#------------------------------------------------------------------------------
#$Date: 2016-04-28 04:41:07 +0300 (Thu, 28 Apr 2016) $
#$Revision: 182298 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/16/2241658.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2241658
_cell_angle_alpha                90.000
_cell_angle_beta                 90.334
_cell_angle_gamma                90.000
_cell_length_a                   9.8310
_cell_length_b                   5.2740
_cell_length_c                   13.6170
_exptl_crystal_F_000             826.40
_reflns_d_resolution_high        0.7833
_cod_data_source_file            vn2110Isup2.hkl
_cod_data_source_block           I
_shelx_title                     '  mir24 in C 2/c'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            424.93
_shelx_f_squared_multiplier      1.000
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 1206.12 962.57 52.28 o
4 0 0 42.61 38.95 10.26 o
6 0 0 101218.64 97195.76 748.45 o
8 0 0 2851.65 2916.99 78.91 o
10 0 0 4971.56 5022.12 117.39 o
12 0 0 23511.64 23602.76 300.80 o
1 1 0 6102.35 5408.54 58.76 o
3 1 0 180563.17 152424.88 13090.33 o
5 1 0 528.76 669.59 27.48 o
7 1 0 7361.94 6547.30 130.44 o
9 1 0 35085.04 35155.68 654.40 o
11 1 0 3196.41 3175.20 72.39 o
0 2 0 113959.29 103695.67 1224.35 o
2 2 0 959.65 1460.30 27.28 o
4 2 0 5070.20 4142.58 212.10 o
6 2 0 79527.16 73127.17 3922.53 o
8 2 0 1473.96 1451.62 90.97 o
10 2 0 1799.66 1914.72 75.16 o
1 3 0 9.23 -42.46 59.62 o
3 3 0 46507.95 44943.09 404.76 o
5 3 0 1217.23 1201.51 68.65 o
7 3 0 1759.40 1618.11 112.45 o
9 3 0 20200.60 18943.07 1216.77 o
11 3 0 1289.34 1233.83 43.76 o
0 4 0 12551.89 11926.69 615.30 o
2 4 0 128.15 131.10 32.35 o
4 4 0 418.95 364.43 14.96 o
6 4 0 9016.92 8353.65 469.30 o
8 4 0 871.02 763.29 77.55 o
10 4 0 821.48 803.78 69.23 o
1 5 0 289.14 264.55 14.35 o
3 5 0 5907.55 5642.53 214.43 o
5 5 0 176.84 181.23 32.52 o
7 5 0 76.35 64.61 25.28 o
0 6 0 696.53 802.37 110.29 o
2 6 0 16.66 4.10 23.99 o
4 6 0 35.09 35.58 24.50 o
-11 1 1 913.46 909.25 34.86 o
-9 1 1 760.21 752.01 28.15 o
-7 1 1 8250.21 7713.25 200.72 o
-5 1 1 10.54 19.93 11.74 o
-3 1 1 721.11 578.86 17.89 o
-1 1 1 6756.69 6979.42 276.69 o
1 1 1 400.72 382.88 16.59 o
3 1 1 2110.07 1711.22 100.41 o
5 1 1 2454.29 2322.23 82.52 o
7 1 1 130.55 124.40 10.24 o
9 1 1 1713.97 1722.44 55.49 o
11 1 1 568.21 576.64 32.70 o
-10 2 1 2186.81 2247.64 103.37 o
-8 2 1 237.69 252.25 32.26 o
-6 2 1 4801.47 4646.94 218.57 o
-4 2 1 14552.61 13587.08 429.50 o
-2 2 1 1918.51 2317.22 54.81 o
0 2 1 10222.67 9464.18 236.60 o
2 2 1 103.63 59.99 7.58 o
4 2 1 731.19 600.54 51.38 o
6 2 1 18157.47 17104.31 738.87 o
8 2 1 1572.19 1525.70 44.02 o
10 2 1 162.99 200.60 16.32 o
-11 3 1 1544.43 1478.61 106.21 o
-9 3 1 1618.21 1591.18 106.07 o
-7 3 1 11072.16 10937.53 493.65 o
-5 3 1 3403.32 3347.59 107.83 o
-3 3 1 11830.88 11704.26 177.66 o
-1 3 1 26677.16 26481.78 429.33 o
1 3 1 2645.92 2536.70 52.11 o
3 3 1 13656.10 13156.34 235.55 o
5 3 1 8015.16 6915.99 661.08 o
7 3 1 642.01 636.80 43.76 o
9 3 1 6903.69 6779.00 376.47 o
11 3 1 43.45 86.14 26.45 o
-10 4 1 7444.47 7378.69 409.61 o
-8 4 1 1693.69 1714.75 76.99 o
-6 4 1 4546.26 4304.66 185.38 o
-4 4 1 5391.37 5557.16 105.57 o
-2 4 1 6722.05 6788.15 83.52 o
0 4 1 24911.90 24772.91 301.60 o
2 4 1 13749.07 13312.71 408.63 o
4 4 1 1574.12 1622.03 61.01 o
6 4 1 13073.41 12196.96 1025.05 o
8 4 1 22.54 44.12 20.14 o
10 4 1 1576.72 1595.74 57.93 o
-7 5 1 6525.03 6269.46 293.04 o
-5 5 1 7786.50 8202.62 111.58 o
-3 5 1 8774.66 8757.23 171.26 o
-1 5 1 7154.61 7127.73 161.29 o
1 5 1 6528.96 6513.04 91.69 o
3 5 1 16116.02 15909.65 645.42 o
5 5 1 1055.93 1064.21 56.93 o
7 5 1 3698.33 3525.41 422.51 o
-4 6 1 6754.57 6560.71 292.60 o
-2 6 1 8935.38 9423.41 204.57 o
0 6 1 7348.41 7851.69 122.78 o
2 6 1 759.08 857.19 46.80 o
4 6 1 8256.65 8164.59 423.41 o
-12 0 2 6731.69 7059.28 274.82 o
-10 0 2 17639.75 17875.50 216.78 o
-8 0 2 3474.98 3320.32 148.51 o
-6 0 2 2617.30 2024.42 52.87 o
-4 0 2 45875.42 42931.85 652.65 o
-2 0 2 68447.56 64944.45 205.16 o
0 0 2 1105.02 714.72 24.43 o
2 0 2 65117.39 70830.18 1447.13 o
4 0 2 11236.81 8674.76 91.39 o
6 0 2 9830.48 10372.06 154.28 o
8 0 2 2499.94 2754.03 132.18 o
10 0 2 21659.34 21543.77 243.07 o
12 0 2 3378.96 3322.97 269.83 o
-11 1 2 2337.01 2273.51 81.73 o
-9 1 2 2293.35 2361.26 67.13 o
-7 1 2 25916.65 24692.31 491.87 o
-5 1 2 35005.52 31069.06 503.16 o
-3 1 2 51.93 34.22 10.62 o
-1 1 2 75003.19 83186.67 2471.91 o
1 1 2 75931.64 81647.76 2062.21 o
3 1 2 6381.88 7603.99 233.34 o
5 1 2 25890.32 26243.03 486.09 o
7 1 2 33934.38 33034.20 463.42 o
9 1 2 3310.38 3404.19 100.60 o
11 1 2 2630.81 2534.93 65.95 o
-10 2 2 9322.26 8900.28 323.06 o
-8 2 2 7595.44 7283.86 277.57 o
-6 2 2 7411.62 6805.59 179.19 o
-4 2 2 27900.59 27463.54 676.11 o
-2 2 2 17716.58 15462.15 533.50 o
0 2 2 78.09 302.66 16.02 o
2 2 2 14652.22 15210.36 478.13 o
4 2 2 51888.65 47859.62 2275.16 o
6 2 2 327.10 408.58 16.87 o
8 2 2 5372.22 5394.21 85.66 o
10 2 2 11143.88 11766.39 250.20 o
-11 3 2 3694.01 3892.74 99.77 o
-9 3 2 8983.59 8985.40 442.57 o
-7 3 2 7703.64 7624.66 358.97 o
-5 3 2 6453.91 5914.67 222.50 o
-3 3 2 3895.40 3584.13 141.51 o
-1 3 2 7241.73 7678.84 98.40 o
1 3 2 34900.60 32311.07 1351.14 o
3 3 2 1588.25 1397.66 46.59 o
5 3 2 3332.85 3090.07 156.66 o
7 3 2 18618.90 18119.53 898.24 o
9 3 2 116.16 70.78 30.53 o
11 3 2 485.10 462.93 27.74 o
-10 4 2 734.20 575.83 47.03 o
-8 4 2 6132.38 6415.88 224.06 o
-6 4 2 5149.37 5127.19 89.21 o
-4 4 2 1903.22 2023.81 49.63 o
-2 4 2 19162.73 18595.58 138.53 o
0 4 2 4932.38 4662.57 107.86 o
2 4 2 1444.64 1480.36 113.97 o
4 4 2 22059.91 20842.59 569.75 o
6 4 2 927.30 916.41 115.13 o
8 4 2 516.47 489.30 49.80 o
-7 5 2 15.84 42.64 27.42 o
-5 5 2 7239.73 7718.47 111.88 o
-3 5 2 9795.77 9849.69 186.45 o
-1 5 2 16.24 -14.47 22.69 o
1 5 2 6561.01 6700.08 227.94 o
3 5 2 4709.53 4520.51 97.77 o
5 5 2 365.49 394.32 17.95 o
7 5 2 5425.06 5262.44 330.27 o
-4 6 2 1028.07 1232.29 43.38 o
-2 6 2 7626.46 8088.80 121.39 o
0 6 2 5181.92 5303.30 95.00 o
2 6 2 388.88 452.20 29.19 o
4 6 2 3237.94 3113.45 168.47 o
-11 1 3 746.20 742.60 30.14 o
-9 1 3 1250.06 1247.60 41.39 o
-7 1 3 140.46 170.19 20.12 o
-5 1 3 4108.99 3857.79 58.45 o
-3 1 3 3492.15 3684.65 68.67 o
-1 1 3 15801.82 16905.10 651.31 o
1 1 3 141.67 196.98 8.69 o
3 1 3 742.40 798.55 37.98 o
5 1 3 5285.67 5168.25 142.30 o
7 1 3 0.43 -1.00 17.78 o
9 1 3 10.70 32.39 20.80 o
11 1 3 1443.37 1510.60 51.06 o
-10 2 3 4223.37 4292.29 120.59 o
-8 2 3 3374.87 3362.41 114.74 o
-6 2 3 4803.84 4583.91 65.95 o
-4 2 3 19620.14 18396.76 324.53 o
-2 2 3 13128.24 14019.65 627.82 o
0 2 3 1386.21 1421.32 45.69 o
2 2 3 43960.12 46918.05 270.77 o
4 2 3 1310.35 1333.49 64.62 o
6 2 3 4226.78 3896.98 81.81 o
8 2 3 8170.70 8202.55 181.78 o
10 2 3 144.66 163.87 19.13 o
-11 3 3 3737.69 3790.16 135.49 o
-9 3 3 1132.40 1160.89 65.56 o
-7 3 3 9591.76 9460.52 389.07 o
-5 3 3 5597.95 5460.94 76.86 o
-3 3 3 2582.88 2522.10 94.96 o
-1 3 3 28495.07 28191.19 708.12 o
1 3 3 3412.29 3362.71 181.47 o
3 3 3 101.80 125.82 15.90 o
5 3 3 24875.10 23794.76 1271.00 o
7 3 3 238.22 235.14 32.77 o
9 3 3 1.20 -5.07 23.79 o
11 3 3 8275.14 8533.68 222.31 o
-8 4 3 4053.02 4267.77 187.04 o
-6 4 3 4445.97 4366.85 237.96 o
-4 4 3 26869.11 27108.74 385.49 o
-2 4 3 3146.23 3041.53 68.83 o
0 4 3 10608.78 10625.35 302.46 o
2 4 3 27287.99 26657.86 1377.79 o
4 4 3 1056.43 976.37 36.18 o
6 4 3 63.58 60.40 21.52 o
8 4 3 17588.57 16921.26 996.54 o
-7 5 3 10537.47 10537.44 305.49 o
-5 5 3 1954.35 2013.59 66.51 o
-3 5 3 7611.35 7400.67 139.53 o
-1 5 3 20170.58 20442.38 165.10 o
1 5 3 170.78 170.32 14.87 o
3 5 3 2340.84 2152.57 55.78 o
5 5 3 20645.98 19992.91 603.75 o
7 5 3 765.32 727.02 90.97 o
-4 6 3 8259.79 8131.98 211.83 o
-2 6 3 94.37 79.02 23.78 o
0 6 3 3123.65 3333.02 76.86 o
2 6 3 16105.50 15513.89 263.91 o
4 6 3 1169.64 1176.99 41.65 o
-12 0 4 149.90 146.37 42.66 o
-10 0 4 3760.50 3764.47 103.41 o
-8 0 4 39504.23 38042.21 397.51 o
-6 0 4 475.91 1566.94 325.07 o
-4 0 4 57997.79 55705.59 1694.64 o
-2 0 4 103416.88 103542.67 339.84 o
0 0 4 4942.56 6694.09 80.60 o
2 0 4 71633.11 70758.13 1015.54 o
4 0 4 35807.82 33402.21 793.11 o
6 0 4 1369.17 1610.11 74.89 o
8 0 4 57408.32 58412.06 1123.30 o
10 0 4 7909.90 8371.22 210.46 o
12 0 4 3663.43 3364.29 188.82 o
-11 1 4 23889.26 24708.72 202.70 o
-9 1 4 713.13 756.89 32.46 o
-7 1 4 9387.27 8720.94 95.01 o
-5 1 4 88647.14 83589.42 708.18 o
-3 1 4 904.23 1133.94 27.30 o
-1 1 4 31517.35 30302.04 1257.78 o
1 1 4 82159.25 91522.37 3523.02 o
3 1 4 179.57 349.03 69.85 o
5 1 4 48387.75 46706.10 745.94 o
7 1 4 18772.30 18446.25 156.88 o
9 1 4 1265.19 1280.16 45.33 o
11 1 4 17024.70 17718.58 195.88 o
-10 2 4 896.46 908.43 35.39 o
-8 2 4 28622.61 28507.86 789.09 o
-6 2 4 1544.61 1642.55 42.46 o
-4 2 4 16635.62 14884.87 133.30 o
-2 2 4 51936.40 51431.33 1789.67 o
0 2 4 2820.15 3161.68 118.18 o
2 2 4 61614.56 66039.09 583.87 o
4 2 4 36346.31 34268.88 1202.53 o
6 2 4 5484.50 5764.92 206.85 o
8 2 4 18206.11 18218.84 359.95 o
10 2 4 3126.56 3171.86 74.61 o
-9 3 4 1264.47 1270.78 44.74 o
-7 3 4 582.62 563.03 27.83 o
-5 3 4 17119.91 15936.44 183.23 o
-3 3 4 2593.70 2768.00 113.82 o
-1 3 4 29318.20 28227.68 802.43 o
1 3 4 33434.45 32224.94 1195.16 o
3 3 4 7632.31 8000.76 170.86 o
5 3 4 14483.73 13625.14 588.84 o
7 3 4 5661.18 5430.80 234.99 o
9 3 4 2519.49 2512.01 92.04 o
-8 4 4 9635.42 9803.83 316.35 o
-6 4 4 2589.42 2652.07 74.56 o
-4 4 4 920.54 905.00 39.99 o
-2 4 4 15307.85 15267.10 503.39 o
0 4 4 3613.92 3813.02 120.68 o
2 4 4 4573.66 4394.54 268.04 o
4 4 4 6604.13 6491.00 160.54 o
6 4 4 2512.56 2492.00 114.94 o
8 4 4 4619.74 4627.64 108.25 o
-7 5 4 1100.55 1183.92 82.51 o
-5 5 4 3979.38 4105.38 124.62 o
-3 5 4 3435.77 3310.11 72.39 o
-1 5 4 421.40 455.06 25.30 o
1 5 4 1450.78 1465.81 92.32 o
3 5 4 2482.18 2427.03 107.93 o
5 5 4 4069.27 3804.26 135.34 o
7 5 4 897.93 890.35 82.62 o
-4 6 4 11.23 105.78 77.74 o
-2 6 4 955.73 1033.10 40.65 o
0 6 4 863.52 821.18 31.87 o
2 6 4 21.71 60.55 20.88 o
4 6 4 162.40 140.51 26.08 o
-11 1 5 2756.62 2777.35 93.25 o
-9 1 5 382.15 417.50 18.77 o
-7 1 5 132.68 132.27 14.82 o
-5 1 5 2713.65 2607.32 46.70 o
-3 1 5 3154.71 3210.69 66.88 o
-1 1 5 820.07 927.54 38.97 o
1 1 5 40723.84 48635.98 1938.39 o
3 1 5 36.56 144.08 31.21 o
5 1 5 18.98 38.58 16.22 o
7 1 5 2379.94 2516.22 55.26 o
9 1 5 429.09 432.69 18.23 o
11 1 5 160.96 143.49 34.01 o
-10 2 5 707.24 711.81 27.04 o
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-6 2 5 745.37 721.15 26.01 o
-4 2 5 4.93 24.86 16.05 o
-2 2 5 19062.86 20060.21 809.81 o
0 2 5 35.98 208.21 100.10 o
2 2 5 3577.81 3870.65 115.15 o
4 2 5 21508.13 21327.09 483.40 o
6 2 5 406.52 389.01 38.08 o
8 2 5 1113.10 1138.22 41.31 o
10 2 5 1754.63 1747.50 61.69 o
-9 3 5 11.88 26.11 25.92 o
-7 3 5 618.77 629.03 24.73 o
-5 3 5 35075.50 33454.61 446.40 o
-3 3 5 56.33 84.75 24.67 o
-1 3 5 78.56 69.92 18.14 o
1 3 5 42444.26 43453.28 1254.12 o
3 3 5 2291.66 2382.75 49.33 o
5 3 5 731.49 742.84 27.99 o
7 3 5 18541.21 18417.71 807.94 o
9 3 5 2106.82 2049.23 76.94 o
-8 4 5 13875.57 14755.25 505.00 o
-6 4 5 169.45 160.78 21.82 o
-4 4 5 673.80 659.30 27.43 o
-2 4 5 32073.41 32616.45 1046.33 o
0 4 5 277.93 296.84 14.73 o
2 4 5 70.42 61.72 21.16 o
4 4 5 16944.18 16690.36 461.87 o
6 4 5 4361.90 4305.99 136.03 o
8 4 5 1861.10 1855.48 95.25 o
-7 5 5 2587.55 2693.96 108.02 o
-5 5 5 20147.59 20634.57 189.04 o
-3 5 5 114.48 102.11 32.91 o
-1 5 5 868.22 898.12 32.97 o
1 5 5 19961.04 19744.77 572.22 o
3 5 5 3660.08 3573.64 208.53 o
5 5 5 75.78 80.51 18.67 o
7 5 5 12840.62 12022.84 924.77 o
-4 6 5 2290.53 2103.73 87.59 o
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0 6 5 3057.67 2916.64 121.45 o
2 6 5 611.36 610.77 44.37 o
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-10 0 6 17651.32 18467.69 237.83 o
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-2 0 6 14776.01 16264.50 282.94 o
0 0 6 25301.18 34964.85 221.11 o
2 0 6 38217.67 37298.74 249.88 o
4 0 6 16150.29 16772.72 524.08 o
6 0 6 2.07 35.01 41.75 o
8 0 6 14949.81 15292.42 683.41 o
10 0 6 11765.54 12184.12 466.74 o
-11 1 6 95.26 75.64 28.44 o
-9 1 6 5146.54 5339.62 87.81 o
-7 1 6 18615.55 18507.63 143.97 o
-5 1 6 6773.36 7049.83 132.52 o
-3 1 6 11401.51 12232.60 254.61 o
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3 1 6 12.02 146.67 53.07 o
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-10 2 6 10105.58 10524.14 197.66 o
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-5 5 6 155.40 191.39 21.73 o
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-1 5 6 10260.99 10295.45 267.86 o
1 5 6 456.61 528.84 46.28 o
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-2 6 6 693.90 702.43 28.76 o
0 6 6 3375.06 3451.66 84.66 o
2 6 6 4332.96 4571.63 150.12 o
-11 1 7 162.01 137.33 21.75 o
-9 1 7 2073.66 2113.28 61.79 o
-7 1 7 701.68 668.27 24.29 o
-5 1 7 1591.39 1626.59 77.64 o
-3 1 7 2709.94 2759.58 105.65 o
-1 1 7 1960.34 2229.19 44.53 o
1 1 7 17.60 23.28 20.45 o
3 1 7 3982.60 3968.89 62.64 o
5 1 7 1449.65 1459.89 92.80 o
7 1 7 2491.06 2519.24 65.92 o
9 1 7 59.96 16.30 29.86 o
11 1 7 433.70 447.22 32.73 o
-10 2 7 0.16 -0.60 26.23 o
-8 2 7 1430.14 1446.27 51.10 o
-6 2 7 9393.36 9318.85 112.89 o
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0 2 7 14832.74 15486.00 318.64 o
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