#------------------------------------------------------------------------------ #$Date: 2016-08-27 04:28:36 +0300 (Sat, 27 Aug 2016) $ #$Revision: 186043 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/18/2241826.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241826 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.2517 _cell_length_b 16.4240 _cell_length_c 31.1181 _exptl_crystal_F_000 2800.00 _reflns_d_resolution_high 0.7692 _cod_data_source_file hb7606Isup2.hkl _cod_data_source_block I _shelx_title ' d1585_a.res in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 401.80 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 35655.39 36420.38 1154.66 o 6 0 0 27488.88 26252.43 931.86 o 8 0 0 163.25 600.38 210.90 o 10 0 0 112.79 91.84 227.90 o 12 0 0 300.12 695.62 295.94 o 14 0 0 262.28 632.69 345.26 o 1 1 0 23025.28 23579.71 488.27 o 2 1 0 6386.33 6423.17 205.79 o 3 1 0 54740.80 57079.27 1722.72 o 4 1 0 751.23 713.83 115.65 o 5 1 0 6064.51 6008.34 283.10 o 6 1 0 786.95 846.52 128.53 o 7 1 0 22604.04 23379.24 619.06 o 8 1 0 52.07 57.21 127.78 o 9 1 0 1599.06 1664.63 255.12 o 10 1 0 1706.13 1946.18 229.78 o 11 1 0 3081.58 2911.57 273.41 o 12 1 0 3500.52 3505.95 457.51 o 13 1 0 1372.26 1349.72 319.75 o 14 1 0 629.84 606.09 235.80 o 0 2 0 57857.62 58035.11 1697.21 o 1 2 0 23333.69 23282.23 356.74 o 2 2 0 35434.27 36452.31 761.71 o 3 2 0 5902.21 6129.40 191.48 o 4 2 0 41647.50 41777.49 904.42 o 5 2 0 20.26 6.69 50.53 o 6 2 0 13362.31 12622.87 279.04 o 7 2 0 14417.30 14609.10 322.41 o 8 2 0 8968.71 8601.61 228.80 o 9 2 0 273.62 259.47 85.16 o 10 2 0 2917.98 3068.46 267.95 o 11 2 0 5398.75 5187.35 343.13 o 12 2 0 244.29 301.42 186.33 o 13 2 0 1941.31 1583.13 262.96 o 14 2 0 4329.63 4487.85 568.06 o 1 3 0 78254.73 80400.38 1173.24 o 2 3 0 10498.49 11274.67 210.59 o 3 3 0 3051.70 3266.42 119.37 o 4 3 0 31844.62 31012.49 708.41 o 5 3 0 626.48 827.41 80.55 o 6 3 0 9394.48 9102.06 231.35 o 7 3 0 12074.15 11622.71 293.63 o 8 3 0 39193.00 38117.41 729.64 o 9 3 0 621.50 603.47 120.59 o 10 3 0 3306.74 3577.98 273.34 o 11 3 0 1504.06 2002.92 364.82 o 12 3 0 1862.53 1933.98 256.61 o 13 3 0 1059.57 1397.87 387.78 o 14 3 0 3081.77 2176.83 457.51 o 0 4 0 130525.22 122694.86 10702.77 o 1 4 0 423.95 385.06 68.82 o 2 4 0 10391.60 10765.78 216.29 o 3 4 0 17275.46 16426.63 292.90 o 4 4 0 3058.51 3113.66 109.96 o 5 4 0 50.00 148.54 94.39 o 6 4 0 10022.39 10367.84 258.58 o 7 4 0 12121.00 11975.01 295.31 o 8 4 0 1883.37 2185.94 137.32 o 9 4 0 149.74 158.45 70.91 o 10 4 0 376.79 413.39 164.49 o 11 4 0 1718.39 1938.85 232.52 o 12 4 0 2639.43 1807.76 432.00 o 13 4 0 2879.70 3142.71 513.64 o 14 4 0 903.98 807.87 408.19 o 1 5 0 16.94 58.39 57.04 o 2 5 0 530.53 309.97 62.86 o 3 5 0 3740.43 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