#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:43:29 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199173 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/22/2242207.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242207 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7876 _cell_length_b 19.4656 _cell_length_c 21.7879 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.6988 _cod_data_source_file ld2140IIIsup4.hkl _cod_data_source_block III _shelx_title ' III in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 220.71 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20174.91 19564.60 199.99 o 4 0 0 228.86 255.75 27.20 o 6 0 0 1896.13 2101.95 73.13 o 8 0 0 345.97 273.30 69.31 o 10 0 0 795.56 747.76 161.16 o 2 1 0 849.06 1008.81 21.45 o 4 1 0 15.18 -3.05 7.92 o 6 1 0 1539.57 1619.12 61.10 o 8 1 0 678.02 590.03 67.06 o 10 1 0 79.61 147.31 48.89 o 0 2 0 45.68 26.65 4.83 o 2 2 0 10646.19 10064.91 103.38 o 4 2 0 3819.80 3880.33 85.71 o 6 2 0 1933.72 1814.50 92.32 o 8 2 0 250.63 232.03 47.22 o 10 2 0 331.52 395.96 64.96 o 2 3 0 13187.10 12381.56 196.29 o 4 3 0 2880.12 3237.89 73.27 o 6 3 0 6571.68 6519.24 126.38 o 8 3 0 66.21 0.22 30.44 o 10 3 0 413.42 393.15 77.08 o 0 4 0 20457.62 19513.46 230.79 o 2 4 0 452.68 392.91 17.00 o 4 4 0 4962.74 5206.49 97.31 o 6 4 0 93.67 67.20 23.11 o 8 4 0 1423.46 1503.10 115.58 o 10 4 0 23.36 52.81 39.27 o 2 5 0 1560.54 1384.39 33.73 o 4 5 0 2363.49 2276.87 64.41 o 6 5 0 410.92 454.98 41.73 o 8 5 0 56.62 63.63 35.60 o 10 5 0 252.11 206.10 56.92 o 0 6 0 20558.01 19253.34 245.18 o 2 6 0 140.49 88.99 13.59 o 4 6 0 5025.07 4921.98 67.26 o 6 6 0 239.68 194.36 33.20 o 8 6 0 91.42 45.77 34.94 o 10 6 0 39.91 29.10 39.81 o 2 7 0 280.93 260.36 20.45 o 4 7 0 5902.10 5498.73 85.95 o 6 7 0 111.51 75.93 25.78 o 8 7 0 246.89 251.94 47.90 o 10 7 0 322.73 254.53 59.94 o 0 8 0 19.73 -1.65 15.53 o 2 8 0 26.02 60.01 13.40 o 4 8 0 15.90 28.93 13.35 o 6 8 0 1372.08 1383.21 83.00 o 8 8 0 46.61 22.60 30.62 o 10 8 0 248.33 219.44 55.39 o 2 9 0 4914.64 4977.13 81.63 o 4 9 0 104.58 125.64 20.59 o 6 9 0 314.61 246.31 36.70 o 8 9 0 283.69 232.96 48.83 o 10 9 0 4.48 -26.07 37.48 o 0 10 0 1880.85 2097.25 70.79 o 2 10 0 11510.76 11526.31 141.74 o 4 10 0 3280.08 3053.38 69.78 o 6 10 0 277.99 247.03 36.48 o 8 10 0 256.68 281.02 52.39 o 10 10 0 173.05 173.39 55.86 o 2 11 0 571.25 703.89 40.60 o 4 11 0 4591.66 4677.55 91.01 o 6 11 0 244.17 205.78 36.44 o 8 11 0 0.02 -4.31 45.21 o 10 11 0 268.99 169.37 51.74 o 0 12 0 3517.48 3444.52 100.31 o 2 12 0 320.55 354.99 30.31 o 4 12 0 95.02 112.27 22.84 o 6 12 0 897.18 823.01 62.24 o 8 12 0 27.23 -19.81 24.20 o 10 12 0 2.77 -32.90 44.90 o 2 13 0 129.13 56.84 21.03 o 4 13 0 1880.09 1706.79 60.01 o 6 13 0 124.23 88.88 31.06 o 8 13 0 732.11 722.56 66.14 o 0 14 0 736.35 729.90 59.00 o 2 14 0 8897.93 8571.29 132.56 o 4 14 0 0.63 -4.13 17.17 o 6 14 0 143.50 131.66 32.88 o 8 14 0 263.55 206.14 43.37 o 2 15 0 8231.02 7859.91 129.17 o 4 15 0 86.71 119.49 24.97 o 6 15 0 635.42 764.62 62.15 o 8 15 0 218.51 178.87 48.70 o 0 16 0 184.18 165.84 37.04 o 2 16 0 1.61 -11.17 20.42 o 4 16 0 564.40 631.27 46.35 o 6 16 0 358.01 356.90 47.34 o 8 16 0 158.75 184.24 47.91 o 2 17 0 744.42 744.73 48.94 o 4 17 0 28.91 -18.31 18.31 o 6 17 0 1029.33 1154.94 78.04 o 8 17 0 1403.43 1606.05 136.84 o 0 18 0 14.00 86.66 69.87 o 2 18 0 6.15 -7.25 17.69 o 4 18 0 0.08 -17.81 17.81 o 6 18 0 1393.41 1381.57 99.86 o 8 18 0 1.78 27.77 61.63 o 2 19 0 31.28 48.98 25.32 o 4 19 0 516.58 542.96 47.55 o 6 19 0 3.22 -39.22 56.12 o 8 19 0 5.79 -8.28 58.73 o 0 20 0 783.29 794.68 76.58 o 2 20 0 92.36 96.64 28.81 o 4 20 0 156.11 214.63 45.01 o 6 20 0 680.24 595.24 84.22 o 2 21 0 580.60 608.95 55.93 o 4 21 0 50.80 2.15 34.03 o 6 21 0 75.29 51.30 48.24 o 0 22 0 64.31 53.97 44.31 o 2 22 0 680.69 725.09 62.30 o 4 22 0 0.22 -8.09 36.31 o 6 22 0 232.42 258.94 66.35 o 2 23 0 21.86 16.79 34.26 o 4 23 0 375.45 385.48 70.62 o 6 23 0 62.90 65.80 71.73 o 0 24 0 3668.38 4354.63 367.10 o 2 24 0 1052.93 1230.98 116.58 o 4 24 0 28.67 68.66 68.10 o 2 25 0 57.31 24.33 58.34 o 4 25 0 271.33 307.98 87.52 o 0 26 0 15.03 184.39 103.93 o 2 26 0 132.38 135.99 65.01 o 2 27 0 2.79 -38.36 102.29 o 1 1 1 20682.59 18839.01 153.36 o 2 1 1 16243.15 15733.86 99.51 o 3 1 1 3738.90 3848.97 34.11 o 4 1 1 304.09 281.98 12.47 o 5 1 1 94.72 87.87 9.43 o 6 1 1 318.12 377.00 20.33 o 7 1 1 43.32 56.20 21.69 o 8 1 1 181.04 162.11 30.56 o 9 1 1 175.20 156.66 31.88 o 10 1 1 0.55 4.00 25.96 o 11 1 1 81.14 90.49 34.90 o 0 2 1 9170.47 8626.24 52.00 o 1 2 1 2794.70 2624.91 21.36 o 2 2 1 1924.71 2014.72 25.98 o 3 2 1 548.64 533.69 15.19 o 4 2 1 133.95 155.31 11.18 o 5 2 1 4.20 12.20 8.57 o 6 2 1 185.47 172.05 18.84 o 7 2 1 1535.16 1501.91 65.32 o 8 2 1 254.90 144.88 29.72 o 9 2 1 53.27 73.53 26.55 o 10 2 1 1067.45 1132.48 70.67 o 11 2 1 12.77 3.19 38.62 o 1 3 1 1320.12 1238.99 15.44 o 2 3 1 17918.87 17572.10 137.70 o 3 3 1 1302.84 1389.77 23.35 o 4 3 1 204.53 301.93 15.62 o 5 3 1 706.37 735.65 33.83 o 6 3 1 706.24 708.02 34.64 o 7 3 1 35.44 25.06 19.81 o 8 3 1 16.65 57.57 23.95 o 9 3 1 50.15 36.79 27.36 o 10 3 1 224.49 264.50 40.00 o 11 3 1 90.70 75.46 34.11 o 0 4 1 10080.95 9557.61 83.66 o 1 4 1 1071.73 1032.74 17.92 o 2 4 1 28130.83 26708.88 153.68 o 3 4 1 182.59 190.98 11.52 o 4 4 1 1747.32 1861.43 28.84 o 5 4 1 411.27 452.05 26.65 o 6 4 1 1920.61 1983.56 49.18 o 7 4 1 1109.56 1051.39 54.18 o 8 4 1 221.45 210.78 32.84 o 9 4 1 36.41 12.24 24.09 o 10 4 1 24.77 -12.43 33.02 o 1 5 1 916.29 889.28 18.10 o 2 5 1 3107.70 2897.55 35.36 o 3 5 1 178.76 197.22 10.84 o 4 5 1 1185.46 1286.18 25.40 o 5 5 1 12.85 19.79 12.37 o 6 5 1 3220.02 3206.85 63.38 o 7 5 1 192.16 199.71 27.35 o 8 5 1 210.31 223.97 33.49 o 9 5 1 24.76 21.37 24.61 o 10 5 1 4.24 53.16 28.69 o 0 6 1 7533.92 6987.29 82.12 o 1 6 1 4271.74 4166.28 43.03 o 2 6 1 33.94 42.13 7.98 o 3 6 1 208.26 268.25 14.63 o 4 6 1 25.12 36.64 10.75 o 5 6 1 236.75 237.64 21.33 o 6 6 1 531.63 558.99 33.29 o 7 6 1 17.58 23.62 15.52 o 8 6 1 8.82 -10.16 20.20 o 9 6 1 19.45 52.21 25.68 o 10 6 1 6.44 1.31 30.20 o 1 7 1 1080.23 1018.21 21.84 o 2 7 1 4277.32 4462.54 52.09 o 3 7 1 607.70 638.08 25.40 o 4 7 1 1350.43 1208.73 27.35 o 5 7 1 158.88 127.26 18.49 o 6 7 1 128.41 97.35 19.15 o 7 7 1 166.19 156.10 22.86 o 8 7 1 221.73 196.50 31.34 o 9 7 1 24.25 71.49 26.36 o 10 7 1 94.83 132.63 35.38 o 0 8 1 1885.04 2153.31 45.70 o 1 8 1 0.08 -6.40 6.40 o 2 8 1 422.72 471.56 19.80 o 3 8 1 6.83 -4.64 8.23 o 4 8 1 785.01 810.40 26.29 o 5 8 1 1.69 11.36 10.29 o 6 8 1 1136.16 996.13 44.02 o 7 8 1 6.63 4.55 16.97 o 8 8 1 399.02 412.22 40.62 o 9 8 1 121.85 86.36 29.92 o 10 8 1 71.01 85.51 32.51 o 1 9 1 383.38 399.57 18.42 o 2 9 1 2477.00 2511.28 39.72 o 3 9 1 2215.83 2200.37 39.00 o 4 9 1 0.60 11.72 9.65 o 5 9 1 31.29 45.18 10.38 o 6 9 1 1166.46 1063.92 46.42 o 7 9 1 514.54 494.80 35.25 o 8 9 1 17.22 -20.23 20.23 o 9 9 1 55.05 96.00 29.67 o 10 9 1 16.99 -26.08 26.08 o 0 10 1 4596.83 4511.80 75.91 o 1 10 1 781.32 813.84 25.64 o 2 10 1 6649.45 6547.44 70.56 o 3 10 1 1952.24 1887.57 37.71 o 4 10 1 724.79 726.62 28.40 o 5 10 1 71.39 70.75 16.92 o 6 10 1 2.12 -13.65 13.65 o 7 10 1 8.32 -3.90 16.26 o 8 10 1 68.14 82.00 26.87 o 9 10 1 2.43 -21.82 21.82 o 10 10 1 94.99 77.47 32.27 o 1 11 1 16.71 26.73 11.11 o 2 11 1 1577.71 1580.78 34.30 o 3 11 1 262.53 297.57 19.92 o 4 11 1 96.23 64.68 13.78 o 5 11 1 9.02 -0.44 14.04 o 6 11 1 29.96 14.41 15.97 o 7 11 1 581.38 550.65 40.42 o 8 11 1 22.09 -3.44 20.04 o 9 11 1 211.39 173.00 34.39 o 10 11 1 0.70 19.34 38.25 o 0 12 1 1723.64 1758.27 50.20 o 1 12 1 328.95 312.52 19.56 o 2 12 1 2600.89 2835.94 47.69 o 3 12 1 357.11 369.48 22.46 o 4 12 1 25.63 42.05 12.74 o 5 12 1 60.18 30.32 16.02 o 6 12 1 500.20 525.56 37.02 o 7 12 1 43.70 54.21 20.25 o 8 12 1 260.17 284.68 32.39 o 9 12 1 744.72 789.62 58.35 o 10 12 1 162.00 152.31 49.76 o 1 13 1 433.30 426.22 23.07 o 2 13 1 504.79 596.26 27.37 o 3 13 1 2480.58 2394.19 47.03 o 4 13 1 3429.44 3401.71 57.96 o 5 13 1 422.38 395.95 30.40 o 6 13 1 717.23 735.89 41.64 o 7 13 1 28.52 17.54 18.60 o 8 13 1 507.47 500.17 39.37 o 9 13 1 109.90 208.73 39.91 o 0 14 1 266.50 237.35 25.91 o 1 14 1 1.78 -10.29 10.29 o 2 14 1 2013.70 1969.53 42.80 o 3 14 1 2235.35 2187.74 46.31 o 4 14 1 2380.61 2347.81 49.33 o 5 14 1 7.07 1.82 15.07 o 6 14 1 357.31 368.30 32.30 o 7 14 1 24.41 13.54 18.64 o 8 14 1 6.24 -18.73 18.73 o 9 14 1 42.40 35.61 38.20 o 1 15 1 1573.98 1448.38 37.53 o 2 15 1 1378.31 1270.92 39.10 o 3 15 1 1129.10 1116.20 38.70 o 4 15 1 766.73 785.10 37.38 o 5 15 1 362.77 321.01 29.63 o 6 15 1 140.65 167.13 25.54 o 7 15 1 0.19 33.45 20.16 o 8 15 1 340.93 383.63 39.45 o 9 15 1 449.72 422.08 64.38 o 0 16 1 867.25 829.67 48.33 o 1 16 1 5.70 10.54 12.37 o 2 16 1 369.05 396.42 25.51 o 3 16 1 136.87 139.30 19.88 o 4 16 1 19.32 58.24 18.12 o 5 16 1 461.36 499.45 40.67 o 6 16 1 344.56 344.64 32.61 o 7 16 1 35.21 39.20 22.44 o 8 16 1 165.67 124.28 32.63 o 9 16 1 1.11 46.37 39.38 o 1 17 1 1.41 -8.04 12.79 o 2 17 1 128.01 118.07 16.95 o 3 17 1 431.14 444.27 28.30 o 4 17 1 76.07 80.62 18.57 o 5 17 1 365.48 376.19 32.75 o 6 17 1 108.40 103.60 26.31 o 7 17 1 274.61 311.68 39.01 o 8 17 1 18.75 -8.74 25.09 o 0 18 1 707.75 768.57 49.14 o 1 18 1 0.04 19.57 13.23 o 2 18 1 6.32 15.02 13.25 o 3 18 1 1187.44 1200.86 45.51 o 4 18 1 76.34 44.10 16.97 o 5 18 1 0.02 -16.19 16.19 o 6 18 1 4.09 33.33 25.55 o 7 18 1 15.90 8.87 36.21 o 8 18 1 5.77 16.56 31.86 o 1 19 1 486.75 486.81 29.16 o 2 19 1 19.79 5.88 14.86 o 3 19 1 63.21 53.75 18.68 o 4 19 1 154.75 137.47 24.01 o 5 19 1 4.79 6.59 22.25 o 6 19 1 41.64 37.84 30.87 o 7 19 1 3.18 -27.20 30.26 o 8 19 1 32.07 28.84 33.04 o 0 20 1 89.21 102.63 25.19 o 1 20 1 12.62 10.44 15.48 o 2 20 1 216.21 270.51 26.96 o 3 20 1 28.81 31.53 17.86 o 4 20 1 158.52 191.77 31.13 o 5 20 1 182.13 139.16 33.16 o 6 20 1 14.14 -18.94 24.86 o 7 20 1 90.18 81.16 35.38 o 1 21 1 75.84 74.18 20.83 o 2 21 1 11.35 21.66 16.86 o 3 21 1 4.19 0.49 19.49 o 4 21 1 0.09 26.41 24.75 o 5 21 1 2.87 4.33 29.55 o 6 21 1 172.63 137.30 40.00 o 7 21 1 10.27 52.62 33.82 o 0 22 1 34.52 4.79 25.41 o 1 22 1 0.43 -21.73 21.73 o 2 22 1 456.70 525.99 41.62 o 3 22 1 71.56 57.09 22.83 o 4 22 1 22.55 35.49 27.34 o 5 22 1 21.15 -21.61 29.19 o 6 22 1 78.22 173.24 40.33 o 1 23 1 10.85 28.86 22.32 o 2 23 1 9.61 -1.54 21.49 o 3 23 1 39.66 43.46 26.75 o 4 23 1 21.91 16.33 43.11 o 5 23 1 11.72 34.51 33.42 o 6 23 1 32.48 -32.15 50.68 o 0 24 1 88.59 137.07 42.80 o 1 24 1 117.34 108.08 32.35 o 2 24 1 34.06 -8.04 27.53 o 3 24 1 1.31 25.78 28.93 o 4 24 1 18.23 -10.29 45.21 o 5 24 1 95.66 119.54 46.19 o 1 25 1 4.44 -24.36 24.36 o 2 25 1 88.27 52.61 33.66 o 3 25 1 90.58 124.84 46.93 o 4 25 1 10.11 -37.40 37.40 o 0 26 1 1017.71 1163.89 139.17 o 1 26 1 16.77 -4.34 41.91 o 2 26 1 0.02 60.37 33.64 o 3 26 1 137.73 176.53 62.27 o 1 27 1 39.15 -14.10 115.31 o 2 27 1 0.02 90.14 49.13 o 0 0 2 15668.42 14191.01 188.62 o 1 0 2 11644.57 10904.27 82.53 o 2 0 2 47.66 29.96 8.36 o 3 0 2 3873.41 4140.85 68.88 o 4 0 2 1727.22 1839.73 42.35 o 5 0 2 3.58 10.86 14.84 o 6 0 2 2721.37 2631.41 56.98 o 7 0 2 700.92 639.56 62.14 o 8 0 2 231.30 264.73 48.83 o 9 0 2 328.81 469.60 65.08 o 10 0 2 4.57 -32.42 39.36 o 11 0 2 164.93 70.38 47.35 o 1 1 2 11355.75 10061.96 74.16 o 2 1 2 26188.23 24256.61 136.95 o 3 1 2 2614.57 2781.68 29.99 o 4 1 2 421.11 422.52 15.25 o 5 1 2 0.34 8.77 9.07 o 6 1 2 242.53 281.69 20.36 o 7 1 2 163.47 133.62 25.72 o 8 1 2 24.91 9.74 22.17 o 9 1 2 104.34 48.32 33.30 o 10 1 2 15.81 25.71 26.54 o 11 1 2 159.76 146.83 38.41 o 0 2 2 8900.00 8329.94 94.98 o 1 2 2 71.54 33.79 4.22 o 2 2 2 9036.23 9163.00 62.44 o 3 2 2 423.42 386.08 16.47 o 4 2 2 50.56 26.34 9.13 o 5 2 2 851.15 900.37 28.43 o 6 2 2 444.88 483.82 27.45 o 7 2 2 88.35 70.87 22.87 o 8 2 2 8.06 -19.60 19.60 o 9 2 2 15.39 9.08 22.79 o 10 2 2 400.46 367.57 45.97 o 11 2 2 393.10 408.14 49.66 o 1 3 2 3962.57 3644.46 28.54 o 2 3 2 574.90 522.29 19.36 o 3 3 2 17.91 10.49 8.55 o 4 3 2 975.64 982.62 30.17 o 5 3 2 63.44 84.00 12.39 o 6 3 2 95.10 105.93 17.20 o 7 3 2 90.57 104.34 21.85 o 8 3 2 23.16 7.85 22.02 o 9 3 2 48.98 20.80 24.55 o 10 3 2 18.62 38.83 27.77 o 11 3 2 7.30 -4.76 30.09 o 0 4 2 14856.88 14167.55 112.39 o 1 4 2 12649.02 12033.51 73.36 o 2 4 2 14473.63 14184.76 92.64 o 3 4 2 56.34 72.26 9.90 o 4 4 2 4668.66 4803.32 61.74 o 5 4 2 120.19 213.80 19.23 o 6 4 2 1517.06 1494.40 59.11 o 7 4 2 1309.74 1324.35 53.90 o 8 4 2 0.76 31.08 22.73 o 9 4 2 510.22 473.19 45.39 o 10 4 2 10.95 65.57 31.73 o 1 5 2 8449.37 7853.57 61.57 o 2 5 2 1441.02 1352.76 23.95 o 3 5 2 3174.66 3404.24 37.85 o 4 5 2 6155.77 6328.35 71.13 o 5 5 2 319.04 358.28 19.06 o 6 5 2 25.51 28.31 15.62 o 7 5 2 17.53 13.92 16.85 o 8 5 2 346.55 349.35 38.12 o 9 5 2 372.56 322.63 39.71 o 10 5 2 74.35 82.80 32.27 o 0 6 2 48714.42 46549.75 416.63 o 1 6 2 86.76 84.57 8.46 o 2 6 2 79.84 149.72 11.10 o 3 6 2 3202.59 3380.68 43.31 o 4 6 2 1880.41 1842.26 37.38 o 5 6 2 350.83 371.34 21.36 o 6 6 2 793.70 843.09 39.87 o 7 6 2 3.75 30.71 15.96 o 8 6 2 4.67 9.56 21.21 o 9 6 2 19.98 11.74 23.03 o 10 6 2 63.67 74.48 30.72 o 1 7 2 4836.72 4717.55 51.46 o 2 7 2 1316.08 1386.14 26.74 o 3 7 2 997.16 880.79 27.88 o 4 7 2 1895.47 1912.50 32.17 o 5 7 2 1307.79 1475.29 36.44 o 6 7 2 38.53 51.32 16.11 o 7 7 2 26.52 38.93 21.10 o 8 7 2 489.45 529.88 45.01 o 9 7 2 31.78 50.77 25.62 o 10 7 2 5.26 23.82 28.71 o 0 8 2 15120.45 15301.86 154.78 o 1 8 2 9.68 16.66 7.28 o 2 8 2 255.21 280.21 15.87 o 3 8 2 200.21 253.53 16.60 o 4 8 2 127.00 112.24 13.10 o 5 8 2 1698.82 1694.74 39.62 o 6 8 2 1.44 3.87 15.15 o 7 8 2 12.51 -3.34 19.68 o 8 8 2 297.75 307.29 37.05 o 9 8 2 22.70 31.86 25.16 o 10 8 2 58.66 0.87 35.91 o 1 9 2 2815.41 2958.09 41.20 o 2 9 2 1140.48 1150.90 27.24 o 3 9 2 160.33 128.96 13.71 o 4 9 2 250.20 273.27 18.40 o 5 9 2 59.47 30.02 12.66 o 6 9 2 163.99 142.15 21.42 o 7 9 2 25.31 -14.31 15.24 o 8 9 2 223.64 198.91 31.80 o 9 9 2 35.01 17.98 24.81 o 10 9 2 14.43 90.94 31.87 o 0 10 2 3951.43 4214.02 80.63 o 1 10 2 272.52 389.46 19.14 o 2 10 2 121.90 96.77 12.78 o 3 10 2 756.00 751.87 27.54 o 4 10 2 1607.78 1565.31 39.60 o 5 10 2 219.38 198.60 26.34 o 6 10 2 113.99 108.41 20.89 o 7 10 2 474.85 463.74 35.43 o 8 10 2 13.52 -18.43 18.43 o 9 10 2 117.43 91.65 29.19 o 10 10 2 6.14 -20.66 30.64 o 1 11 2 85.07 67.00 11.38 o 2 11 2 167.50 192.32 19.40 o 3 11 2 1063.86 1071.27 32.97 o 4 11 2 3.77 7.94 11.81 o 5 11 2 67.20 94.02 16.85 o 6 11 2 1.31 -0.83 14.84 o 7 11 2 56.23 50.60 19.34 o 8 11 2 229.77 245.93 31.99 o 9 11 2 208.57 180.96 34.93 o 10 11 2 51.97 9.58 39.38 o 0 12 2 2064.32 2003.08 55.22 o 1 12 2 159.25 154.82 15.14 o 2 12 2 42.45 48.96 11.16 o 3 12 2 132.68 156.31 16.43 o 4 12 2 448.01 450.85 25.14 o 5 12 2 155.99 181.48 22.77 o 6 12 2 325.54 324.14 29.53 o 7 12 2 34.91 -4.43 17.74 o 8 12 2 12.09 -0.58 19.51 o 9 12 2 44.14 23.12 29.13 o 10 12 2 30.52 30.50 39.72 o 1 13 2 48.81 29.93 13.50 o 2 13 2 5.35 23.03 11.81 o 3 13 2 526.89 550.03 27.58 o 4 13 2 2125.08 2128.15 45.84 o 5 13 2 845.77 852.84 41.95 o 6 13 2 92.63 76.91 20.56 o 7 13 2 6.52 18.06 17.83 o 8 13 2 333.10 336.45 36.74 o 9 13 2 392.76 456.39 51.47 o 0 14 2 474.34 419.61 32.82 o 1 14 2 21.49 4.68 11.93 o 2 14 2 19.17 27.56 11.75 o 3 14 2 720.52 755.44 32.51 o 4 14 2 132.72 128.15 17.39 o 5 14 2 500.47 468.54 33.11 o 6 14 2 312.73 281.80 28.99 o 7 14 2 42.27 28.98 19.92 o 8 14 2 163.93 203.84 31.66 o 9 14 2 663.59 666.30 61.22 o 1 15 2 25.09 39.99 12.52 o 2 15 2 51.37 68.86 14.50 o 3 15 2 1401.65 1457.52 40.77 o 4 15 2 320.82 296.69 23.60 o 5 15 2 61.62 42.07 18.32 o 6 15 2 86.13 89.43 21.93 o 7 15 2 56.24 67.21 24.94 o 8 15 2 436.79 422.19 40.39 o 9 15 2 12.07 1.25 34.96 o 0 16 2 4188.27 4036.80 88.62 o 1 16 2 271.04 266.10 20.69 o 2 16 2 79.44 92.35 15.65 o 3 16 2 241.17 226.62 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