#------------------------------------------------------------------------------ #$Date: 2016-06-11 05:09:59 +0300 (Sat, 11 Jun 2016) $ #$Revision: 183352 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/17/2241715.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241715 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.1926 _cell_length_b 36.3044 _cell_length_c 5.2930 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.7550 _cod_data_source_file wm5297Isup2.hkl _cod_data_source_block I _shelx_title ' Zn(NCS)2(isonicotinamide)2 in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 335.34 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 10 0 -6 1088.46 867.87 165.32 o 10 2 -6 143.47 104.63 102.46 o 12 2 -6 1453.18 1162.50 111.37 o 10 4 -6 828.61 806.57 142.51 o 12 4 -6 1.40 53.72 104.52 o 10 6 -6 80.79 27.16 135.53 o 12 6 -6 958.31 855.47 107.31 o 10 8 -6 547.75 878.68 138.16 o 12 8 -6 8.46 24.65 165.72 o 10 10 -6 34.41 -68.16 133.68 o 10 12 -6 668.24 517.98 138.82 o 10 14 -6 151.76 290.56 134.08 o 0 18 -6 1992.01 2016.15 163.08 o 2 18 -6 183.23 179.95 133.68 o 4 18 -6 572.14 532.35 137.24 o 6 18 -6 30.76 99.27 133.15 o 8 18 -6 428.00 471.97 111.40 o 2 20 -6 645.12 646.52 130.25 o 4 20 -6 142.51 292.28 110.74 o 6 20 -6 790.78 582.45 138.69 o 0 22 -6 25.23 -123.66 133.68 o 2 22 -6 145.50 254.54 159.06 o 4 22 -6 484.19 375.87 105.19 o 7 1 -5 121.19 82.42 104.06 o 9 1 -5 384.67 526.72 98.26 o 11 1 -5 2031.68 2174.41 76.38 o 13 1 -5 631.28 800.02 98.15 o 15 1 -5 522.78 514.32 95.27 o 17 1 -5 270.77 308.25 71.31 o 7 3 -5 827.51 1079.08 103.69 o 9 3 -5 1969.42 2130.43 128.08 o 11 3 -5 439.93 465.14 73.51 o 13 3 -5 348.66 450.61 69.55 o 15 3 -5 1128.71 1133.88 171.35 o 17 3 -5 137.07 184.80 73.55 o 7 5 -5 2172.42 2263.06 112.00 o 9 5 -5 350.39 317.07 103.72 o 11 5 -5 1540.14 1675.71 87.50 o 13 5 -5 784.24 816.89 80.61 o 15 5 -5 399.19 482.12 73.50 o 17 5 -5 230.73 210.78 69.86 o 7 7 -5 1660.19 1771.86 141.33 o 9 7 -5 2511.21 2417.70 111.88 o 11 7 -5 324.01 543.78 92.16 o 13 7 -5 754.97 780.60 73.39 o 15 7 -5 363.77 247.40 72.16 o 17 7 -5 503.90 375.16 78.32 o 7 9 -5 2112.58 2434.33 146.47 o 9 9 -5 1154.35 1061.89 109.75 o 11 9 -5 1843.58 1977.00 91.65 o 13 9 -5 994.54 1107.94 73.08 o 15 9 -5 231.23 357.16 79.32 o 1 11 -5 1504.08 1617.35 138.95 o 3 11 -5 3436.07 3526.19 143.30 o 5 11 -5 16.65 -130.78 130.78 o 7 11 -5 313.76 387.59 83.44 o 9 11 -5 882.56 888.26 76.70 o 11 11 -5 520.65 510.41 109.15 o 13 11 -5 637.99 678.16 90.62 o 15 11 -5 172.54 225.31 71.26 o 1 13 -5 395.61 416.85 93.49 o 3 13 -5 2160.70 1973.68 100.56 o 5 13 -5 611.20 677.37 131.44 o 7 13 -5 1565.19 1512.24 159.45 o 9 13 -5 1065.49 1107.31 86.00 o 11 13 -5 450.46 526.86 69.13 o 13 13 -5 1641.27 1547.63 92.85 o 15 13 -5 49.96 11.32 76.23 o 1 15 -5 1524.49 1719.64 104.73 o 3 15 -5 2488.04 2505.52 103.48 o 5 15 -5 284.42 273.18 89.15 o 7 15 -5 2174.02 2102.28 87.83 o 9 15 -5 1351.84 1260.54 94.86 o 11 15 -5 557.50 585.55 71.22 o 13 15 -5 132.99 310.98 73.84 o 15 15 -5 431.69 398.40 91.28 o 1 17 -5 2259.70 2353.41 107.42 o 3 17 -5 219.78 318.08 86.92 o 5 17 -5 2205.71 2158.86 106.23 o 7 17 -5 664.16 639.12 81.88 o 9 17 -5 593.53 624.22 84.48 o 11 17 -5 1305.72 1265.44 185.67 o 13 17 -5 291.36 289.00 78.82 o 15 17 -5 472.10 408.82 94.67 o 1 19 -5 631.08 765.66 106.98 o 3 19 -5 1293.06 1391.21 81.84 o 5 19 -5 1247.96 1190.58 88.00 o 7 19 -5 683.63 672.39 68.50 o 9 19 -5 944.39 1019.96 144.82 o 11 19 -5 685.96 660.05 76.62 o 13 19 -5 254.66 217.37 71.44 o 1 21 -5 1044.17 1023.56 68.91 o 3 21 -5 614.29 771.28 146.43 o 5 21 -5 1226.66 1295.91 115.71 o 7 21 -5 228.96 259.77 67.12 o 9 21 -5 418.37 419.26 72.88 o 11 21 -5 140.80 180.52 67.25 o 13 21 -5 144.57 138.65 96.23 o 1 23 -5 288.74 222.03 66.78 o 3 23 -5 200.13 244.14 67.58 o 5 23 -5 1042.95 1093.10 85.44 o 7 23 -5 501.72 526.22 65.65 o 9 23 -5 382.99 308.14 75.40 o 11 23 -5 413.37 348.38 99.66 o 1 25 -5 2072.88 1965.76 69.18 o 3 25 -5 168.03 136.91 64.28 o 5 25 -5 911.95 889.35 69.66 o 7 25 -5 305.94 341.02 82.86 o 9 25 -5 353.89 273.29 65.86 o 11 25 -5 113.07 100.73 71.14 o 1 27 -5 378.06 356.73 64.91 o 3 27 -5 1173.01 1150.73 67.16 o 5 27 -5 1262.86 1082.76 73.84 o 7 27 -5 354.20 312.64 88.33 o 9 27 -5 356.42 210.82 69.27 o 1 29 -5 157.32 127.36 75.62 o 3 29 -5 1208.10 1163.07 72.71 o 5 29 -5 344.84 278.13 70.84 o 7 29 -5 1023.95 720.70 68.49 o 1 31 -5 553.43 528.04 82.63 o 3 31 -5 324.18 319.17 69.49 o 5 31 -5 303.82 387.30 79.72 o 1 33 -5 330.87 294.36 72.28 o 4 0 -4 1476.17 1403.25 165.06 o 8 0 -4 13564.31 14479.15 567.22 o 12 0 -4 2275.90 2580.59 108.95 o 16 0 -4 1214.85 1498.93 102.49 o 20 0 -4 90.08 73.81 134.14 o 4 2 -4 513.28 600.15 133.30 o 6 2 -4 7096.95 6936.71 136.06 o 8 2 -4 291.79 303.68 80.92 o 10 2 -4 2179.58 2364.47 87.91 o 12 2 -4 1792.85 2081.41 76.74 o 14 2 -4 685.94 810.37 67.77 o 16 2 -4 158.62 161.54 66.86 o 18 2 -4 1044.64 1121.84 109.61 o 20 2 -4 271.61 320.42 68.88 o 4 4 -4 8210.11 8062.01 196.24 o 6 4 -4 3106.14 3378.01 109.91 o 8 4 -4 7391.16 7656.51 264.14 o 10 4 -4 817.57 1146.37 140.01 o 12 4 -4 1196.12 1399.40 82.87 o 14 4 -4 580.17 836.27 74.33 o 16 4 -4 1192.22 1219.76 83.80 o 18 4 -4 20.48 137.78 66.53 o 20 4 -4 524.63 422.54 72.32 o 2 6 -4 6783.71 6528.21 163.48 o 4 6 -4 1140.62 1147.75 111.14 o 6 6 -4 6294.24 6364.26 94.49 o 8 6 -4 214.24 318.85 64.48 o 10 6 -4 4598.73 4921.50 123.31 o 12 6 -4 684.26 755.85 72.69 o 14 6 -4 2163.73 2313.33 104.85 o 16 6 -4 737.15 903.74 72.07 o 18 6 -4 606.38 656.04 69.31 o 20 6 -4 277.38 241.20 66.44 o 0 8 -4 17495.69 17364.26 203.82 o 2 8 -4 1574.01 1618.61 116.60 o 4 8 -4 8628.24 8521.35 149.37 o 6 8 -4 4347.44 4480.99 92.29 o 8 8 -4 2600.11 2709.46 72.73 o 10 8 -4 1058.70 1050.73 68.62 o 12 8 -4 3832.17 3858.00 164.36 o 14 8 -4 15.02 139.60 73.39 o 16 8 -4 1755.30 1838.66 65.94 o 18 8 -4 624.40 736.06 71.92 o 20 8 -4 1099.67 961.44 81.84 o 2 10 -4 4169.77 4183.83 142.78 o 4 10 -4 881.02 1000.02 95.38 o 6 10 -4 10184.86 10214.23 152.00 o 8 10 -4 511.04 444.24 77.53 o 10 10 -4 10360.81 11178.02 261.69 o 12 10 -4 305.95 401.61 66.57 o 14 10 -4 3663.46 3924.00 73.68 o 16 10 -4 1321.86 1257.17 72.86 o 18 10 -4 969.69 822.35 74.23 o 20 10 -4 0.98 140.27 144.62 o 0 12 -4 2563.96 2635.52 163.48 o 2 12 -4 1100.67 1170.08 91.16 o 4 12 -4 13952.18 14075.55 96.70 o 6 12 -4 152.59 143.96 66.35 o 8 12 -4 3179.12 3449.31 79.49 o 10 12 -4 174.92 377.01 69.97 o 12 12 -4 1974.33 2015.77 66.44 o 14 12 -4 154.21 224.80 60.99 o 16 12 -4 2283.52 2158.87 63.04 o 18 12 -4 249.24 293.88 68.16 o 2 14 -4 1744.99 1789.41 82.34 o 4 14 -4 840.97 866.72 81.82 o 6 14 -4 4806.47 4736.67 114.43 o 8 14 -4 317.26 332.70 62.73 o 10 14 -4 4185.16 4084.43 78.60 o 12 14 -4 399.02 430.81 69.94 o 14 14 -4 2479.10 2788.30 105.11 o 16 14 -4 545.04 557.06 68.67 o 18 14 -4 371.76 301.70 60.52 o 0 16 -4 5310.75 5278.67 144.56 o 2 16 -4 930.50 1046.62 74.20 o 4 16 -4 616.34 607.94 59.28 o 6 16 -4 1750.60 1901.24 69.12 o 8 16 -4 1841.01 2091.77 69.24 o 10 16 -4 279.43 321.24 62.29 o 12 16 -4 3321.19 3441.26 89.76 o 14 16 -4 439.29 599.95 60.22 o 16 16 -4 455.92 463.77 58.46 o 18 16 -4 308.15 325.75 97.09 o 2 18 -4 5470.84 5826.38 76.31 o 4 18 -4 3082.49 3075.78 75.89 o 6 18 -4 224.51 276.97 66.55 o 8 18 -4 162.17 202.45 64.34 o 10 18 -4 1528.93 1477.91 67.51 o 12 18 -4 296.31 376.59 52.91 o 14 18 -4 617.91 635.69 59.19 o 16 18 -4 90.70 121.35 59.29 o 18 18 -4 750.55 617.95 62.32 o 0 20 -4 335.75 451.29 102.32 o 2 20 -4 157.05 219.05 72.65 o 4 20 -4 5459.05 5606.56 103.43 o 6 20 -4 2007.55 2034.32 60.00 o 8 20 -4 3478.20 3605.15 72.24 o 10 20 -4 12.62 111.43 63.48 o 12 20 -4 2701.03 2795.31 65.96 o 14 20 -4 774.67 866.24 58.10 o 16 20 -4 259.87 207.54 58.40 o 2 22 -4 8824.79 9090.75 82.64 o 4 22 -4 375.17 643.61 70.49 o 6 22 -4 4347.26 4506.10 65.91 o 8 22 -4 92.39 188.02 62.13 o 10 22 -4 1133.23 1241.53 74.98 o 12 22 -4 81.66 102.44 60.10 o 14 22 -4 380.75 260.06 60.62 o 16 22 -4 357.53 307.23 55.62 o 0 24 -4 7597.94 7898.84 117.54 o 2 24 -4 96.49 215.33 65.87 o 4 24 -4 3780.22 3832.47 116.41 o 6 24 -4 153.04 347.23 60.42 o 8 24 -4 2381.90 2358.39 70.78 o 10 24 -4 67.31 1.72 59.65 o 12 24 -4 2522.39 2284.35 69.05 o 14 24 -4 79.51 160.55 65.59 o 16 24 -4 349.99 269.76 69.80 o 2 26 -4 5395.08 5284.17 77.99 o 4 26 -4 399.95 384.78 70.40 o 6 26 -4 946.11 1108.10 62.98 o 8 26 -4 30.88 113.10 53.35 o 10 26 -4 1770.09 1705.45 61.49 o 12 26 -4 249.34 134.82 60.09 o 14 26 -4 455.97 267.83 89.08 o 0 28 -4 4347.00 4446.41 112.25 o 2 28 -4 333.52 342.78 68.64 o 4 28 -4 1341.01 1463.08 68.08 o 6 28 -4 192.64 322.28 59.85 o 8 28 -4 718.81 640.79 62.39 o 10 28 -4 94.90 59.37 55.35 o 12 28 -4 423.59 389.28 65.42 o 14 28 -4 224.26 184.65 62.15 o 2 30 -4 562.79 633.93 83.61 o 4 30 -4 168.56 328.50 66.19 o 6 30 -4 1867.40 1864.74 57.08 o 8 30 -4 24.03 90.91 55.91 o 10 30 -4 533.58 611.29 77.15 o 12 30 -4 22.57 57.03 60.35 o 0 32 -4 3225.65 3173.24 97.33 o 2 32 -4 422.06 471.09 69.73 o 4 32 -4 674.30 634.36 70.47 o 6 32 -4 155.90 93.03 62.70 o 8 32 -4 545.60 596.31 63.90 o 10 32 -4 24.42 119.87 54.64 o 2 34 -4 780.51 779.08 68.07 o 4 34 -4 149.72 265.64 66.71 o 6 34 -4 819.05 775.38 73.12 o 8 34 -4 221.56 199.04 61.81 o 10 34 -4 990.10 697.54 96.53 o 0 36 -4 700.02 725.30 103.37 o 2 36 -4 302.76 324.51 72.32 o 4 36 -4 720.64 651.80 150.75 o 6 36 -4 16.78 70.33 70.92 o 8 36 -4 796.98 558.08 87.12 o 2 38 -4 432.03 416.78 68.23 o 4 38 -4 15.80 103.14 71.18 o 3 1 -3 16588.04 16481.52 461.36 o 5 1 -3 7550.33 7560.14 95.92 o 7 1 -3 8861.37 9401.61 158.11 o 9 1 -3 5985.84 6114.14 133.94 o 11 1 -3 3213.86 3201.91 84.04 o 13 1 -3 3132.33 3267.44 116.05 o 15 1 -3 3722.28 3950.57 129.11 o 17 1 -3 1988.65 2005.66 135.58 o 19 1 -3 1947.86 2047.18 101.58 o 21 1 -3 767.27 657.25 115.68 o 1 3 -3 5003.76 4762.02 181.80 o 3 3 -3 1093.76 1062.07 103.87 o 5 3 -3 28339.93 28920.00 339.59 o 7 3 -3 14777.04 14748.79 321.61 o 9 3 -3 14827.50 15334.38 380.75 o 11 3 -3 7826.30 8486.29 224.94 o 13 3 -3 2738.26 2974.17 82.12 o 15 3 -3 902.40 997.60 73.73 o 17 3 -3 1862.64 2111.23 119.41 o 19 3 -3 1157.02 1198.17 61.35 o 21 3 -3 211.98 241.79 81.82 o 1 5 -3 9904.96 9432.75 141.13 o 3 5 -3 19313.11 19454.94 186.71 o 5 5 -3 12534.72 12526.11 144.87 o 7 5 -3 11635.77 12028.78 207.21 o 9 5 -3 896.60 992.16 75.90 o 11 5 -3 1814.12 1952.95 77.25 o 13 5 -3 197.88 181.41 76.25 o 15 5 -3 903.50 1044.88 72.40 o 17 5 -3 4829.25 4905.07 198.64 o 19 5 -3 1549.14 1658.74 91.05 o 21 5 -3 939.80 954.29 67.08 o 1 7 -3 5320.83 5258.33 100.30 o 3 7 -3 6094.76 6031.33 85.27 o 5 7 -3 1822.28 1727.75 68.51 o 7 7 -3 12689.70 12288.79 86.19 o 9 7 -3 14558.38 14671.05 210.87 o 11 7 -3 1533.51 1471.86 93.94 o 13 7 -3 4566.27 5125.46 117.42 o 15 7 -3 4389.71 4715.09 110.48 o 17 7 -3 302.53 357.68 71.85 o 19 7 -3 86.07 147.05 65.76 o 21 7 -3 6.61 112.43 69.18 o 1 9 -3 5369.45 5043.95 93.22 o 3 9 -3 16998.99 16322.55 87.88 o 5 9 -3 1317.50 1246.29 76.35 o 7 9 -3 5709.93 5871.80 77.39 o 9 9 -3 361.68 391.04 70.57 o 11 9 -3 234.36 340.30 68.88 o 13 9 -3 8006.11 8492.23 220.05 o 15 9 -3 233.44 251.28 56.81 o 17 9 -3 1401.74 1484.34 69.03 o 19 9 -3 594.31 743.12 70.99 o 21 9 -3 575.19 626.05 67.31 o 1 11 -3 3173.57 3124.48 87.68 o 3 11 -3 3061.22 3013.77 73.69 o 5 11 -3 6751.14 6501.35 131.01 o 7 11 -3 8618.74 8782.01 81.93 o 9 11 -3 3565.42 3501.67 74.46 o 11 11 -3 2551.15 2770.66 75.33 o 13 11 -3 2490.36 2716.16 66.61 o 15 11 -3 459.24 456.51 59.90 o 17 11 -3 1558.58 1737.27 72.90 o 19 11 -3 550.75 587.18 62.89 o 21 11 -3 110.26 69.75 65.73 o 1 13 -3 577.22 642.12 84.84 o 3 13 -3 6531.39 6524.59 81.86 o 5 13 -3 15012.33 15186.57 157.35 o 7 13 -3 5797.02 5946.66 64.64 o 9 13 -3 3700.75 3889.01 70.57 o 11 13 -3 4138.12 4226.15 68.46 o 13 13 -3 1583.27 1664.29 60.85 o 15 13 -3 958.08 1142.48 59.19 o 17 13 -3 1171.81 1258.62 56.32 o 19 13 -3 328.55 358.87 93.09 o 21 13 -3 797.48 726.32 71.97 o 1 15 -3 22758.50 22944.43 171.62 o 3 15 -3 13533.69 13612.22 132.67 o 5 15 -3 9125.32 9363.86 119.59 o 7 15 -3 2286.41 2532.45 64.82 o 9 15 -3 838.70 914.24 61.31 o 11 15 -3 2228.53 2314.15 63.26 o 13 15 -3 2800.84 2693.40 72.06 o 15 15 -3 1760.72 1869.76 58.38 o 17 15 -3 1697.28 1797.37 59.88 o 19 15 -3 776.90 477.52 63.84 o 21 15 -3 661.07 638.10 62.72 o 1 17 -3 8155.42 8466.72 103.23 o 3 17 -3 4286.87 4368.31 80.90 o 5 17 -3 8504.68 8813.48 162.77 o 7 17 -3 3969.92 3890.71 68.86 o 9 17 -3 10116.44 9865.94 186.56 o 11 17 -3 4884.66 5415.89 67.73 o 13 17 -3 5778.99 5999.03 82.93 o 15 17 -3 2833.03 2868.44 70.27 o 17 17 -3 35.99 43.87 58.84 o 19 17 -3 395.90 415.83 95.50 o 1 19 -3 6397.16 6814.07 87.86 o 3 19 -3 16232.91 16227.75 136.16 o 5 19 -3 5317.09 5199.65 74.13 o 7 19 -3 1154.75 1342.51 60.96 o 9 19 -3 1388.98 1511.32 51.06 o 11 19 -3 2911.57 3069.64 59.49 o 13 19 -3 438.17 518.70 54.97 o 15 19 -3 1034.35 1014.36 54.15 o 17 19 -3 749.36 737.60 56.69 o 19 19 -3 674.42 626.66 88.35 o 1 21 -3 6934.34 7103.61 93.55 o 3 21 -3 1356.49 1457.19 69.87 o 5 21 -3 4116.52 4323.49 70.92 o 7 21 -3 1791.92 1816.68 64.14 o 9 21 -3 5100.96 5405.78 65.20 o 11 21 -3 2320.00 2201.01 54.72 o 13 21 -3 350.15 395.00 55.87 o 15 21 -3 801.37 902.28 53.09 o 17 21 -3 564.85 422.98 68.15 o 19 21 -3 361.45 304.78 57.59 o 1 23 -3 6519.36 6758.37 95.92 o 3 23 -3 641.88 812.91 69.53 o 5 23 -3 525.91 652.38 65.47 o 7 23 -3 2590.35 2733.62 57.27 o 9 23 -3 594.98 631.31 53.97 o 11 23 -3 1219.26 1192.74 59.83 o 13 23 -3 1086.04 1106.07 55.79 o 15 23 -3 813.89 921.20 55.56 o 17 23 -3 195.60 140.28 50.89 o 19 23 -3 35.46 257.95 63.02 o 1 25 -3 3334.51 3581.58 81.72 o 3 25 -3 5356.08 5564.92 67.77 o 5 25 -3 845.01 773.52 61.61 o 7 25 -3 326.80 360.65 55.48 o 9 25 -3 1629.35 1593.51 60.59 o 11 25 -3 456.24 568.30 67.74 o 13 25 -3 954.16 1090.02 53.01 o 15 25 -3 871.82 838.99 51.38 o 17 25 -3 192.51 172.00 51.39 o 1 27 -3 538.61 637.26 69.63 o 3 27 -3 1912.11 2072.06 72.38 o 5 27 -3 2441.26 2339.39 62.87 o 7 27 -3 1949.77 2022.27 61.72 o 9 27 -3 2489.31 2667.54 93.28 o 11 27 -3 2164.06 2198.15 59.66 o 13 27 -3 2217.91 2071.70 57.54 o 15 27 -3 215.32 209.07 52.91 o 17 27 -3 129.95 43.11 49.20 o 1 29 -3 4368.94 4309.51 73.63 o 3 29 -3 3420.09 3892.74 92.38 o 5 29 -3 1100.41 1067.50 59.01 o 7 29 -3 1994.45 2010.62 58.71 o 9 29 -3 214.39 323.86 49.05 o 11 29 -3 1259.25 1235.50 75.49 o 13 29 -3 430.78 370.53 51.93 o 15 29 -3 58.92 180.27 61.35 o 1 31 -3 1583.37 1760.96 74.38 o 3 31 -3 2062.36 2175.97 67.52 o 5 31 -3 1250.39 1264.61 58.16 o 7 31 -3 1105.48 1216.20 57.17 o 9 31 -3 1230.43 1188.54 53.21 o 11 31 -3 1193.99 1061.57 52.10 o 13 31 -3 1400.87 1192.03 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9146.14 8598.49 74.46 o 8 8 2 3720.12 4055.01 58.40 o 10 8 2 7188.58 6627.43 90.37 o 12 8 2 4131.14 3977.14 57.30 o 14 8 2 9044.61 8953.88 120.47 o 16 8 2 1149.13 1126.62 53.37 o 18 8 2 2491.28 2586.95 50.01 o 20 8 2 47.42 45.60 49.86 o 22 8 2 1083.31 905.32 47.60 o 0 10 2 50642.45 50292.98 234.98 o 2 10 2 12033.02 11850.23 101.07 o 4 10 2 31795.99 31091.71 156.08 o 6 10 2 2000.83 1933.02 63.37 o 8 10 2 31263.68 29813.01 103.38 o 10 10 2 846.96 802.57 55.55 o 12 10 2 15631.31 15601.09 103.99 o 14 10 2 187.06 213.26 52.33 o 16 10 2 1020.70 1226.93 49.80 o 18 10 2 95.16 41.91 48.19 o 20 10 2 1366.50 1517.67 48.40 o 22 10 2 208.42 208.90 47.26 o 2 12 2 59222.10 58060.63 357.62 o 4 12 2 591.38 829.02 69.24 o 6 12 2 31104.20 29756.54 155.10 o 8 12 2 2775.25 2697.83 66.56 o 10 12 2 10315.26 10078.13 74.41 o 12 12 2 133.27 187.48 54.67 o 14 12 2 141.88 196.57 51.54 o 16 12 2 489.27 581.02 48.68 o 18 12 2 5335.91 5218.43 85.34 o 20 12 2 225.96 266.04 44.78 o 22 12 2 1283.13 1121.81 48.03 o 0 14 2 65753.65 63809.80 670.33 o 2 14 2 29331.69 28983.62 211.22 o 4 14 2 4453.13 4279.60 68.19 o 6 14 2 3629.02 3392.22 61.79 o 8 14 2 28482.38 27690.17 200.16 o 10 14 2 2392.35 2294.30 64.31 o 12 14 2 2236.02 2135.58 61.28 o 14 14 2 1161.65 1151.32 52.80 o 16 14 2 3479.72 3444.96 50.64 o 18 14 2 35.60 46.92 44.52 o 20 14 2 472.91 509.09 54.86 o 22 14 2 14.67 33.34 49.98 o 2 16 2 26644.85 25044.26 107.44 o 4 16 2 7510.25 7376.35 76.85 o 6 16 2 4871.03 4680.49 60.65 o 8 16 2 5058.81 4943.81 65.82 o 10 16 2 432.17 560.64 56.38 o 12 16 2 3015.60 3047.26 55.55 o 14 16 2 5397.43 5635.50 107.03 o 16 16 2 1037.63 1185.03 61.69 o 18 16 2 426.35 390.85 47.31 o 20 16 2 0.33 51.51 43.08 o 22 16 2 1253.22 1012.02 71.42 o 0 18 2 10963.97 10157.08 101.47 o 2 18 2 1740.48 1776.65 59.59 o 4 18 2 5175.89 4928.61 61.92 o 6 18 2 3544.72 3609.53 62.30 o 8 18 2 12024.79 11721.97 87.85 o 10 18 2 703.97 693.16 59.53 o 12 18 2 3376.58 3259.41 57.73 o 14 18 2 1941.25 1962.51 55.21 o 16 18 2 1697.13 1767.64 69.87 o 18 18 2 577.06 641.62 43.88 o 20 18 2 392.12 415.39 42.27 o 22 18 2 300.20 222.35 47.45 o 2 20 2 7746.18 7225.11 87.73 o 4 20 2 986.03 981.16 64.15 o 6 20 2 13395.34 12760.29 94.79 o 8 20 2 441.07 420.86 57.47 o 10 20 2 9601.96 9618.35 89.75 o 12 20 2 154.12 209.88 49.88 o 14 20 2 2214.11 2500.32 73.96 o 16 20 2 304.83 431.77 54.43 o 18 20 2 1627.03 1622.38 49.90 o 20 20 2 557.31 620.35 59.82 o 0 22 2 28865.39 27818.48 248.86 o 2 22 2 2684.86 2457.89 62.14 o 4 22 2 13980.46 13437.50 96.59 o 6 22 2 979.48 1085.79 57.82 o 8 22 2 5021.55 5064.73 76.63 o 10 22 2 199.81 248.23 54.89 o 12 22 2 6177.20 6161.49 89.95 o 14 22 2 73.97 194.71 62.17 o 16 22 2 3315.30 3313.98 83.85 o 18 22 2 389.22 343.82 42.91 o 20 22 2 857.10 817.03 74.08 o 2 24 2 8361.67 8293.82 68.69 o 4 24 2 3077.29 2898.38 61.50 o 6 24 2 6825.34 6903.50 60.78 o 8 24 2 622.64 616.36 58.04 o 10 24 2 9435.89 9287.50 72.91 o 12 24 2 107.93 215.48 48.99 o 14 24 2 10096.63 10051.50 172.63 o 16 24 2 47.03 73.68 46.60 o 18 24 2 356.24 416.43 44.11 o 20 24 2 143.74 199.23 47.34 o 0 26 2 5084.87 5066.53 84.38 o 2 26 2 2871.31 2703.09 58.74 o 4 26 2 9100.24 8819.41 83.09 o 6 26 2 2644.76 2720.95 55.57 o 8 26 2 2285.61 2264.13 54.05 o 10 26 2 358.67 532.53 48.52 o 12 26 2 4289.88 4507.13 103.32 o 14 26 2 766.11 767.19 47.41 o 16 26 2 1838.87 1652.06 80.55 o 18 26 2 60.46 83.16 46.38 o 2 28 2 929.42 1047.70 62.99 o 4 28 2 1565.81 1604.36 53.68 o 6 28 2 4465.91 4775.53 60.17 o 8 28 2 822.97 816.92 59.99 o 10 28 2 4106.46 4188.83 66.16 o 12 28 2 1007.05 1017.72 46.69 o 14 28 2 1230.75 1244.22 65.29 o 16 28 2 161.33 234.06 47.33 o 18 28 2 989.52 779.24 48.12 o 0 30 2 5980.69 6000.85 145.63 o 2 30 2 1632.16 1766.25 64.55 o 4 30 2 1792.99 1875.18 50.82 o 6 30 2 872.82 1007.61 46.69 o 8 30 2 2474.50 2528.61 71.77 o 10 30 2 363.82 406.46 48.32 o 12 30 2 1041.88 1137.14 49.55 o 14 30 2 18.36 54.24 45.97 o 16 30 2 1343.53 1242.68 59.13 o 18 30 2 10.26 78.97 46.86 o 2 32 2 6374.11 6371.13 75.89 o 4 32 2 326.42 503.54 52.45 o 6 32 2 1993.47 1968.43 99.03 o 8 32 2 342.63 424.34 45.90 o 10 32 2 2222.40 2235.01 97.34 o 12 32 2 427.27 390.23 47.29 o 14 32 2 1242.30 1175.39 51.32 o 16 32 2 125.75 109.04 49.01 o 0 34 2 3046.21 3115.83 81.23 o 2 34 2 68.43 38.64 47.68 o 4 34 2 4578.44 4457.39 85.73 o 6 34 2 720.19 800.71 52.98 o 8 34 2 1402.19 1476.73 50.87 o 10 34 2 7.67 91.93 48.97 o 12 34 2 3073.28 2840.22 50.04 o 14 34 2 13.57 45.99 42.60 o 16 34 2 32.66 119.66 45.93 o 2 36 2 4716.04 4673.97 61.35 o 4 36 2 184.19 91.93 48.93 o 6 36 2 1361.13 1251.33 48.63 o 8 36 2 113.46 133.38 43.65 o 10 36 2 1212.04 1283.18 56.68 o 12 36 2 22.95 156.36 54.16 o 14 36 2 44.17 97.20 50.77 o 0 38 2 1685.71 1767.13 77.77 o 2 38 2 210.84 285.49 44.50 o 4 38 2 1895.86 1832.70 52.94 o 6 38 2 61.46 234.31 59.49 o 8 38 2 1366.95 1361.23 49.33 o 10 38 2 95.50 152.21 54.27 o 12 38 2 474.53 428.42 53.01 o 2 40 2 1835.63 1851.76 64.90 o 4 40 2 380.73 506.90 76.53 o 6 40 2 864.63 814.43 48.50 o 8 40 2 60.21 85.57 43.30 o 10 40 2 364.68 513.49 66.69 o 0 42 2 1348.23 1297.14 107.28 o 2 42 2 29.32 78.19 44.50 o 4 42 2 1140.20 1022.07 61.86 o 6 42 2 6.88 -47.44 47.44 o 8 42 2 487.75 393.75 51.37 o 2 44 2 848.75 814.40 46.32 o 4 44 2 56.75 96.53 44.25 o 6 44 2 851.08 674.19 50.78 o 1 1 3 11487.95 10494.98 69.80 o 3 1 3 15715.11 15254.89 119.06 o 5 1 3 6314.55 6014.09 58.99 o 7 1 3 10245.71 10393.36 61.97 o 9 1 3 6396.26 6218.68 64.45 o 11 1 3 2706.14 2617.87 60.90 o 13 1 3 3447.19 3409.75 56.48 o 15 1 3 3593.44 3675.72 49.83 o 17 1 3 2458.97 2450.80 57.81 o 19 1 3 1851.59 1732.47 48.82 o 21 1 3 714.74 687.83 46.05 o 1 3 3 3944.15 3767.89 52.27 o 3 3 3 1923.83 1895.67 48.35 o 5 3 3 27767.90 27472.49 83.69 o 7 3 3 15651.75 15030.00 72.70 o 9 3 3 14084.33 13732.23 112.15 o 11 3 3 8025.67 8182.46 94.08 o 13 3 3 3298.58 3367.14 58.89 o 15 3 3 1330.42 1384.62 65.11 o 17 3 3 1751.44 1795.03 53.00 o 19 3 3 1123.64 1064.78 43.92 o 21 3 3 155.20 209.38 44.00 o 1 5 3 10579.39 10312.82 58.30 o 3 5 3 20346.86 20283.12 137.73 o 5 5 3 12247.16 11904.06 87.85 o 7 5 3 10690.72 10577.02 64.15 o 9 5 3 1184.71 1124.46 60.92 o 11 5 3 1625.91 1525.68 58.76 o 13 5 3 362.94 471.10 50.68 o 15 5 3 1024.99 1072.71 51.27 o 17 5 3 4968.39 4616.15 114.56 o 19 5 3 1364.11 1356.34 43.22 o 21 5 3 955.78 1006.73 43.73 o 1 7 3 5976.37 5959.13 62.71 o 3 7 3 4671.98 4580.82 57.46 o 5 7 3 2143.82 1844.14 60.68 o 7 7 3 12991.81 12531.87 109.68 o 9 7 3 14332.97 14010.30 108.74 o 11 7 3 2085.02 2038.75 59.94 o 13 7 3 4835.19 4948.74 56.95 o 15 7 3 4107.05 4261.98 60.04 o 17 7 3 138.16 217.62 49.20 o 19 7 3 23.86 119.93 43.58 o 21 7 3 25.41 95.81 44.36 o 1 9 3 5462.90 5192.47 61.93 o 3 9 3 16958.08 16066.98 96.14 o 5 9 3 1575.24 1471.31 65.31 o 7 9 3 5087.73 5032.77 65.05 o 9 9 3 671.89 802.04 55.25 o 11 9 3 458.86 352.97 52.38 o 13 9 3 7312.21 7562.76 74.84 o 15 9 3 285.44 382.01 49.16 o 17 9 3 1139.17 1159.81 94.50 o 19 9 3 837.59 852.50 49.07 o 21 9 3 521.36 533.68 44.36 o 1 11 3 4032.37 3941.17 63.47 o 3 11 3 2728.61 2588.41 60.86 o 5 11 3 7670.12 7338.79 63.82 o 7 11 3 7647.24 7592.69 89.33 o 9 11 3 3291.90 3176.22 60.56 o 11 11 3 2089.61 2117.51 56.04 o 13 11 3 1808.61 1651.94 58.38 o 15 11 3 542.65 538.49 48.79 o 17 11 3 1665.17 1695.78 51.36 o 19 11 3 658.49 693.92 53.96 o 21 11 3 190.63 211.50 47.16 o 1 13 3 335.59 442.30 70.33 o 3 13 3 6728.89 6701.86 66.10 o 5 13 3 15700.73 15525.44 103.71 o 7 13 3 5220.13 5173.31 64.05 o 9 13 3 4068.63 3949.57 64.20 o 11 13 3 4032.34 3933.79 54.98 o 13 13 3 1261.25 1279.96 50.42 o 15 13 3 1123.41 1198.47 53.00 o 17 13 3 913.68 1011.10 47.83 o 19 13 3 290.46 252.64 49.36 o 21 13 3 876.08 656.38 65.56 o 1 15 3 24007.90 23287.09 125.18 o 3 15 3 13070.66 12477.19 134.76 o 5 15 3 9761.87 9925.61 99.89 o 7 15 3 2110.15 2329.98 61.87 o 9 15 3 505.20 548.65 55.62 o 11 15 3 2557.98 2518.34 52.11 o 13 15 3 2601.57 2465.55 51.07 o 15 15 3 1519.63 1522.96 47.78 o 17 15 3 1574.27 1600.20 59.93 o 19 15 3 854.17 748.35 50.47 o 21 15 3 623.16 466.04 48.26 o 1 17 3 8867.26 8820.88 81.00 o 3 17 3 4561.66 4547.99 76.75 o 5 17 3 7807.35 7827.78 78.20 o 7 17 3 3981.95 3797.95 63.14 o 9 17 3 10545.35 9990.04 64.97 o 11 17 3 4990.07 5250.22 59.00 o 13 17 3 5841.05 5696.49 70.97 o 15 17 3 2834.43 2828.25 51.90 o 17 17 3 11.68 40.28 47.25 o 19 17 3 381.86 394.78 45.67 o 21 17 3 0.04 -3.82 92.60 o 1 19 3 5928.79 6089.74 87.44 o 3 19 3 17106.76 16296.11 74.50 o 5 19 3 5605.68 5306.94 84.32 o 7 19 3 799.42 1000.92 52.34 o 9 19 3 1258.66 1284.12 58.72 o 11 19 3 3029.56 3198.85 53.30 o 13 19 3 652.30 702.93 44.28 o 15 19 3 909.54 964.96 46.72 o 17 19 3 802.85 822.50 45.46 o 19 19 3 718.68 577.69 46.39 o 1 21 3 6165.17 6097.30 59.60 o 3 21 3 1984.54 1836.14 59.40 o 5 21 3 4144.27 4185.86 78.92 o 7 21 3 2120.26 2126.51 59.23 o 9 21 3 4758.64 4687.36 56.23 o 11 21 3 2087.38 2035.14 51.62 o 13 21 3 518.20 490.30 47.36 o 15 21 3 765.91 841.33 45.90 o 17 21 3 613.04 613.22 45.64 o 19 21 3 371.19 281.45 46.82 o 1 23 3 5684.48 5612.24 55.25 o 3 23 3 318.46 560.86 59.21 o 5 23 3 354.07 393.53 55.87 o 7 23 3 3152.03 3342.82 53.77 o 9 23 3 474.93 572.67 46.80 o 11 23 3 1399.06 1276.92 52.08 o 13 23 3 1252.81 1377.19 50.98 o 15 23 3 662.73 848.42 45.40 o 17 23 3 250.24 265.53 44.20 o 19 23 3 27.66 106.52 50.55 o 1 25 3 3129.40 3115.07 55.78 o 3 25 3 5620.22 5614.77 55.88 o 5 25 3 474.97 361.81 50.65 o 7 25 3 138.41 214.72 48.65 o 9 25 3 1474.49 1399.60 49.90 o 11 25 3 366.76 309.48 49.48 o 13 25 3 1145.55 1199.25 49.27 o 15 25 3 809.52 807.16 50.75 o 17 25 3 298.17 346.54 46.01 o 1 27 3 553.29 654.00 64.68 o 3 27 3 1786.69 1942.12 51.36 o 5 27 3 1989.23 1886.81 50.37 o 7 27 3 2047.27 1995.56 53.66 o 9 27 3 2707.19 2768.73 90.20 o 11 27 3 2161.22 2254.40 63.03 o 13 27 3 2325.38 2325.37 51.58 o 15 27 3 358.40 350.91 50.59 o 17 27 3 155.89 142.06 48.12 o 1 29 3 4276.32 4088.91 49.65 o 3 29 3 3277.19 3465.79 50.46 o 5 29 3 1248.34 1180.86 49.79 o 7 29 3 2118.40 2120.35 50.71 o 9 29 3 214.25 351.91 49.39 o 11 29 3 1391.44 1397.65 45.31 o 13 29 3 431.68 463.11 45.96 o 15 29 3 133.19 205.46 48.50 o 1 31 3 1761.48 1798.37 44.73 o 3 31 3 1783.84 1777.83 48.35 o 5 31 3 1371.29 1500.44 66.66 o 7 31 3 1242.05 1360.24 49.10 o 9 31 3 1304.80 1306.56 47.48 o 11 31 3 1091.47 969.33 44.25 o 13 31 3 1408.17 1321.14 45.32 o 15 31 3 966.01 804.73 48.65 o 1 33 3 1391.29 1190.21 46.77 o 3 33 3 2776.03 2636.71 78.17 o 5 33 3 215.91 212.36 60.73 o 7 33 3 750.62 844.08 46.71 o 9 33 3 841.73 833.80 49.30 o 11 33 3 500.13 569.61 43.83 o 13 33 3 844.83 695.45 49.64 o 1 35 3 1198.47 1258.01 59.15 o 3 35 3 656.12 741.71 45.18 o 5 35 3 1061.12 1152.95 47.23 o 7 35 3 300.44 244.93 46.91 o 9 35 3 236.44 402.02 48.56 o 11 35 3 289.62 239.23 52.52 o 13 35 3 709.00 519.43 46.45 o 1 37 3 453.06 558.06 44.64 o 3 37 3 408.94 405.43 46.59 o 5 37 3 1036.29 1108.91 59.79 o 7 37 3 874.29 911.82 47.76 o 9 37 3 340.12 153.94 49.30 o 11 37 3 215.55 130.52 47.57 o 1 39 3 1628.09 1520.34 45.20 o 3 39 3 342.42 362.22 48.85 o 5 39 3 365.06 433.70 49.17 o 7 39 3 230.65 250.95 48.44 o 9 39 3 296.85 260.73 48.10 o 1 41 3 398.30 452.73 45.00 o 3 41 3 136.20 191.22 44.73 o 5 41 3 854.54 761.25 44.43 o 7 41 3 114.56 178.93 68.57 o 1 43 3 207.38 263.87 68.09 o 0 0 4 23667.48 23843.51 443.39 o 4 0 4 1586.56 1544.62 64.75 o 8 0 4 13391.93 13438.99 100.48 o 12 0 4 2967.91 3181.06 163.82 o 16 0 4 1079.83 1236.56 91.66 o 20 0 4 196.49 126.26 65.89 o 2 2 4 15016.78 15132.92 87.83 o 4 2 4 530.67 597.32 42.33 o 6 2 4 6641.23 6484.97 51.98 o 8 2 4 293.93 311.15 48.89 o 10 2 4 3121.71 2990.70 50.88 o 12 2 4 1813.13 1858.50 47.37 o 14 2 4 842.90 903.51 45.69 o 16 2 4 151.43 153.47 43.61 o 18 2 4 1029.58 979.09 45.21 o 20 2 4 271.23 204.95 47.84 o 0 4 4 4379.66 4008.08 61.35 o 2 4 4 1321.01 1287.53 44.50 o 4 4 4 8265.29 7918.95 61.80 o 6 4 4 3117.60 3244.47 52.95 o 8 4 4 6669.44 6412.73 57.30 o 10 4 4 815.70 972.43 47.75 o 12 4 4 1141.06 1215.71 54.03 o 14 4 4 564.18 542.76 42.46 o 16 4 4 1324.84 1301.77 48.29 o 18 4 4 21.54 110.65 48.14 o 20 4 4 595.05 461.36 61.72 o 2 6 4 6107.72 5633.27 48.68 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o 6 12 4 166.85 163.70 50.17 o 8 12 4 3012.29 3086.25 52.77 o 10 12 4 171.88 237.13 48.74 o 12 12 4 2383.61 2350.14 51.91 o 14 12 4 151.21 189.63 51.57 o 16 12 4 2242.13 1942.23 51.27 o 18 12 4 249.36 173.68 50.80 o 2 14 4 2289.16 2214.15 57.55 o 4 14 4 870.85 953.22 56.60 o 6 14 4 5205.71 5084.86 51.78 o 8 14 4 324.45 377.09 47.10 o 10 14 4 3841.98 3763.45 51.10 o 12 14 4 411.00 401.85 47.65 o 14 14 4 2485.16 2521.49 58.39 o 16 14 4 518.39 555.50 50.71 o 18 14 4 376.07 422.42 49.75 o 0 16 4 4603.98 4501.44 151.81 o 2 16 4 967.56 960.36 52.89 o 4 16 4 802.89 890.36 52.21 o 6 16 4 1729.13 1880.02 52.05 o 8 16 4 2306.48 2505.66 58.48 o 10 16 4 274.49 296.43 48.17 o 12 16 4 3314.57 3279.60 66.56 o 14 16 4 451.69 505.92 46.54 o 16 16 4 439.98 349.85 48.06 o 18 16 4 311.02 268.12 45.93 o 2 18 4 5579.20 5884.12 84.25 o 4 18 4 3042.30 3062.44 56.38 o 6 18 4 352.01 503.05 48.84 o 8 18 4 162.40 191.84 46.82 o 10 18 4 1320.01 1292.63 53.17 o 12 18 4 291.60 320.28 47.75 o 14 18 4 570.32 602.19 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