#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:50:18 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199198 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/22/2242235.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242235 _cell_angle_alpha 103.065 _cell_angle_beta 110.140 _cell_angle_gamma 92.776 _cell_length_a 6.6642 _cell_length_b 8.7537 _cell_length_c 8.9250 _exptl_crystal_F_000 299.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file xu5901Isup2.hkl _cod_data_source_block I _shelx_title ' a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.42 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6.90 17.32 0.60 o 2 0 0 2597.54 2944.08 23.97 o 3 0 0 3842.56 3846.98 42.20 o 4 0 0 576.97 620.64 7.63 o 5 0 0 42.71 46.30 4.75 o 6 0 0 281.72 289.24 7.14 o 7 0 0 19.02 17.26 4.05 o -7 1 0 5.49 5.18 1.73 o -6 1 0 1857.32 1906.85 34.99 o -5 1 0 11.98 10.88 1.33 o -4 1 0 513.90 589.00 7.41 o -3 1 0 2243.83 2153.90 20.23 o -2 1 0 12192.94 10701.45 109.04 o -1 1 0 1592.11 1537.40 21.71 o 0 1 0 172.67 159.29 3.35 o 1 1 0 131.61 94.57 2.97 o 2 1 0 3438.51 3387.20 27.31 o 3 1 0 61.83 50.30 1.71 o 4 1 0 271.14 256.85 4.29 o 5 1 0 706.26 736.35 9.25 o 6 1 0 18.35 16.21 1.86 o 7 1 0 129.63 152.38 7.78 o -7 2 0 214.02 221.60 10.04 o -6 2 0 126.63 114.58 6.48 o -5 2 0 0.43 0.00 0.32 o -4 2 0 5664.42 5682.53 80.56 o -3 2 0 354.64 336.51 8.75 o -2 2 0 48.95 38.66 2.27 o -1 2 0 2747.94 2659.85 34.07 o 0 2 0 2.19 1.19 0.76 o 1 2 0 788.05 700.91 8.22 o 2 2 0 991.73 929.12 7.84 o 3 2 0 9.12 6.43 0.70 o 4 2 0 541.69 521.07 11.17 o 5 2 0 103.76 103.34 3.75 o 6 2 0 15.94 12.96 2.48 o 7 2 0 374.58 370.53 13.18 o -7 3 0 567.72 566.75 17.39 o -6 3 0 37.20 29.70 4.00 o -5 3 0 176.57 171.28 7.56 o -4 3 0 1666.93 1642.05 28.94 o -3 3 0 0.34 0.00 0.22 o -2 3 0 124.35 86.40 3.67 o -1 3 0 459.44 478.83 8.91 o 0 3 0 24.53 18.14 0.93 o 1 3 0 1714.55 1533.00 23.06 o 2 3 0 300.51 364.59 5.81 o 3 3 0 580.59 564.05 7.02 o 4 3 0 576.74 592.38 11.99 o 5 3 0 8.43 8.64 1.94 o 6 3 0 268.14 299.68 11.45 o -7 4 0 76.57 88.23 6.37 o -6 4 0 54.95 57.88 4.75 o -5 4 0 486.46 479.82 13.93 o -4 4 0 49.98 59.07 4.00 o -3 4 0 389.10 377.87 10.15 o -2 4 0 334.30 297.72 9.34 o -1 4 0 257.37 341.06 5.82 o 0 4 0 714.31 661.42 8.91 o 1 4 0 1163.95 1149.18 26.94 o 2 4 0 895.18 938.15 12.04 o 3 4 0 1521.33 1543.78 16.60 o 4 4 0 246.89 261.78 9.61 o 5 4 0 3.00 2.92 1.19 o 6 4 0 313.91 327.11 12.74 o -6 5 0 128.76 121.93 7.24 o -5 5 0 53.71 53.56 4.21 o -4 5 0 105.85 116.85 5.94 o -3 5 0 1000.76 984.94 17.82 o -2 5 0 19.86 31.90 1.72 o -1 5 0 69.15 59.74 2.32 o 0 5 0 650.99 611.70 8.98 o 1 5 0 13.16 10.90 1.08 o 2 5 0 118.22 114.64 3.25 o 3 5 0 774.64 779.72 19.01 o 4 5 0 106.37 116.20 6.59 o 5 5 0 82.28 91.90 6.16 o -6 6 0 78.66 88.02 6.26 o -5 6 0 29.71 20.73 3.13 o -4 6 0 178.51 175.09 6.26 o -3 6 0 480.59 493.46 9.05 o -2 6 0 173.25 196.33 6.21 o -1 6 0 996.50 982.42 13.59 o 0 6 0 20.82 22.24 1.49 o 1 6 0 88.19 102.38 5.51 o 2 6 0 3006.88 3042.94 52.16 o 3 6 0 59.75 53.46 4.43 o 4 6 0 257.78 254.11 10.69 o 5 6 0 431.10 451.20 15.88 o -6 7 0 35.07 27.65 4.00 o -5 7 0 78.37 72.68 5.29 o -4 7 0 969.06 1030.15 22.79 o -3 7 0 67.39 66.50 3.05 o -2 7 0 399.45 432.08 15.34 o -1 7 0 1357.45 1323.94 17.54 o 0 7 0 2105.04 2149.83 38.99 o 1 7 0 5.52 10.37 2.16 o 2 7 0 114.59 119.77 6.80 o 3 7 0 55.47 56.16 4.75 o 4 7 0 897.27 878.85 23.33 o -5 8 0 56.01 67.71 5.18 o -4 8 0 83.62 78.30 5.29 o -3 8 0 171.07 187.40 5.76 o -2 8 0 3073.31 3039.71 50.06 o -1 8 0 34.14 36.61 3.46 o 0 8 0 33.51 38.77 3.67 o 1 8 0 730.58 747.75 19.87 o 2 8 0 36.01 33.48 4.43 o 3 8 0 38.58 41.15 5.18 o -4 9 0 406.49 444.50 14.47 o -3 9 0 85.29 89.96 5.51 o -2 9 0 138.24 135.75 7.13 o -1 9 0 20.13 16.42 2.92 o 0 9 0 694.47 775.18 20.84 o 1 9 0 44.64 50.11 4.64 o 2 9 0 5.60 4.64 1.62 o -1 10 0 13.29 12.53 2.70 o 0 10 0 628.57 657.68 19.65 o -1 -10 1 724.08 736.63 21.49 o 0 -10 1 0.57 1.94 0.97 o 1 -10 1 2.96 4.43 1.40 o 2 -10 1 54.66 52.81 4.64 o -2 -9 1 166.56 173.22 9.18 o -1 -9 1 429.48 469.23 15.66 o 0 -9 1 407.10 411.02 14.15 o 1 -9 1 218.60 209.40 9.40 o 2 -9 1 181.47 204.43 9.40 o 3 -9 1 5.48 4.31 1.13 o 4 -9 1 252.85 238.56 9.83 o -4 -8 1 213.39 217.07 10.80 o -3 -8 1 20.46 24.19 3.67 o -2 -8 1 4.09 1.51 0.97 o -1 -8 1 8.01 11.23 2.48 o 0 -8 1 184.21 198.28 8.86 o 1 -8 1 26.81 37.15 3.56 o 2 -8 1 24.27 25.26 2.59 o 3 -8 1 1031.58 1036.90 16.08 o 4 -8 1 3.60 5.67 1.01 o 5 -8 1 139.30 144.28 7.99 o -5 -7 1 182.88 189.85 9.94 o -4 -7 1 47.68 45.79 5.29 o -3 -7 1 366.47 377.01 13.18 o -2 -7 1 1.49 4.32 1.30 o -1 -7 1 152.00 154.86 7.45 o 0 -7 1 2243.38 2160.85 38.99 o 1 -7 1 148.71 152.42 4.41 o 2 -7 1 20.55 19.62 1.84 o 3 -7 1 266.03 269.05 6.71 o 4 -7 1 6.68 5.32 1.06 o 5 -7 1 279.73 282.73 11.23 o -5 -6 1 56.92 64.80 5.18 o -4 -6 1 45.77 40.28 4.75 o -3 -6 1 104.75 112.53 6.37 o -2 -6 1 229.75 225.38 8.86 o -1 -6 1 1178.16 1196.68 24.51 o 0 -6 1 1011.57 1025.51 13.44 o 1 -6 1 479.91 516.06 8.63 o 2 -6 1 1487.94 1500.93 19.12 o 3 -6 1 635.46 645.34 12.69 o 4 -6 1 47.59 49.79 3.89 o 5 -6 1 150.28 160.69 7.99 o 6 -6 1 2.35 0.76 0.65 o -6 -5 1 21.50 14.80 2.81 o -5 -5 1 161.72 145.04 7.67 o -4 -5 1 1996.77 2061.39 38.66 o -3 -5 1 310.39 301.63 10.26 o -2 -5 1 37.66 37.37 3.13 o -1 -5 1 1551.09 1521.09 17.38 o 0 -5 1 405.35 408.56 6.61 o 1 -5 1 193.90 187.87 6.97 o 2 -5 1 2873.05 2862.69 31.52 o 3 -5 1 9.40 10.69 1.84 o 4 -5 1 37.84 36.50 4.00 o 5 -5 1 110.02 108.21 6.37 o 6 -5 1 136.41 131.97 7.67 o -6 -4 1 43.07 50.11 4.43 o -5 -4 1 280.11 308.32 11.02 o -4 -4 1 1283.69 1289.27 16.83 o -3 -4 1 2.67 6.49 2.65 o -2 -4 1 1564.09 1512.64 16.84 o -1 -4 1 1036.41 974.27 11.46 o 0 -4 1 1394.40 1455.68 29.21 o 1 -4 1 2641.05 2573.85 27.44 o 2 -4 1 152.17 189.85 6.16 o 3 -4 1 124.15 131.00 5.62 o 4 -4 1 1368.61 1353.81 26.03 o 5 -4 1 4.09 1.40 0.76 o 6 -4 1 399.97 423.44 14.26 o -7 -3 1 229.37 235.53 10.15 o -6 -3 1 1.47 0.86 0.65 o -5 -3 1 810.62 773.67 18.25 o -4 -3 1 335.85 326.05 4.97 o -3 -3 1 106.15 110.57 2.34 o -2 -3 1 3990.95 3914.82 39.54 o -1 -3 1 830.49 797.61 9.09 o 0 -3 1 420.04 375.41 5.27 o 1 -3 1 637.31 541.02 7.45 o 2 -3 1 126.18 162.53 5.29 o 3 -3 1 3230.97 3306.67 49.25 o 4 -3 1 466.40 485.43 12.74 o 5 -3 1 2.93 1.73 0.97 o 6 -3 1 597.78 605.52 17.28 o 7 -3 1 62.52 60.69 5.29 o -7 -2 1 3.44 4.75 1.40 o -6 -2 1 121.60 129.92 6.48 o -5 -2 1 667.42 676.35 8.62 o -4 -2 1 136.01 132.88 2.87 o -3 -2 1 1910.62 1846.89 17.46 o -2 -2 1 222.99 205.66 2.83 o -1 -2 1 266.05 217.93 5.51 o 0 -2 1 211.00 195.61 3.06 o 1 -2 1 437.15 441.37 8.21 o 2 -2 1 1104.94 1053.59 17.82 o 3 -2 1 2303.74 2160.63 33.91 o 4 -2 1 0.61 0.86 0.43 o 5 -2 1 692.52 689.54 16.85 o 6 -2 1 35.40 39.53 4.54 o 7 -2 1 18.54 14.26 2.92 o -7 -1 1 105.74 107.99 6.16 o -6 -1 1 369.88 382.80 6.49 o -5 -1 1 0.81 0.56 0.54 o -4 -1 1 1051.54 1103.20 11.35 o -3 -1 1 1665.72 1615.77 20.13 o -2 -1 1 5668.92 5653.66 55.86 o -1 -1 1 5408.82 4940.61 76.35 o 0 -1 1 1369.55 1343.79 29.64 o 1 -1 1 305.84 376.36 7.02 o 2 -1 1 3776.53 3638.85 50.76 o 3 -1 1 1399.10 1423.70 17.14 o 4 -1 1 113.24 134.97 4.01 o 5 -1 1 185.93 197.06 5.50 o 6 -1 1 4.54 1.73 0.76 o 7 -1 1 203.87 204.11 9.61 o -7 0 1 204.37 221.60 9.40 o -6 0 1 276.29 279.57 5.42 o -5 0 1 5.06 5.26 0.86 o -4 0 1 407.40 413.51 7.74 o -3 0 1 17.83 14.78 0.86 o -2 0 1 1372.85 1581.64 13.49 o -1 0 1 4529.23 4119.46 140.01 o 0 0 1 876.95 833.93 11.99 o 1 0 1 1758.24 1663.47 17.88 o 2 0 1 312.77 259.01 4.58 o 3 0 1 472.18 535.30 8.28 o 4 0 1 619.93 614.84 11.72 o 5 0 1 279.33 278.84 9.50 o 6 0 1 19.70 17.45 1.99 o 7 0 1 52.32 51.95 4.43 o -7 1 1 263.25 292.02 11.23 o -6 1 1 10.63 10.97 1.44 o -5 1 1 75.78 76.75 2.38 o -4 1 1 4.47 3.48 1.48 o -3 1 1 107.36 131.82 3.58 o -2 1 1 3565.67 3388.21 33.18 o -1 1 1 2324.65 2208.04 21.57 o 0 1 1 150.06 190.72 4.00 o 1 1 1 20.57 33.47 2.05 o 2 1 1 3.21 1.67 0.23 o 3 1 1 735.91 742.18 13.43 o 4 1 1 418.85 401.61 6.37 o 5 1 1 422.00 416.25 13.01 o 6 1 1 161.90 162.92 5.50 o -7 2 1 15.77 10.26 2.16 o -6 2 1 588.01 584.46 15.88 o -5 2 1 416.77 439.43 11.66 o -4 2 1 650.98 668.02 10.18 o -3 2 1 518.62 478.89 7.52 o -2 2 1 734.05 638.14 10.58 o -1 2 1 1251.91 1341.71 14.51 o 0 2 1 2150.69 2149.87 22.07 o 1 2 1 199.69 162.21 4.32 o 2 2 1 4.13 1.82 0.31 o 3 2 1 388.49 341.19 4.21 o 4 2 1 14.83 18.23 2.70 o 5 2 1 12.82 7.84 1.57 o 6 2 1 764.75 751.29 14.85 o -7 3 1 52.72 51.73 4.64 o -6 3 1 498.57 543.86 15.55 o -5 3 1 406.71 406.06 12.10 o -4 3 1 4.18 1.94 0.76 o -3 3 1 640.73 611.35 13.28 o -2 3 1 48.64 38.53 1.53 o -1 3 1 0.89 2.18 0.46 o 0 3 1 6115.08 5569.25 196.01 o 1 3 1 786.44 970.09 19.33 o 2 3 1 13.03 7.90 0.84 o 3 3 1 898.83 888.20 10.49 o 4 3 1 31.35 28.12 1.96 o 5 3 1 335.67 334.48 7.75 o 6 3 1 258.78 251.41 10.80 o -7 4 1 83.89 88.56 6.37 o -6 4 1 348.14 348.50 12.31 o -5 4 1 22.67 26.78 3.46 o -4 4 1 632.51 629.06 15.12 o -3 4 1 352.57 367.19 14.47 o -2 4 1 42.29 32.55 1.60 o -1 4 1 1436.79 1314.49 15.65 o 0 4 1 293.83 268.35 11.02 o 1 4 1 310.27 349.77 6.14 o 2 4 1 1947.98 1856.27 30.62 o 3 4 1 508.39 491.38 8.58 o 4 4 1 177.14 172.14 7.88 o 5 4 1 271.23 269.23 11.02 o -7 5 1 227.16 221.06 10.48 o -6 5 1 47.34 49.25 4.32 o -5 5 1 0.63 0.76 0.54 o -4 5 1 1527.29 1517.45 19.52 o -3 5 1 18.86 17.73 1.63 o -2 5 1 141.33 151.63 7.61 o -1 5 1 688.80 645.74 41.15 o 0 5 1 1.08 0.97 0.31 o 1 5 1 1638.06 1626.68 43.85 o 2 5 1 734.65 761.69 11.42 o 3 5 1 61.76 55.29 4.32 o 4 5 1 907.63 908.55 22.57 o 5 5 1 27.67 27.32 4.00 o -6 6 1 21.43 17.39 3.13 o -5 6 1 254.25 263.07 10.37 o -4 6 1 860.81 904.45 20.19 o -3 6 1 54.64 60.04 2.70 o -2 6 1 314.20 314.11 6.64 o -1 6 1 795.99 808.61 12.00 o 0 6 1 185.13 184.21 4.72 o 1 6 1 1535.06 1549.10 19.56 o 2 6 1 99.71 96.22 5.83 o 3 6 1 403.29 397.31 13.28 o 4 6 1 109.70 123.22 7.45 o -6 7 1 32.75 41.90 5.08 o -5 7 1 315.96 316.75 11.66 o -4 7 1 2.44 4.97 1.40 o -3 7 1 233.53 237.80 8.86 o -2 7 1 257.87 253.73 6.18 o -1 7 1 318.75 307.19 6.76 o 0 7 1 1112.23 1095.54 15.50 o 1 7 1 289.10 284.35 10.69 o 2 7 1 36.37 33.05 4.10 o 3 7 1 377.05 379.92 13.72 o 4 7 1 10.63 13.39 2.81 o -5 8 1 3.39 3.78 1.08 o -4 8 1 12.76 14.15 2.48 o -3 8 1 1268.17 1297.98 26.35 o -2 8 1 40.44 37.27 2.29 o -1 8 1 323.98 312.43 11.02 o 0 8 1 364.40 367.50 12.53 o 1 8 1 143.63 128.40 7.34 o 2 8 1 183.84 177.22 9.07 o 3 8 1 503.26 497.20 16.85 o -4 9 1 459.86 471.93 15.01 o -3 9 1 337.98 336.62 11.66 o -1 9 1 220.73 214.69 9.50 o 0 9 1 60.38 60.58 4.97 o 1 9 1 14.04 18.25 3.24 o -1 -10 2 24.56 24.62 3.89 o 0 -10 2 7.98 4.75 1.62 o 1 -10 2 200.61 190.61 9.50 o 2 -10 2 1.05 0.43 0.65 o -3 -9 2 303.81 291.04 12.53 o -2 -9 2 157.08 161.34 8.75 o -1 -9 2 7.72 7.88 1.94 o 0 -9 2 338.79 320.20 12.10 o 1 -9 2 5.81 6.05 1.73 o 2 -9 2 49.24 43.52 4.10 o 3 -9 2 655.30 669.02 19.01 o 4 -9 2 1.08 1.30 0.52 o -4 -8 2 127.76 119.98 7.56 o -3 -8 2 328.11 324.85 12.64 o -2 -8 2 0.66 0.00 0.54 o -1 -8 2 503.22 506.38 15.55 o 0 -8 2 50.64 47.09 4.10 o 1 -8 2 65.90 66.52 4.86 o 2 -8 2 1113.86 1158.13 31.37 o 3 -8 2 27.17 34.21 2.82 o 4 -8 2 0.56 0.75 0.49 o -5 -7 2 1.38 1.19 0.86 o -4 -7 2 708.58 729.93 20.19 o -3 -7 2 75.94 82.62 5.62 o -2 -7 2 127.28 129.59 6.91 o -1 -7 2 2568.77 2430.40 43.41 o 0 -7 2 58.13 50.22 4.00 o 1 -7 2 49.58 47.80 2.31 o 2 -7 2 952.36 993.40 14.90 o 3 -7 2 178.12 181.53 6.43 o 4 -7 2 124.55 131.45 4.89 o 5 -7 2 213.66 215.45 9.83 o -5 -6 2 141.68 136.18 7.56 o -4 -6 2 128.33 112.31 6.59 o -3 -6 2 13.11 18.68 2.92 o -2 -6 2 753.85 735.33 17.93 o -1 -6 2 1007.87 946.67 20.52 o 0 -6 2 5.61 4.58 0.86 o 1 -6 2 1431.05 1429.02 17.88 o 2 -6 2 185.51 177.49 4.86 o 3 -6 2 264.50 260.88 6.48 o 4 -6 2 679.26 743.11 18.36 o 5 -6 2 12.69 12.74 2.59 o 6 -6 2 1.02 1.62 0.97 o -6 -5 2 77.96 79.48 5.72 o -5 -5 2 674.13 689.43 18.25 o -4 -5 2 13.75 13.81 1.62 o -3 -5 2 183.20 187.26 7.67 o -2 -5 2 1563.32 1627.90 30.02 o -1 -5 2 4.38 4.54 1.30 o 0 -5 2 363.30 309.91 5.41 o 1 -5 2 2039.83 2046.16 23.31 o 2 -5 2 245.56 268.90 7.99 o 3 -5 2 165.65 154.86 6.48 o 4 -5 2 65.79 74.41 4.86 o 5 -5 2 15.89 15.77 2.70 o 6 -5 2 532.31 559.95 17.50 o -6 -4 2 20.30 17.93 2.81 o -5 -4 2 764.86 759.17 12.18 o -4 -4 2 33.21 38.45 2.07 o -3 -4 2 85.98 83.48 4.54 o -2 -4 2 20.98 9.94 1.73 o -1 -4 2 1327.83 1525.39 16.28 o 0 -4 2 5007.17 4866.63 48.33 o 1 -4 2 1467.99 1804.38 20.45 o 2 -4 2 17.49 13.82 1.84 o 3 -4 2 821.47 841.70 17.60 o 4 -4 2 113.76 121.82 6.16 o 5 -4 2 123.31 130.13 7.02 o 6 -4 2 327.85 334.35 12.74 o -7 -3 2 7.52 7.56 1.73 o -6 -3 2 620.28 627.77 16.63 o -5 -3 2 47.79 47.47 2.40 o -4 -3 2 1.07 2.62 0.65 o -3 -3 2 1612.48 1720.35 15.48 o -2 -3 2 890.23 877.88 16.85 o -1 -3 2 42.80 18.68 1.62 o 0 -3 2 25.04 20.34 0.98 o 1 -3 2 1020.30 1135.34 18.25 o 2 -3 2 1370.26 1389.13 23.22 o 3 -3 2 6.85 4.97 1.19 o 4 -3 2 29.53 30.45 3.56 o 5 -3 2 399.17 404.55 12.85 o 6 -3 2 21.37 20.84 3.24 o -6 -2 2 7.37 6.24 1.06 o -5 -2 2 11.29 15.47 1.20 o -4 -2 2 3415.16 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