#------------------------------------------------------------------------------ #$Date: 2018-01-13 08:05:34 +0200 (Sat, 13 Jan 2018) $ #$Revision: 205170 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/23/2242321.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242321 _cell_angle_alpha 73.682 _cell_angle_beta 86.600 _cell_angle_gamma 88.884 _cell_length_a 12.0684 _cell_length_b 13.9953 _cell_length_c 14.0634 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file su5416Isup2.hkl _cod_data_source_block I _shelx_title ' NM2F2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 272.40 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14816.21 15828.31 157.34 o 3 0 0 468.13 523.97 14.69 o 4 0 0 416.78 445.45 16.09 o 5 0 0 1707.90 1815.58 35.11 o 6 0 0 7776.94 8410.28 110.84 o 7 0 0 0.76 5.21 3.86 o 8 0 0 3379.21 3344.79 45.10 o 9 0 0 0.19 3.72 4.52 o 10 0 0 373.38 341.92 16.67 o 11 0 0 144.99 177.75 19.78 o 12 0 0 772.80 750.53 34.00 o 13 0 0 285.47 280.66 28.80 o 14 0 0 41.63 25.75 14.85 o 15 0 0 5.68 19.85 15.95 o -15 1 0 180.75 224.01 26.67 o -14 1 0 772.95 782.69 42.81 o -13 1 0 54.37 34.51 34.99 o -12 1 0 2.14 10.93 16.48 o -11 1 0 14.47 40.39 12.83 o -10 1 0 168.01 165.25 12.20 o -9 1 0 173.91 152.11 14.49 o -8 1 0 2834.77 2690.25 53.13 o -7 1 0 2213.46 2153.13 43.96 o -6 1 0 6344.47 6221.37 79.54 o -5 1 0 9932.49 9842.66 105.09 o -4 1 0 3706.81 3544.04 47.13 o -3 1 0 28623.37 29388.96 424.92 o -2 1 0 16893.31 17405.14 172.11 o 2 1 0 15181.32 15843.24 233.18 o 3 1 0 24304.73 25233.65 188.97 o 4 1 0 3434.94 3310.82 38.90 o 5 1 0 9434.33 9836.90 116.55 o 6 1 0 5169.56 5195.29 54.67 o 7 1 0 3380.87 3541.98 53.05 o 8 1 0 164.20 212.51 10.15 o 9 1 0 73.01 71.41 8.81 o 10 1 0 29.58 26.47 13.69 o 11 1 0 640.38 614.96 30.19 o 12 1 0 96.93 58.68 12.62 o 13 1 0 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