#------------------------------------------------------------------------------ #$Date: 2017-08-16 09:02:27 +0300 (Wed, 16 Aug 2017) $ #$Revision: 199795 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/22/2242285.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242285 _cell_angle_alpha 90.000 _cell_angle_beta 98.914 _cell_angle_gamma 90.000 _cell_length_a 7.1074 _cell_length_b 32.7540 _cell_length_c 16.1505 _exptl_crystal_F_000 1808.00 _reflns_d_resolution_high 0.7612 _cod_data_source_file bt69952sup3.hkl _cod_data_source_block 2 _shelx_title ' ba590_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 496.17 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8.86 119.12 78.22 o 2 0 0 76365.30 76581.29 4007.77 o 3 0 0 25.24 -18.25 135.38 o 4 0 0 303.90 275.32 172.66 o 5 0 0 4.97 65.14 180.33 o 6 0 0 29913.21 29484.33 990.03 o 7 0 0 7.16 105.65 267.70 o 8 0 0 433.38 436.59 497.37 o 9 0 0 65.80 56.30 522.07 o 1 1 0 9.36 50.73 46.01 o 2 1 0 870.69 589.49 117.37 o 3 1 0 19.14 8.68 104.79 o 4 1 0 5611.19 5526.15 286.95 o 5 1 0 1635.53 1761.63 224.77 o 6 1 0 2106.82 2161.16 270.69 o 7 1 0 1513.63 1595.17 282.52 o 8 1 0 3021.29 3220.31 534.36 o 9 1 0 35.25 -71.77 358.92 o 0 2 0 5125.08 2768.39 2347.67 o 1 2 0 52874.43 54426.54 2760.17 o 2 2 0 4338.48 4185.91 203.78 o 3 2 0 18854.79 19068.31 580.10 o 4 2 0 441.80 593.25 143.23 o 5 2 0 5071.07 5709.59 338.75 o 6 2 0 12.41 92.36 164.10 o 7 2 0 77.07 100.51 194.67 o 8 2 0 14.38 -52.69 251.06 o 9 2 0 4.58 -218.16 344.02 o 1 3 0 20.99 29.31 59.91 o 2 3 0 1280.96 1565.31 143.82 o 3 3 0 773.87 1037.82 153.47 o 4 3 0 6304.84 6327.01 329.03 o 5 3 0 7946.36 8371.66 408.79 o 6 3 0 3113.60 3279.35 313.09 o 7 3 0 5019.95 5054.73 415.94 o 8 3 0 1897.00 1964.64 390.03 o 9 3 0 28.92 -148.53 352.61 o 0 4 0 8828.77 9777.57 170.56 o 1 4 0 8154.39 7621.93 569.07 o 2 4 0 615.40 567.72 109.11 o 3 4 0 9842.23 9239.17 309.21 o 4 4 0 12715.30 12336.07 409.87 o 5 4 0 4109.09 4202.16 308.18 o 6 4 0 329.14 461.27 189.67 o 7 4 0 304.31 126.90 191.03 o 8 4 0 203.74 321.24 277.70 o 9 4 0 16.42 396.97 441.96 o 1 5 0 278.22 359.85 103.34 o 2 5 0 48293.41 47680.03 753.97 o 3 5 0 3818.56 3987.09 238.77 o 4 5 0 89.86 201.68 128.78 o 5 5 0 16885.55 18043.03 711.44 o 6 5 0 108.70 150.12 160.34 o 7 5 0 8830.11 9707.81 611.96 o 8 5 0 119.19 172.69 262.09 o 9 5 0 173.34 620.30 476.62 o 0 6 0 1333.84 1406.18 130.46 o 1 6 0 246181.56 246697.56 2926.96 o 2 6 0 4184.04 4140.67 254.58 o 3 6 0 111.22 107.19 133.26 o 4 6 0 1295.54 1203.87 185.75 o 5 6 0 3798.23 3950.99 362.59 o 6 6 0 591.67 590.72 196.82 o 7 6 0 1575.40 1306.60 310.93 o 8 6 0 69.03 250.44 276.25 o 9 6 0 60.91 -198.41 390.50 o 1 7 0 35023.90 36378.21 429.50 o 2 7 0 21788.78 20458.54 451.23 o 3 7 0 7788.76 7527.09 364.06 o 4 7 0 382.03 391.43 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