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Information card for entry 2242048
Preview
| Coordinates | 2242048.cif |
|---|---|
| Structure factors | 2242048.hkl |
| Original IUCr paper | HTML |
| Chemical name | 1,2-Di-<i>tert</i>-butyl-1,1,2,2-tetraphenyldisilane |
|---|---|
| Formula | C32 H38 Si2 |
| Calculated formula | C32 H38 Si2 |
| Title of publication | Crystal structures of three sterically congested disilanes |
| Authors of publication | Pichaandi, Kothanda Rama; Mague, Joel T.; Fink, Mark J. |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2017 |
| Journal volume | 73 |
| Journal issue | 3 |
| Pages of publication | 448 - 452 |
| a | 8.5622 ± 0.0005 Å |
| b | 10.2107 ± 0.0006 Å |
| c | 15.4586 ± 0.001 Å |
| α | 90° |
| β | 95.452 ± 0.001° |
| γ | 90° |
| Cell volume | 1345.37 ± 0.14 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0418 |
| Residual factor for significantly intense reflections | 0.0344 |
| Weighted residual factors for significantly intense reflections | 0.0875 |
| Weighted residual factors for all reflections included in the refinement | 0.092 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 192759 (current) | 2017-03-02 | cif/ hkl/ Adding structures of 2242046, 2242047, 2242048 via cif-deposit CGI script. |
2242048.cif 2242048.hkl |
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