#------------------------------------------------------------------------------ #$Date: 2016-07-13 04:28:23 +0300 (Wed, 13 Jul 2016) $ #$Revision: 184420 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/17/2241763.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241763 _cell_angle_alpha 90.000 _cell_angle_beta 107.032 _cell_angle_gamma 90.000 _cell_length_a 11.9423 _cell_length_b 12.1314 _cell_length_c 12.8974 _exptl_crystal_F_000 982.00 _reflns_d_resolution_high 0.7694 _cod_data_source_file su5299Isup3.hkl _cod_data_source_block I _shelx_title ' import in P 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 257.04 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -15 0 61.36 95.13 123.54 o 2 -15 0 283.89 224.49 232.56 o 3 -15 0 255.93 5.39 246.27 o 4 -15 0 22.15 138.56 259.49 o 0 -14 0 298.29 153.00 133.17 o 1 -14 0 427.39 565.86 134.50 o 2 -14 0 1228.64 1175.15 171.69 o 3 -14 0 517.94 504.54 247.99 o 4 -14 0 657.89 545.42 267.82 o 5 -14 0 748.11 528.78 173.57 o 6 -14 0 426.55 259.25 265.61 o 1 -13 0 1288.70 1366.09 154.17 o 2 -13 0 904.17 531.46 127.42 o 3 -13 0 730.20 651.99 130.73 o 4 -13 0 125.76 268.55 228.65 o 5 -13 0 162.04 28.64 140.76 o 6 -13 0 679.49 540.53 266.59 o 7 -13 0 353.33 264.63 224.98 o 8 -13 0 95.79 63.89 184.09 o 0 -12 0 2860.42 2381.95 222.77 o 1 -12 0 1120.25 1097.17 134.76 o 2 -12 0 495.31 411.20 150.80 o 3 -12 0 53.27 17.37 98.64 o 4 -12 0 288.32 360.84 134.89 o 5 -12 0 513.75 482.26 201.72 o 6 -12 0 168.21 194.37 166.96 o 7 -12 0 436.59 465.86 238.93 o 8 -12 0 505.54 582.39 224.24 o 9 -12 0 22.72 1.22 190.21 o 1 -11 0 1710.26 1787.34 110.80 o 2 -11 0 2059.60 2028.53 401.10 o 3 -11 0 1678.42 1626.79 147.73 o 4 -11 0 24.09 65.25 77.45 o 5 -11 0 1530.25 1556.71 249.21 o 6 -11 0 320.82 235.99 153.98 o 7 -11 0 774.80 1097.70 253.13 o 8 -11 0 53.33 76.38 245.05 o 9 -11 0 120.47 472.72 250.19 o 10 -11 0 156.23 401.72 314.82 o 0 -10 0 674.30 733.45 129.38 o 1 -10 0 2149.08 2439.82 123.75 o 2 -10 0 1737.32 1796.80 110.42 o 3 -10 0 820.13 888.41 84.25 o 4 -10 0 1917.72 1839.17 113.02 o 5 -10 0 173.42 167.08 126.13 o 6 -10 0 1546.28 1821.59 248.23 o 7 -10 0 61.52 18.61 120.20 o 8 -10 0 147.51 188.74 152.76 o 9 -10 0 894.71 868.57 198.54 o 10 -10 0 329.77 335.14 191.19 o 11 -10 0 204.46 409.07 242.85 o 1 -9 0 2110.45 2263.24 117.24 o 2 -9 0 627.18 623.98 63.06 o 3 -9 0 850.78 886.98 67.26 o 4 -9 0 468.03 525.79 74.45 o 5 -9 0 629.25 563.40 163.04 o 6 -9 0 2340.06 2770.45 309.19 o 7 -9 0 806.83 772.60 234.03 o 8 -9 0 1231.54 1032.34 266.59 o 9 -9 0 627.35 462.44 212.49 o 10 -9 0 84.97 322.41 251.41 o 11 -9 0 188.15 195.60 184.58 o 0 -8 0 8814.75 8984.83 293.22 o 1 -8 0 2585.31 2744.38 102.18 o 2 -8 0 940.63 908.02 67.80 o 3 -8 0 2947.12 3307.90 99.09 o 4 -8 0 3140.22 3278.63 100.40 o 5 -8 0 3981.33 4242.71 331.22 o 6 -8 0 1365.61 1167.72 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237.77 80.22 o 12 0 0 65.07 107.48 88.13 o 13 0 0 197.76 278.01 107.45 o 14 0 0 225.43 13.46 230.12 o 2 1 0 3616.81 2904.09 105.32 o 3 1 0 8570.45 9094.89 240.98 o 4 1 0 6147.97 5881.36 177.49 o 5 1 0 13506.43 14053.36 487.17 o 6 1 0 4938.50 5857.72 141.45 o 7 1 0 12645.01 14124.21 475.88 o 8 1 0 4015.69 4677.71 229.99 o 9 1 0 1833.55 2148.08 81.60 o 10 1 0 849.40 930.12 62.17 o 11 1 0 97.91 29.33 65.56 o 12 1 0 1357.96 1317.85 139.05 o 13 1 0 842.88 1050.37 141.92 o 14 1 0 347.07 464.73 229.63 o 0 2 0 2566.21 2535.94 105.02 o 1 2 0 3423.32 3132.14 148.76 o 2 2 0 26278.35 26762.40 415.16 o 3 2 0 9316.98 9420.80 330.68 o 4 2 0 38002.86 35652.48 1238.76 o 5 2 0 1268.56 1132.61 70.49 o 6 2 0 10201.32 9948.44 420.42 o 7 2 0 2030.05 2215.22 110.43 o 8 2 0 34.40 31.40 32.57 o 9 2 0 1834.72 1839.33 74.91 o 10 2 0 1039.59 1511.13 137.80 o 11 2 0 699.56 702.95 242.85 o 12 2 0 736.89 724.40 181.28 o 13 2 0 98.25 249.41 108.49 o 14 2 0 339.05 282.52 143.58 o 1 3 0 7180.38 7377.27 257.84 o 2 3 0 25092.05 23381.08 461.22 o 3 3 0 15080.26 16087.83 356.88 o 4 3 0 314.17 310.02 43.54 o 5 3 0 4279.27 4516.28 186.58 o 6 3 0 3662.72 3919.75 124.95 o 7 3 0 185.70 138.35 61.60 o 8 3 0 834.55 789.21 60.67 o 9 3 0 3525.53 3660.81 335.89 o 10 3 0 1266.60 1437.91 131.23 o 11 3 0 2244.92 2061.86 208.33 o 12 3 0 309.52 298.62 220.94 o 13 3 0 38.44 59.52 109.00 o 14 3 0 161.77 222.77 162.55 o 0 4 0 12015.18 11546.10 505.15 o 1 4 0 648.42 758.18 35.12 o 2 4 0 13811.05 14028.16 365.96 o 3 4 0 2413.03 2296.73 56.43 o 4 4 0 1747.52 1786.85 51.44 o 5 4 0 3499.05 4130.46 169.09 o 6 4 0 1836.72 1736.54 112.48 o 7 4 0 2436.47 2537.44 155.92 o 8 4 0 2395.33 2794.85 135.69 o 9 4 0 777.76 664.56 137.31 o 10 4 0 2080.97 2032.09 166.71 o 11 4 0 531.34 470.74 90.82 o 12 4 0 319.18 493.47 131.36 o 13 4 0 580.55 371.20 140.42 o 14 4 0 44.42 108.69 185.07 o 1 5 0 1578.51 1608.49 67.67 o 2 5 0 1645.83 1434.47 64.48 o 3 5 0 1940.09 1922.52 125.65 o 4 5 0 1659.09 1879.89 76.19 o 5 5 0 2192.16 2119.98 116.16 o 6 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