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Information card for entry 2242192
Preview
| Coordinates | 2242192.cif |
|---|---|
| Structure factors | 2242192.hkl |
| Original IUCr paper | HTML |
| Chemical name | <i>cis</i>-(<i>N</i>-{2-[2,6-bis(propan-2-yl)phenylimino]pentan-3-ylidene}-\ 2,6-bis(propan-2-yl)aniline)dichloridopalladium(II) 1,2-dichloroethane monosolvate |
|---|---|
| Formula | C31 H46 Cl4 N2 Pd |
| Calculated formula | C31 H46 Cl4 N2 Pd |
| Title of publication | Crystal structure of unsymmetrical α-diimine palladium(II) complex <i>cis</i>-[{ArN=C(Me)‒(Et)C=NAr}PdCl~2~] [Ar = 2,6-(iPr)~2~C~6~H~3~] |
| Authors of publication | Ellandula, Shravan Kumar; Opoku Amoako, Cosmos; Mague, Joel T.; Chandrasekaran, Perumalreddy |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2017 |
| Journal volume | 73 |
| Journal issue | 8 |
| Pages of publication | 1148 - 1150 |
| a | 8.7203 ± 0.0012 Å |
| b | 20.124 ± 0.003 Å |
| c | 19.526 ± 0.003 Å |
| α | 90° |
| β | 100.405 ± 0.002° |
| γ | 90° |
| Cell volume | 3370.2 ± 0.9 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0526 |
| Residual factor for significantly intense reflections | 0.0362 |
| Weighted residual factors for significantly intense reflections | 0.0763 |
| Weighted residual factors for all reflections included in the refinement | 0.0841 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 199162 (current) | 2017-07-25 | cif/ hkl/ Adding structures of 2242192 via cif-deposit CGI script. |
2242192.cif 2242192.hkl |
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Users of the data should acknowledge the original authors of the
structural data.