#------------------------------------------------------------------------------ #$Date: 2016-06-29 04:33:47 +0300 (Wed, 29 Jun 2016) $ #$Revision: 184035 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/17/2241752.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241752 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 5.6788 _cell_length_b 5.6788 _cell_length_c 18.3368 _exptl_crystal_F_000 547.47 _reflns_d_resolution_high 0.6196 _cod_data_source_file wm5296Isup2.hkl _cod_data_source_block I _shelx_title ' P-3m1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 254.73 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z' 'x-y, -y, -z' '-x, -x+y, -z' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z' '-x+y, y, z' 'x, x-y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 231.96 248.44 2.38 o -1 2 0 4074.23 3839.89 48.96 o 0 2 0 115.33 91.47 2.15 o -1 3 0 75.21 81.67 1.29 o 0 3 0 1986.64 1989.87 19.05 o -2 4 0 64889.03 53096.86 1030.74 o -1 4 0 50.66 53.50 1.74 o 0 4 0 152.00 160.33 4.13 o -2 5 0 239.97 233.89 3.55 o -1 5 0 1440.75 1473.67 12.09 o 0 5 0 86.81 80.46 3.35 o -3 6 0 1650.38 1633.65 20.26 o -2 6 0 63.64 68.13 1.87 o -1 6 0 0.03 1.17 2.57 o 0 6 0 17633.51 16386.47 242.52 o -3 7 0 29.53 26.00 1.45 o -2 7 0 388.81 393.87 5.55 o -1 7 0 69.01 70.05 2.01 o 0 7 0 159.19 159.91 7.50 o -4 8 0 11149.67 10732.75 225.59 o -3 8 0 15.88 14.70 2.01 o -2 8 0 44.48 43.14 2.61 o -1 8 0 744.71 783.93 11.48 o -4 9 0 93.23 101.09 3.87 o -3 9 0 315.09 324.59 9.94 o -1 1 1 287.04 326.85 4.44 o 0 1 1 196.82 221.10 2.40 o -2 2 1 2482.67 2531.15 28.04 o -1 2 1 113.75 116.39 1.13 o 0 2 1 3617.65 3816.52 40.32 o -3 3 1 78.85 76.35 1.96 o -2 3 1 68.98 71.68 1.21 o -1 3 1 107.34 110.90 1.41 o 0 3 1 73.33 72.31 1.62 o -4 4 1 1636.15 1640.83 18.84 o -3 4 1 23.29 22.74 1.13 o -2 4 1 25.80 26.43 1.14 o -1 4 1 35.65 34.45 1.02 o 0 4 1 1291.64 1307.72 14.61 o -5 5 1 99.38 95.72 2.98 o -4 5 1 39.07 38.37 1.66 o -3 5 1 255.64 248.73 2.94 o -2 5 1 202.98 197.06 3.08 o -1 5 1 42.79 41.03 1.82 o 0 5 1 73.44 67.98 3.44 o -6 6 1 6.22 5.66 1.20 o -5 6 1 9.13 7.67 0.92 o -4 6 1 666.37 680.43 7.40 o -3 6 1 32.78 32.45 0.88 o -2 6 1 827.97 837.46 8.86 o -1 6 1 10.13 9.69 1.63 o 0 6 1 5.81 4.05 1.19 o -7 7 1 182.39 187.18 5.38 o -6 7 1 40.45 40.52 1.96 o -5 7 1 19.55 19.91 1.19 o -4 7 1 38.88 35.32 1.62 o -3 7 1 46.94 44.24 1.75 o -2 7 1 15.50 15.04 1.08 o -1 7 1 48.24 47.97 2.11 o 0 7 1 149.66 153.11 6.34 o -7 8 1 12.51 10.19 1.71 o -6 8 1 337.82 343.71 6.97 o -5 8 1 0.68 -1.63 1.63 o -4 8 1 3.25 2.90 1.81 o -3 8 1 0.38 1.21 1.55 o -2 8 1 284.83 287.51 6.21 o -1 8 1 14.65 17.94 1.81 o -5 9 1 106.94 113.49 4.10 o -4 9 1 86.59 85.25 3.68 o 0 0 2 27.05 23.21 0.53 o -1 1 2 1045.14 1104.87 9.94 o 0 1 2 596.80 646.89 7.30 o -2 2 2 2440.56 2314.89 28.68 o -1 2 2 7.26 7.33 0.30 o 0 2 2 3042.63 2989.30 31.04 o -3 3 2 115.42 116.71 2.99 o -2 3 2 49.84 50.69 1.13 o -1 3 2 54.61 57.67 0.92 o 0 3 2 77.96 77.54 1.69 o -4 4 2 2585.04 2672.49 30.54 o -3 4 2 293.77 297.97 2.99 o -2 4 2 24.45 25.89 1.31 o -1 4 2 502.54 506.37 4.08 o 0 4 2 2467.03 2538.89 30.68 o -5 5 2 75.53 79.02 3.02 o -4 5 2 22.00 18.54 1.16 o -3 5 2 653.28 654.33 5.66 o -2 5 2 382.35 377.91 3.45 o -1 5 2 29.14 24.67 1.80 o 0 5 2 49.31 46.73 2.67 o -6 6 2 18.68 17.25 1.53 o -5 6 2 117.45 117.01 1.95 o -4 6 2 1675.84 1731.81 16.89 o -3 6 2 0.53 0.81 0.69 o -2 6 2 1682.55 1739.90 17.38 o -1 6 2 67.47 67.45 1.47 o 0 6 2 22.89 23.74 1.54 o -7 7 2 304.86 309.88 6.77 o -6 7 2 195.79 197.14 3.28 o -5 7 2 53.71 57.57 2.05 o -4 7 2 11.58 11.40 1.08 o -3 7 2 20.23 21.61 1.42 o -2 7 2 37.14 38.48 1.39 o -1 7 2 315.97 322.57 4.87 o 0 7 2 180.14 186.72 5.54 o -7 8 2 6.69 4.04 1.60 o -6 8 2 945.12 965.43 15.94 o -5 8 2 156.35 162.83 4.42 o -4 8 2 19.19 16.54 5.35 o -3 8 2 238.55 250.63 5.42 o -2 8 2 901.60 910.89 15.29 o -1 8 2 3.87 3.09 1.76 o -5 9 2 223.99 237.67 6.40 o -4 9 2 135.41 132.27 4.30 o 0 0 3 0.39 0.57 0.23 o -1 1 3 219.82 216.83 1.94 o 0 1 3 147.22 154.89 2.22 o -2 2 3 3252.66 3825.09 48.20 o -1 2 3 123.76 126.58 1.25 o 0 2 3 2113.39 2482.56 28.23 o -3 3 3 436.06 453.92 6.35 o -2 3 3 152.95 155.15 1.86 o -1 3 3 94.05 96.97 1.82 o 0 3 3 616.46 636.30 7.56 o -4 4 3 529.24 504.11 7.33 o -3 4 3 79.62 81.84 2.03 o -2 4 3 2.69 3.03 0.55 o -1 4 3 130.78 130.66 2.26 o 0 4 3 448.49 405.01 5.29 o -5 5 3 23.46 19.08 2.61 o -4 5 3 235.73 228.06 3.22 o -3 5 3 75.15 77.45 1.77 o -2 5 3 65.16 66.95 1.53 o -1 5 3 140.66 136.10 2.54 o 0 5 3 39.42 38.50 1.73 o -6 6 3 14.42 14.06 1.27 o -5 6 3 92.48 90.46 1.62 o -4 6 3 196.77 199.30 2.58 o -3 6 3 78.55 77.25 2.72 o -2 6 3 319.80 320.78 4.07 o -1 6 3 87.38 85.05 1.66 o 0 6 3 24.07 24.02 1.57 o -7 7 3 34.77 38.96 2.44 o -6 7 3 22.86 23.82 1.26 o -5 7 3 211.38 212.43 3.57 o -4 7 3 34.16 31.79 1.56 o -3 7 3 26.43 24.72 1.72 o -2 7 3 263.53 269.21 3.97 o -1 7 3 37.27 36.26 2.38 o 0 7 3 48.87 47.98 3.88 o -7 8 3 73.54 73.44 3.72 o -6 8 3 146.56 149.55 4.22 o -5 8 3 93.40 93.16 3.35 o -4 8 3 17.60 17.21 2.08 o -3 8 3 86.82 84.00 2.94 o -2 8 3 84.61 81.08 3.15 o -1 8 3 43.57 46.02 2.41 o -5 9 3 18.90 16.98 2.64 o -4 9 3 20.58 22.54 2.58 o 0 0 4 4673.70 4673.72 132.52 o -1 1 4 200.80 202.49 2.06 o 0 1 4 286.45 294.54 3.37 o -2 2 4 1707.32 1845.04 21.97 o -1 2 4 11179.24 10086.04 99.91 o 0 2 4 960.81 1060.60 14.10 o -3 3 4 7268.28 7089.91 102.62 o -2 3 4 187.92 190.03 2.25 o -1 3 4 110.09 111.39 1.69 o 0 3 4 8370.89 7886.42 88.21 o -4 4 4 358.63 350.70 6.54 o -3 4 4 98.54 93.54 1.88 o -2 4 4 1468.10 1432.59 11.06 o -1 4 4 82.39 81.19 2.00 o 0 4 4 605.95 588.68 7.31 o -5 5 4 47.78 45.81 1.86 o -4 5 4 4449.12 4426.26 36.30 o -3 5 4 95.05 96.39 2.51 o -2 5 4 167.10 166.10 2.50 o -1 5 4 3978.99 3915.85 31.71 o 0 5 4 83.79 84.19 3.12 o -6 6 4 514.98 510.36 8.12 o -5 6 4 33.69 33.62 1.59 o -4 6 4 307.33 307.03 3.78 o -3 6 4 3122.26 3131.43 30.94 o -2 6 4 199.87 200.13 4.06 o -1 6 4 21.91 22.02 0.91 o 0 6 4 528.94 526.24 9.04 o -7 7 4 44.75 47.04 3.00 o -6 7 4 37.09 37.27 1.54 o -5 7 4 1867.32 1856.79 22.45 o -4 7 4 39.90 37.13 1.83 o -3 7 4 22.54 20.09 1.33 o -2 7 4 2303.69 2321.73 25.92 o -1 7 4 21.95 22.26 1.30 o 0 7 4 77.99 81.44 3.85 o -7 8 4 1084.86 1120.38 14.41 o -6 8 4 99.57 105.28 5.69 o -5 8 4 11.99 11.33 1.99 o -4 8 4 346.67 344.11 6.43 o -3 8 4 11.94 10.94 1.76 o -2 8 4 164.84 164.08 6.07 o -1 8 4 977.59 991.32 14.00 o -5 9 4 24.49 27.09 4.54 o -4 9 4 43.23 43.17 3.71 o 0 0 5 233.36 225.80 4.09 o -1 1 5 1688.54 1752.53 17.19 o 0 1 5 1614.77 1690.39 17.31 o -2 2 5 10329.00 11566.52 210.86 o -1 2 5 0.04 0.62 0.23 o 0 2 5 17214.47 19392.88 312.44 o -3 3 5 335.63 349.55 5.24 o -2 3 5 512.93 487.77 5.37 o -1 3 5 559.03 538.46 4.47 o 0 3 5 385.73 412.17 5.94 o -4 4 5 5258.09 5146.58 57.34 o -3 4 5 505.52 495.56 4.87 o -2 4 5 189.18 192.00 1.98 o -1 4 5 451.08 442.32 4.11 o 0 4 5 3216.30 3202.98 35.26 o -5 5 5 210.24 209.67 5.97 o -4 5 5 109.90 105.64 2.74 o -3 5 5 767.06 762.94 7.08 o -2 5 5 714.42 716.60 7.59 o -1 5 5 107.24 103.74 1.89 o 0 5 5 200.53 204.11 3.83 o -6 6 5 132.96 133.76 2.92 o -5 6 5 76.36 77.83 2.13 o -4 6 5 1521.24 1512.63 16.41 o -3 6 5 4.27 4.51 0.83 o -2 6 5 2473.85 2503.35 27.36 o -1 6 5 114.50 112.97 1.90 o 0 6 5 107.62 106.31 3.13 o -7 7 5 373.68 388.87 7.50 o -6 7 5 150.92 152.79 2.71 o -5 7 5 179.81 179.87 3.42 o -4 7 5 87.63 86.01 3.81 o -3 7 5 105.28 100.85 2.92 o -2 7 5 208.90 213.22 3.58 o -1 7 5 136.38 133.62 2.62 o 0 7 5 316.19 323.57 11.40 o -7 8 5 15.38 19.23 1.84 o -6 8 5 973.15 983.05 15.12 o -5 8 5 48.08 43.80 2.27 o -4 8 5 96.32 91.64 2.96 o -3 8 5 27.17 23.31 1.96 o -2 8 5 607.12 611.93 9.29 o -1 8 5 25.71 29.76 2.82 o -5 9 5 205.74 209.51 9.21 o 0 0 6 5.50 4.62 0.59 o -1 1 6 4649.26 4987.42 59.76 o 0 1 6 6008.87 6391.79 63.59 o -2 2 6 3209.43 3444.11 34.93 o -1 2 6 3.01 3.17 0.22 o 0 2 6 5021.84 5423.60 64.45 o -3 3 6 110.06 112.86 1.88 o -2 3 6 4477.86 4683.96 39.22 o -1 3 6 6146.89 6378.45 48.40 o 0 3 6 148.52 152.39 3.84 o -4 4 6 2026.37 2069.70 24.64 o -3 4 6 2644.73 2691.97 23.57 o -2 4 6 20.67 24.51 1.33 o -1 4 6 2002.37 2044.60 17.83 o 0 4 6 1305.37 1318.46 16.13 o -5 5 6 3246.63 3316.27 37.70 o -4 5 6 45.43 42.84 1.88 o -3 5 6 1177.06 1214.95 11.64 o -2 5 6 1469.10 1519.94 12.89 o -1 5 6 35.35 33.60 2.07 o 0 5 6 2307.99 2365.78 33.02 o -6 6 6 26.28 24.69 1.58 o -5 6 6 1062.65 1070.31 11.48 o -4 6 6 756.56 759.62 8.68 o -3 6 6 0.14 0.43 0.74 o -2 6 6 1157.26 1155.57 13.13 o -1 6 6 1478.28 1482.09 15.57 o 0 6 6 20.33 19.72 1.38 o -7 7 6 273.18 286.43 6.67 o -6 7 6 491.14 495.62 6.09 o -5 7 6 62.86 63.26 2.00 o -4 7 6 1278.70 1278.62 17.67 o -3 7 6 1805.53 1804.46 22.57 o -2 7 6 85.19 85.68 2.16 o -1 7 6 377.72 388.54 5.36 o 0 7 6 322.83 345.03 8.22 o -7 8 6 5.51 5.80 1.68 o -6 8 6 438.53 468.97 7.30 o -5 8 6 457.20 457.13 7.91 o -4 8 6 20.64 20.99 1.93 o -3 8 6 331.59 329.85 6.28 o -2 8 6 261.98 274.34 7.16 o -1 8 6 8.48 7.59 1.88 o 0 0 7 88.81 81.51 3.07 o -1 1 7 1619.76 1651.44 19.10 o 0 1 7 2262.14 2351.59 24.90 o -2 2 7 1947.22 2019.30 21.68 o -1 2 7 7.61 7.65 0.41 o 0 2 7 2400.35 2502.34 25.87 o -3 3 7 36.19 36.04 2.21 o -2 3 7 2241.02 2320.80 18.79 o -1 3 7 2875.69 2990.09 21.45 o 0 3 7 21.39 22.63 1.83 o -4 4 7 923.17 913.24 12.66 o -3 4 7 1409.86 1386.52 12.43 o -2 4 7 101.27 110.18 2.27 o -1 4 7 1023.97 1010.15 9.27 o 0 4 7 663.64 644.06 8.14 o -5 5 7 1472.88 1474.29 22.25 o -4 5 7 7.15 7.56 1.13 o -3 5 7 336.57 339.22 4.88 o -2 5 7 476.32 481.13 5.02 o -1 5 7 10.42 9.82 0.90 o 0 5 7 1218.51 1251.43 17.03 o -6 6 7 55.44 52.51 1.96 o -5 6 7 797.21 800.15 8.20 o -4 6 7 351.85 351.39 4.70 o -3 6 7 0.11 0.73 1.11 o -2 6 7 546.56 542.22 6.77 o -1 6 7 1066.10 1077.31 10.80 o 0 6 7 58.12 55.10 2.52 o -7 7 7 37.45 38.60 2.56 o -6 7 7 306.08 313.39 4.29 o -5 7 7 21.66 21.14 1.37 o -4 7 7 774.88 793.17 10.73 o -3 7 7 968.40 977.65 12.81 o -2 7 7 14.60 12.49 1.31 o -1 7 7 215.07 211.89 3.23 o 0 7 7 55.39 55.22 3.05 o -7 8 7 3.85 5.04 1.75 o -6 8 7 210.94 225.58 5.66 o -5 8 7 522.28 518.27 8.31 o -4 8 7 43.79 42.93 2.24 o -3 8 7 365.30 364.17 6.39 o -2 8 7 131.73 131.95 3.28 o -1 8 7 2.21 -0.23 1.94 o 0 0 8 751.26 1268.30 26.40 o -1 1 8 18.27 17.44 0.92 o 0 1 8 28.86 29.58 1.82 o -2 2 8 1953.57 2002.84 22.57 o -1 2 8 53.86 53.49 1.29 o 0 2 8 2174.30 2274.92 23.87 o -3 3 8 4.35 4.51 1.35 o -2 3 8 293.12 300.16 3.15 o -1 3 8 174.88 177.13 2.08 o 0 3 8 7.45 7.77 0.74 o -4 4 8 923.93 913.07 12.75 o -3 4 8 24.84 20.61 1.51 o -2 4 8 382.62 446.00 4.20 o -1 4 8 30.52 28.06 1.57 o 0 4 8 826.75 814.88 10.62 o -5 5 8 210.08 204.67 6.03 o -4 5 8 61.37 59.57 3.06 o -3 5 8 36.88 35.83 2.01 o -2 5 8 54.65 52.71 1.85 o -1 5 8 54.37 52.83 1.58 o 0 5 8 332.87 335.01 5.31 o -6 6 8 495.56 497.77 8.10 o -5 6 8 92.12 90.53 1.75 o -4 6 8 531.36 527.50 6.70 o -3 6 8 199.76 205.30 3.96 o -2 6 8 598.40 600.13 6.85 o -1 6 8 52.02 48.86 1.36 o 0 6 8 498.30 501.60 7.67 o -7 7 8 42.24 48.26 3.40 o -6 7 8 14.41 11.92 1.25 o -5 7 8 1.26 2.04 1.09 o -4 7 8 185.53 183.95 3.17 o -3 7 8 114.26 110.63 2.50 o -2 7 8 1.29 2.03 1.04 o -1 7 8 8.16 7.03 1.16 o 0 7 8 46.83 53.27 4.86 o -7 8 8 166.27 185.13 4.05 o -6 8 8 202.37 214.51 5.03 o -5 8 8 11.80 12.57 1.76 o -4 8 8 371.93 372.35 6.49 o -3 8 8 16.85 13.96 1.89 o -2 8 8 181.93 178.50 3.39 o -1 8 8 161.18 166.11 4.41 o 0 0 9 23.23 25.48 1.37 o -1 1 9 21.23 21.15 1.48 o 0 1 9 13.45 12.22 0.87 o -2 2 9 3350.16 3501.99 42.59 o -1 2 9 106.67 113.21 2.49 o 0 2 9 3330.34 3481.85 37.29 o -3 3 9 95.70 97.57 3.36 o -2 3 9 253.62 243.74 2.70 o -1 3 9 192.74 188.67 2.38 o 0 3 9 67.79 70.63 3.05 o -4 4 9 1694.54 1691.51 22.52 o -3 4 9 23.67 28.12 1.77 o -2 4 9 0.16 2.63 1.27 o -1 4 9 42.06 52.72 2.11 o 0 4 9 1672.89 1658.67 21.34 o -5 5 9 198.27 189.92 3.88 o -4 5 9 49.86 48.06 3.81 o -3 5 9 18.80 18.02 1.39 o -2 5 9 32.86 29.53 1.32 o -1 5 9 63.20 61.79 1.18 o 0 5 9 243.31 241.00 4.18 o -6 6 9 0.31 0.53 1.13 o -5 6 9 98.64 100.58 2.04 o -4 6 9 1083.02 1079.57 12.66 o -3 6 9 52.76 51.31 1.57 o -2 6 9 1098.03 1099.49 11.88 o -1 6 9 68.27 67.85 1.67 o 0 6 9 0.24 0.81 1.09 o -7 7 9 35.33 30.71 3.41 o -6 7 9 4.47 3.56 1.19 o -5 7 9 35.80 37.51 1.80 o -4 7 9 152.68 145.57 2.79 o -3 7 9 120.65 115.75 2.93 o -2 7 9 24.01 20.49 1.33 o -1 7 9 2.97 2.14 1.16 o 0 7 9 42.72 42.73 2.89 o -7 8 9 22.81 28.53 2.73 o -6 8 9 484.85 498.51 10.66 o -5 8 9 13.62 12.53 1.76 o -4 8 9 0.00 3.71 1.64 o -3 8 9 22.54 21.02 1.82 o -2 8 9 458.30 467.84 6.44 o -1 8 9 24.82 29.75 2.61 o 0 0 10 23.38 22.56 1.45 o -1 1 10 616.67 622.58 7.83 o 0 1 10 794.65 799.15 9.93 o -2 2 10 25073.76 27222.47 356.22 o -1 2 10 1.01 2.04 0.47 o 0 2 10 18319.29 20183.60 220.64 o -3 3 10 16.43 15.43 1.81 o -2 3 10 90.79 93.39 2.19 o -1 3 10 161.44 168.95 2.73 o 0 3 10 10.67 9.86 1.17 o -4 4 10 8587.90 8967.59 117.37 o -3 4 10 478.55 470.99 5.14 o -2 4 10 20.44 21.49 1.80 o -1 4 10 363.78 361.55 4.45 o 0 4 10 11851.15 12199.38 153.94 o -5 5 10 43.22 39.76 2.61 o -4 5 10 5.14 5.31 1.88 o -3 5 10 426.30 429.34 7.52 o -2 5 10 500.29 508.33 5.98 o -1 5 10 3.98 3.98 0.63 o 0 5 10 74.23 70.84 1.99 o -6 6 10 15.18 14.49 2.07 o -5 6 10 83.03 80.82 2.13 o -4 6 10 6865.70 6828.94 78.62 o -3 6 10 5.37 3.93 0.88 o -2 6 10 4963.61 5058.28 55.91 o -1 6 10 129.66 134.80 2.40 o 0 6 10 16.80 16.50 1.50 o -7 7 10 208.93 220.22 6.60 o -6 7 10 265.93 270.19 4.28 o -5 7 10 10.32 11.37 1.31 o -4 7 10 27.96 25.07 1.50 o -3 7 10 21.21 18.58 1.43 o -2 7 10 8.01 8.03 1.15 o -1 7 10 227.75 229.06 3.81 o 0 7 10 223.82 228.91 5.72 o -6 8 10 1853.94 1858.75 24.06 o -5 8 10 227.60 213.52 4.58 o -4 8 10 15.30 12.71 1.83 o -3 8 10 185.18 188.52 3.99 o -2 8 10 2668.38 2626.85 31.10 o 0 0 11 0.02 -0.58 1.80 o -1 1 11 445.09 441.23 5.74 o 0 1 11 650.52 656.04 8.42 o -2 2 11 14367.39 15085.46 186.17 o -1 2 11 298.14 300.86 3.01 o 0 2 11 11195.70 11724.00 135.34 o -3 3 11 621.46 596.52 10.61 o -2 3 11 379.13 368.76 3.97 o -1 3 11 618.42 607.08 6.25 o 0 3 11 349.51 348.54 8.02 o -4 4 11 5403.85 5645.79 71.16 o -3 4 11 512.95 524.21 6.86 o -2 4 11 0.49 0.62 1.25 o -1 4 11 340.95 343.88 5.71 o 0 4 11 6783.41 6901.98 93.53 o -5 5 11 258.75 259.77 5.02 o -4 5 11 149.20 147.97 2.42 o -3 5 11 167.88 167.98 5.29 o -2 5 11 229.05 230.05 3.33 o -1 5 11 264.79 261.45 3.32 o 0 5 11 149.12 148.92 3.05 o -6 6 11 8.28 8.84 2.33 o -5 6 11 225.45 220.73 3.51 o -4 6 11 3871.66 3834.11 44.61 o -3 6 11 56.29 51.33 1.57 o -2 6 11 3113.41 3116.81 33.33 o -1 6 11 360.48 367.58 4.70 o 0 6 11 14.49 15.87 1.86 o -7 7 11 38.01 40.00 3.76 o -6 7 11 172.85 172.39 3.38 o -5 7 11 348.91 351.02 5.44 o -4 7 11 121.96 117.98 2.58 o -3 7 11 208.87 207.32 3.73 o -2 7 11 206.42 200.91 3.70 o -1 7 11 122.12 126.42 2.61 o 0 7 11 42.52 47.33 3.05 o -6 8 11 1336.83 1327.50 16.68 o -5 8 11 274.87 265.87 5.27 o -4 8 11 10.72 10.72 1.81 o -3 8 11 182.66 183.12 3.93 o -2 8 11 1682.89 1643.76 20.07 o 0 0 12 4350.03 4161.07 82.43 o -1 1 12 18.80 19.71 1.48 o 0 1 12 24.87 24.41 1.49 o -2 2 12 1636.75 1620.72 19.96 o -1 2 12 345.39 334.96 3.51 o 0 2 12 2530.10 2552.67 30.97 o -3 3 12 337.31 343.50 6.82 o -2 3 12 73.51 72.99 2.34 o -1 3 12 130.72 125.83 2.34 o 0 3 12 214.94 227.21 8.13 o -4 4 12 1421.03 1422.11 21.64 o -3 4 12 25.26 25.56 2.06 o -2 4 12 3120.44 3115.61 27.53 o -1 4 12 15.98 16.18 1.45 o 0 4 12 894.95 900.02 14.59 o -5 5 12 124.80 123.88 3.34 o -4 5 12 172.36 169.88 2.70 o -3 5 12 6.97 5.43 0.86 o -2 5 12 4.40 4.05 0.78 o -1 5 12 250.00 252.42 3.25 o 0 5 12 71.21 69.26 2.41 o -6 6 12 1365.67 1334.63 22.91 o -5 6 12 29.38 28.01 1.50 o -4 6 12 537.61 535.10 7.18 o -3 6 12 214.61 202.23 3.32 o -2 6 12 872.28 865.31 10.44 o -1 6 12 52.16 53.43 1.63 o 0 6 12 1347.75 1345.55 21.00 o -7 7 12 7.85 6.81 4.92 o -6 7 12 2.34 2.49 1.51 o -5 7 12 163.90 158.46 3.66 o -4 7 12 43.88 42.72 1.71 o -3 7 12 77.53 74.53 2.24 o -2 7 12 92.52 90.18 2.63 o -1 7 12 2.65 2.24 1.23 o 0 7 12 9.89 9.67 2.25 o -6 8 12 458.60 464.47 9.65 o -5 8 12 16.35 14.18 2.05 o -4 8 12 945.08 938.58 13.72 o -3 8 12 9.68 7.74 1.74 o -2 8 12 294.00 298.09 7.93 o 0 0 13 269.11 285.45 12.28 o -1 1 13 270.05 283.47 5.00 o 0 1 13 159.36 162.07 3.81 o -2 2 13 151.18 150.40 4.58 o -1 2 13 4.93 4.77 0.70 o 0 2 13 117.41 110.00 4.71 o -3 3 13 100.00 102.30 6.36 o -2 3 13 82.15 82.30 2.52 o -1 3 13 98.30 93.46 2.23 o 0 3 13 128.21 126.81 4.97 o -4 4 13 54.68 55.04 3.67 o -3 4 13 41.07 42.21 3.42 o -2 4 13 145.48 147.92 3.52 o -1 4 13 54.63 51.89 1.66 o 0 4 13 92.49 96.47 2.58 o -5 5 13 74.73 73.26 2.68 o -4 5 13 48.29 47.46 1.42 o -3 5 13 217.32 218.70 3.71 o -2 5 13 123.48 121.08 2.38 o -1 5 13 45.89 46.61 1.30 o 0 5 13 48.55 50.84 2.50 o -6 6 13 34.65 32.55 2.32 o -5 6 13 24.91 23.52 1.43 o -4 6 13 86.44 84.89 2.24 o -3 6 13 2.09 1.51 0.96 o -2 6 13 61.45 60.33 1.76 o -1 6 13 39.93 36.42 1.49 o 0 6 13 45.75 45.81 2.33 o -7 7 13 189.76 211.53 7.52 o -6 7 13 11.99 10.55 1.76 o -5 7 13 97.51 94.76 3.81 o -4 7 13 26.33 24.64 1.61 o -3 7 13 46.68 45.46 1.89 o -2 7 13 110.45 110.82 2.79 o -1 7 13 20.15 18.73 1.71 o 0 7 13 113.62 118.23 4.93 o -5 8 13 24.33 22.25 2.30 o -4 8 13 17.78 15.07 2.05 o -3 8 13 23.15 19.70 1.85 o 0 0 14 18.87 13.47 2.42 o -1 1 14 1435.90 1417.96 16.86 o 0 1 14 2228.73 2217.67 26.25 o -2 2 14 1546.98 1518.23 19.07 o -1 2 14 99.84 101.94 2.94 o 0 2 14 977.78 957.14 12.11 o -3 3 14 106.19 104.41 3.82 o -2 3 14 712.55 711.22 7.22 o -1 3 14 1054.87 1084.86 10.22 o 0 3 14 187.15 194.30 4.68 o -4 4 14 688.68 675.02 11.23 o -3 4 14 1340.96 1353.19 14.25 o -2 4 14 17.71 18.20 1.00 o -1 4 14 868.23 877.06 11.95 o 0 4 14 1069.65 1041.06 16.64 o -5 5 14 257.89 242.33 5.31 o -4 5 14 79.94 82.92 2.00 o -3 5 14 843.70 839.45 10.98 o -2 5 14 1339.74 1359.21 17.21 o -1 5 14 45.14 44.80 1.55 o 0 5 14 185.07 180.84 4.15 o -6 6 14 17.80 14.02 2.24 o -5 6 14 327.77 320.65 5.42 o -4 6 14 715.48 701.51 10.17 o -3 6 14 13.52 12.65 1.24 o -2 6 14 462.78 452.87 6.38 o -1 6 14 490.95 487.60 6.50 o 0 6 14 12.98 16.71 2.54 o -6 7 14 604.01 611.87 10.13 o -5 7 14 65.01 65.48 2.66 o -4 7 14 136.98 128.69 2.95 o -3 7 14 194.30 184.99 3.60 o -2 7 14 109.93 110.60 2.71 o -1 7 14 383.70 387.18 6.99 o -4 8 14 13.36 14.22 2.41 o 0 0 15 1500.96 1479.66 31.92 o -1 1 15 1120.65 1102.66 13.59 o 0 1 15 1164.02 1149.11 14.18 o -2 2 15 278.51 280.06 8.58 o -1 2 15 3.01 3.27 0.92 o 0 2 15 179.56 176.82 5.10 o -3 3 15 28.86 27.15 3.25 o -2 3 15 441.32 437.98 7.44 o -1 3 15 442.50 455.04 5.59 o 0 3 15 35.75 31.00 1.56 o -4 4 15 80.83 82.43 2.54 o -3 4 15 555.66 558.41 6.70 o -2 4 15 792.63 785.46 10.21 o -1 4 15 561.11 571.62 8.03 o 0 4 15 108.39 107.59 3.36 o -5 5 15 119.37 113.00 3.36 o -4 5 15 25.46 28.11 1.55 o -3 5 15 787.54 785.92 10.95 o -2 5 15 858.03 851.16 11.22 o -1 5 15 15.78 14.92 1.06 o 0 5 15 114.18 113.68 4.60 o -6 6 15 285.61 293.74 7.54 o -5 6 15 136.26 132.49 3.12 o -4 6 15 39.10 37.56 2.20 o -3 6 15 12.19 11.23 1.68 o -2 6 15 30.03 30.45 1.60 o -1 6 15 112.73 106.68 2.53 o 0 6 15 272.43 278.80 9.34 o -6 7 15 264.72 272.74 5.63 o -5 7 15 37.64 37.38 2.26 o -4 7 15 68.13 63.18 3.60 o -3 7 15 62.44 58.12 3.13 o -2 7 15 39.41 32.92 2.48 o -1 7 15 264.59 271.02 5.13 o 0 0 16 11797.94 11293.59 219.39 o -1 1 16 1014.04 989.26 12.40 o 0 1 16 588.09 566.12 7.97 o -2 2 16 162.96 162.15 6.33 o -1 2 16 2713.69 2666.82 22.12 o 0 2 16 110.74 111.34 3.23 o -3 3 16 2330.12 2257.97 29.66 o -2 3 16 307.61 316.11 4.42 o -1 3 16 175.03 178.22 3.50 o 0 3 16 2226.78 2193.86 36.82 o -4 4 16 64.69 61.46 2.27 o -3 4 16 325.76 315.98 5.29 o -2 4 16 5971.72 5694.21 67.85 o -1 4 16 559.17 565.52 7.47 o 0 4 16 82.91 82.63 3.80 o -5 5 16 22.48 22.23 2.07 o -4 5 16 1113.30 1093.00 16.02 o -3 5 16 794.02 785.60 11.07 o -2 5 16 461.98 461.08 7.06 o -1 5 16 1167.24 1147.84 14.19 o 0 5 16 38.76 36.29 2.48 o -6 6 16 2310.35 2266.58 42.88 o -5 6 16 141.87 141.53 4.72 o -4 6 16 52.15 52.11 2.56 o -3 6 16 627.98 612.45 9.18 o -2 6 16 34.31 36.14 2.08 o -1 6 16 82.55 80.89 2.49 o 0 6 16 2301.38 2305.54 48.44 o -6 7 16 190.64 197.65 8.22 o -5 7 16 874.39 875.97 11.99 o -4 7 16 34.61 21.06 2.44 o -3 7 16 19.51 19.85 1.81 o -2 7 16 804.22 803.04 11.12 o -1 7 16 324.81 328.41 6.28 o 0 0 17 966.36 967.67 23.50 o -1 1 17 2034.44 1998.98 24.10 o 0 1 17 1283.20 1274.97 15.08 o -2 2 17 178.41 177.77 5.28 o -1 2 17 26.89 27.08 2.22 o 0 2 17 291.03 284.17 8.39 o -3 3 17 27.96 28.24 4.39 o -2 3 17 1179.40 1161.61 14.10 o -1 3 17 704.95 699.79 7.90 o 0 3 17 45.42 44.68 2.08 o -4 4 17 159.80 158.44 3.93 o -3 4 17 757.48 740.38 9.14 o -2 4 17 507.37 498.79 7.50 o -1 4 17 1211.05 1197.48 14.78 o 0 4 17 97.77 101.17 3.23 o -5 5 17 248.47 246.55 6.30 o -4 5 17 20.32 20.56 1.66 o -3 5 17 1203.95 1190.46 16.65 o -2 5 17 792.53 791.61 11.21 o -1 5 17 12.50 15.79 1.29 o 0 5 17 433.02 439.15 8.89 o -6 6 17 199.26 192.42 11.43 o -5 6 17 510.74 499.20 7.78 o -4 6 17 75.69 73.93 2.62 o -3 6 17 4.19 4.37 1.58 o -2 6 17 117.37 120.03 3.04 o -1 6 17 304.22 304.60 5.74 o 0 6 17 210.12 209.51 6.98 o -5 7 17 13.92 13.08 1.94 o -4 7 17 307.12 304.37 6.03 o -3 7 17 176.75 171.90 3.93 o -2 7 17 24.65 21.40 2.08 o 0 0 18 583.55 585.55 15.62 o -1 1 18 346.69 343.96 5.80 o 0 1 18 224.51 224.42 3.67 o -2 2 18 923.29 923.36 13.68 o -1 2 18 217.59 215.39 3.86 o 0 2 18 553.77 561.96 9.14 o -3 3 18 145.50 143.35 3.62 o -2 3 18 79.94 80.31 1.65 o -1 3 18 44.99 43.82 1.81 o 0 3 18 150.25 146.02 3.87 o -4 4 18 445.81 442.84 8.47 o -3 4 18 206.08 209.89 3.51 o -2 4 18 304.53 310.62 4.85 o -1 4 18 293.17 291.39 4.45 o 0 4 18 717.27 713.53 13.23 o -5 5 18 42.44 41.19 3.25 o -4 5 18 115.56 114.98 3.05 o -3 5 18 368.73 366.19 5.92 o -2 5 18 266.34 271.03 4.76 o -1 5 18 111.68 114.68 2.73 o 0 5 18 23.90 23.00 2.55 o -6 6 18 100.48 88.59 4.87 o -5 6 18 101.84 95.10 3.15 o -4 6 18 495.55 486.42 7.60 o -3 6 18 126.06 128.66 3.46 o -2 6 18 310.78 319.80 6.69 o -1 6 18 68.32 63.15 2.64 o 0 6 18 101.38 99.11 4.89 o -5 7 18 44.84 46.57 3.76 o -4 7 18 11.09 10.49 1.93 o -3 7 18 15.08 11.34 1.93 o -2 7 18 48.94 44.62 2.73 o 0 0 19 179.04 178.50 11.29 o -1 1 19 108.19 108.84 2.48 o 0 1 19 84.16 87.46 3.48 o -2 2 19 171.97 172.47 7.39 o -1 2 19 260.89 257.46 3.34 o 0 2 19 207.23 206.39 4.16 o -3 3 19 213.24 209.85 4.34 o -2 3 19 43.20 46.47 1.47 o -1 3 19 38.27 40.85 1.42 o 0 3 19 368.86 363.05 7.47 o -4 4 19 139.63 143.03 3.82 o -3 4 19 53.78 54.22 2.08 o -2 4 19 135.74 135.85 2.75 o -1 4 19 83.33 81.00 2.06 o 0 4 19 103.62 108.39 5.02 o -5 5 19 19.72 15.67 2.86 o -4 5 19 244.29 244.50 4.85 o -3 5 19 97.64 95.92 2.56 o -2 5 19 72.98 69.53 2.26 o -1 5 19 145.39 145.97 3.32 o 0 5 19 12.37 11.18 2.43 o -6 6 19 98.64 94.92 5.09 o -5 6 19 35.84 29.48 2.41 o -4 6 19 65.02 66.65 2.61 o -3 6 19 141.40 139.73 3.63 o -2 6 19 91.96 92.69 3.49 o -1 6 19 20.68 20.02 2.02 o 0 6 19 118.22 114.63 5.56 o -4 7 19 8.70 8.43 2.55 o -3 7 19 10.11 10.15 2.32 o 0 0 20 10010.90 9273.69 193.69 o -1 1 20 31.64 31.67 1.33 o 0 1 20 47.32 47.83 3.85 o -2 2 20 970.53 953.99 15.16 o -1 2 20 19.17 17.88 0.89 o 0 2 20 1187.23 1171.81 18.34 o -3 3 20 29.47 28.35 2.94 o -2 3 20 67.54 70.22 1.63 o -1 3 20 108.02 106.75 2.31 o 0 3 20 17.49 17.29 1.73 o -4 4 20 731.63 709.12 12.82 o -3 4 20 35.04 33.54 1.74 o -2 4 20 5995.90 5698.69 69.22 o -1 4 20 22.42 21.65 1.32 o 0 4 20 608.91 603.85 11.54 o -5 5 20 103.84 113.59 5.75 o -4 5 20 18.72 18.97 1.63 o -3 5 20 1.45 1.34 1.39 o -2 5 20 1.93 3.96 1.37 o -1 5 20 33.04 33.61 2.48 o 0 5 20 63.36 64.88 3.49 o -5 6 20 32.54 31.75 2.53 o -4 6 20 383.61 397.52 7.13 o -3 6 20 38.69 45.72 2.59 o -2 6 20 463.59 462.02 7.44 o -1 6 20 52.29 50.64 2.52 o 0 0 21 788.55 827.94 18.60 o -1 1 21 97.45 102.79 2.35 o 0 1 21 88.94 86.33 2.34 o -2 2 21 3512.36 3452.86 51.79 o -1 2 21 2.63 3.00 0.70 o 0 2 21 5660.00 5572.73 82.94 o -3 3 21 41.38 39.88 2.10 o -2 3 21 220.02 221.86 3.35 o -1 3 21 211.59 216.16 3.64 o 0 3 21 33.99 32.05 2.09 o -4 4 21 3529.72 3524.01 75.60 o -3 4 21 93.81 92.13 2.72 o -2 4 21 544.85 534.01 8.00 o -1 4 21 114.02 111.82 2.55 o 0 4 21 2201.15 2218.88 37.54 o -5 5 21 188.23 182.17 6.68 o -4 5 21 19.50 20.79 1.80 o -3 5 21 3.99 3.57 1.50 o -2 5 21 3.47 3.46 1.41 o -1 5 21 27.18 28.21 1.87 o 0 5 21 173.50 174.86 9.06 o -5 6 21 191.85 197.32 7.32 o -4 6 21 1406.56 1398.78 20.52 o -3 6 21 4.97 1.40 1.82 o -2 6 21 2270.63 2221.88 29.37 o -1 6 21 158.45 164.89 5.18 o 0 0 22 30.56 30.81 2.26 o -1 1 22 98.99 100.58 2.48 o 0 1 22 152.14 157.34 3.43 o -2 2 22 1420.18 1392.99 21.79 o -1 2 22 159.72 163.71 2.56 o 0 2 22 1388.64 1379.93 23.87 o -3 3 22 187.22 186.61 4.57 o -2 3 22 157.12 151.78 3.28 o -1 3 22 256.78 258.02 4.18 o 0 3 22 116.17 119.39 4.23 o -4 4 22 898.09 895.61 21.18 o -3 4 22 96.81 100.93 2.96 o -2 4 22 12.70 11.78 1.38 o -1 4 22 61.89 64.52 2.14 o 0 4 22 888.03 889.09 16.23 o -5 5 22 263.31 251.00 8.19 o -4 5 22 89.86 92.18 3.17 o -3 5 22 22.01 20.42 1.91 o -2 5 22 29.54 29.34 2.04 o -1 5 22 138.80 138.95 3.46 o 0 5 22 155.84 162.40 6.11 o -4 6 22 608.64 612.22 11.70 o -3 6 22 101.42 104.84 3.89 o -2 6 22 623.50 628.97 10.36 o 0 0 23 1009.08 1003.68 22.41 o -1 1 23 12.57 11.85 1.28 o 0 1 23 22.32 23.66 1.47 o -2 2 23 464.10 457.95 8.17 o -1 2 23 284.88 286.72 3.95 o 0 2 23 792.15 770.45 14.13 o -3 3 23 351.18 357.51 7.26 o -2 3 23 7.35 7.05 1.25 o -1 3 23 4.25 4.59 1.15 o 0 3 23 239.78 242.12 5.80 o -4 4 23 543.69 526.11 13.65 o -3 4 23 2.03 2.39 1.41 o -2 4 23 726.73 729.58 11.40 o -1 4 23 1.37 1.76 1.24 o 0 4 23 313.22 319.74 7.26 o -4 5 23 139.66 139.07 4.26 o -3 5 23 32.28 29.37 2.19 o -2 5 23 52.40 53.68 2.55 o -1 5 23 207.15 211.66 4.42 o 0 0 24 19.42 27.45 3.39 o -1 1 24 203.41 199.75 4.17 o 0 1 24 168.56 165.83 3.68 o -2 2 24 219.99 220.63 4.79 o -1 2 24 71.08 74.95 1.92 o 0 2 24 381.75 392.64 8.18 o -3 3 24 32.11 29.86 2.47 o -2 3 24 361.47 367.26 6.15 o -1 3 24 253.99 252.93 4.22 o 0 3 24 41.95 42.22 2.63 o -4 4 24 259.64 264.82 8.49 o -3 4 24 100.76 96.61 2.81 o -2 4 24 23.27 21.17 1.89 o -1 4 24 128.79 130.49 3.15 o 0 4 24 149.61 155.36 4.95 o -4 5 24 55.68 57.25 8.67 o -3 5 24 33.55 34.87 2.35 o -2 5 24 43.12 42.91 2.46 o -1 5 24 46.16 54.53 3.31 o 0 0 25 0.02 2.60 2.47 o -1 1 25 174.55 177.65 4.63 o 0 1 25 109.81 113.28 2.80 o -2 2 25 295.60 296.33 5.96 o -1 2 25 129.91 132.09 3.06 o 0 2 25 493.13 494.69 9.86 o -3 3 25 124.08 125.64 5.49 o -2 3 25 217.13 222.47 4.18 o -1 3 25 146.77 148.86 3.31 o 0 3 25 89.51 88.95 3.51 o -4 4 25 345.63 338.51 10.09 o -3 4 25 66.78 65.73 2.50 o -2 4 25 0.22 -0.52 1.64 o -1 4 25 103.61 106.68 3.09 o 0 4 25 209.59 226.26 6.88 o 0 0 26 4.42 3.11 2.59 o -1 1 26 421.47 426.46 7.38 o 0 1 26 484.20 494.21 9.66 o -2 2 26 1675.91 1668.71 25.94 o -1 2 26 31.82 32.95 1.70 o 0 2 26 949.01 954.05 17.20 o -3 3 26 29.30 32.06 3.72 o -2 3 26 603.03 601.86 8.63 o -1 3 26 697.96 686.89 9.85 o 0 3 26 19.89 22.97 2.43 o -3 4 26 268.61 260.23 6.04 o -2 4 26 6.26 8.36 2.04 o -1 4 26 232.23 235.21 4.86 o 0 0 27 91.06 84.00 5.53 o -1 1 27 164.70 168.32 3.98 o 0 1 27 195.25 194.85 5.95 o -2 2 27 188.73 194.34 7.59 o -1 2 27 531.87 532.53 7.51 o 0 2 27 293.82 292.94 7.87 o -3 3 27 576.38 596.67 17.81 o -2 3 27 179.45 189.15 4.14 o -1 3 27 182.16 187.75 4.00 o 0 3 27 423.50 440.88 9.30 o 0 0 28 27.94 29.58 5.38 o -1 1 28 78.67 84.28 3.20 o 0 1 28 115.44 114.25 4.55 o -2 2 28 594.21 614.37 15.50 o -1 2 28 457.81 461.33 6.76 o 0 2 28 1055.17 1056.45 21.69 o 0 0 29 98.82 114.11 21.13 o -1 1 29 5.02 10.34 2.47 o 0 1 29 4.01 3.80 2.64 o