#------------------------------------------------------------------------------ #$Date: 2018-01-13 08:05:58 +0200 (Sat, 13 Jan 2018) $ #$Revision: 205171 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/23/2242322.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242322 _cell_angle_alpha 90.000 _cell_angle_beta 103.294 _cell_angle_gamma 90.000 _cell_length_a 8.8193 _cell_length_b 15.3698 _cell_length_c 15.4209 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.6519 _cod_data_source_file hb4193Isup2.hkl _cod_data_source_block I _shelx_title ' SFP37_Mo in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -23 0 93.43 64.87 45.67 o 0 -22 0 174.02 183.59 51.87 o 1 -22 0 10.90 9.32 33.33 o 2 -22 0 37.95 55.13 37.33 o 3 -22 0 35.24 -3.49 38.64 o 4 -22 0 22.51 -22.31 49.72 o 1 -21 0 80.84 83.07 43.81 o 2 -21 0 98.98 105.93 37.49 o 3 -21 0 37.69 3.26 38.40 o 4 -21 0 50.47 40.27 38.59 o 5 -21 0 84.09 81.83 39.80 o 0 -20 0 59.28 44.08 26.57 o 1 -20 0 44.43 33.10 17.79 o 2 -20 0 26.53 66.30 17.12 o 3 -20 0 225.95 222.07 34.65 o 4 -20 0 91.50 165.73 36.83 o 5 -20 0 25.30 13.03 52.92 o 6 -20 0 69.06 12.54 85.64 o 1 -19 0 9.85 -5.63 16.14 o 2 -19 0 292.72 318.32 29.60 o 3 -19 0 77.95 60.55 29.72 o 4 -19 0 110.53 80.74 24.53 o 5 -19 0 93.04 79.26 25.41 o 6 -19 0 27.79 -9.90 38.17 o 7 -19 0 51.80 18.96 31.47 o 0 -18 0 57.42 40.50 20.09 o 1 -18 0 87.20 73.10 16.44 o 2 -18 0 66.37 62.39 21.29 o 3 -18 0 427.38 422.10 31.94 o 4 -18 0 109.03 110.71 20.94 o 5 -18 0 78.53 24.95 23.91 o 6 -18 0 85.82 62.37 25.22 o 7 -18 0 12.37 25.52 34.44 o 8 -18 0 8.41 40.80 27.43 o 1 -17 0 20.76 -14.21 14.21 o 2 -17 0 493.36 532.23 23.44 o 3 -17 0 135.84 109.10 15.03 o 4 -17 0 502.09 519.94 28.53 o 5 -17 0 347.45 357.46 28.03 o 6 -17 0 27.10 11.87 18.00 o 7 -17 0 30.75 43.76 21.07 o 8 -17 0 32.97 43.00 23.72 o 9 -17 0 0.34 -31.84 50.04 o 0 -16 0 430.32 478.28 31.12 o 1 -16 0 170.95 152.68 13.92 o 2 -16 0 398.14 435.57 20.87 o 3 -16 0 762.84 741.58 26.93 o 4 -16 0 135.94 109.20 16.55 o 5 -16 0 215.82 238.01 21.77 o 6 -16 0 201.87 130.29 22.32 o 7 -16 0 89.97 101.32 23.01 o 8 -16 0 0.02 -21.38 28.90 o 9 -16 0 27.69 70.93 28.56 o 1 -15 0 806.75 801.70 23.26 o 2 -15 0 682.63 632.88 23.53 o 3 -15 0 302.52 267.88 18.88 o 4 -15 0 224.10 239.55 21.52 o 5 -15 0 374.79 392.63 25.55 o 6 -15 0 205.58 228.02 25.47 o 7 -15 0 56.80 12.93 21.61 o 8 -15 0 253.02 279.87 33.99 o 9 -15 0 12.97 19.10 22.78 o 10 -15 0 12.44 -3.66 20.06 o 0 -14 0 2793.50 2806.80 43.81 o 1 -14 0 100.33 88.90 10.64 o 2 -14 0 417.07 434.12 19.68 o 3 -14 0 326.84 335.52 19.46 o 4 -14 0 179.62 177.48 16.52 o 5 -14 0 106.81 78.85 14.01 o 6 -14 0 221.50 229.08 20.92 o 7 -14 0 435.16 456.51 38.41 o 8 -14 0 11.11 22.74 20.52 o 9 -14 0 187.30 191.98 31.49 o 10 -14 0 34.20 52.91 51.55 o 1 -13 0 2416.63 2344.93 35.64 o 2 -13 0 189.70 177.87 9.61 o 3 -13 0 314.72 316.64 15.30 o 4 -13 0 237.74 229.22 15.19 o 5 -13 0 764.38 731.14 23.80 o 6 -13 0 260.06 252.39 17.77 o 7 -13 0 33.71 27.35 20.01 o 8 -13 0 466.98 503.23 41.43 o 9 -13 0 5.19 -13.74 22.13 o 10 -13 0 117.94 31.04 27.09 o 0 -12 0 7319.73 7514.77 65.02 o 1 -12 0 429.77 397.62 14.02 o 2 -12 0 1217.39 1195.95 21.52 o 3 -12 0 438.12 408.55 14.68 o 4 -12 0 44.51 48.23 8.91 o 5 -12 0 110.79 97.78 12.14 o 6 -12 0 548.95 550.84 29.73 o 7 -12 0 581.00 587.22 28.56 o 8 -12 0 17.66 8.74 15.25 o 9 -12 0 355.61 387.35 30.45 o 10 -12 0 34.24 51.89 26.92 o 1 -11 0 6149.63 6180.74 48.28 o 2 -11 0 630.85 576.77 14.95 o 3 -11 0 513.59 482.10 12.46 o 4 -11 0 37.27 34.63 7.89 o 5 -11 0 607.00 525.57 22.38 o 6 -11 0 362.65 375.53 20.41 o 7 -11 0 81.53 49.00 14.03 o 8 -11 0 1019.30 1112.60 46.40 o 9 -11 0 22.33 -7.86 16.78 o 10 -11 0 127.16 196.56 29.15 o 11 -11 0 23.79 50.20 38.90 o 0 -10 0 7079.11 6882.08 54.62 o 1 -10 0 184.69 166.49 7.08 o 2 -10 0 2570.54 2575.84 29.22 o 3 -10 0 2579.93 2637.91 26.06 o 4 -10 0 976.19 989.70 21.61 o 5 -10 0 684.73 689.82 20.81 o 6 -10 0 723.78 739.35 26.16 o 7 -10 0 811.26 834.59 26.92 o 8 -10 0 35.19 26.80 12.57 o 9 -10 0 265.09 262.43 23.72 o 10 -10 0 107.14 112.86 23.84 o 11 -10 0 61.27 121.78 41.63 o 1 -9 0 1926.83 1857.13 20.12 o 2 -9 0 1574.38 1547.97 18.68 o 3 -9 0 2130.37 2149.15 23.19 o 4 -9 0 1168.89 1156.57 22.50 o 5 -9 0 2373.12 2375.03 37.61 o 6 -9 0 920.34 901.35 22.94 o 7 -9 0 11.63 10.94 9.00 o 8 -9 0 944.30 956.15 32.33 o 9 -9 0 120.85 100.51 18.39 o 10 -9 0 93.18 64.67 17.14 o 11 -9 0 160.70 139.91 28.52 o 12 -9 0 23.27 0.98 31.58 o 0 -8 0 1621.77 1596.58 28.44 o 1 -8 0 49.02 22.49 3.50 o 2 -8 0 999.13 996.75 13.71 o 3 -8 0 4924.29 4677.37 32.32 o 4 -8 0 2735.32 2662.44 30.85 o 5 -8 0 1399.02 1427.36 28.36 o 6 -8 0 2027.59 2013.11 31.31 o 7 -8 0 788.83 746.05 22.12 o 8 -8 0 48.60 38.85 12.73 o 9 -8 0 175.97 181.22 18.95 o 10 -8 0 210.46 169.11 22.26 o 11 -8 0 7.11 -18.74 18.74 o 12 -8 0 75.86 28.18 81.22 o 1 -7 0 2210.49 2320.36 16.31 o 2 -7 0 5936.91 6303.89 34.55 o 3 -7 0 2072.02 2234.58 19.86 o 4 -7 0 1574.01 1581.84 21.93 o 5 -7 0 1676.29 1741.49 25.35 o 6 -7 0 2101.77 2070.97 34.01 o 7 -7 0 439.40 384.22 14.09 o 8 -7 0 185.52 189.20 17.17 o 9 -7 0 211.68 209.25 20.87 o 10 -7 0 219.01 228.23 24.61 o 11 -7 0 199.81 231.29 35.03 o 12 -7 0 78.62 109.05 42.13 o 0 -6 0 194.38 278.50 8.08 o 1 -6 0 6441.19 6575.89 40.01 o 2 -6 0 1089.73 1231.81 11.94 o 3 -6 0 17412.28 17156.87 83.93 o 4 -6 0 2141.22 2023.55 23.58 o 5 -6 0 1996.71 1814.62 27.70 o 6 -6 0 1964.66 1983.09 31.08 o 7 -6 0 32.34 23.35 10.08 o 8 -6 0 112.76 100.45 19.06 o 9 -6 0 16.20 9.72 14.38 o 10 -6 0 220.06 215.52 24.76 o 11 -6 0 29.12 -8.65 17.02 o 12 -6 0 141.28 154.94 29.67 o 1 -5 0 1960.29 1870.64 14.59 o 2 -5 0 19545.63 21101.03 81.68 o 3 -5 0 2957.62 3140.17 19.32 o 4 -5 0 1801.22 1970.76 19.14 o 5 -5 0 5158.84 5248.19 67.45 o 6 -5 0 1368.77 1257.29 34.21 o 7 -5 0 234.45 215.35 16.56 o 8 -5 0 86.86 61.66 14.51 o 9 -5 0 75.18 90.64 18.19 o 10 -5 0 72.92 70.68 18.18 o 11 -5 0 351.09 416.58 35.02 o 12 -5 0 100.58 170.31 24.63 o 0 -4 0 16324.07 15729.13 97.06 o 1 -4 0 4329.73 4223.06 18.28 o 2 -4 0 3420.18 3706.42 19.39 o 3 -4 0 12743.99 13073.15 63.71 o 4 -4 0 1528.89 1409.99 19.13 o 5 -4 0 4595.57 4535.65 52.92 o 6 -4 0 3787.41 3808.70 51.36 o 7 -4 0 1941.78 2019.39 43.92 o 8 -4 0 142.00 114.72 16.98 o 9 -4 0 486.34 471.70 30.11 o 10 -4 0 372.35 384.18 26.70 o 11 -4 0 56.94 80.75 20.15 o 12 -4 0 116.84 91.41 19.82 o 1 -3 0 1555.57 1519.13 10.21 o 2 -3 0 1782.91 1939.82 14.48 o 3 -3 0 3359.86 3608.18 25.16 o 4 -3 0 3721.15 4035.65 29.83 o 5 -3 0 5115.93 5206.82 49.82 o 6 -3 0 2305.67 2296.00 29.88 o 7 -3 0 81.25 72.84 8.93 o 8 -3 0 2489.55 2277.55 60.14 o 9 -3 0 70.89 82.31 17.82 o 10 -3 0 49.62 49.63 16.01 o 11 -3 0 312.33 327.84 29.75 o 12 -3 0 27.40 60.93 18.79 o 1 -2 0 9778.38 9454.67 40.82 o 2 -2 0 11111.93 11086.31 47.55 o 3 -2 0 10410.13 10369.36 81.91 o 4 -2 0 4948.35 4953.92 34.57 o 5 -2 0 1476.91 1540.75 22.46 o 6 -2 0 2885.32 2866.25 36.44 o 7 -2 0 3250.97 3328.99 40.90 o 8 -2 0 214.02 188.80 15.46 o 9 -2 0 1223.94 1322.73 42.36 o 10 -2 0 210.15 214.40 23.29 o 11 -2 0 119.15 106.94 22.50 o 12 -2 0 80.51 136.51 23.22 o 2 -1 0 14411.89 15067.73 59.74 o 3 -1 0 4574.39 4634.00 32.12 o 4 -1 0 410.18 397.11 10.33 o 5 -1 0 2438.15 2470.12 32.99 o 6 -1 0 2521.20 2536.23 34.78 o 7 -1 0 36.43 14.53 8.60 o 8 -1 0 2423.04 2556.62 49.77 o 9 -1 0 57.19 26.43 16.75 o 10 -1 0 349.74 360.98 26.43 o 11 -1 0 64.30 78.70 18.74 o 12 -1 0 3.19 10.04 27.32 o 2 0 0 5549.22 5938.70 30.98 o 3 0 0 1745.88 1709.91 18.67 o 4 0 0 208.70 235.58 8.82 o 5 0 0 110.16 117.08 9.44 o 6 0 0 2662.88 2543.90 41.81 o 7 0 0 3079.14 2992.34 41.82 o 8 0 0 52.94 23.05 12.56 o 9 0 0 984.22 1058.16 35.30 o 10 0 0 319.65 369.39 26.36 o 11 0 0 209.05 204.93 20.71 o 12 0 0 4.13 -6.86 21.42 o 2 1 0 14990.38 15901.96 79.61 o 3 1 0 4688.18 4794.02 34.53 o 4 1 0 454.47 433.58 13.31 o 5 1 0 2514.49 2620.18 36.96 o 6 1 0 2437.36 2409.36 41.52 o 7 1 0 45.21 23.54 8.86 o 8 1 0 2431.69 2459.34 46.71 o 9 1 0 57.96 50.23 12.04 o 10 1 0 350.86 406.16 25.75 o 11 1 0 60.97 48.18 15.70 o 12 1 0 3.99 -20.96 20.96 o 1 2 0 9868.13 9679.77 32.00 o 2 2 0 11605.19 11605.20 41.08 o 3 2 0 10534.07 10542.78 56.46 o 4 2 0 5050.08 5122.49 39.09 o 5 2 0 1408.33 1482.43 27.51 o 6 2 0 2850.02 2860.74 46.00 o 7 2 0 3260.78 3322.75 48.48 o 8 2 0 197.08 158.23 11.94 o 9 2 0 1215.48 1258.81 32.24 o 10 2 0 200.25 195.70 20.52 o 11 2 0 128.61 147.98 20.58 o 12 2 0 80.44 77.36 21.04 o 13 2 0 55.63 123.18 40.02 o 1 3 0 1101.51 1042.73 8.85 o 2 3 0 1429.60 1542.91 13.28 o 3 3 0 3479.65 3664.78 23.85 o 4 3 0 3847.11 4128.87 32.80 o 5 3 0 5219.50 5319.99 41.58 o 6 3 0 2257.65 2287.58 32.19 o 7 3 0 93.80 80.60 8.98 o 8 3 0 2497.85 2408.56 33.76 o 9 3 0 74.65 66.54 11.09 o 10 3 0 51.38 31.97 15.03 o 11 3 0 327.96 339.27 26.57 o 12 3 0 26.58 67.75 20.17 o 13 3 0 20.22 -49.26 66.37 o 0 4 0 16904.18 16349.66 64.23 o 1 4 0 4120.82 3979.86 17.26 o 2 4 0 2948.92 3170.74 18.02 o 3 4 0 12646.90 12892.49 58.42 o 4 4 0 1416.92 1283.01 16.73 o 5 4 0 4572.81 4552.25 36.77 o 6 4 0 3798.25 3696.57 35.75 o 7 4 0 2001.34 2039.76 29.58 o 8 4 0 132.31 118.53 9.95 o 9 4 0 476.16 522.20 20.41 o 10 4 0 394.87 395.55 23.22 o 11 4 0 60.61 50.34 16.52 o 12 4 0 115.91 81.93 24.37 o 1 5 0 1799.35 1685.98 13.38 o 2 5 0 19746.40 21157.94 92.35 o 3 5 0 2949.71 3093.30 21.36 o 4 5 0 1677.88 1811.74 20.57 o 5 5 0 5116.49 5328.83 40.81 o 6 5 0 1425.32 1400.08 23.05 o 7 5 0 289.90 259.38 12.74 o 8 5 0 94.28 83.86 8.95 o 9 5 0 90.37 84.43 12.06 o 10 5 0 66.95 51.64 13.89 o 11 5 0 355.92 290.58 24.60 o 12 5 0 97.41 116.84 26.88 o 0 6 0 182.80 252.91 11.26 o 1 6 0 6352.16 6351.19 29.35 o 2 6 0 1074.74 1198.88 13.18 o 3 6 0 17363.31 16980.73 63.67 o 4 6 0 2224.17 2111.55 21.04 o 5 6 0 1931.49 1842.39 22.85 o 6 6 0 1950.70 1995.42 28.46 o 7 6 0 28.19 19.16 8.51 o 8 6 0 107.13 101.18 11.69 o 9 6 0 15.88 7.14 8.46 o 10 6 0 221.15 209.48 21.98 o 11 6 0 30.67 30.52 15.97 o 12 6 0 141.95 270.52 80.19 o 1 7 0 2200.13 2228.22 18.97 o 2 7 0 5939.89 6211.72 30.75 o 3 7 0 2245.01 2408.15 19.93 o 4 7 0 1741.95 1751.74 18.82 o 5 7 0 1726.79 1846.85 22.64 o 6 7 0 2042.56 2024.63 26.37 o 7 7 0 424.94 424.97 15.32 o 8 7 0 169.75 154.34 12.10 o 9 7 0 198.88 201.64 17.57 o 10 7 0 220.82 234.13 19.03 o 11 7 0 203.93 230.65 29.67 o 12 7 0 79.94 81.52 31.92 o 0 8 0 1511.11 1497.48 28.69 o 1 8 0 80.36 54.06 5.02 o 2 8 0 1092.41 1051.89 13.06 o 3 8 0 4919.90 4621.17 30.71 o 4 8 0 2586.21 2508.28 22.23 o 5 8 0 1424.43 1468.53 20.76 o 6 8 0 2024.90 2121.42 28.48 o 7 8 0 779.16 780.38 19.10 o 8 8 0 44.19 41.00 9.02 o 9 8 0 184.04 197.17 16.70 o 10 8 0 197.34 185.20 19.09 o 11 8 0 5.17 -19.11 19.11 o 12 8 0 74.76 -3.71 28.42 o 1 9 0 1875.82 1820.60 20.06 o 2 9 0 1673.28 1622.96 20.34 o 3 9 0 2060.86 2088.97 21.51 o 4 9 0 1248.24 1221.30 17.11 o 5 9 0 2361.95 2375.59 26.42 o 6 9 0 912.03 930.08 19.95 o 7 9 0 11.28 9.34 7.32 o 8 9 0 973.32 1006.01 28.37 o 9 9 0 112.40 118.65 17.57 o 10 9 0 94.33 90.94 15.88 o 11 9 0 161.82 150.35 25.27 o 12 9 0 24.50 133.96 46.41 o 0 10 0 6880.78 6861.41 97.85 o 1 10 0 161.72 146.88 6.61 o 2 10 0 2552.71 2602.84 25.06 o 3 10 0 2619.81 2636.41 25.57 o 4 10 0 962.13 999.61 17.53 o 5 10 0 681.75 657.04 13.62 o 6 10 0 691.26 689.71 17.42 o 7 10 0 802.69 803.63 19.81 o 8 10 0 34.26 28.06 10.07 o 9 10 0 265.58 278.96 21.66 o 10 10 0 98.26 89.86 16.69 o 11 10 0 53.54 46.26 22.51 o 1 11 0 6171.40 6169.37 43.10 o 2 11 0 662.04 592.14 13.62 o 3 11 0 529.34 478.27 10.86 o 4 11 0 29.62 20.06 5.88 o 5 11 0 643.70 604.54 18.94 o 6 11 0 377.06 382.35 16.47 o 7 11 0 85.16 71.07 10.40 o 8 11 0 1000.44 1088.08 30.44 o 9 11 0 21.93 3.45 12.97 o 10 11 0 127.07 124.54 28.01 o 11 11 0 25.20 70.09 28.79 o 0 12 0 7405.64 7589.59 78.94 o 1 12 0 464.92 455.50 14.99 o 2 12 0 1120.64 1114.87 19.09 o 3 12 0 390.56 368.46 13.16 o 4 12 0 45.82 64.27 9.89 o 5 12 0 106.87 102.40 11.45 o 6 12 0 558.11 600.15 20.10 o 7 12 0 564.78 552.33 20.12 o 8 12 0 15.46 -5.72 10.03 o 9 12 0 352.81 420.86 26.13 o 10 12 0 34.88 24.55 17.28 o 11 12 0 49.67 67.77 31.85 o 1 13 0 2497.12 2454.65 32.57 o 2 13 0 186.89 169.70 9.70 o 3 13 0 319.16 319.27 13.69 o 4 13 0 247.80 261.20 14.24 o 5 13 0 763.65 756.57 22.22 o 6 13 0 259.09 250.12 14.84 o 7 13 0 38.51 26.30 10.25 o 8 13 0 465.66 489.89 22.96 o 9 13 0 5.85 20.54 16.90 o 10 13 0 118.60 110.13 38.03 o 0 14 0 2765.57 2881.06 58.06 o 1 14 0 81.80 83.52 10.73 o 2 14 0 433.37 456.83 13.90 o 3 14 0 335.26 331.28 14.67 o 4 14 0 180.40 163.99 12.50 o 5 14 0 107.05 81.96 10.43 o 6 14 0 223.70 222.32 13.96 o 7 14 0 420.96 483.91 20.85 o 8 14 0 10.04 -13.02 14.49 o 9 14 0 187.14 206.55 21.49 o 10 14 0 32.87 22.09 25.63 o 1 15 0 820.43 813.74 25.69 o 2 15 0 690.05 670.69 23.57 o 3 15 0 305.44 284.83 17.36 o 4 15 0 227.37 256.37 17.39 o 5 15 0 386.67 402.60 17.43 o 6 15 0 199.33 197.64 15.17 o 7 15 0 60.72 66.97 13.30 o 8 15 0 258.47 284.90 30.12 o 9 15 0 13.52 -17.72 21.70 o 0 16 0 419.93 492.82 30.51 o 1 16 0 175.07 187.79 16.28 o 2 16 0 393.42 458.42 22.42 o 3 16 0 720.64 698.72 25.10 o 4 16 0 150.67 116.08 15.73 o 5 16 0 216.58 193.62 17.78 o 6 16 0 208.52 195.26 18.22 o 7 16 0 91.00 91.67 17.00 o 8 16 0 0.04 -6.19 20.93 o 9 16 0 27.30 80.33 46.64 o 1 17 0 15.75 -13.67 14.09 o 2 17 0 486.00 552.32 29.15 o 3 17 0 155.10 146.04 18.81 o 4 17 0 500.87 540.12 27.32 o 5 17 0 348.54 350.47 23.60 o 6 17 0 26.64 26.28 15.41 o 7 17 0 35.76 34.29 17.06 o 8 17 0 34.11 83.49 26.92 o 0 18 0 57.07 61.56 18.82 o 1 18 0 81.62 81.75 16.93 o 2 18 0 65.50 67.17 17.32 o 3 18 0 425.16 415.74 26.33 o 4 18 0 109.27 91.30 16.54 o 5 18 0 78.31 43.47 13.75 o 6 18 0 89.95 56.69 18.33 o 7 18 0 13.13 -14.22 26.32 o 8 18 0 8.00 -60.28 60.28 o 1 19 0 8.75 1.91 15.92 o 2 19 0 299.84 397.14 28.59 o 3 19 0 76.49 93.07 21.48 o 4 19 0 112.70 117.83 18.80 o 5 19 0 87.37 108.41 18.02 o 6 19 0 30.67 4.24 17.00 o 7 19 0 51.86 49.60 36.87 o 0 20 0 56.16 11.89 57.56 o 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