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Information card for entry 2242222
Preview
| Coordinates | 2242222.cif |
|---|---|
| Structure factors | 2242222.hkl |
| Original IUCr paper | HTML |
| Chemical name | {2-[(Bis{[2-(methylsulfanyl)ethyl]aminomethyl}aminomethyl)amino]ethanethiolato}cobalt(III) bis(hexafluoridophosphate) |
|---|---|
| Formula | C11 H27 Co F12 N4 P2 S3 |
| Calculated formula | C11 H27 Co F12 N4 P2 S3 |
| Title of publication | Synthesis and crystallographic characterization of a mononuclear cobalt(III) complex possessing both thiolate and thioether donors: reactivity of an thiolate-bridged pentanuclear Co~2~Ag~3~ complex with iodomethane |
| Authors of publication | Fukuda, Yosuke; Yoshinari, Nobuto; Konno, Takumi |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2017 |
| Journal volume | 73 |
| Journal issue | 5 |
| Pages of publication | 678 - 681 |
| a | 32.44 ± 0.003 Å |
| b | 10.3197 ± 0.0008 Å |
| c | 29.869 ± 0.002 Å |
| α | 90° |
| β | 110.629 ± 0.008° |
| γ | 90° |
| Cell volume | 9358.1 ± 1.4 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0754 |
| Residual factor for significantly intense reflections | 0.0556 |
| Weighted residual factors for significantly intense reflections | 0.1409 |
| Weighted residual factors for all reflections included in the refinement | 0.1523 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 199187 (current) | 2017-07-25 | cif/ hkl/ Adding structures of 2242222 via cif-deposit CGI script. |
2242222.cif 2242222.hkl |
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