#------------------------------------------------------------------------------ #$Date: 2016-04-28 04:41:37 +0300 (Thu, 28 Apr 2016) $ #$Revision: 182299 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/16/2241659.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241659 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.4259 _cell_length_b 11.4264 _cell_length_c 45.7055 _exptl_crystal_F_000 1912.00 _reflns_d_resolution_high 0.7709 _cod_data_source_file xu5886Isup2.hkl _cod_data_source_block I _shelx_title ' cg-5 in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 252.27 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 36114.32 33720.89 404.94 o 4 0 0 4726.03 4326.54 92.89 o 6 0 0 9.73 -31.31 42.53 o 8 0 0 47.82 58.58 58.11 o 10 0 0 0.01 14.07 58.03 o 1 1 0 8696.24 8209.80 71.46 o 2 1 0 47.76 8.81 19.02 o 3 1 0 63.15 56.23 22.05 o 4 1 0 678.84 724.75 28.08 o 5 1 0 1501.29 1757.48 43.25 o 6 1 0 71.22 73.43 28.54 o 7 1 0 193.23 346.12 37.60 o 8 1 0 1494.21 1436.28 68.10 o 9 1 0 0.29 48.24 43.48 o 10 1 0 78.16 -0.81 33.27 o 0 2 0 63642.18 56649.82 871.39 o 1 2 0 16851.29 16481.98 174.26 o 2 2 0 0.72 -7.46 17.10 o 3 2 0 446.78 366.90 47.61 o 4 2 0 1464.57 1722.69 39.11 o 5 2 0 87.78 39.01 20.75 o 6 2 0 1185.32 1165.01 40.47 o 7 2 0 75.92 116.95 38.38 o 8 2 0 0.01 2.96 31.77 o 9 2 0 127.87 168.01 55.95 o 10 2 0 56.38 -41.86 49.26 o 1 3 0 6558.26 5881.51 89.38 o 2 3 0 1966.56 2348.51 52.52 o 3 3 0 94.59 93.90 29.54 o 4 3 0 9.23 -3.32 24.70 o 5 3 0 352.02 301.94 43.21 o 6 3 0 9.91 30.95 27.67 o 7 3 0 186.08 187.82 38.87 o 8 3 0 1248.00 1175.68 64.59 o 9 3 0 26.49 2.24 41.52 o 10 3 0 39.45 37.34 50.61 o 0 4 0 6325.14 6881.94 285.11 o 1 4 0 2291.56 2161.89 65.48 o 2 4 0 8763.76 8912.12 139.28 o 3 4 0 744.38 699.31 54.02 o 4 4 0 7585.38 7380.29 110.15 o 5 4 0 329.55 475.66 43.63 o 6 4 0 1236.98 1296.11 55.15 o 7 4 0 172.16 108.55 42.44 o 8 4 0 34.77 39.08 39.87 o 9 4 0 12.39 10.49 40.57 o 10 4 0 2.62 71.51 58.78 o 1 5 0 1425.27 1442.28 56.17 o 2 5 0 2758.80 2962.43 70.62 o 3 5 0 1332.10 1260.82 56.45 o 4 5 0 131.09 129.16 35.68 o 5 5 0 3.59 -3.53 30.21 o 6 5 0 1179.17 1190.96 65.53 o 7 5 0 282.02 223.93 49.03 o 8 5 0 91.42 90.13 45.95 o 9 5 0 9.78 1.19 36.87 o 10 5 0 20.83 58.06 60.35 o 0 6 0 1128.89 1174.48 77.62 o 1 6 0 902.97 896.76 56.28 o 2 6 0 2843.09 3072.41 79.20 o 3 6 0 389.00 520.08 49.41 o 4 6 0 1688.87 1794.55 85.58 o 5 6 0 0.01 11.27 32.14 o 6 6 0 776.45 803.09 65.31 o 7 6 0 0.08 11.24 43.22 o 8 6 0 172.94 100.01 51.02 o 9 6 0 1.51 0.18 47.89 o 1 7 0 1134.12 1153.74 61.57 o 2 7 0 182.85 127.62 45.40 o 3 7 0 128.28 193.33 51.75 o 4 7 0 634.75 651.32 58.44 o 5 7 0 3.16 56.45 56.02 o 6 7 0 3107.60 3053.95 107.42 o 7 7 0 23.84 16.08 63.32 o 8 7 0 189.44 107.46 57.89 o 9 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111.91 178.64 95.61 o 2 12 0 288.69 273.50 94.74 o 3 12 0 78.29 164.39 79.19 o 4 12 0 162.19 320.80 89.04 o 5 12 0 8.08 132.92 87.43 o 6 12 0 1.79 192.32 94.05 o 1 13 0 6.05 51.92 83.58 o 2 13 0 5.83 20.54 81.66 o 3 13 0 62.33 254.32 115.46 o 4 13 0 72.83 245.58 91.15 o 5 13 0 168.68 192.58 107.94 o 0 14 0 139.74 119.59 128.65 o 1 14 0 58.22 -40.57 88.09 o 2 14 0 164.71 95.18 132.07 o 3 14 0 6.51 43.99 101.24 o 2 0 1 22476.50 21979.94 184.69 o 3 0 1 3678.69 3308.58 46.68 o 4 0 1 599.06 561.72 29.39 o 5 0 1 1552.28 1625.25 50.85 o 6 0 1 214.18 202.03 34.04 o 7 0 1 708.77 829.60 84.73 o 8 0 1 10.78 2.36 27.73 o 9 0 1 31.66 -1.96 35.05 o 10 0 1 6.16 -4.06 36.51 o -10 1 1 0.12 0.34 32.41 o -9 1 1 0.94 -20.12 30.55 o -8 1 1 33.23 64.65 36.95 o -7 1 1 776.20 837.56 47.24 o -6 1 1 1420.28 1472.99 50.90 o -5 1 1 1340.85 1348.77 42.02 o -4 1 1 4025.38 4024.05 51.83 o -3 1 1 1519.52 1542.12 34.85 o -2 1 1 26108.57 25367.47 234.63 o -1 1 1 2768.28 2623.00 29.64 o 1 1 1 2782.40 2651.45 39.87 o 2 1 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509.11 544.70 39.93 o -4 3 1 2677.80 2810.23 70.86 o -3 3 1 3379.13 3489.39 62.04 o -2 3 1 1014.52 971.76 39.56 o -1 3 1 1546.56 1626.51 48.45 o 0 3 1 12989.04 11959.74 151.24 o 1 3 1 1559.30 1563.64 54.56 o 2 3 1 985.80 866.36 45.53 o 3 3 1 3403.21 3572.82 58.98 o 4 3 1 2638.95 2755.62 65.64 o 5 3 1 503.21 515.15 59.80 o 6 3 1 432.55 517.96 46.54 o 7 3 1 25.77 57.03 36.25 o 8 3 1 315.37 330.00 46.84 o 9 3 1 3.40 -7.53 44.41 o 10 3 1 42.92 2.30 59.43 o -10 4 1 25.82 89.79 69.56 o -9 4 1 36.78 3.11 46.29 o -8 4 1 244.49 235.08 50.11 o -7 4 1 7.76 -4.65 32.16 o -6 4 1 548.18 561.81 49.59 o -5 4 1 714.86 766.55 48.14 o -4 4 1 3160.86 3115.53 72.91 o -3 4 1 2.09 4.14 22.82 o -2 4 1 3513.41 3804.23 82.52 o -1 4 1 9014.47 8992.41 132.45 o 0 4 1 1785.87 1912.58 88.98 o 1 4 1 8996.02 9100.09 141.98 o 2 4 1 3557.93 3727.82 79.28 o 3 4 1 2.12 -24.76 24.76 o 4 4 1 3193.54 3135.09 72.63 o 5 4 1 712.62 785.90 48.61 o 6 4 1 539.73 539.38 47.81 o 7 4 1 7.81 33.31 32.17 o 8 4 1 248.17 169.16 50.83 o 9 4 1 37.88 46.26 45.99 o 10 4 1 26.97 180.12 106.53 o -10 5 1 5.83 101.49 72.39 o -9 5 1 52.04 20.94 45.97 o -8 5 1 56.86 51.45 46.65 o -7 5 1 107.93 47.83 46.78 o -6 5 1 297.80 258.15 61.07 o -5 5 1 99.08 136.88 35.32 o -4 5 1 371.01 320.24 45.53 o -3 5 1 2427.96 2304.75 60.94 o -2 5 1 1225.39 1336.16 56.32 o -1 5 1 559.26 789.74 50.54 o 0 5 1 7793.07 7858.65 126.20 o 1 5 1 543.99 647.34 53.53 o 2 5 1 1244.97 1261.65 60.26 o 3 5 1 2450.85 2497.29 75.93 o 4 5 1 384.94 424.05 39.34 o 5 5 1 98.01 113.10 37.45 o 6 5 1 284.92 285.93 52.98 o 7 5 1 102.68 101.52 40.34 o 8 5 1 57.07 79.59 44.32 o 9 5 1 49.85 64.19 45.66 o 10 5 1 5.50 165.62 70.90 o -9 6 1 13.22 66.28 53.47 o -8 6 1 267.45 179.83 63.85 o -7 6 1 116.99 48.08 52.15 o -6 6 1 590.42 710.97 67.36 o -5 6 1 28.78 55.89 36.31 o -4 6 1 79.77 147.29 43.02 o -3 6 1 229.64 248.12 52.62 o -2 6 1 1825.89 1766.18 68.87 o -1 6 1 2275.00 2585.24 74.52 o 0 6 1 301.34 448.66 49.41 o 1 6 1 2303.18 2428.68 71.27 o 2 6 1 1805.55 1817.60 63.96 o 3 6 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18.17 o -3 1 2 4605.91 4655.95 58.20 o -2 1 2 12275.17 11757.27 118.10 o -1 1 2 5487.75 5149.69 49.20 o 1 1 2 5366.80 5105.74 47.10 o 2 1 2 12253.08 11657.32 119.59 o 3 1 2 4627.76 4658.64 55.96 o 4 1 2 70.05 45.10 17.67 o 5 1 2 1127.64 1172.30 34.42 o 6 1 2 1773.93 1819.30 54.91 o 7 1 2 930.49 962.67 50.25 o 8 1 2 115.51 81.11 39.90 o 9 1 2 324.15 224.09 80.75 o 10 1 2 17.27 8.28 43.44 o -10 2 2 59.78 58.53 52.66 o -9 2 2 30.91 26.37 45.32 o -8 2 2 38.13 20.48 35.10 o -7 2 2 126.53 154.96 36.38 o -6 2 2 20.79 23.11 23.71 o -5 2 2 83.15 76.68 21.32 o -4 2 2 2114.27 2190.27 46.71 o -3 2 2 434.35 414.93 29.72 o -2 2 2 1103.66 1042.52 45.59 o -1 2 2 15823.50 15825.37 167.43 o 0 2 2 6343.28 6367.77 75.89 o 1 2 2 15674.61 15217.68 158.00 o 2 2 2 1055.31 1024.25 31.15 o 3 2 2 433.96 420.75 29.42 o 4 2 2 2123.77 2161.17 46.51 o 5 2 2 83.95 59.39 22.16 o 6 2 2 21.75 57.70 23.49 o 7 2 2 126.12 157.34 36.49 o 8 2 2 36.37 18.43 31.98 o 9 2 2 33.65 28.49 41.17 o 10 2 2 60.31 20.77 52.86 o -10 3 2 141.13 65.81 65.14 o -9 3 2 172.92 190.03 50.20 o -8 3 2 24.03 40.10 40.07 o -7 3 2 150.55 97.96 36.97 o -6 3 2 268.46 372.09 58.23 o -5 3 2 302.80 396.38 33.86 o -4 3 2 178.34 111.83 30.81 o -3 3 2 1410.97 1372.44 50.23 o -2 3 2 1759.08 1863.61 44.09 o -1 3 2 4753.06 4601.30 172.99 o 0 3 2 510.22 494.23 33.81 o 1 3 2 4837.27 4657.30 73.66 o 2 3 2 1778.65 1833.98 51.69 o 3 3 2 1397.36 1391.86 45.92 o 4 3 2 168.16 144.10 33.76 o 5 3 2 305.54 382.22 33.06 o 6 3 2 260.43 432.50 53.40 o 7 3 2 153.63 139.35 36.38 o 8 3 2 26.40 49.75 40.03 o 9 3 2 174.70 154.44 49.61 o 10 3 2 138.82 69.32 58.17 o -10 4 2 11.35 -46.06 56.96 o -9 4 2 36.78 13.56 47.31 o -8 4 2 270.32 282.02 48.73 o -7 4 2 833.13 866.51 51.66 o -6 4 2 788.40 735.43 102.47 o -5 4 2 59.06 45.09 33.59 o -4 4 2 27.92 15.00 28.06 o -3 4 2 227.65 205.79 32.61 o -2 4 2 2109.40 1878.65 99.55 o -1 4 2 8313.35 8336.28 127.45 o 0 4 2 7724.17 7789.09 112.92 o 1 4 2 8322.35 8285.34 126.49 o 2 4 2 2149.37 2007.48 58.45 o 3 4 2 220.86 212.05 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