 432.88 o 5 19 0 447.21 328.78 100.63 o 6 19 0 2852.82 2573.65 188.45 o 7 19 0 3280.54 2757.18 193.96 o 8 19 0 244.06 213.95 95.15 o 9 19 0 3329.75 2781.25 231.65 o 10 19 0 3130.23 2995.63 219.58 o 11 19 0 1095.55 1065.55 141.20 o 12 19 0 2161.94 2227.43 183.62 o 13 19 0 1580.99 1489.19 146.75 o 14 19 0 12.67 37.32 41.69 o 15 19 0 113.24 80.31 43.89 o 0 20 0 4864.94 4560.30 433.41 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0 62.89 106.44 43.29 o 4 22 0 113.46 151.51 49.60 o 5 22 0 1415.82 1335.09 138.53 o 6 22 0 1.82 -58.51 56.61 o 7 22 0 879.23 693.98 127.95 o 8 22 0 56.40 -7.70 48.53 o 9 22 0 184.03 257.10 254.79 o 10 22 0 76.10 59.19 50.06 o 11 22 0 404.54 394.27 78.61 o 12 22 0 697.50 695.58 97.34 o 13 22 0 1.74 -79.00 40.68 o 14 22 0 48.49 -41.92 43.37 o 1 23 0 63.02 56.68 34.53 o 2 23 0 4249.11 3260.01 241.49 o 3 23 0 12861.05 9206.90 355.01 o 4 23 0 109.56 43.17 41.00 o 5 23 0 165.05 157.69 59.04 o 6 23 0 425.28 361.07 76.35 o 7 23 0 235.57 157.77 57.60 o 8 23 0 127.67 115.79 87.47 o 9 23 0 33.43 -71.69 143.72 o 10 23 0 900.14 813.21 163.95 o 11 23 0 924.72 782.51 188.79 o 12 23 0 411.79 406.59 72.99 o 13 23 0 506.79 458.07 94.75 o 14 23 0 44.30 27.06 30.79 o 0 24 0 1332.66 1077.38 140.08 o 1 24 0 1550.83 1084.03 100.60 o 2 24 0 4007.47 2917.70 196.94 o 3 24 0 8.63 -4.36 32.80 o 4 24 0 3264.66 2401.68 221.01 o 5 24 0 388.23 291.29 66.86 o 6 24 0 1270.69 1148.78 184.09 o 7 24 0 10.78 10.25 48.77 o 8 24 0 164.93 200.95 164.87 o 9 24 0 514.80 460.55 75.54 o 10 24 0 1586.30 1613.50 152.98 o 11 24 0 802.83 745.64 101.18 o 12 24 0 1789.73 1749.86 201.11 o 13 24 0 2.61 -28.98 33.13 o 14 24 0 25.78 -4.47 27.50 o 1 25 0 408.35 271.13 59.73 o 2 25 0 613.67 498.05 82.84 o 3 25 0 5983.17 4575.45 285.22 o 4 25 0 1640.92 1372.30 140.77 o 5 25 0 379.63 434.61 109.77 o 6 25 0 566.13 635.34 144.97 o 7 25 0 1.04 19.48 56.35 o 8 25 0 13.14 45.32 125.40 o 9 25 0 239.98 285.66 65.94 o 10 25 0 187.68 124.76 54.21 o 11 25 0 98.69 186.69 59.42 o 12 25 0 1.97 46.49 32.34 o 13 25 0 0.04 57.95 41.49 o 0 26 0 13.81 -95.52 82.79 o 1 26 0 1787.97 1261.37 153.08 o 2 26 0 4501.77 3388.93 424.88 o 3 26 0 13.82 74.10 50.73 o 4 26 0 5476.93 4534.03 344.63 o 5 26 0 302.19 209.37 100.04 o 6 26 0 509.91 434.16 114.86 o 7 26 0 13.50 81.44 53.46 o 8 26 0 305.80 275.69 93.98 o 9 26 0 1167.84 1413.83 192.59 o 10 26 0 190.17 135.80 52.71 o 11 26 0 1269.48 1216.17 162.56 o 12 26 0 812.99 1034.55 141.50 o 13 26 0 14.68 23.77 28.25 o 1 27 0 73.50 1.61 64.82 o 2 27 0 1069.21 802.70 136.82 o 3 27 0 402.76 350.82 92.88 o 4 27 0 1104.29 1010.57 149.70 o 5 27 0 1229.36 1038.36 193.97 o 6 27 0 5.91 45.41 57.94 o 7 27 0 894.77 910.84 176.20 o 8 27 0 61.82 78.22 53.49 o 9 27 0 281.76 375.19 107.40 o 10 27 0 1253.21 1454.81 192.21 o 11 27 0 419.80 473.68 113.17 o 12 27 0 126.63 182.55 63.63 o 0 28 0 2147.84 2278.24 320.75 o 1 28 0 25.93 65.92 71.76 o 2 28 0 5288.01 4539.35 321.86 o 3 28 0 2854.74 2275.25 229.59 o 4 28 0 87.99 43.06 82.99 o 5 28 0 12.89 36.56 96.09 o 6 28 0 28.19 62.85 60.75 o 7 28 0 219.99 104.02 56.64 o 8 28 0 12.64 50.81 60.59 o 9 28 0 317.07 279.94 95.36 o 10 28 0 1.38 53.01 75.52 o 11 28 0 408.16 602.17 110.51 o 12 28 0 745.37 1196.68 131.67 o 1 29 0 5767.12 4599.72 330.78 o 2 29 0 425.64 374.08 107.09 o 3 29 0 3351.62 3224.30 267.83 o 4 29 0 24.99 14.86 70.82 o 5 29 0 2723.46 2891.33 320.85 o 6 29 0 216.31 193.59 99.81 o 7 29 0 0.39 -71.15 68.65 o 8 29 0 153.64 147.33 55.90 o 9 29 0 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