#------------------------------------------------------------------------------ #$Date: 2018-01-13 08:05:03 +0200 (Sat, 13 Jan 2018) $ #$Revision: 205169 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/23/2242320.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242320 _cell_angle_alpha 90.000 _cell_angle_beta 104.116 _cell_angle_gamma 90.000 _cell_length_a 11.8359 _cell_length_b 12.0825 _cell_length_c 16.5811 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.8373 _cod_data_source_file hb77235dsup4.hkl _cod_data_source_block 5d _shelx_title ' d1773_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.59 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1290.61 1352.33 78.94 o 4 0 0 18514.54 20679.35 1176.32 o 6 0 0 33.61 13.29 2.42 o 8 0 0 9.39 2.37 0.76 o 10 0 0 954.62 972.10 19.57 o 12 0 0 406.17 383.18 13.55 o 1 1 0 10709.85 9379.45 237.59 o 2 1 0 217.02 221.26 9.68 o 3 1 0 9399.77 9274.40 373.47 o 4 1 0 15186.02 14507.82 472.51 o 5 1 0 2.43 2.01 1.61 o 6 1 0 137.41 127.56 6.27 o 7 1 0 2903.36 2921.15 118.33 o 8 1 0 609.44 588.09 8.13 o 9 1 0 43.34 50.07 1.74 o 10 1 0 19.55 18.32 1.00 o 11 1 0 528.23 536.47 9.15 o 12 1 0 2.24 3.40 0.84 o 13 1 0 951.85 991.01 23.45 o 0 2 0 22269.08 19374.41 779.08 o 1 2 0 14539.50 13896.91 327.66 o 2 2 0 434.28 435.14 12.53 o 3 2 0 507.84 694.08 57.80 o 4 2 0 5862.76 6032.62 197.86 o 5 2 0 157.45 160.69 5.88 o 6 2 0 4629.86 4826.14 194.48 o 7 2 0 778.50 800.25 29.66 o 8 2 0 1901.07 1868.48 24.68 o 9 2 0 1350.30 1325.81 22.32 o 10 2 0 136.96 147.90 2.74 o 11 2 0 30.80 29.16 1.14 o 12 2 0 328.32 311.32 6.69 o 13 2 0 151.93 132.61 4.35 o 1 3 0 7163.88 6746.40 171.63 o 2 3 0 182.13 177.21 5.44 o 3 3 0 7689.51 7210.43 183.09 o 4 3 0 1242.37 1232.00 31.55 o 5 3 0 4267.70 4510.90 128.36 o 6 3 0 23.01 20.96 1.01 o 7 3 0 1056.76 952.19 14.92 o 8 3 0 2618.62 2507.39 32.90 o 9 3 0 25.84 32.28 1.03 o 10 3 0 55.56 42.99 1.34 o 11 3 0 53.20 48.03 1.96 o 12 3 0 4.15 1.14 0.90 o 13 3 0 171.34 162.97 4.88 o 0 4 0 700.87 708.95 29.19 o 1 4 0 1939.91 1817.76 42.31 o 2 4 0 515.28 528.47 11.63 o 3 4 0 68.78 72.33 2.28 o 4 4 0 6.28 18.53 1.00 o 5 4 0 177.36 147.42 4.87 o 6 4 0 983.38 1019.51 29.50 o 7 4 0 1317.61 1290.16 18.20 o 8 4 0 806.15 822.02 12.58 o 9 4 0 463.31 427.06 7.64 o 10 4 0 441.18 432.93 7.80 o 11 4 0 380.05 396.08 6.87 o 12 4 0 5.63 6.05 0.89 o 13 4 0 0.40 -0.93 0.93 o 1 5 0 947.75 948.84 21.25 o 2 5 0 33.57 36.48 1.23 o 3 5 0 438.48 525.33 12.60 o 4 5 0 1025.85 1130.74 29.07 o 5 5 0 780.90 902.14 26.28 o 6 5 0 124.49 117.25 2.49 o 7 5 0 292.54 283.18 4.70 o 8 5 0 1247.25 1237.31 19.25 o 9 5 0 327.76 350.55 5.73 o 10 5 0 57.95 64.66 1.94 o 11 5 0 6.70 7.09 0.83 o 12 5 0 570.56 550.02 10.92 o 0 6 0 1212.11 1051.23 30.25 o 1 6 0 599.78 604.05 14.33 o 2 6 0 1386.19 1460.22 34.14 o 3 6 0 616.62 675.93 17.57 o 4 6 0 137.06 105.76 4.32 o 5 6 0 917.03 931.89 15.65 o 6 6 0 787.64 705.04 11.14 o 7 6 0 56.12 60.82 1.49 o 8 6 0 18.49 9.98 0.87 o 9 6 0 52.01 43.27 2.19 o 10 6 0 583.05 566.69 9.47 o 11 6 0 225.62 235.92 4.36 o 12 6 0 847.77 805.12 16.46 o 1 7 0 290.63 259.19 7.06 o 2 7 0 612.49 608.41 15.95 o 3 7 0 13.46 15.29 0.80 o 4 7 0 828.47 786.07 11.39 o 5 7 0 6.65 4.72 0.59 o 6 7 0 540.70 539.03 8.58 o 7 7 0 143.25 132.90 2.79 o 8 7 0 882.37 895.72 14.61 o 9 7 0 48.00 45.64 1.35 o 10 7 0 45.89 55.52 1.52 o 11 7 0 2.24 1.38 0.53 o 0 8 0 1211.77 1293.21 28.07 o 1 8 0 56.47 44.53 1.05 o 2 8 0 8.72 13.77 0.62 o 3 8 0 22.73 22.41 0.71 o 4 8 0 149.00 143.52 2.48 o 5 8 0 341.71 347.89 5.29 o 6 8 0 679.06 717.27 11.71 o 7 8 0 414.94 446.34 7.00 o 8 8 0 0.06 1.13 0.62 o 9 8 0 28.50 37.30 1.17 o 10 8 0 506.35 490.55 8.39 o 11 8 0 74.13 66.62 1.98 o 1 9 0 22.21 22.43 0.82 o 2 9 0 139.16 116.17 1.96 o 3 9 0 116.94 110.96 2.05 o 4 9 0 459.75 489.89 7.80 o 5 9 0 8.13 11.04 1.14 o 6 9 0 12.23 13.41 0.88 o 7 9 0 231.80 242.93 4.20 o 8 9 0 420.61 428.57 7.16 o 9 9 0 23.21 21.47 1.00 o 10 9 0 2.33 1.33 0.62 o 0 10 0 21.40 20.27 1.11 o 1 10 0 815.86 844.87 12.68 o 2 10 0 1.48 3.32 0.67 o 3 10 0 56.17 58.34 1.38 o 4 10 0 198.75 208.08 3.50 o 5 10 0 114.70 126.74 2.67 o 6 10 0 1028.86 1064.48 17.84 o 7 10 0 47.61 52.16 1.53 o 8 10 0 1.27 -0.18 0.64 o 9 10 0 1.63 1.73 0.60 o 1 11 0 0.31 -0.04 0.67 o 2 11 0 6.95 6.33 0.74 o 3 11 0 14.80 9.60 0.80 o 4 11 0 950.30 965.10 16.91 o 5 11 0 11.19 12.82 0.93 o 6 11 0 119.14 130.82 2.89 o 7 11 0 14.50 10.04 0.86 o 8 11 0 0.72 2.20 0.65 o 0 12 0 170.05 183.54 5.03 o 1 12 0 74.66 80.43 2.00 o 2 12 0 19.61 18.92 0.85 o 3 12 0 0.95 -0.07 0.79 o 4 12 0 30.87 26.50 1.24 o 5 12 0 3.73 3.23 0.80 o 6 12 0 12.34 14.45 0.89 o 7 12 0 10.90 6.62 0.80 o 1 13 0 7.82 7.73 0.88 o 2 13 0 269.15 257.79 5.35 o 3 13 0 66.29 60.61 1.87 o 4 13 0 7.21 5.62 0.82 o 5 13 0 114.36 96.18 2.35 o 0 14 0 327.09 321.77 9.80 o 1 14 0 1.52 0.06 0.73 o 2 14 0 12.47 10.03 1.12 o 3 14 0 42.18 34.07 5.18 o -13 0 1 26.85 33.73 2.63 o -11 0 1 145.34 165.79 4.29 o -9 0 1 620.43 655.09 16.07 o -7 0 1 1608.45 1501.71 86.99 o -5 0 1 54.09 48.84 2.61 o -3 0 1 7013.60 7674.91 438.16 o -1 0 1 5417.51 4984.67 164.07 o 1 0 1 36.18 49.35 2.80 o 3 0 1 2210.30 1983.37 238.01 o 5 0 1 130.52 159.09 10.07 o 7 0 1 919.72 804.68 27.71 o 9 0 1 74.80 71.54 2.52 o 11 0 1 1491.88 1454.18 34.74 o 13 0 1 13.03 11.36 1.59 o -13 1 1 10.14 6.27 0.78 o -12 1 1 360.75 333.73 6.06 o -11 1 1 49.93 55.28 1.62 o -10 1 1 1504.77 1426.20 22.20 o -9 1 1 276.67 282.15 4.69 o -8 1 1 537.98 479.25 7.26 o -7 1 1 949.89 1025.93 81.13 o -6 1 1 2919.16 3066.99 105.09 o -5 1 1 1064.76 1154.28 36.39 o -4 1 1 6213.98 5983.83 152.07 o -3 1 1 4032.00 4007.90 131.51 o -2 1 1 1211.80 1186.91 41.04 o -1 1 1 53.21 45.29 1.22 o 0 1 1 3925.87 3870.20 83.23 o 1 1 1 3399.31 3416.42 87.39 o 2 1 1 46.98 36.28 1.54 o 3 1 1 4132.44 3882.96 127.48 o 4 1 1 5.70 11.15 2.34 o 5 1 1 91.05 107.13 5.13 o 6 1 1 2493.99 2701.53 109.36 o 7 1 1 1088.81 1161.56 24.93 o 8 1 1 780.46 767.45 10.22 o 9 1 1 55.12 49.24 1.39 o 10 1 1 1049.29 1011.44 15.45 o 11 1 1 2.09 4.37 1.05 o 12 1 1 152.68 159.40 3.66 o 13 1 1 93.62 82.06 2.48 o -13 2 1 27.05 25.37 1.33 o -12 2 1 58.91 61.62 1.79 o -11 2 1 414.65 440.43 7.27 o -10 2 1 110.61 98.76 2.20 o -9 2 1 60.20 70.63 1.63 o -8 2 1 363.97 383.92 5.48 o -7 2 1 1945.82 1716.05 141.55 o -6 2 1 193.45 244.03 8.67 o -5 2 1 9425.34 9567.53 272.04 o -4 2 1 451.46 452.59 13.19 o -3 2 1 994.62 1083.54 44.00 o -2 2 1 1706.60 1711.66 43.55 o -1 2 1 104.27 119.58 3.20 o 0 2 1 507.24 475.62 11.21 o 1 2 1 4477.39 4611.57 118.82 o 2 2 1 182.84 205.02 6.04 o 3 2 1 4888.95 4838.58 173.99 o 4 2 1 65.05 56.04 2.27 o 5 2 1 10.84 5.41 1.26 o 6 2 1 3.60 1.57 1.26 o 7 2 1 107.84 107.42 2.37 o 8 2 1 4.62 4.62 0.57 o 9 2 1 254.32 221.80 3.38 o 10 2 1 48.10 38.41 1.21 o 11 2 1 382.63 417.91 8.48 o 12 2 1 11.29 9.52 0.99 o 13 2 1 11.82 10.06 0.94 o -13 3 1 118.95 126.65 3.20 o -12 3 1 86.75 90.87 2.42 o -11 3 1 634.96 613.29 9.88 o -10 3 1 1705.76 1637.79 24.46 o -9 3 1 531.43 504.87 8.20 o -8 3 1 43.28 41.57 1.18 o -7 3 1 535.09 522.40 7.84 o -6 3 1 451.89 429.57 12.88 o -5 3 1 20.33 33.71 2.13 o -4 3 1 64.28 89.88 2.69 o -3 3 1 37.45 35.16 1.11 o -2 3 1 339.36 327.96 8.57 o -1 3 1 324.83 326.00 10.21 o 0 3 1 18.20 25.50 1.18 o 1 3 1 4914.41 5062.38 128.84 o 2 3 1 13239.17 12969.64 383.19 o 3 3 1 625.81 621.93 18.07 o 4 3 1 8.93 21.53 1.30 o 5 3 1 4.33 8.19 1.16 o 6 3 1 1190.19 1192.49 40.00 o 7 3 1 0.34 3.15 0.57 o 8 3 1 295.70 275.93 4.42 o 9 3 1 0.76 2.12 0.71 o 10 3 1 1.01 1.24 0.83 o 11 3 1 163.63 150.24 3.78 o 12 3 1 27.54 22.06 1.31 o 13 3 1 2.82 5.54 0.91 o -13 4 1 184.88 178.14 4.57 o -12 4 1 2.87 4.33 0.82 o -11 4 1 1330.93 1385.61 23.23 o -10 4 1 996.18 1009.71 17.11 o -9 4 1 1308.66 1261.39 21.24 o -8 4 1 436.73 441.70 9.17 o -7 4 1 475.87 504.24 8.47 o -6 4 1 615.00 680.42 20.03 o -5 4 1 1287.41 1265.85 32.53 o -4 4 1 280.41 276.96 6.82 o -3 4 1 130.56 134.34 3.52 o -2 4 1 4678.64 4415.40 112.27 o -1 4 1 2028.11 2010.12 57.29 o 0 4 1 172.69 177.52 4.86 o 1 4 1 1092.23 1165.63 27.27 o 2 4 1 1681.29 1724.28 40.20 o 3 4 1 2556.63 2714.46 77.18 o 4 4 1 167.40 199.22 6.23 o 5 4 1 294.06 299.04 9.10 o 6 4 1 13.92 4.98 0.80 o 7 4 1 172.73 188.22 3.04 o 8 4 1 116.50 119.13 2.35 o 9 4 1 71.48 67.76 1.84 o 10 4 1 138.17 141.03 2.88 o 11 4 1 28.95 48.38 1.73 o 12 4 1 7.59 9.43 0.93 o -12 5 1 13.55 11.34 0.74 o -11 5 1 173.19 182.89 3.66 o -10 5 1 81.74 74.76 2.02 o -9 5 1 4.41 1.48 0.81 o -8 5 1 679.35 674.39 11.12 o -7 5 1 175.97 173.14 2.85 o -6 5 1 275.03 267.67 4.83 o -5 5 1 1232.48 1370.26 45.34 o -4 5 1 2808.97 2770.42 76.72 o -3 5 1 3.74 3.57 0.65 o -2 5 1 1135.66 1058.28 21.57 o -1 5 1 213.07 258.71 6.35 o 0 5 1 374.44 369.13 8.87 o 1 5 1 33.64 29.93 1.15 o 2 5 1 1438.91 1468.73 37.61 o 3 5 1 84.63 93.89 3.35 o 4 5 1 275.58 327.31 9.91 o 5 5 1 110.86 100.25 3.60 o 6 5 1 2002.78 1950.14 27.17 o 7 5 1 94.83 95.85 2.10 o 8 5 1 216.16 193.84 3.65 o 9 5 1 154.42 174.63 3.26 o 10 5 1 84.90 79.40 2.05 o 11 5 1 171.30 179.91 3.92 o 12 5 1 4.94 6.57 0.93 o -12 6 1 14.69 23.35 0.96 o -11 6 1 18.98 21.43 0.98 o -10 6 1 18.45 16.27 1.02 o -9 6 1 562.94 573.76 10.86 o -8 6 1 183.90 181.98 3.71 o -7 6 1 59.50 57.04 1.41 o -6 6 1 2.53 2.83 0.53 o -5 6 1 1214.17 1128.67 20.30 o -4 6 1 133.10 107.81 3.76 o -3 6 1 97.15 106.65 3.30 o -2 6 1 405.54 399.10 9.67 o -1 6 1 5316.72 5331.01 107.07 o 0 6 1 1050.98 1017.48 23.95 o 1 6 1 676.11 654.26 15.54 o 2 6 1 3.93 3.62 0.85 o 3 6 1 401.93 460.46 13.74 o 4 6 1 2.07 3.31 0.92 o 5 6 1 1007.36 953.06 13.48 o 6 6 1 1.00 3.88 0.67 o 7 6 1 468.33 473.00 7.02 o 8 6 1 216.27 216.22 3.73 o 9 6 1 5.40 4.46 0.82 o 10 6 1 1042.60 1027.64 17.31 o 11 6 1 57.43 56.82 1.74 o 12 6 1 1.37 1.21 0.64 o -12 7 1 678.14 571.50 31.80 o -11 7 1 3.73 2.57 0.54 o -10 7 1 69.90 56.42 1.44 o -9 7 1 203.77 205.57 4.00 o -8 7 1 407.29 437.98 7.67 o -7 7 1 80.06 80.78 1.90 o -6 7 1 60.63 62.38 1.49 o -5 7 1 466.14 453.74 6.72 o -4 7 1 89.45 121.26 2.10 o -3 7 1 28.70 27.19 1.16 o -2 7 1 2252.93 2382.74 60.70 o -1 7 1 75.58 93.98 2.99 o 0 7 1 22.60 36.32 1.68 o 1 7 1 61.61 78.18 2.39 o 2 7 1 428.70 403.63 10.73 o 3 7 1 1104.29 1101.05 20.07 o 4 7 1 10.14 14.58 0.66 o 5 7 1 617.81 596.90 9.81 o 6 7 1 187.49 177.22 3.34 o 7 7 1 152.95 158.24 2.87 o 8 7 1 1615.13 1609.56 24.78 o 9 7 1 4.97 2.47 0.71 o 10 7 1 21.62 25.88 1.00 o 11 7 1 10.33 12.28 0.68 o -11 8 1 134.12 137.89 2.74 o -10 8 1 250.39 263.33 4.77 o -9 8 1 44.23 37.99 1.23 o -8 8 1 241.71 232.65 3.89 o -7 8 1 550.81 571.29 8.75 o -6 8 1 1073.45 1115.37 16.67 o -5 8 1 34.45 35.19 1.14 o -4 8 1 7.95 10.10 0.74 o -3 8 1 540.94 551.49 8.35 o -2 8 1 180.71 195.85 2.99 o -1 8 1 239.37 228.36 3.65 o 0 8 1 1131.23 1224.08 18.81 o 1 8 1 2202.36 2141.09 30.56 o 2 8 1 149.36 114.56 1.92 o 3 8 1 679.62 662.73 9.70 o 4 8 1 132.30 129.32 2.31 o 5 8 1 598.29 584.04 9.22 o 6 8 1 99.85 92.53 1.94 o 7 8 1 5.50 7.29 0.71 o 8 8 1 22.40 25.59 1.02 o 9 8 1 74.27 83.58 1.89 o 10 8 1 228.59 240.25 5.24 o 11 8 1 27.77 19.07 1.25 o -10 9 1 1.56 2.16 0.59 o -9 9 1 600.61 595.60 11.80 o -8 9 1 92.29 91.47 2.02 o -7 9 1 61.34 64.94 1.62 o -6 9 1 576.36 560.73 9.57 o -5 9 1 15.50 15.24 0.86 o -4 9 1 654.72 643.55 10.51 o -3 9 1 333.74 338.61 5.31 o -2 9 1 944.09 954.70 13.81 o -1 9 1 71.92 78.89 1.50 o 0 9 1 61.17 64.78 1.35 o 1 9 1 249.17 271.57 4.33 o 2 9 1 796.32 814.16 11.50 o 3 9 1 130.32 121.24 2.18 o 4 9 1 1492.81 1570.93 24.17 o 5 9 1 48.95 46.40 1.25 o 6 9 1 73.07 63.82 1.60 o 7 9 1 117.33 107.95 2.20 o 8 9 1 32.63 32.66 1.34 o 9 9 1 65.52 76.55 1.73 o 10 9 1 47.54 48.45 1.41 o -9 10 1 63.55 64.39 1.62 o -8 10 1 4.14 2.78 0.70 o -7 10 1 30.91 33.27 1.16 o -6 10 1 421.10 456.29 8.27 o -5 10 1 210.17 219.52 3.80 o -4 10 1 10.91 15.11 0.82 o -3 10 1 9.17 10.18 0.75 o -2 10 1 243.10 283.17 4.69 o -1 10 1 7.62 8.12 0.61 o 0 10 1 158.40 172.76 2.86 o 1 10 1 14.44 16.34 0.90 o 2 10 1 4.75 5.09 0.63 o 3 10 1 43.91 44.82 1.51 o 4 10 1 523.13 576.30 9.11 o 5 10 1 68.15 70.93 1.85 o 6 10 1 433.51 444.51 7.75 o 7 10 1 8.99 9.96 0.92 o 8 10 1 4.25 9.04 0.69 o 9 10 1 319.86 315.38 6.33 o -9 11 1 249.25 245.64 15.71 o -8 11 1 178.87 176.55 3.58 o -7 11 1 83.73 86.20 2.05 o -6 11 1 0.98 1.49 0.76 o -5 11 1 35.09 28.81 1.11 o -4 11 1 875.95 917.24 14.82 o -3 11 1 178.68 183.12 3.18 o -2 11 1 153.22 168.86 3.05 o -1 11 1 328.10 328.27 5.03 o 0 11 1 11.50 13.24 0.82 o 1 11 1 19.28 17.51 0.88 o 2 11 1 35.52 34.70 1.21 o 3 11 1 243.73 251.94 4.44 o 4 11 1 723.71 748.31 12.16 o 5 11 1 17.74 16.26 0.85 o 6 11 1 85.47 81.01 2.09 o 7 11 1 206.11 203.99 4.19 o 8 11 1 702.72 706.64 13.02 o -7 12 1 136.25 137.17 3.46 o -6 12 1 386.43 380.36 7.69 o -5 12 1 59.04 54.49 1.72 o -4 12 1 312.90 314.38 6.14 o -3 12 1 141.70 143.68 3.07 o -2 12 1 352.51 373.69 6.88 o -1 12 1 2.89 2.96 0.79 o 0 12 1 379.84 389.39 7.15 o 1 12 1 8.88 13.27 0.81 o 2 12 1 286.22 272.96 4.71 o 3 12 1 19.03 19.68 1.02 o 4 12 1 23.79 25.79 1.16 o 5 12 1 12.85 16.88 0.98 o 6 12 1 147.26 155.55 3.31 o 7 12 1 213.22 229.20 5.91 o -6 13 1 195.04 206.27 10.88 o -5 13 1 19.64 20.66 0.93 o -4 13 1 207.45 210.74 4.75 o -3 13 1 1.17 1.42 0.69 o -2 13 1 5.48 4.26 0.81 o -1 13 1 3.81 2.79 0.95 o 0 13 1 12.11 14.86 1.04 o 1 13 1 90.52 81.70 2.14 o 2 13 1 148.82 159.35 4.14 o 3 13 1 6.09 7.26 0.86 o 4 13 1 55.80 55.01 1.70 o 5 13 1 520.18 502.48 11.22 o -3 14 1 192.30 193.11 9.82 o -2 14 1 2.09 1.16 0.92 o -1 14 1 69.63 59.40 1.97 o 0 14 1 58.20 62.92 3.27 o 1 14 1 0.13 -0.04 0.72 o 2 14 1 3.22 0.96 0.86 o 3 14 1 17.45 27.39 3.62 o -12 0 2 256.99 249.78 7.25 o -10 0 2 574.41 543.34 13.46 o -8 0 2 833.27 818.63 17.06 o -6 0 2 1392.17 1702.82 69.06 o -4 0 2 3952.73 4444.75 253.29 o -2 0 2 4921.82 4959.07 172.20 o 0 0 2 15167.83 13246.54 544.97 o 2 0 2 1032.94 1064.18 48.73 o 4 0 2 3290.97 3356.63 190.91 o 6 0 2 7785.36 8059.10 458.29 o 8 0 2 0.20 1.30 0.79 o 10 0 2 232.65 217.90 9.23 o 12 0 2 146.11 152.72 5.08 o -13 1 2 237.25 247.68 5.24 o 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1382.87 45.65 o -2 2 2 1452.02 1473.14 37.54 o -1 2 2 2329.80 2313.14 59.12 o 0 2 2 2478.06 2415.26 61.38 o 1 2 2 34588.12 31833.05 1179.48 o 2 2 2 14635.02 14539.49 483.35 o 3 2 2 1845.91 1896.29 62.40 o 4 2 2 30.69 41.88 2.16 o 5 2 2 7658.30 7801.04 344.96 o 6 2 2 1721.09 1662.14 55.34 o 7 2 2 90.34 87.87 1.76 o 8 2 2 60.23 55.94 1.57 o 9 2 2 182.89 175.16 3.13 o 10 2 2 253.27 242.32 4.12 o 11 2 2 8.68 11.86 1.23 o 12 2 2 149.51 151.31 3.76 o 13 2 2 43.77 53.03 2.96 o -13 3 2 290.96 295.50 6.51 o -12 3 2 23.02 18.08 0.89 o -11 3 2 486.38 429.30 7.28 o -10 3 2 270.62 253.66 4.57 o -9 3 2 445.71 454.15 7.44 o -8 3 2 19.31 29.80 1.05 o -7 3 2 127.42 136.10 3.25 o -6 3 2 84.16 85.36 2.98 o -5 3 2 211.35 201.68 5.35 o -4 3 2 2445.05 2378.58 60.59 o -3 3 2 3695.39 3627.41 84.09 o -2 3 2 2625.87 2713.86 77.28 o -1 3 2 439.70 500.72 18.46 o 0 3 2 2278.19 2245.25 57.02 o 1 3 2 35988.39 32880.83 943.64 o 2 3 2 1517.05 1698.41 54.48 o 3 3 2 1829.47 1779.30 50.65 o 4 3 2 441.95 480.91 16.35 o 5 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