#------------------------------------------------------------------------------ #$Date: 2016-04-09 04:23:35 +0300 (Sat, 09 Apr 2016) $ #$Revision: 181991 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/16/2241640.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241640 _cell_angle_alpha 90.000 _cell_angle_beta 91.031 _cell_angle_gamma 90.000 _cell_length_a 4.8888 _cell_length_b 24.6650 _cell_length_c 15.5956 _exptl_crystal_F_000 824.00 _reflns_d_resolution_high 0.8288 _cod_data_source_file hg5472IIsup3.hkl _cod_data_source_block II _shelx_title ' x13498 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 171.24 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 69.36 112.77 3.41 o 2 0 0 62.72 71.49 2.89 o 3 0 0 3733.34 3680.42 92.80 o 4 0 0 3.26 5.14 0.95 o 5 0 0 2454.19 2375.49 53.33 o 1 1 0 10001.84 9342.01 166.36 o 2 1 0 1234.17 1328.49 23.89 o 3 1 0 85.78 109.76 2.86 o 4 1 0 52.47 43.44 1.10 o 5 1 0 22.28 28.75 1.40 o 0 2 0 261.41 253.77 4.31 o 1 2 0 169.14 190.38 1.96 o 2 2 0 1009.56 1044.52 18.87 o 3 2 0 314.63 322.91 7.43 o 4 2 0 376.14 362.59 4.77 o 5 2 0 139.14 123.38 2.66 o 1 3 0 9630.62 9311.20 96.83 o 2 3 0 766.25 664.10 12.17 o 3 3 0 238.77 170.01 3.52 o 4 3 0 2.11 2.80 0.74 o 5 3 0 11.95 13.89 1.10 o 0 4 0 233.12 234.60 4.14 o 1 4 0 1601.50 1693.36 17.55 o 2 4 0 39.54 43.18 0.78 o 3 4 0 20.54 30.65 1.65 o 4 4 0 61.00 52.44 1.45 o 5 4 0 17.87 23.08 1.34 o 1 5 0 2991.94 2885.35 31.97 o 2 5 0 1986.29 2055.24 23.09 o 3 5 0 2566.24 2491.80 31.05 o 4 5 0 0.78 2.56 0.90 o 5 5 0 593.57 575.28 11.24 o 0 6 0 19907.35 18995.48 296.59 o 1 6 0 2551.29 2389.74 26.89 o 2 6 0 0.69 0.69 0.50 o 3 6 0 0.16 1.39 0.57 o 4 6 0 0.56 2.19 0.89 o 5 6 0 713.40 718.47 13.88 o 1 7 0 708.39 674.86 8.22 o 2 7 0 20.68 19.29 0.93 o 3 7 0 1915.49 1938.88 23.44 o 4 7 0 425.48 412.10 6.97 o 5 7 0 412.35 402.57 8.00 o 0 8 0 2.74 4.48 0.88 o 1 8 0 2070.07 2160.68 28.53 o 2 8 0 8.50 8.67 1.08 o 3 8 0 580.70 612.46 8.64 o 4 8 0 829.79 813.22 13.05 o 5 8 0 71.01 66.89 2.12 o 1 9 0 1876.37 2062.82 26.30 o 2 9 0 80.56 59.98 2.07 o 3 9 0 2831.88 2792.51 34.71 o 4 9 0 163.03 168.41 3.42 o 5 9 0 1.21 1.79 0.99 o 0 10 0 3563.40 3749.33 56.39 o 1 10 0 544.70 543.36 9.06 o 2 10 0 73.14 99.10 2.65 o 3 10 0 29.60 32.80 0.99 o 4 10 0 0.92 1.57 1.12 o 5 10 0 56.37 58.91 2.16 o 1 11 0 1149.73 1220.87 21.06 o 2 11 0 756.38 721.07 12.94 o 3 11 0 296.95 315.07 4.10 o 4 11 0 410.83 413.15 6.97 o 5 11 0 3.95 5.58 1.07 o 0 12 0 14785.43 15399.07 231.02 o 1 12 0 391.12 440.06 9.33 o 2 12 0 44.55 35.73 0.95 o 3 12 0 80.93 97.19 1.73 o 4 12 0 390.37 419.74 7.60 o 5 12 0 1260.84 1276.02 28.91 o 1 13 0 378.01 401.25 8.67 o 2 13 0 65.52 60.95 1.20 o 3 13 0 2.04 -0.16 0.68 o 4 13 0 1315.51 1379.10 23.76 o 5 13 0 100.74 100.97 2.89 o 0 14 0 4307.45 4217.63 140.05 o 1 14 0 10.01 20.97 1.66 o 2 14 0 144.75 146.19 2.09 o 3 14 0 14.69 11.76 0.76 o 4 14 0 68.59 75.42 2.59 o 5 14 0 29.51 26.70 1.39 o 1 15 0 0.46 3.88 1.36 o 2 15 0 589.28 544.02 6.35 o 3 15 0 134.54 118.20 2.16 o 4 15 0 159.72 168.08 4.32 o 5 15 0 195.23 181.98 5.00 o 1 16 0 40.35 29.27 1.30 o 2 16 0 185.54 196.54 2.93 o 3 16 0 819.12 857.56 12.55 o 4 16 0 54.09 57.52 1.81 o 1 17 0 45.37 47.91 2.13 o 2 17 0 341.72 307.43 4.23 o 3 17 0 500.66 522.09 9.29 o 4 17 0 27.98 29.28 1.70 o 1 18 0 246.02 214.42 4.94 o 2 18 0 338.67 341.51 4.93 o 3 18 0 87.36 91.33 2.76 o 4 18 0 326.59 325.00 9.28 o 1 19 0 27.21 23.17 1.64 o 2 19 0 49.68 53.39 1.64 o 3 19 0 1603.91 1751.23 34.97 o 4 19 0 479.03 464.33 10.55 o 0 20 0 1175.95 1023.34 52.44 o 1 20 0 483.13 459.79 13.94 o 2 20 0 329.07 307.70 5.12 o 3 20 0 74.35 70.80 2.32 o 4 20 0 35.89 30.83 1.96 o 1 21 0 1184.11 1129.14 24.25 o 2 21 0 981.88 966.89 15.81 o 3 21 0 605.20 643.04 13.06 o 4 21 0 202.20 186.82 6.42 o 0 22 0 260.55 230.51 13.56 o 1 22 0 0.73 2.00 1.26 o 2 22 0 286.98 295.97 5.23 o 3 22 0 398.78 403.21 8.89 o 1 23 0 0.52 1.56 1.24 o 2 23 0 99.64 88.00 2.43 o 3 23 0 652.88 689.20 14.99 o 0 24 0 54.83 33.35 2.80 o 1 24 0 194.20 192.73 4.80 o 2 24 0 65.84 50.34 1.94 o 3 24 0 1.78 3.73 0.85 o 1 25 0 2.81 2.46 1.26 o 2 25 0 99.90 100.94 3.19 o 3 25 0 6.07 5.14 1.14 o 0 26 0 164.04 191.15 8.04 o 1 26 0 539.30 528.36 30.49 o 2 26 0 239.58 239.48 7.60 o 1 27 0 0.81 3.97 2.42 o 2 27 0 114.07 97.71 3.56 o 1 28 0 96.86 86.76 4.25 o -5 1 1 77.62 71.44 1.56 o -4 1 1 82.53 74.79 1.38 o -3 1 1 52.53 50.37 2.00 o -2 1 1 2670.46 2553.60 45.57 o -1 1 1 26.47 28.69 0.54 o 0 1 1 285.59 291.44 4.84 o 1 1 1 5182.64 5236.68 51.02 o 2 1 1 782.84 799.80 14.54 o 3 1 1 479.56 417.30 10.40 o 4 1 1 976.28 932.70 11.97 o 5 1 1 293.16 275.72 5.62 o -5 2 1 177.20 172.47 3.20 o -4 2 1 786.43 738.25 8.88 o -3 2 1 129.85 119.87 3.26 o -2 2 1 5.38 1.97 0.99 o -1 2 1 7733.77 7711.15 82.61 o 0 2 1 90.19 80.79 1.05 o 1 2 1 4948.04 4896.24 49.77 o 2 2 1 556.71 531.72 10.55 o 3 2 1 158.44 187.96 4.56 o 4 2 1 172.54 192.55 3.16 o 5 2 1 361.22 366.85 8.12 o -5 3 1 50.41 55.34 1.70 o -4 3 1 145.97 154.77 2.32 o -3 3 1 335.85 339.68 6.31 o -2 3 1 538.92 511.71 9.50 o -1 3 1 278.33 281.03 3.00 o 0 3 1 451.90 447.21 5.81 o 1 3 1 1233.03 1133.19 11.54 o 2 3 1 67.29 81.40 1.14 o 3 3 1 153.87 163.49 3.20 o 4 3 1 702.20 706.89 10.19 o 5 3 1 0.20 1.59 1.23 o -5 4 1 743.65 738.70 13.07 o -4 4 1 112.31 108.82 1.94 o -3 4 1 1294.70 1321.98 18.93 o -2 4 1 26.04 15.16 0.60 o -1 4 1 2092.45 2127.45 21.52 o 0 4 1 2660.45 2620.75 32.05 o 1 4 1 2133.39 2141.50 23.09 o 2 4 1 340.60 355.53 3.78 o 3 4 1 482.30 490.16 6.80 o 4 4 1 134.13 136.69 2.58 o 5 4 1 32.46 34.26 1.88 o -5 5 1 55.31 52.87 1.93 o -4 5 1 372.39 372.47 5.73 o -3 5 1 73.77 59.83 1.21 o -2 5 1 453.44 379.68 4.44 o -1 5 1 268.69 336.38 3.95 o 0 5 1 3692.45 3681.30 39.02 o 1 5 1 3395.55 3372.91 36.60 o 2 5 1 2394.95 2605.71 32.02 o 3 5 1 1116.17 1052.68 12.91 o 4 5 1 688.81 687.74 11.00 o 5 5 1 410.73 437.31 9.71 o -5 6 1 41.74 37.70 1.53 o -4 6 1 2.47 2.02 0.88 o -3 6 1 4.59 7.81 0.54 o -2 6 1 71.50 77.15 1.34 o -1 6 1 568.53 457.78 5.39 o 0 6 1 109.45 88.01 1.39 o 1 6 1 1508.43 1469.29 20.94 o 2 6 1 0.16 0.68 0.55 o 3 6 1 169.59 163.04 2.33 o 4 6 1 105.59 107.90 2.23 o 5 6 1 0.92 2.82 1.45 o -5 7 1 12.36 11.05 1.14 o -4 7 1 251.43 248.93 4.21 o -3 7 1 2280.06 2146.48 23.54 o -2 7 1 2956.37 3006.41 43.57 o -1 7 1 2210.24 2084.15 25.49 o 0 7 1 360.21 399.01 4.51 o 1 7 1 313.59 290.45 4.65 o 2 7 1 1931.84 2053.97 31.30 o 3 7 1 913.49 860.27 10.57 o 4 7 1 572.89 564.02 8.94 o 5 7 1 517.39 499.01 9.81 o -5 8 1 575.60 614.62 12.74 o -4 8 1 766.36 749.28 11.46 o -3 8 1 563.85 526.30 6.58 o -2 8 1 3451.85 3754.77 64.26 o -1 8 1 722.07 711.29 9.72 o 0 8 1 4359.87 4290.58 45.42 o 1 8 1 231.85 211.79 3.36 o 2 8 1 1342.39 1332.18 23.12 o 3 8 1 1458.69 1473.96 19.19 o 4 8 1 63.64 61.21 1.90 o 5 8 1 1.51 3.22 1.01 o -5 9 1 10.29 10.25 1.20 o -4 9 1 0.96 0.79 1.05 o -3 9 1 108.37 115.73 1.90 o -2 9 1 644.65 703.15 12.51 o -1 9 1 0.40 -0.08 0.77 o 0 9 1 13541.22 13409.62 142.03 o 1 9 1 691.08 688.41 9.78 o 2 9 1 0.26 -1.02 1.02 o 3 9 1 140.54 115.96 2.02 o 4 9 1 395.14 431.02 7.95 o 5 9 1 293.97 316.32 6.39 o -5 10 1 546.45 577.38 13.37 o -4 10 1 240.14 242.09 4.44 o -3 10 1 309.82 324.79 4.87 o -2 10 1 379.15 346.84 6.62 o -1 10 1 2431.33 2775.97 38.19 o 0 10 1 94.20 102.94 1.67 o 1 10 1 3183.19 3385.63 54.75 o 2 10 1 605.42 676.21 12.10 o 3 10 1 2.85 7.90 0.61 o 4 10 1 645.82 664.60 11.75 o 5 10 1 177.82 180.07 4.00 o -5 11 1 25.47 26.50 1.57 o -4 11 1 98.54 101.40 2.53 o -3 11 1 0.85 2.12 0.67 o -2 11 1 1404.64 1458.94 25.46 o -1 11 1 14.52 9.91 1.19 o 0 11 1 357.30 352.89 4.20 o 1 11 1 111.53 123.53 3.12 o 2 11 1 94.55 96.11 2.76 o 3 11 1 1696.71 1734.30 20.37 o 4 11 1 86.79 83.12 2.18 o 5 11 1 36.10 30.94 1.35 o -5 12 1 19.96 26.94 1.51 o -4 12 1 20.80 19.50 0.98 o -3 12 1 568.01 614.72 7.83 o -2 12 1 279.31 258.06 3.82 o -1 12 1 232.70 228.52 5.37 o 0 12 1 1403.95 1248.68 14.36 o 1 12 1 553.68 638.27 13.14 o 2 12 1 626.39 615.79 7.92 o 3 12 1 1106.03 1126.06 13.68 o 4 12 1 51.17 47.47 1.63 o 5 12 1 62.62 68.17 2.18 o -5 13 1 0.93 0.81 0.97 o -4 13 1 22.05 26.04 1.91 o -3 13 1 842.83 861.06 10.48 o -2 13 1 3093.66 3057.48 35.26 o -1 13 1 1430.42 1400.30 28.01 o 0 13 1 293.26 244.18 4.55 o 1 13 1 6.82 -0.28 1.30 o 2 13 1 1615.05 1618.59 19.32 o 3 13 1 351.08 333.23 7.00 o 4 13 1 1058.11 1126.35 19.56 o 5 13 1 13.20 8.42 1.10 o -5 14 1 46.41 47.53 1.85 o -4 14 1 863.13 901.59 16.63 o -3 14 1 29.05 31.91 1.20 o -2 14 1 1166.18 1177.16 12.85 o -1 14 1 2446.43 2754.52 54.37 o 0 14 1 1315.04 1262.60 43.06 o 1 14 1 2098.19 2108.68 41.81 o 2 14 1 0.21 -0.50 0.65 o 3 14 1 693.43 684.06 9.35 o 4 14 1 544.95 535.39 9.51 o 5 14 1 18.26 18.77 1.80 o -5 15 1 60.59 48.85 1.68 o -4 15 1 597.28 663.61 14.50 o -3 15 1 93.91 88.01 1.97 o -2 15 1 1860.50 1776.98 21.10 o -1 15 1 3.20 1.49 1.07 o 1 15 1 264.86 250.73 5.10 o 2 15 1 30.77 25.66 0.84 o 3 15 1 14.25 14.54 0.84 o 4 15 1 873.14 905.36 15.73 o 5 15 1 34.88 33.55 2.17 o -4 16 1 1800.81 1875.62 37.07 o -3 16 1 1978.04 2070.18 29.88 o -2 16 1 41.97 37.96 1.16 o -1 16 1 193.92 184.90 3.56 o 1 16 1 1501.63 1390.01 28.32 o 2 16 1 96.68 97.08 1.88 o 3 16 1 0.41 -0.25 0.78 o 4 16 1 4.27 4.77 0.93 o -4 17 1 42.19 40.28 1.97 o -3 17 1 151.57 178.70 3.19 o -2 17 1 49.30 56.28 1.45 o -1 17 1 32.95 31.14 1.32 o 1 17 1 115.92 109.10 2.97 o 2 17 1 4257.96 4379.74 54.73 o 3 17 1 42.17 39.87 1.47 o 4 17 1 56.68 53.11 1.71 o -4 18 1 4.74 5.50 1.62 o -3 18 1 293.21 299.19 5.48 o -2 18 1 8.31 6.99 0.84 o -1 18 1 328.92 295.79 5.84 o 1 18 1 1178.20 1040.22 21.13 o 2 18 1 470.35 469.20 9.73 o 3 18 1 44.54 41.55 1.48 o 4 18 1 86.01 77.42 2.21 o -4 19 1 458.62 463.99 13.43 o -3 19 1 170.04 187.00 4.87 o -2 19 1 1842.39 1853.54 28.57 o -1 19 1 59.63 48.30 2.39 o 1 19 1 682.27 616.14 14.86 o 2 19 1 1170.74 1177.44 18.35 o 3 19 1 1417.76 1529.66 26.44 o 4 19 1 395.33 406.04 15.96 o -4 20 1 56.11 57.73 2.93 o -3 20 1 78.34 69.54 2.44 o -2 20 1 1132.58 1178.69 18.30 o -1 20 1 453.98 478.92 11.89 o 0 20 1 307.12 288.41 15.95 o 1 20 1 4.27 6.04 1.59 o 2 20 1 1145.49 1156.99 18.92 o 3 20 1 399.92 422.31 8.86 o 4 20 1 9.37 5.49 0.77 o -4 21 1 126.72 140.17 5.04 o -3 21 1 1192.49 1303.14 28.13 o -2 21 1 1086.88 1149.22 17.98 o -1 21 1 298.21 282.92 7.47 o 0 21 1 181.56 156.40 7.05 o 1 21 1 152.43 129.17 4.29 o 2 21 1 966.09 1044.40 19.33 o 3 21 1 54.25 58.16 2.05 o 4 21 1 9.66 11.45 1.41 o -3 22 1 454.82 489.70 10.83 o -2 22 1 219.05 216.06 3.99 o -1 22 1 5.31 10.36 1.34 o 0 22 1 115.45 110.37 7.24 o 1 22 1 98.11 112.27 3.80 o 2 22 1 1480.08 1535.44 25.24 o 3 22 1 11.61 13.30 1.16 o -3 23 1 55.55 66.66 2.51 o -2 23 1 2.81 0.99 1.03 o -1 23 1 120.05 111.47 3.01 o 0 23 1 10.28 5.39 1.48 o 1 23 1 9.68 11.35 1.51 o 2 23 1 263.49 270.93 5.18 o 3 23 1 102.97 100.78 2.54 o -3 24 1 4.30 2.30 0.88 o -2 24 1 199.05 221.69 4.50 o -1 24 1 1.84 3.26 1.23 o 0 24 1 566.15 530.17 13.98 o 1 24 1 551.12 575.87 14.18 o 2 24 1 417.07 453.84 8.73 o 3 24 1 50.57 42.20 1.94 o -3 25 1 81.46 78.41 2.44 o -2 25 1 64.81 75.42 3.50 o -1 25 1 58.77 43.95 2.33 o 0 25 1 139.84 132.47 3.69 o 1 25 1 146.19 131.02 3.94 o 2 25 1 0.82 0.85 1.34 o 3 25 1 93.73 102.30 2.95 o -2 26 1 49.73 59.94 2.76 o -1 26 1 376.15 374.64 28.52 o 0 26 1 100.56 99.05 3.59 o 1 26 1 79.47 112.85 5.97 o 2 26 1 0.62 0.67 1.29 o -2 27 1 137.85 151.32 7.22 o -1 27 1 151.28 134.21 5.40 o 0 27 1 2.36 0.94 1.47 o 1 27 1 81.55 80.96 4.55 o 2 27 1 14.19 8.15 1.25 o -1 28 1 11.38 8.15 1.73 o 0 28 1 4.09 1.56 1.45 o 1 28 1 526.75 435.08 22.67 o 0 29 1 114.51 107.96 3.76 o -5 0 2 241.14 218.29 4.45 o -4 0 2 14.97 17.44 1.09 o -3 0 2 4.62 10.98 1.81 o -2 0 2 69.21 85.83 3.24 o -1 0 2 10309.97 9943.46 143.53 o 0 0 2 14696.10 13732.40 320.28 o 1 0 2 27.13 13.07 0.89 o 2 0 2 776.00 922.99 14.05 o 3 0 2 14.49 19.49 1.54 o 4 0 2 53.64 43.23 1.85 o 5 0 2 495.04 479.23 16.06 o -5 1 2 171.82 160.48 2.42 o -4 1 2 299.82 254.11 3.23 o -3 1 2 146.30 161.83 3.35 o -2 1 2 149.84 166.27 3.57 o -1 1 2 18619.63 18546.45 413.40 o 0 1 2 2781.44 2802.03 30.29 o 1 1 2 15838.01 15133.10 160.47 o 2 1 2 1476.32 1368.87 14.32 o 3 1 2 104.43 99.39 2.29 o 4 1 2 500.11 475.15 6.31 o 5 1 2 210.88 210.91 11.17 o -5 2 2 82.61 91.77 2.05 o -4 2 2 602.71 560.42 6.88 o -3 2 2 4000.83 3994.89 62.82 o -2 2 2 1951.15 1973.72 35.32 o -1 2 2 15.78 27.44 0.66 o 0 2 2 1667.80 1674.79 18.67 o 1 2 2 1606.32 1427.83 14.87 o 2 2 2 1940.61 2052.20 21.97 o 3 2 2 11.59 19.36 1.36 o 4 2 2 25.62 33.53 1.47 o 5 2 2 435.80 448.32 14.87 o -5 3 2 59.00 68.97 1.90 o -4 3 2 17.30 20.35 0.81 o -3 3 2 1247.86 1181.26 16.93 o -2 3 2 5987.07 5855.78 89.98 o -1 3 2 816.75 713.61 7.32 o 0 3 2 24522.91 23242.03 541.45 o 1 3 2 16768.83 16659.11 199.64 o 2 3 2 16.23 13.98 0.46 o 3 3 2 3228.86 3129.58 39.61 o 4 3 2 26.23 32.16 1.63 o 5 3 2 1574.19 1597.34 36.93 o -5 4 2 706.47 660.43 11.53 o -4 4 2 466.91 434.67 5.86 o -3 4 2 0.92 1.19 0.70 o -2 4 2 1346.44 1384.98 15.60 o -1 4 2 4844.95 4817.67 48.87 o 0 4 2 532.94 520.55 6.13 o 1 4 2 101.34 84.77 1.23 o 2 4 2 61.40 51.39 0.96 o 3 4 2 29.27 48.88 1.35 o 4 4 2 98.16 92.88 1.87 o 5 4 2 49.95 54.50 3.05 o -5 5 2 848.74 837.04 14.49 o -4 5 2 1213.48 1171.92 15.98 o -3 5 2 1082.94 1059.20 12.70 o -2 5 2 872.64 964.79 10.65 o -1 5 2 556.06 508.51 5.59 o 0 5 2 10942.98 10782.75 123.10 o 1 5 2 1286.51 1220.86 16.39 o 2 5 2 2704.33 2691.94 42.78 o 3 5 2 52.39 59.67 1.21 o 4 5 2 624.51 642.59 12.72 o 5 5 2 209.28 224.92 5.35 o -5 6 2 391.37 402.10 7.75 o -4 6 2 13.49 16.48 1.18 o -3 6 2 16.18 19.92 0.66 o -2 6 2 1273.86 1260.84 17.67 o -1 6 2 9775.33 9428.48 105.96 o 0 6 2 1007.15 959.19 11.15 o 1 6 2 11.92 9.96 0.64 o 2 6 2 173.29 121.07 2.43 o 3 6 2 352.16 325.93 4.63 o 4 6 2 103.06 95.15 2.33 o 5 6 2 10.72 9.73 1.32 o -5 7 2 452.67 428.86 8.22 o -4 7 2 0.20 5.28 1.02 o -3 7 2 366.25 403.63 5.05 o -2 7 2 210.86 198.67 3.68 o -1 7 2 941.56 967.84 12.05 o 0 7 2 220.30 195.05 2.48 o 1 7 2 779.92 824.57 11.18 o 2 7 2 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