#------------------------------------------------------------------------------ #$Date: 2016-06-23 04:15:41 +0300 (Thu, 23 Jun 2016) $ #$Revision: 183841 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/17/2241729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241729 _cell_angle_alpha 90.000 _cell_angle_beta 98.786 _cell_angle_gamma 90.000 _cell_length_a 14.4354 _cell_length_b 14.1925 _cell_length_c 19.1682 _exptl_crystal_F_000 1720.00 _reflns_d_resolution_high 0.7600 _cod_data_source_file hb7592Isup2.hkl _cod_data_source_block I _shelx_title ' shelxt_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 314.73 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 99053.98 107760.07 1834.82 o 4 0 0 23356.80 24744.04 439.35 o 6 0 0 1908.94 2234.86 65.59 o 8 0 0 1783.02 1736.69 112.29 o 10 0 0 735.07 757.29 55.77 o 12 0 0 2666.62 2417.60 107.48 o 14 0 0 540.68 372.68 58.02 o 16 0 0 1626.17 1723.02 105.74 o 18 0 0 716.51 701.13 101.56 o 1 1 0 55818.43 61089.45 691.14 o 2 1 0 2.92 10.44 4.30 o 3 1 0 2586.90 2738.86 37.04 o 4 1 0 8027.61 8433.52 99.00 o 5 1 0 1437.79 1614.52 31.28 o 6 1 0 5572.25 5398.37 77.60 o 7 1 0 4458.55 4369.90 68.28 o 8 1 0 143.82 157.94 20.94 o 9 1 0 462.93 473.41 29.92 o 10 1 0 688.22 685.87 39.07 o 11 1 0 546.19 504.04 35.12 o 12 1 0 2.52 -22.05 22.05 o 13 1 0 48.94 12.35 26.01 o 14 1 0 356.76 372.16 39.53 o 15 1 0 167.06 242.97 42.57 o 16 1 0 129.59 240.73 51.05 o 17 1 0 914.23 868.21 61.79 o 18 1 0 37.72 32.44 42.43 o 0 2 0 16200.73 17811.83 271.25 o 1 2 0 9757.82 10444.92 123.52 o 2 2 0 1445.05 1526.50 23.78 o 3 2 0 10898.33 11350.51 128.51 o 4 2 0 6236.79 6368.00 78.45 o 5 2 0 25698.46 26264.85 289.02 o 6 2 0 11231.97 11375.69 135.53 o 7 2 0 31118.42 31276.99 369.46 o 8 2 0 2709.65 2556.68 53.45 o 9 2 0 9384.84 8777.87 134.23 o 10 2 0 469.44 379.15 33.43 o 11 2 0 3083.70 2909.15 87.84 o 12 2 0 293.49 271.15 41.76 o 13 2 0 85.56 112.51 30.27 o 14 2 0 379.20 340.57 39.41 o 15 2 0 54.40 21.11 30.75 o 16 2 0 5.56 -8.04 34.26 o 17 2 0 13.50 -26.48 36.62 o 18 2 0 48.54 50.73 47.29 o 1 3 0 423.76 400.35 13.23 o 2 3 0 1101.68 1100.80 21.99 o 3 3 0 775.75 768.49 18.87 o 4 3 0 876.62 836.61 20.93 o 5 3 0 11411.83 11517.71 135.90 o 6 3 0 21070.63 21500.61 242.82 o 7 3 0 560.84 468.34 19.61 o 8 3 0 6438.67 6527.06 89.28 o 9 3 0 17.27 33.37 14.05 o 10 3 0 10769.97 9938.68 325.24 o 11 3 0 800.32 863.77 43.91 o 12 3 0 722.25 760.96 44.67 o 13 3 0 3256.12 3340.34 172.29 o 14 3 0 389.00 302.22 38.31 o 15 3 0 210.61 232.61 38.59 o 16 3 0 285.93 272.45 49.34 o 17 3 0 63.13 82.81 45.38 o 18 3 0 11.69 56.65 46.34 o 0 4 0 21.33 23.65 11.12 o 1 4 0 5729.24 5706.93 70.70 o 2 4 0 5257.99 5376.42 67.78 o 3 4 0 3.57 -6.98 6.98 o 4 4 0 8178.50 7886.89 97.45 o 5 4 0 528.20 512.59 20.68 o 6 4 0 903.01 802.60 24.85 o 7 4 0 782.62 782.39 25.74 o 8 4 0 42.34 25.14 15.01 o 9 4 0 163.70 189.42 17.11 o 10 4 0 3457.96 3415.22 67.78 o 11 4 0 776.88 772.13 49.22 o 12 4 0 6525.21 6521.00 123.21 o 13 4 0 948.03 918.93 51.47 o 14 4 0 1470.33 1488.54 65.33 o 15 4 0 60.02 -23.35 33.28 o 16 4 0 137.71 161.08 44.25 o 17 4 0 22.05 -3.32 43.19 o 18 4 0 46.42 7.41 48.47 o 1 5 0 5965.98 6375.54 74.72 o 2 5 0 4424.25 4706.89 62.87 o 3 5 0 7035.06 6936.57 87.56 o 4 5 0 16796.17 17414.13 199.20 o 5 5 0 22388.75 23007.53 259.91 o 6 5 0 2215.41 2167.28 41.37 o 7 5 0 3021.02 2954.86 54.32 o 8 5 0 3325.72 3317.39 57.34 o 9 5 0 6.38 17.43 14.41 o 10 5 0 310.18 332.25 28.01 o 11 5 0 1026.95 938.08 56.22 o 12 5 0 106.75 59.83 26.83 o 13 5 0 2783.63 2857.92 93.03 o 14 5 0 100.90 95.85 49.20 o 15 5 0 637.78 608.90 55.42 o 16 5 0 77.31 62.69 42.05 o 17 5 0 379.15 394.57 63.85 o 18 5 0 243.25 310.54 67.27 o 0 6 0 7987.57 9238.18 158.80 o 1 6 0 159.63 185.88 11.68 o 2 6 0 183.74 211.33 12.99 o 3 6 0 9885.90 9719.05 119.01 o 4 6 0 11782.53 11986.39 144.30 o 5 6 0 5375.46 4932.62 71.11 o 6 6 0 5513.43 5393.37 78.19 o 7 6 0 1409.97 1408.28 36.35 o 8 6 0 1402.31 1460.05 38.95 o 9 6 0 33.15 12.77 15.79 o 10 6 0 74.03 66.37 20.45 o 11 6 0 120.12 108.29 30.39 o 12 6 0 1559.00 1493.20 67.74 o 13 6 0 17.38 -34.13 34.13 o 14 6 0 76.97 105.92 37.21 o 15 6 0 719.45 752.31 61.60 o 16 6 0 89.11 62.61 51.04 o 17 6 0 356.89 405.21 66.75 o 1 7 0 7286.40 6800.34 89.22 o 2 7 0 4974.76 5068.59 77.78 o 3 7 0 648.42 616.26 21.11 o 4 7 0 3516.42 3454.07 54.81 o 5 7 0 1914.51 1893.69 56.76 o 6 7 0 4402.55 4401.31 68.71 o 7 7 0 2053.09 2011.82 44.00 o 8 7 0 1832.47 1887.84 62.34 o 9 7 0 996.51 918.56 38.41 o 10 7 0 1889.41 1831.37 80.82 o 11 7 0 15.15 9.38 26.39 o 12 7 0 84.00 76.59 42.03 o 13 7 0 2.74 -4.24 36.99 o 14 7 0 2.36 -9.19 41.69 o 15 7 0 187.05 200.62 53.80 o 16 7 0 17.84 -18.42 50.29 o 17 7 0 155.18 142.31 56.60 o 0 8 0 20347.20 20566.45 296.55 o 1 8 0 3104.78 2884.60 45.93 o 2 8 0 14148.63 14303.95 185.08 o 3 8 0 1064.95 1044.05 34.87 o 4 8 0 249.04 288.60 17.32 o 5 8 0 400.05 360.19 20.39 o 6 8 0 3960.81 3815.90 71.76 o 7 8 0 1264.35 1235.75 42.25 o 8 8 0 2150.55 2170.90 56.66 o 9 8 0 596.57 618.11 37.99 o 10 8 0 725.23 772.08 43.71 o 11 8 0 714.65 642.66 87.66 o 12 8 0 387.22 377.95 51.39 o 13 8 0 169.13 192.85 47.64 o 14 8 0 33.74 -19.26 44.78 o 15 8 0 181.97 224.90 55.00 o 16 8 0 172.33 165.37 55.81 o 1 9 0 8538.70 8491.81 112.53 o 2 9 0 17.08 61.16 16.56 o 3 9 0 559.94 589.07 28.93 o 4 9 0 405.13 422.50 26.35 o 5 9 0 1727.15 1544.01 51.22 o 6 9 0 63.65 74.38 19.32 o 7 9 0 1588.18 1542.27 79.61 o 8 9 0 1498.41 1547.48 50.64 o 9 9 0 57.07 72.71 26.23 o 10 9 0 105.59 146.17 33.71 o 11 9 0 66.33 22.06 35.93 o 12 9 0 24.75 98.49 41.39 o 13 9 0 5.41 -6.78 63.55 o 14 9 0 139.15 230.56 53.12 o 15 9 0 2.94 54.13 48.83 o 16 9 0 237.31 414.24 66.61 o 0 10 0 7216.58 7145.75 133.02 o 1 10 0 133.89 141.04 17.64 o 2 10 0 1465.14 1501.41 41.30 o 3 10 0 1253.77 1295.66 70.81 o 4 10 0 360.57 371.59 26.84 o 5 10 0 3647.06 3549.20 71.20 o 6 10 0 731.85 695.21 37.28 o 7 10 0 4515.25 4395.55 137.55 o 8 10 0 25.54 26.11 24.97 o 9 10 0 3016.86 2972.57 84.42 o 10 10 0 38.81 16.90 30.11 o 11 10 0 200.43 275.87 41.34 o 12 10 0 62.49 65.18 42.27 o 13 10 0 46.16 48.37 46.05 o 14 10 0 42.89 -35.96 87.97 o 15 10 0 110.53 161.88 60.14 o 1 11 0 1285.09 1422.58 58.19 o 2 11 0 106.65 137.56 22.64 o 3 11 0 163.06 168.46 23.51 o 4 11 0 61.26 79.69 25.24 o 5 11 0 155.35 176.04 28.56 o 6 11 0 891.44 885.38 48.01 o 7 11 0 180.16 223.20 31.96 o 8 11 0 1152.65 1194.89 56.55 o 9 11 0 83.61 80.58 32.82 o 10 11 0 105.39 97.10 35.31 o 11 11 0 347.40 392.79 46.66 o 12 11 0 11.92 24.48 43.46 o 13 11 0 307.21 386.16 59.59 o 14 11 0 268.81 269.76 60.18 o 15 11 0 104.86 153.14 60.01 o 0 12 0 4525.57 4400.20 107.74 o 1 12 0 51.55 16.62 18.05 o 2 12 0 1715.75 1720.49 58.49 o 3 12 0 629.17 618.87 40.70 o 4 12 0 1275.51 1251.22 55.15 o 5 12 0 39.46 -24.54 24.54 o 6 12 0 1527.31 1520.76 70.75 o 7 12 0 359.32 355.88 37.49 o 8 12 0 2.00 -33.66 36.40 o 9 12 0 60.66 50.92 30.93 o 10 12 0 790.24 857.48 60.19 o 11 12 0 250.84 265.13 44.46 o 12 12 0 1015.57 947.93 77.03 o 13 12 0 359.13 332.11 61.93 o 14 12 0 644.94 654.37 74.91 o 1 13 0 13.06 28.92 24.00 o 2 13 0 756.70 736.21 43.38 o 3 13 0 804.48 816.69 47.32 o 4 13 0 1272.02 1307.47 61.44 o 5 13 0 375.77 481.13 41.11 o 6 13 0 11.91 -26.93 26.93 o 7 13 0 91.70 22.29 28.64 o 8 13 0 22.90 23.20 30.30 o 9 13 0 62.66 18.22 31.73 o 10 13 0 40.22 17.07 36.95 o 11 13 0 373.60 333.24 48.79 o 12 13 0 59.38 6.01 50.23 o 13 13 0 444.61 504.83 75.77 o 0 14 0 122.77 87.10 57.50 o 1 14 0 108.06 41.86 37.69 o 2 14 0 49.67 48.46 27.36 o 3 14 0 1326.06 1522.69 71.44 o 4 14 0 10.52 34.89 29.02 o 5 14 0 840.03 762.52 49.55 o 6 14 0 3.39 -27.79 27.79 o 7 14 0 55.22 57.86 31.70 o 8 14 0 21.90 -23.10 31.86 o 9 14 0 18.33 37.43 38.50 o 10 14 0 59.96 32.02 41.16 o 11 14 0 20.48 25.03 46.93 o 12 14 0 178.51 105.28 54.13 o 1 15 0 1705.74 1817.15 96.46 o 2 15 0 415.03 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21746.97 22462.82 246.71 o -3 2 1 238.40 241.02 11.60 o -2 2 1 18423.20 19748.16 215.19 o -1 2 1 2133.16 2169.54 30.22 o 0 2 1 23412.31 26074.16 278.66 o 1 2 1 335.47 330.03 9.86 o 2 2 1 3324.56 3351.54 45.65 o 3 2 1 51203.56 55222.70 586.68 o 4 2 1 198.78 180.14 11.12 o 5 2 1 11851.54 12188.65 142.10 o 6 2 1 9764.79 10206.86 131.39 o 7 2 1 64.72 82.97 11.55 o 8 2 1 2111.71 1986.89 38.52 o 9 2 1 5344.52 5551.74 88.17 o 10 2 1 712.19 758.51 39.35 o 11 2 1 2753.43 2631.60 76.70 o 12 2 1 3767.91 3906.88 97.45 o 13 2 1 451.07 386.82 38.15 o 14 2 1 203.71 218.62 35.16 o 15 2 1 226.80 289.86 39.81 o 16 2 1 308.45 218.45 41.29 o 17 2 1 2.63 0.81 36.72 o 18 2 1 19.03 74.83 48.95 o -18 3 1 282.78 324.54 55.93 o -17 3 1 419.88 538.71 58.37 o -16 3 1 0.59 -32.94 32.94 o -15 3 1 49.99 69.06 32.45 o -14 3 1 951.01 916.23 53.95 o -13 3 1 1893.10 1952.10 68.77 o -12 3 1 158.74 188.05 30.25 o -11 3 1 1198.11 1166.94 50.05 o -10 3 1 1305.51 1288.60 48.59 o -9 3 1 93.23 115.73 18.01 o -8 3 1 120.36 138.28 13.28 o -7 3 1 894.34 939.69 26.05 o -6 3 1 12.64 1.34 10.08 o -5 3 1 9774.84 9991.29 119.98 o -4 3 1 5980.28 6063.72 76.90 o -3 3 1 49.40 47.73 8.46 o -2 3 1 22393.95 24657.96 267.53 o -1 3 1 97370.37 106317.77 1118.42 o 0 3 1 54904.33 59781.89 673.42 o 1 3 1 430.12 391.63 13.20 o 2 3 1 18174.63 19399.97 245.87 o 3 3 1 13803.98 14525.82 163.59 o 4 3 1 33234.47 34927.65 378.80 o 5 3 1 39.50 25.69 9.22 o 6 3 1 11581.53 11346.85 136.91 o 7 3 1 4889.93 4911.24 70.54 o 8 3 1 1203.33 1213.96 31.55 o 9 3 1 933.73 988.20 45.24 o 10 3 1 1642.81 1698.11 66.81 o 11 3 1 2125.53 2170.46 64.86 o 12 3 1 8.69 23.62 25.39 o 13 3 1 294.34 205.98 33.70 o 14 3 1 0.69 -22.68 28.07 o 15 3 1 188.08 265.83 45.17 o 16 3 1 59.70 58.50 40.98 o 17 3 1 14.80 54.11 44.68 o 18 3 1 0.37 39.84 46.73 o -18 4 1 184.19 125.36 49.64 o -17 4 1 67.49 68.05 44.64 o -16 4 1 386.88 413.18 72.09 o -15 4 1 764.78 756.62 53.63 o -14 4 1 477.46 473.79 42.68 o -13 4 1 2791.74 2527.33 77.58 o -12 4 1 54.16 74.76 26.17 o -11 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