#------------------------------------------------------------------------------ #$Date: 2017-09-06 08:46:47 +0300 (Wed, 06 Sep 2017) $ #$Revision: 200204 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/23/2242302.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242302 _cell_angle_alpha 90.000 _cell_angle_beta 94.820 _cell_angle_gamma 90.000 _cell_length_a 5.2243 _cell_length_b 6.7414 _cell_length_c 11.2772 _exptl_crystal_F_000 168.00 _reflns_d_resolution_high 0.7583 _cod_data_source_file wm5409Isup2.hkl _cod_data_source_block I _shelx_title ' HR634_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 84.37 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 753.57 821.13 5.93 o 2 0 0 2428.11 2641.92 31.88 o 3 0 0 734.65 773.89 9.17 o 4 0 0 51.34 42.73 2.45 o 5 0 0 6.56 6.85 1.99 o 6 0 0 199.99 189.46 5.58 o 1 1 0 1272.79 1228.21 6.64 o 2 1 0 84.10 67.90 1.29 o 3 1 0 468.71 541.80 4.79 o 4 1 0 617.91 620.91 6.15 o 5 1 0 49.39 46.91 2.08 o 6 1 0 92.36 97.12 3.19 o 0 2 0 211.42 226.38 6.27 o 1 2 0 118.26 126.99 1.40 o 2 2 0 46.07 49.89 1.26 o 3 2 0 143.39 153.09 2.39 o 4 2 0 1.27 0.20 1.00 o 5 2 0 29.40 31.55 1.87 o 6 2 0 4.19 2.52 1.56 o 1 3 0 36.46 46.97 1.08 o 2 3 0 36.98 43.35 1.15 o 3 3 0 30.94 31.50 1.30 o 4 3 0 229.31 234.19 3.87 o 5 3 0 0.66 -0.03 1.21 o 6 3 0 58.41 64.30 2.87 o 0 4 0 1736.74 1721.19 13.64 o 1 4 0 329.67 344.18 3.16 o 2 4 0 221.76 217.24 2.59 o 3 4 0 407.37 402.02 4.36 o 4 4 0 40.62 43.19 2.02 o 5 4 0 34.86 41.80 2.27 o 6 4 0 45.76 46.14 3.23 o 1 5 0 797.18 770.62 6.04 o 2 5 0 22.01 20.43 1.22 o 3 5 0 246.19 226.27 3.36 o 4 5 0 189.17 184.50 3.89 o 5 5 0 68.77 66.99 2.83 o 0 6 0 438.01 441.91 6.26 o 1 6 0 76.93 78.86 1.89 o 2 6 0 122.95 119.06 2.78 o 3 6 0 211.64 208.71 3.69 o 4 6 0 2.30 0.47 1.73 o 5 6 0 45.96 40.00 6.53 o 1 7 0 57.43 61.33 2.65 o 2 7 0 17.56 20.34 3.10 o 3 7 0 2.34 1.12 1.89 o 4 7 0 3.94 1.48 2.53 o 0 8 0 0.42 0.63 3.18 o 1 8 0 31.77 28.95 2.91 o 2 8 0 3.38 1.37 2.06 o -6 1 1 124.23 129.45 3.41 o -5 1 1 59.87 57.56 2.23 o -4 1 1 388.77 373.91 4.54 o -3 1 1 379.09 417.05 4.07 o -2 1 1 16.10 28.73 0.93 o -1 1 1 944.14 932.31 7.01 o 0 1 1 749.33 741.82 4.49 o 1 1 1 248.09 226.07 1.68 o 2 1 1 35.70 31.30 0.88 o 3 1 1 72.39 86.48 1.96 o 4 1 1 99.97 109.93 2.81 o 5 1 1 58.60 55.09 3.36 o 6 1 1 11.41 11.03 1.88 o -6 2 1 0.38 1.34 1.44 o -5 2 1 342.92 338.70 4.81 o -4 2 1 22.81 29.54 1.61 o -3 2 1 1191.47 1179.05 9.07 o -2 2 1 324.34 307.70 3.23 o -1 2 1 2819.17 2986.54 16.97 o 0 2 1 1754.65 1748.05 9.25 o 1 2 1 556.40 543.26 3.50 o 2 2 1 0.93 0.57 0.50 o 3 2 1 1447.08 1460.27 10.62 o 4 2 1 823.41 808.91 7.79 o 5 2 1 122.09 124.55 3.00 o 6 2 1 282.84 281.99 5.02 o -6 3 1 234.95 244.01 5.63 o -5 3 1 2.16 2.11 1.28 o -4 3 1 1177.36 1171.65 10.45 o -3 3 1 743.93 748.10 6.27 o -2 3 1 289.21 311.69 3.00 o -1 3 1 974.10 991.54 5.95 o 0 3 1 30.01 26.77 0.88 o 1 3 1 0.09 -0.24 0.49 o 2 3 1 226.64 226.20 2.38 o 3 3 1 11.53 14.76 1.07 o 4 3 1 430.39 427.27 5.23 o 5 3 1 254.84 261.26 6.80 o 6 3 1 102.71 97.99 3.25 o -6 4 1 32.10 31.20 2.84 o -5 4 1 97.66 95.84 3.05 o -4 4 1 0.23 0.27 1.19 o -3 4 1 116.31 120.53 2.45 o -2 4 1 128.83 127.30 2.05 o -1 4 1 13.11 24.25 3.06 o 0 4 1 470.28 484.37 4.00 o 1 4 1 135.57 143.81 2.02 o 2 4 1 51.91 53.14 1.39 o 3 4 1 165.03 168.25 2.68 o 4 4 1 74.34 78.95 2.41 o 5 4 1 3.17 2.53 1.45 o 6 4 1 110.95 118.34 5.41 o -5 5 1 7.05 7.42 1.70 o -4 5 1 2.13 3.19 1.43 o -3 5 1 4.63 4.96 1.23 o -2 5 1 70.43 72.10 1.90 o -1 5 1 2.52 2.07 1.02 o 0 5 1 62.58 63.65 1.65 o 1 5 1 5.46 5.51 0.89 o 2 5 1 1.53 1.07 0.97 o 3 5 1 44.00 49.55 2.22 o 4 5 1 0.03 -1.60 1.56 o 5 5 1 12.61 9.37 2.53 o -5 6 1 14.37 14.65 2.51 o -4 6 1 1.23 -0.20 1.46 o -3 6 1 18.59 20.85 1.65 o -2 6 1 49.97 50.69 1.88 o -1 6 1 2.04 1.07 0.96 o 0 6 1 411.16 409.18 4.16 o 1 6 1 159.47 160.06 3.08 o 2 6 1 89.45 86.19 2.73 o 3 6 1 173.22 171.58 4.21 o 4 6 1 26.12 30.26 2.78 o -4 7 1 307.44 311.43 7.06 o -3 7 1 174.75 174.63 3.86 o -2 7 1 94.58 102.81 3.03 o -1 7 1 175.92 177.72 3.42 o 0 7 1 9.94 8.18 1.52 o 1 7 1 6.07 5.18 1.62 o 2 7 1 97.38 95.84 3.65 o 3 7 1 9.80 10.85 2.23 o 4 7 1 163.42 175.81 5.95 o -2 8 1 83.03 78.06 5.99 o -1 8 1 23.44 17.87 2.31 o 0 8 1 130.01 123.99 4.40 o 1 8 1 57.96 51.61 3.32 o 2 8 1 5.06 3.90 2.19 o -6 0 2 27.30 28.16 2.92 o -5 0 2 377.80 382.17 7.19 o -4 0 2 4.75 9.81 1.77 o -3 0 2 2.43 9.68 1.27 o -2 0 2 0.31 2.99 0.84 o -1 0 2 889.31 807.68 6.22 o 0 0 2 2023.86 2026.37 27.52 o 1 0 2 7118.48 7089.22 61.29 o 2 0 2 513.02 602.30 8.83 o 3 0 2 3078.16 3283.68 27.04 o 4 0 2 422.04 408.54 6.57 o 5 0 2 20.96 29.53 2.45 o 6 0 2 195.30 210.19 7.12 o -6 1 2 177.60 177.85 3.90 o -5 1 2 14.83 9.90 1.46 o -4 1 2 650.76 625.42 6.23 o -3 1 2 779.55 829.58 6.21 o -2 1 2 0.92 2.02 0.55 o -1 1 2 1232.85 1232.34 7.42 o 0 1 2 2908.45 2928.70 31.39 o 1 1 2 78.40 89.68 1.22 o 2 1 2 692.46 698.05 6.00 o 3 1 2 133.05 124.25 2.18 o 4 1 2 195.11 209.28 3.08 o 5 1 2 123.65 121.67 2.91 o 6 1 2 17.89 17.55 1.93 o -6 2 2 0.48 0.10 1.44 o -5 2 2 22.78 23.89 1.76 o -4 2 2 30.80 36.89 1.76 o -3 2 2 20.54 23.43 1.22 o -2 2 2 94.75 102.24 1.76 o -1 2 2 9.57 15.30 0.59 o 0 2 2 62.97 63.04 1.21 o 1 2 2 78.34 73.16 1.20 o 2 2 2 4.84 3.95 0.61 o 3 2 2 108.12 114.54 2.05 o 4 2 2 87.03 92.98 2.28 o 5 2 2 14.81 14.25 1.47 o 6 2 2 29.36 28.46 2.11 o -6 3 2 3.26 2.79 1.59 o -5 3 2 10.49 8.59 1.48 o -4 3 2 118.39 122.86 2.81 o -3 3 2 358.69 360.20 4.19 o -2 3 2 16.40 22.63 1.09 o -1 3 2 456.87 464.81 3.53 o 0 3 2 11.79 10.90 0.63 o 1 3 2 42.38 48.01 1.12 o 2 3 2 0.06 0.25 0.62 o 3 3 2 40.25 41.68 1.62 o 4 3 2 12.12 14.20 1.64 o 5 3 2 40.82 40.52 2.72 o 6 3 2 26.20 27.62 2.58 o -6 4 2 0.01 -2.47 1.65 o -5 4 2 128.66 123.70 4.28 o -4 4 2 55.97 54.79 2.17 o -3 4 2 22.58 24.21 1.50 o -2 4 2 104.08 98.69 1.94 o -1 4 2 1.41 2.22 0.72 o 0 4 2 553.45 556.74 4.74 o 1 4 2 562.52 554.48 4.49 o 2 4 2 62.41 61.94 1.62 o 3 4 2 753.72 732.20 6.87 o 4 4 2 262.82 252.03 4.70 o 5 4 2 13.98 19.84 2.68 o -5 5 2 43.45 42.65 2.98 o -4 5 2 372.10 381.08 5.45 o -3 5 2 210.94 200.79 3.39 o -2 5 2 17.01 10.81 1.10 o -1 5 2 387.59 379.20 4.16 o 0 5 2 1184.09 1120.74 8.45 o 1 5 2 24.56 23.70 1.23 o 2 5 2 627.87 609.82 6.05 o 3 5 2 7.90 7.79 1.47 o 4 5 2 141.02 131.63 4.24 o 5 5 2 36.56 40.13 3.48 o -5 6 2 78.77 83.05 3.58 o -4 6 2 37.88 36.90 2.35 o -3 6 2 34.05 34.58 1.90 o -2 6 2 147.59 150.52 2.77 o -1 6 2 11.05 6.91 1.28 o 0 6 2 127.88 132.10 3.03 o 1 6 2 257.45 254.61 4.04 o 2 6 2 0.27 -0.29 1.24 o 3 6 2 274.07 268.76 5.17 o 4 6 2 128.34 125.68 4.40 o -4 7 2 3.59 5.18 1.76 o -3 7 2 0.52 3.01 1.57 o -2 7 2 0.01 -2.30 1.53 o -1 7 2 5.05 3.93 1.49 o 0 7 2 21.33 22.91 1.85 o 1 7 2 1.40 1.59 1.56 o 2 7 2 63.96 68.45 3.05 o 3 7 2 9.87 8.97 2.06 o 4 7 2 16.70 17.72 3.09 o -2 8 2 33.40 38.30 3.09 o -1 8 2 39.66 38.46 2.60 o 0 8 2 32.60 32.37 3.90 o 1 8 2 3.82 3.67 1.98 o 2 8 2 0.08 3.68 2.10 o -6 1 3 109.65 106.73 3.24 o -5 1 3 0.66 1.50 1.24 o -4 1 3 300.90 290.94 4.02 o -3 1 3 350.14 350.57 3.53 o -2 1 3 5.51 5.78 0.66 o -1 1 3 720.02 721.31 4.72 o 0 1 3 2649.88 2649.11 20.44 o 1 1 3 32.95 34.88 1.02 o 2 1 3 496.40 504.11 4.00 o 3 1 3 114.44 114.99 1.95 o 4 1 3 3.86 4.24 1.04 o 5 1 3 12.04 14.36 1.47 o 6 1 3 15.13 12.97 1.78 o -6 2 3 39.50 41.79 2.37 o -5 2 3 101.03 97.18 2.99 o -4 2 3 978.56 960.46 8.50 o -3 2 3 99.29 101.38 2.07 o -2 2 3 1054.74 1081.98 7.15 o -1 2 3 109.78 95.54 1.42 o 0 2 3 1737.22 1739.47 14.91 o 1 2 3 152.15 139.08 2.06 o 2 2 3 64.40 75.58 1.41 o 3 2 3 476.13 471.51 4.72 o 4 2 3 711.86 694.59 7.11 o 5 2 3 20.83 20.67 2.01 o 6 2 3 410.33 420.86 10.15 o -6 3 3 61.07 64.87 2.80 o -5 3 3 46.58 49.15 2.28 o -4 3 3 174.60 176.53 3.27 o -3 3 3 1254.76 1237.12 9.71 o -2 3 3 90.79 87.05 1.86 o -1 3 3 2424.21 2561.20 15.14 o 0 3 3 1618.96 1613.43 10.37 o 1 3 3 0.56 0.14 0.55 o 2 3 3 344.99 327.54 3.22 o 3 3 3 337.72 330.44 3.93 o 4 3 3 8.80 8.78 1.62 o 5 3 3 201.69 192.64 5.45 o 6 3 3 46.86 41.39 3.63 o -6 4 3 3.60 2.28 1.64 o -5 4 3 99.26 108.34 3.05 o -4 4 3 96.19 96.72 2.65 o -3 4 3 0.08 -0.09 1.00 o -2 4 3 116.97 118.79 2.26 o -1 4 3 153.20 151.41 2.75 o 0 4 3 59.58 60.47 1.44 o 1 4 3 322.40 320.09 3.66 o 2 4 3 0.01 0.93 0.75 o 3 4 3 134.89 132.73 2.75 o 4 4 3 52.48 53.64 2.95 o 5 4 3 8.31 8.08 2.38 o -5 5 3 8.55 7.80 1.60 o -4 5 3 25.55 24.39 1.75 o -3 5 3 7.63 7.72 1.27 o -2 5 3 5.82 8.69 1.22 o -1 5 3 11.32 9.99 1.12 o 0 5 3 23.11 21.71 1.38 o 1 5 3 38.62 39.31 1.58 o 2 5 3 7.14 7.52 1.36 o 3 5 3 0.65 -0.03 1.26 o 4 5 3 5.18 5.59 2.02 o 5 5 3 6.12 6.76 2.51 o -4 6 3 47.48 51.95 3.01 o -3 6 3 0.35 -0.02 1.23 o -2 6 3 6.88 9.30 1.53 o -1 6 3 22.53 19.37 1.67 o 0 6 3 8.91 10.92 1.76 o 1 6 3 149.94 142.87 4.08 o 2 6 3 1.09 0.15 1.45 o 3 6 3 196.83 196.73 4.48 o 4 6 3 64.47 58.86 3.44 o -4 7 3 40.73 43.31 3.05 o -3 7 3 345.64 349.73 8.02 o -2 7 3 7.52 7.28 2.03 o -1 7 3 421.87 426.49 6.42 o 0 7 3 196.10 194.34 4.31 o 1 7 3 1.20 -0.83 1.37 o 2 7 3 66.69 60.88 2.93 o 3 7 3 114.68 114.18 3.93 o -2 8 3 142.45 146.20 5.39 o -1 8 3 45.66 44.43 3.08 o 0 8 3 64.53 70.53 3.04 o 1 8 3 91.75 98.56 3.67 o 2 8 3 1.15 0.71 1.93 o -6 0 4 224.08 237.26 6.33 o -5 0 4 669.01 645.91 9.89 o -4 0 4 1161.41 1128.51 13.37 o -3 0 4 19.34 20.21 1.65 o -2 0 4 101.86 93.72 2.20 o -1 0 4 140.66 132.76 2.08 o 0 0 4 1114.00 1140.69 19.28 o 1 0 4 525.62 482.20 5.25 o 2 0 4 412.69 399.43 5.15 o 3 0 4 626.09 641.70 7.61 o 4 0 4 874.83 866.24 10.49 o 5 0 4 1.66 -1.24 1.58 o 6 0 4 226.04 236.17 7.14 o -6 1 4 99.20 100.25 3.16 o -5 1 4 96.39 96.59 3.01 o -4 1 4 144.39 142.15 2.72 o -3 1 4 631.75 615.73 5.09 o -2 1 4 1.19 -0.15 0.53 o -1 1 4 1219.44 1232.96 7.52 o 0 1 4 1361.28 1328.52 11.29 o 1 1 4 373.85 371.06 4.60 o 2 1 4 354.12 349.46 3.22 o 3 1 4 1019.14 1035.34 7.66 o 4 1 4 66.43 67.90 2.25 o 5 1 4 222.32 231.69 5.56 o 6 1 4 69.39 74.61 4.12 o -6 2 4 2.16 3.47 1.55 o -5 2 4 10.76 10.67 1.51 o -4 2 4 89.36 85.42 2.29 o -3 2 4 16.95 17.36 1.10 o -2 2 4 127.26 134.48 2.26 o -1 2 4 90.36 86.34 1.64 o 0 2 4 34.60 41.98 1.63 o 1 2 4 11.99 10.09 1.14 o 2 2 4 22.96 21.01 0.94 o 3 2 4 0.10 -1.21 0.81 o 4 2 4 81.60 80.15 2.67 o 5 2 4 15.32 17.23 2.41 o 6 2 4 40.39 30.16 3.04 o -6 3 4 0.54 -1.56 1.57 o -5 3 4 0.04 -1.21 1.27 o -4 3 4 2.20 3.61 1.15 o -3 3 4 87.60 84.53 2.03 o -2 3 4 53.67 55.59 1.58 o -1 3 4 366.32 377.60 4.07 o 0 3 4 339.49 335.91 4.15 o 1 3 4 0.02 -0.43 0.92 o 2 3 4 17.61 15.06 1.04 o 3 3 4 79.59 83.87 2.29 o 4 3 4 49.47 50.33 2.38 o 5 3 4 23.70 25.16 2.72 o 6 3 4 16.15 11.65 3.87 o -6 4 4 52.87 46.03 4.18 o -5 4 4 143.57 140.88 3.41 o -4 4 4 457.25 444.59 5.42 o -3 4 4 60.86 51.64 2.06 o -2 4 4 110.22 115.12 2.58 o -1 4 4 207.26 201.66 3.17 o 0 4 4 11.05 9.78 1.08 o 1 4 4 127.69 120.52 2.53 o 2 4 4 53.43 54.27 1.81 o 3 4 4 155.21 156.46 3.92 o 4 4 4 302.00 294.39 5.20 o 5 4 4 2.45 0.75 2.21 o -5 5 4 114.77 115.04 3.46 o -4 5 4 192.90 198.15 4.40 o -3 5 4 305.58 333.97 4.93 o -2 5 4 0.03 -0.99 1.13 o -1 5 4 150.86 166.27 3.42 o 0 5 4 640.70 610.12 6.82 o 1 5 4 285.92 267.16 3.71 o 2 5 4 392.66 367.12 5.14 o 3 5 4 651.81 627.36 9.35 o 4 5 4 0.00 -2.55 1.73 o 5 5 4 114.75 115.91 5.85 o -4 6 4 182.65 181.89 6.76 o -3 6 4 9.64 6.94 1.78 o -2 6 4 146.23 152.63 4.89 o -1 6 4 114.57 111.83 3.19 o 0 6 4 0.04 -1.22 1.29 o 1 6 4 78.94 81.22 2.55 o 2 6 4 101.51 103.09 2.75 o 3 6 4 7.25 6.13 1.69 o 4 6 4 196.09 202.77 6.80 o -3 7 4 18.12 16.63 2.49 o -2 7 4 0.63 0.80 1.72 o -1 7 4 0.34 -2.32 1.55 o 0 7 4 0.22 -0.80 1.56 o 1 7 4 10.42 10.21 1.90 o 2 7 4 0.28 -2.35 1.57 o 3 7 4 34.02 29.77 2.59 o -2 8 4 18.53 19.95 2.67 o -1 8 4 32.12 30.49 2.60 o 0 8 4 25.24 23.05 2.43 o 1 8 4 2.58 0.42 1.65 o 2 8 4 15.31 13.10 2.28 o -6 1 5 14.05 16.67 1.89 o -5 1 5 125.45 122.35 3.06 o -4 1 5 3.34 0.85 1.05 o -3 1 5 117.96 114.37 2.05 o -2 1 5 6.11 4.72 0.68 o -1 1 5 103.06 101.59 1.47 o 0 1 5 808.74 786.29 7.30 o 1 1 5 373.57 379.14 3.83 o 2 1 5 413.39 406.83 3.97 o 3 1 5 663.05 664.03 5.23 o 4 1 5 11.25 11.57 1.46 o 5 1 5 38.67 44.32 2.80 o 6 1 5 31.27 34.14 3.44 o -6 2 5 25.50 25.78 2.14 o -5 2 5 86.79 83.84 2.74 o -4 2 5 583.98 567.33 5.71 o -3 2 5 789.45 751.57 5.97 o -2 2 5 77.18 80.00 1.73 o -1 2 5 2493.02 2475.72 15.45 o 0 2 5 265.28 263.83 3.86 o 1 2 5 368.26 355.47 4.66 o 2 2 5 92.66 91.87 2.24 o 3 2 5 24.58 22.18 1.30 o 4 2 5 138.54 143.62 3.39 o 5 2 5 77.49 79.14 3.74 o 6 2 5 58.29 51.59 5.21 o -6 3 5 47.96 47.22 2.53 o -5 3 5 67.24 72.38 2.93 o -4 3 5 24.40 23.50 1.50 o -3 3 5 105.44 108.79 2.21 o -2 3 5 368.79 364.23 3.79 o -1 3 5 91.96 98.61 1.87 o 0 3 5 1874.18 1889.11 16.57 o 1 3 5 166.96 165.90 3.85 o 2 3 5 477.84 460.92 5.97 o 3 3 5 633.00 610.52 6.86 o 4 3 5 96.53 97.29 3.11 o 5 3 5 44.52 48.37 3.38 o -5 4 5 33.87 32.70 2.22 o -4 4 5 157.36 153.25 3.37 o -3 4 5 25.65 27.13 1.64 o -2 4 5 22.88 28.63 1.46 o -1 4 5 190.94 181.72 4.19 o 0 4 5 165.20 165.55 3.43 o 1 4 5 136.90 130.87 3.58 o 2 4 5 214.21 214.72 4.19 o 3 4 5 18.44 19.80 1.50 o 4 4 5 77.37 79.66 3.07 o 5 4 5 1.43 1.30 2.26 o -5 5 5 4.58 3.19 1.61 o -4 5 5 5.47 5.86 1.79 o -3 5 5 5.46 4.53 1.44 o -2 5 5 40.40 41.49 2.55 o -1 5 5 26.03 29.67 1.83 o 0 5 5 4.08 0.88 1.42 o 1 5 5 1.36 3.05 1.46 o 2 5 5 0.25 -0.57 1.09 o 3 5 5 20.02 23.40 2.08 o 4 5 5 0.55 -0.23 1.97 o -4 6 5 189.27 200.24 5.39 o -3 6 5 27.04 26.49 2.38 o -2 6 5 30.11 39.73 2.40 o -1 6 5 77.94 79.45 2.87 o 0 6 5 60.79 59.63 2.50 o 1 6 5 14.61 14.23 1.56 o 2 6 5 66.33 65.88 2.50 o 3 6 5 11.16 11.78 1.82 o 4 6 5 67.33 62.09 3.65 o -3 7 5 49.84 48.49 3.32 o -2 7 5 152.95 156.10 4.44 o -1 7 5 48.64 48.48 2.70 o 0 7 5 391.00 393.41 6.16 o 1 7 5 18.45 22.49 2.17 o 2 7 5 93.71 93.95 2.95 o 3 7 5 130.50 130.51 4.16 o -2 8 5 20.76 17.54 2.95 o -1 8 5 193.26 193.25 4.85 o 0 8 5 20.50 18.15 2.31 o 1 8 5 93.20 92.52 3.33 o -6 0 6 255.01 247.20 6.57 o -5 0 6 0.99 -0.29 2.55 o -4 0 6 1466.51 1441.64 16.24 o -3 0 6 664.23 656.16 7.66 o -2 0 6 510.98 545.25 6.05 o -1 0 6 1403.18 1350.12 15.25 o 0 0 6 804.66 825.28 13.09 o 1 0 6 42.67 49.02 1.62 o 2 0 6 839.74 842.09 9.16 o 3 0 6 267.92 274.39 5.60 o 4 0 6 223.41 239.49 7.49 o 5 0 6 158.11 159.84 9.91 o -6 1 6 0.80 0.72 1.54 o -5 1 6 260.66 256.29 4.28 o -4 1 6 199.57 195.62 3.19 o -3 1 6 90.30 86.94 1.89 o -2 1 6 342.62 334.10 3.41 o -1 1 6 85.37 90.47 1.55 o 0 1 6 552.24 497.34 5.32 o 1 1 6 77.53 83.74 1.99 o 2 1 6 60.09 51.94 1.64 o 3 1 6 469.01 467.23 5.12 o 4 1 6 331.14 321.29 6.14 o 5 1 6 26.72 23.57 3.82 o -6 2 6 6.55 7.33 1.74 o -5 2 6 0.00 0.44 1.29 o -4 2 6 24.80 26.11 1.66 o -3 2 6 93.68 90.25 1.88 o -2 2 6 1.87 0.48 0.74 o -1 2 6 300.67 299.20 3.90 o 0 2 6 19.17 17.77 1.37 o 1 2 6 32.70 31.12 1.63 o 2 2 6 19.44 17.47 1.28 o 3 2 6 19.84 23.20 1.62 o 4 2 6 0.01 -1.87 1.25 o 5 2 6 55.51 48.94 3.47 o -6 3 6 6.03 3.89 1.83 o -5 3 6 1.20 -0.97 1.41 o -4 3 6 14.64 10.58 1.29 o -3 3 6 11.13 8.47 1.21 o -2 3 6 29.78 31.11 1.33 o -1 3 6 0.25 -0.16 1.00 o 0 3 6 216.50 234.41 5.49 o 1 3 6 0.33 -0.16 1.11 o 2 3 6 79.99 78.18 3.11 o 3 3 6 41.08 42.49 2.00 o 4 3 6 28.91 28.72 2.10 o 5 3 6 0.00 -1.28 2.31 o -5 4 6 7.77 6.35 1.63 o -4 4 6 397.66 402.60 6.33 o -3 4 6 273.02 277.12 4.35 o -2 4 6 81.13 88.63 2.69 o -1 4 6 655.69 654.04 9.22 o 0 4 6 252.54 249.64 4.25 o 1 4 6 11.79 10.14 2.21 o 2 4 6 216.54 208.12 4.12 o 3 4 6 49.36 48.51 2.38 o 4 4 6 51.50 49.79 2.57 o 5 4 6 61.04 62.15 4.50 o -5 5 6 324.03 313.20 6.86 o -4 5 6 113.31 112.77 4.45 o -3 5 6 195.56 205.19 4.80 o -2 5 6 152.12 161.44 3.66 o -1 5 6 35.09 47.39 2.33 o 0 5 6 130.32 142.60 3.66 o 1 5 6 180.31 175.61 4.24 o 2 5 6 5.99 4.25 1.63 o 3 5 6 496.62 485.37 5.65 o 4 5 6 180.05 172.18 4.94 o -4 6 6 112.24 123.30 4.50 o -3 6 6 151.10 155.05 4.20 o -2 6 6 29.15 28.02 2.55 o -1 6 6 322.30 327.86 5.59 o 0 6 6 38.22 37.71 2.13 o 1 6 6 32.29 34.64 2.09 o 2 6 6 75.42 75.46 2.85 o 3 6 6 50.27 51.35 2.50 o 4 6 6 9.60 13.11 6.85 o -3 7 6 17.27 19.46 2.73 o -2 7 6 40.92 45.69 2.84 o -1 7 6 0.07 -1.11 1.66 o 0 7 6 6.69 5.91 1.77 o 1 7 6 1.12 2.14 1.54 o 2 7 6 9.14 8.45 1.73 o -1 8 6 65.64 62.49 3.26 o 0 8 6 21.41 23.92 2.45 o -6 1 7 8.92 6.82 1.75 o -5 1 7 193.12 193.24 3.76 o -4 1 7 213.12 206.47 3.26 o -3 1 7 7.83 7.10 0.95 o -2 1 7 86.63 87.98 1.82 o -1 1 7 13.79 13.40 1.23 o 0 1 7 0.41 1.28 0.87 o 1 1 7 193.69 191.78 3.07 o 2 1 7 4.41 4.96 1.37 o 3 1 7 382.04 369.00 4.94 o 4 1 7 158.62 163.52 5.08 o 5 1 7 56.11 51.10 4.63 o -6 2 7 133.01 132.80 3.80 o -5 2 7 16.57 15.96 2.39 o -4 2 7 238.87 237.60 3.48 o -3 2 7 270.66 251.64 3.63 o -2 2 7 1.25 -0.40 0.74 o -1 2 7 1021.82 988.47 8.96 o 0 2 7 1553.31 1511.77 13.74 o 1 2 7 25.70 21.13 1.60 o 2 2 7 805.70 783.82 7.57 o 3 2 7 209.66 217.58 3.55 o 4 2 7 14.70 16.98 1.82 o 5 2 7 92.86 92.42 5.85 o -5 3 7 283.97 277.51 4.75 o -4 3 7 164.27 163.43 4.05 o -3 3 7 1.82 -0.32 1.18 o -2 3 7 175.78 179.76 3.20 o -1 3 7 293.32 292.56 4.24 o 0 3 7 78.23 83.43 3.41 o 1 3 7 508.83 516.10 7.45 o 2 3 7 4.66 4.09 1.69 o 3 3 7 464.08 447.34 7.71 o 4 3 7 164.72 164.93 4.08 o 5 3 7 14.00 6.89 2.66 o -5 4 7 11.18 9.50 2.29 o -4 4 7 115.20 116.09 3.65 o -3 4 7 73.65 71.96 2.81 o -2 4 7 14.07 21.23 1.87 o -1 4 7 53.97 56.29 2.80 o 0 4 7 157.01 149.55 4.26 o 1 4 7 22.46 23.02 2.30 o 2 4 7 268.34 268.05 8.84 o 3 4 7 140.72 141.93 3.34 o 4 4 7 58.00 55.66 2.75 o -4 5 7 15.68 14.73 2.48 o -3 5 7 0.19 2.17 1.57 o -2 5 7 0.12 2.94 1.48 o -1 5 7 24.44 26.59 2.15 o 0 5 7 0.48 -0.27 1.36 o 1 5 7 21.46 21.59 2.52 o 2 5 7 4.13 3.47 1.60 o 3 5 7 2.13 3.64 1.34 o 4 5 7 1.69 2.22 1.81 o -4 6 7 77.07 77.60 3.95 o -3 6 7 80.26 83.15 5.01 o -2 6 7 20.78 18.69 2.19 o -1 6 7 136.34 151.12 3.72 o 0 6 7 78.73 82.56 3.41 o 1 6 7 1.40 0.72 1.61 o 2 6 7 93.30 92.82 3.03 o 3 6 7 63.02 61.33 3.03 o -3 7 7 2.93 4.79 3.64 o -2 7 7 88.36 90.21 4.45 o -1 7 7 90.61 85.58 5.01 o 0 7 7 67.43 71.25 3.03 o 1 7 7 133.98 135.31 5.30 o 2 7 7 9.46 6.82 1.99 o -6 0 8 23.76 15.87 3.17 o -5 0 8 183.37 178.73 6.31 o -4 0 8 34.06 29.70 2.43 o -3 0 8 708.83 696.58 8.06 o -2 0 8 1.84 3.40 1.38 o -1 0 8 1249.52 1215.04 14.41 o 0 0 8 644.80 623.09 8.32 o 1 0 8 5.70 10.47 1.64 o 2 0 8 441.15 420.96 8.33 o 3 0 8 725.58 723.25 18.47 o 5 0 8 241.93 231.42 12.22 o -6 1 8 4.35 2.32 1.85 o -5 1 8 132.98 128.50 4.07 o -4 1 8 431.30 421.67 4.79 o -3 1 8 76.25 72.75 2.07 o -2 1 8 377.40 380.88 3.84 o -1 1 8 560.83 539.12 6.07 o 0 1 8 35.15 28.74 1.53 o 1 1 8 190.11 181.21 3.10 o 2 1 8 1.82 1.89 2.66 o 3 1 8 60.38 51.16 2.85 o 4 1 8 93.44 100.11 5.19 o 5 1 8 14.90 12.16 3.26 o -5 2 8 1.12 0.30 1.71 o -4 2 8 0.11 -1.45 1.27 o -3 2 8 18.23 19.27 1.60 o -2 2 8 50.36 49.87 1.90 o -1 2 8 39.16 41.68 1.77 o 0 2 8 174.89 165.04 3.23 o 1 2 8 10.94 13.80 1.78 o 2 2 8 54.72 52.14 2.75 o 3 2 8 5.51 5.79 1.90 o 4 2 8 4.26 2.64 1.87 o 5 2 8 2.93 1.04 3.95 o -5 3 8 47.91 46.41 3.23 o -4 3 8 19.14 17.76 2.03 o -3 3 8 17.97 18.92 1.82 o -2 3 8 4.61 4.51 1.31 o -1 3 8 117.40 116.05 3.01 o 0 3 8 0.49 -2.01 1.34 o 1 3 8 57.11 63.76 2.93 o 2 3 8 13.58 9.77 1.83 o 3 3 8 38.76 35.45 2.38 o 4 3 8 0.74 1.38 1.66 o -5 4 8 33.10 24.90 2.72 o -4 4 8 20.66 25.91 2.38 o -3 4 8 191.89 197.30 4.61 o -2 4 8 6.50 6.31 1.56 o -1 4 8 360.92 384.75 7.83 o 0 4 8 406.23 408.33 9.22 o 1 4 8 0.03 -0.27 1.70 o 2 4 8 255.12 250.35 6.01 o 3 4 8 218.17 226.90 4.72 o 4 4 8 2.97 0.79 1.81 o -4 5 8 447.01 448.19 8.13 o -3 5 8 15.08 14.34 2.06 o -2 5 8 392.93 399.39 5.90 o -1 5 8 173.72 185.83 4.31 o 0 5 8 14.69 21.40 2.72 o 1 5 8 91.52 93.75 4.08 o 2 5 8 50.72 51.39 4.23 o 3 5 8 35.31 37.76 2.28 o 4 5 8 170.21 172.70 8.49 o -3 6 8 92.00 89.41 3.59 o -2 6 8 62.42 62.48 3.25 o -1 6 8 119.13 114.23 3.33 o 0 6 8 235.31 233.91 6.26 o 1 6 8 5.70 4.24 2.52 o 2 6 8 104.92 106.65 4.72 o 3 6 8 38.65 36.72 2.39 o -2 7 8 23.96 14.97 2.30 o -1 7 8 31.39 29.89 2.45 o 0 7 8 9.70 6.22 2.22 o 1 7 8 19.69 21.58 2.52 o -5 1 9 30.99 29.51 2.33 o -4 1 9 345.16 347.84 5.16 o -3 1 9 38.27 39.97 2.08 o -2 1 9 223.64 229.72 3.92 o -1 1 9 168.03 163.92 3.75 o 0 1 9 29.87 34.28 1.75 o 1 1 9 2.98 3.63 1.46 o 2 1 9 146.38 147.78 5.50 o 3 1 9 5.10 4.19 1.64 o 4 1 9 140.99 140.08 5.97 o -5 2 9 177.41 192.13 5.66 o -4 2 9 7.83 6.10 1.73 o -3 2 9 118.16 128.39 3.30 o -2 2 9 32.28 29.82 1.67 o -1 2 9 66.19 66.04 2.12 o 0 2 9 535.29 531.15 7.75 o 1 2 9 106.65 122.51 3.75 o 2 2 9 389.21 371.56 7.96 o 3 2 9 563.41 582.93 11.93 o 4 2 9 16.46 19.76 3.73 o -5 3 9 166.80 171.09 5.12 o -4 3 9 402.77 408.19 7.62 o -3 3 9 24.28 22.62 2.02 o -2 3 9 172.22 180.43 3.55 o -1 3 9 423.38 433.97 5.91 o 0 3 9 134.19 132.37 3.79 o 1 3 9 158.15 153.40 5.60 o 2 3 9 297.82 304.45 12.16 o 3 3 9 3.52 -0.33 1.84 o 4 3 9 166.21 164.89 5.40 o -4 4 9 0.78 2.41 1.86 o -3 4 9 151.19 144.78 3.78 o -2 4 9 13.12 14.43 2.23 o -1 4 9 45.26 42.71 2.89 o 0 4 9 12.53 12.79 2.14 o 1 4 9 44.42 45.06 2.94 o 2 4 9 1.00 2.54 2.00 o 3 4 9 199.67 210.73 6.12 o 4 4 9 25.15 24.66 3.17 o -4 5 9 3.85 2.08 2.25 o -3 5 9 5.72 4.83 1.92 o -2 5 9 5.32 1.87 1.61 o -1 5 9 3.32 5.64 1.77 o 0 5 9 3.41 -0.22 2.12 o 1 5 9 1.25 -0.17 3.29 o 2 5 9 10.13 8.47 2.53 o 3 5 9 0.78 2.36 2.74 o -3 6 9 45.83 43.88 3.81 o -2 6 9 6.26 3.87 1.84 o -1 6 9 65.63 62.14 3.18 o 0 6 9 53.96 56.76 3.88 o 1 6 9 0.79 1.70 2.41 o 2 6 9 38.88 44.51 4.70 o -1 7 9 161.63 165.69 6.06 o 0 7 9 28.24 27.93 3.94 o -5 0 10 180.61 190.39 5.88 o -4 0 10 207.24 195.00 7.85 o -3 0 10 67.20 69.52 3.82 o -2 0 10 431.46 460.25 10.21 o -1 0 10 9.38 19.14 3.80 o 0 0 10 453.39 446.76 12.96 o 1 0 10 57.02 61.97 3.42 o 2 0 10 126.02 102.39 5.70 o 3 0 10 383.16 384.04 13.18 o -5 1 10 34.94 37.68 4.00 o -4 1 10 170.75 176.13 4.87 o -3 1 10 114.07 109.58 3.59 o -2 1 10 37.01 38.44 2.86 o -1 1 10 692.57 668.51 12.35 o 0 1 10 258.97 259.03 9.02 o 1 1 10 204.74 198.80 4.57 o 2 1 10 301.43 312.11 8.21 o 3 1 10 1.46 0.80 1.83 o 4 1 10 36.71 32.40 4.99 o -5 2 10 17.72 16.66 2.85 o -4 2 10 0.03 -2.65 1.77 o -3 2 10 0.01 -0.75 1.42 o -2 2 10 22.21 22.75 1.56 o -1 2 10 41.86 46.50 2.86 o 0 2 10 58.04 58.41 4.47 o 1 2 10 62.07 54.76 4.92 o 2 2 10 30.53 34.19 5.51 o 3 2 10 32.07 27.63 3.10 o 4 2 10 0.32 0.57 2.24 o -4 3 10 38.49 38.58 2.66 o -3 3 10 0.25 -1.37 2.00 o -2 3 10 3.05 0.78 1.34 o -1 3 10 64.20 68.65 3.10 o 0 3 10 80.92 73.62 4.40 o 1 3 10 28.78 29.51 3.84 o 2 3 10 53.64 57.48 4.76 o 3 3 10 3.86 -0.97 4.54 o 4 3 10 4.18 0.54 3.11 o -4 4 10 41.93 42.86 2.89 o -3 4 10 22.60 24.32 2.24 o -2 4 10 105.41 107.46 3.14 o -1 4 10 0.08 -2.86 2.03 o 0 4 10 171.00 178.94 7.85 o 1 4 10 45.73 48.63 4.78 o 2 4 10 82.79 87.32 4.33 o 3 4 10 184.96 192.85 11.81 o -3 5 10 154.24 149.64 4.74 o -2 5 10 74.29 76.88 3.00 o -1 5 10 476.13 481.10 8.88 o 0 5 10 52.41 45.16 3.37 o 1 5 10 81.80 92.94 8.76 o 2 5 10 154.16 148.71 7.42 o -2 6 10 83.74 82.35 3.83 o -1 6 10 31.08 31.19 3.32 o 0 6 10 120.09 125.34 5.24 o 1 6 10 92.25 95.53 4.71 o -4 1 11 48.03 45.36 4.04 o -3 1 11 147.04 156.08 4.78 o -2 1 11 37.11 37.90 2.65 o -1 1 11 354.78 354.58 9.83 o 0 1 11 26.11 27.13 2.66 o 1 1 11 16.13 13.16 2.04 o 2 1 11 64.74 68.84 4.74 o 3 1 11 94.77 95.17 5.18 o 4 1 11 0.88 4.47 3.58 o -4 2 11 173.62 173.02 4.63 o -3 2 11 43.87 47.16 3.19 o -2 2 11 210.73 219.45 4.74 o -1 2 11 47.18 56.23 3.71 o 0 2 11 40.72 35.53 5.51 o 1 2 11 153.17 160.74 9.24 o 2 2 11 0.90 3.05 4.02 o 3 2 11 209.74 212.36 11.77 o -4 3 11 171.86 172.49 4.83 o -3 3 11 146.54 150.92 4.17 o -2 3 11 46.66 45.06 2.91 o -1 3 11 340.74 328.03 9.81 o 0 3 11 156.25 150.22 6.71 o 1 3 11 16.19 13.03 5.06 o 2 3 11 281.65 264.57 12.89 o 3 3 11 125.23 143.76 10.50 o -3 4 11 14.78 11.14 2.24 o -2 4 11 199.10 200.01 8.17 o -1 4 11 0.18 1.36 2.36 o 0 4 11 43.19 39.46 3.51 o 1 4 11 3.54 5.61 7.26 o 2 4 11 11.41 13.21 3.95 o 3 4 11 3.26 -3.28 4.84 o -2 5 11 1.37 -2.97 1.98 o -1 5 11 10.00 14.78 3.20 o 0 5 11 0.64 3.41 2.69 o 1 5 11 3.94 1.77 2.67 o 2 5 11 0.33 1.66 3.09 o -4 0 12 217.48 209.30 12.07 o -3 0 12 10.80 4.85 4.47 o -2 0 12 332.35 338.30 12.48 o -1 0 12 367.58 363.78 12.81 o 0 0 12 18.16 19.81 4.17 o 1 0 12 222.41 225.43 11.92 o 2 0 12 23.80 28.14 4.17 o -4 1 12 42.35 34.56 4.66 o -3 1 12 54.96 55.62 6.05 o -2 1 12 0.95 0.20 1.92 o -1 1 12 80.10 86.01 5.85 o 0 1 12 264.36 268.62 8.89 o 1 1 12 1.69 1.04 2.60 o 2 1 12 322.04 340.84 13.18 o 3 1 12 149.07 159.02 9.98 o -4 2 12 6.60 3.98 3.07 o -3 2 12 5.03 4.98 2.57 o -2 2 12 1.75 2.93 2.22 o -1 2 12 22.76 20.74 2.94 o 0 2 12 13.34 16.83 4.84 o 1 2 12 58.00 61.45 6.85 o 2 2 12 24.32 33.15 5.96 o 3 2 12 23.61 27.56 6.33 o -3 3 12 2.16 2.53 1.86 o -2 3 12 11.24 8.88 2.91 o -1 3 12 8.65 14.97 5.66 o 0 3 12 30.06 25.47 6.03 o 1 3 12 0.70 -2.09 4.25 o 2 3 12 73.59 79.10 8.42 o -3 4 12 0.01 -1.11 1.94 o -2 4 12 112.16 109.67 5.37 o -1 4 12 109.50 115.81 4.59 o 0 4 12 1.93 0.95 3.56 o 1 4 12 95.86 86.25 9.09 o 2 4 12 9.14 3.13 4.99 o -1 5 12 141.11 149.80 13.87 o 0 5 12 156.69 161.31 5.83 o -3 1 13 36.97 39.27 3.81 o -2 1 13 60.89 63.94 3.86 o -1 1 13 68.38 71.45 4.77 o 0 1 13 119.99 124.46 8.42 o 1 1 13 10.75 5.29 4.17 o 2 1 13 57.00 52.30 6.59 o -3 2 13 6.58 5.67 2.84 o -2 2 13 226.45 235.92 19.65 o -1 2 13 251.00 266.51 13.18 o 0 2 13 4.61 4.84 4.69 o 1 2 13 127.10 138.09 9.31 o 2 2 13 104.31 118.73 9.09 o -2 3 13 53.34 45.71 4.52 o -1 3 13 61.46 72.99 8.86 o 0 3 13 153.61 159.25 10.87 o 1 3 13 2.90 2.76 4.69 o -1 4 13 145.06 122.01 11.17 o 0 4 13 12.02 14.60 5.96 o -2 0 14 80.17 80.02 9.24 o -1 0 14 351.21 363.26 13.85 o 0 0 14 45.63 51.58 4.38 o 1 0 14 126.25 119.55 8.27 o -2 1 14 39.77 39.33 3.19 o -1 1 14 0.30 -6.37 4.25 o 0 1 14 33.55 33.07 5.96 o 1 1 14 49.54 58.69 6.55 o -2 2 14 13.87 11.31 3.50 o -1 2 14 1.13 -2.23 5.21 o 0 2 14 6.97 13.48 5.36 o 1 2 14 0.01 0.07 4.39 o